CN111718784A - Preparation process of emulsified oil complexing agent for hydraulic support - Google Patents
Preparation process of emulsified oil complexing agent for hydraulic support Download PDFInfo
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- CN111718784A CN111718784A CN202010726107.XA CN202010726107A CN111718784A CN 111718784 A CN111718784 A CN 111718784A CN 202010726107 A CN202010726107 A CN 202010726107A CN 111718784 A CN111718784 A CN 111718784A
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- agent
- complexing agent
- water bath
- preparation process
- emulsified oil
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/042—Mixtures of base-materials and additives the additives being compounds of unknown or incompletely defined constitution only
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/106—Naphthenic fractions
- C10M2203/1065—Naphthenic fractions used as base material
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
Abstract
The invention discloses a preparation process of an emulsified oil complexing agent for a hydraulic bracket, which relates to the technical field of production of emulsified liquid complexing agents and comprises the following steps of S1, pouring a certain amount of deionized water into a container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10; s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃; s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution. The invention adopts various proportioning modes, obtains the optimal proportioning through data comparison, has better oil removing and dirt removing effects and relatively lower preparation cost, can greatly reduce the expense of large-scale production of enterprises, and improves the market competitiveness of products.
Description
Technical Field
The invention relates to the technical field of emulsion complexing agent production, in particular to a preparation process of an emulsified oil complexing agent for a hydraulic support.
Background
The emulsified oil complexing agent can improve the oil removing, stain removing and foam increasing effects of various oil removing agents and cleaning agents such as washing powder, liquid detergent, laundry detergent, liquid soap and the like, has a wide application range and can be used in a plurality of machining industries.
When the existing emulsified oil complexing agent is prepared, due to the fact that multiple adding reagents are needed, when a proportioned stock solution is mixed with naphthenic base oil according to a volume ratio, the final oil removal and decontamination effects of a product can be affected due to different contents of the stock solution, and the change of production cost can be brought due to the different contents of the stock solution, the preparation process of the emulsified oil complexing agent for the hydraulic support is provided.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a preparation process of an emulsified oil complexing agent for a hydraulic bracket.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation process of an emulsified oil complexing agent for a hydraulic bracket comprises the following steps,
s1, pouring a certain amount of deionized water into the container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10;
s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃;
s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution;
s4, taking the prepared stock solution and the naphthenic base oil according to the volume ratio of 15-30%: 70-85% of the mixture is mixed to prepare an emulsion complexing agent product which can be directly applied;
and S5, performing pH adjustment on the finally prepared product, wherein the product is qualified when the pH is adjusted to 7-8.5.
Preferably, the preservative is one or more of carbazone, 1, 2-hexanediol and ethylene glycol phenyl ether, and the corrosion inhibitor is one or more of borax, phosphate, nitrite, nitrate and molybdate.
Preferably, the anti-thickening agent comprises methylchlorosilanes, modified water-soluble polyacrylonitriles, organotin catalysts and fluorocarbon siloxane polyethers.
Preferably, the deodorant comprises one or more of sodium hypochlorite, a divalent iron ion salt, a trivalent iron derivative and a ligand of a metal complex.
Preferably, the bactericide is one or more of chlorophenols, quaternary ammonium salts, chloramines and allicin.
Preferably, the antirust agent is one or more of sodium sulfite, sodium carbonate and borax of inorganic salt.
The invention provides a plurality of proportioning modes, and the optimal proportioning is obtained through data comparison, under the proportioning, the oil removal and decontamination effects are better, the preparation cost is relatively low, the expense of large-scale production of enterprises can be greatly reduced, and the market competitiveness of products is improved.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments.
Example one
A preparation process of an emulsified oil complexing agent for a hydraulic bracket comprises the following steps,
s1, pouring a certain amount of deionized water into the container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10;
s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃;
s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution;
s4, taking the prepared stock solution and the naphthenic base oil according to the volume ratio of 15%: 85 percent of the mixture is mixed to prepare an emulsion complexing agent product which can be directly applied;
and S5, performing pH adjustment on the finally prepared product, wherein the product is qualified when the pH is adjusted to 7-8.5.
The corrosion inhibitor is one or more of carbazone, 1, 2-hexanediol and ethylene glycol phenyl ether, the corrosion inhibitor is one or more of borax, phosphate, nitrite, nitrate and molybdate, the thickening inhibitor comprises methyl chlorosilane, modified water-soluble polyacrylonitrile, an organic tin catalyst and fluorocarbon siloxane polyether, the odor inhibitor comprises one or more of sodium hypochlorite, a ferrous ion salt, a ferric iron derivative and a ligand of a metal complex, the bactericide is one or more of chlorophenols, quaternary ammonium salts, chloramines and allicin, and the antirust agent is one or more of sodium sulfite of inorganic salt, sodium carbonate and borax.
Example two
A preparation process of an emulsified oil complexing agent for a hydraulic bracket comprises the following steps,
s1, pouring a certain amount of deionized water into the container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10;
s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃;
s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution;
s4, taking the prepared stock solution and the naphthenic base oil according to the volume ratio of 20%: 80 percent of the mixture is mixed to prepare an emulsion complexing agent product which can be directly applied;
and S5, performing pH adjustment on the finally prepared product, wherein the product is qualified when the pH is adjusted to 7-8.5.
The corrosion inhibitor is one or more of carbazone, 1, 2-hexanediol and ethylene glycol phenyl ether, the corrosion inhibitor is one or more of borax, phosphate, nitrite, nitrate and molybdate, the thickening inhibitor comprises methyl chlorosilane, modified water-soluble polyacrylonitrile, an organic tin catalyst and fluorocarbon siloxane polyether, the odor inhibitor comprises one or more of sodium hypochlorite, a ferrous ion salt, a ferric iron derivative and a ligand of a metal complex, the bactericide is one or more of chlorophenols, quaternary ammonium salts, chloramines and allicin, and the antirust agent is one or more of sodium sulfite of inorganic salt, sodium carbonate and borax.
EXAMPLE III
A preparation process of an emulsified oil complexing agent for a hydraulic bracket comprises the following steps,
s1, pouring a certain amount of deionized water into the container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10;
s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃;
s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution;
s4, taking the prepared stock solution and the naphthenic base oil according to the volume ratio of 25%: 75 percent of the mixture is mixed to prepare an emulsion complexing agent product which can be directly applied;
and S5, performing pH adjustment on the finally prepared product, wherein the product is qualified when the pH is adjusted to 7-8.5.
The corrosion inhibitor is one or more of carbazone, 1, 2-hexanediol and ethylene glycol phenyl ether, the corrosion inhibitor is one or more of borax, phosphate, nitrite, nitrate and molybdate, the thickening inhibitor comprises methyl chlorosilane, modified water-soluble polyacrylonitrile, an organic tin catalyst and fluorocarbon siloxane polyether, the odor inhibitor comprises one or more of sodium hypochlorite, a ferrous ion salt, a ferric iron derivative and a ligand of a metal complex, the bactericide is one or more of chlorophenols, quaternary ammonium salts, chloramines and allicin, and the antirust agent is one or more of sodium sulfite of inorganic salt, sodium carbonate and borax.
Example four
A preparation process of an emulsified oil complexing agent for a hydraulic bracket comprises the following steps,
s1, pouring a certain amount of deionized water into the container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10;
s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃;
s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution;
s4, taking the prepared stock solution and the naphthenic base oil according to the volume ratio of 30%: 70 percent of the mixture is mixed to prepare an emulsion complexing agent product which can be directly applied;
and S5, performing pH adjustment on the finally prepared product, wherein the product is qualified when the pH is adjusted to 7-8.5.
The corrosion inhibitor is one or more of carbazone, 1, 2-hexanediol and ethylene glycol phenyl ether, the corrosion inhibitor is one or more of borax, phosphate, nitrite, nitrate and molybdate, the thickening inhibitor comprises methyl chlorosilane, modified water-soluble polyacrylonitrile, an organic tin catalyst and fluorocarbon siloxane polyether, the odor inhibitor comprises one or more of sodium hypochlorite, a ferrous ion salt, a ferric iron derivative and a ligand of a metal complex, the bactericide is one or more of chlorophenols, quaternary ammonium salts, chloramines and allicin, and the antirust agent is one or more of sodium sulfite of inorganic salt, sodium carbonate and borax.
| Stock solution/%) | Cycloalkyl base oil/% | Metal sheet decontamination and rust prevention time/min |
| 15 | 85 | 5.8 |
| 20 | 80 | 3.4 |
| 25 | 75 | 4.5 |
| 30 | 70 | 6.3 |
In summary, it is clear from the comparison of the above data that the volume ratio of the stock solution to the naphthenic base oil is 20%: under the condition of 80%, the product has the shortest decontamination and rust prevention time and the best action effect, and under the volume ratio, the consumption of the stock solution is relatively small, the preparation cost is relatively saved, and the requirement of large-scale production of enterprises is facilitated.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (6)
1. A preparation process of an emulsified oil complexing agent for a hydraulic bracket comprises the following steps,
s1, pouring a certain amount of deionized water into the container, adding an alkaline preparation into the deionized water, and adjusting the pH of the solution to 9-10;
s2, preparing a water bath, putting the alkali washing solution container prepared in the S1 into the water bath, and heating in a water bath at the temperature of 40 ℃;
s3, adding an antirust agent, a lubricating complexing agent, glycerol, an antioxidant, a bactericide, a preservative, a corrosion inhibitor, a coloring agent, an anti-coagulant, an odor-resistant agent and a thickening-resistant agent into the solution heated in the water bath, and stirring to fully and uniformly mix the mixture to obtain a stock solution;
s4, taking the prepared stock solution and the naphthenic base oil according to the volume ratio of 15-30%: 70-85% of the mixture is mixed to prepare an emulsion complexing agent product which can be directly applied;
and S5, performing pH adjustment on the finally prepared product, wherein the product is qualified when the pH is adjusted to 7-8.5.
2. The preparation process of the emulsified oil complexing agent for the hydraulic bracket according to claim 1, wherein the preservative is one or more of carbazone, 1, 2-hexanediol and ethylene glycol phenyl ether, and the corrosion inhibitor is one or more of borax, phosphate, nitrite, nitrate and molybdate.
3. The preparation process of the emulsified oil complexing agent for the hydraulic support according to claim 1, wherein the thickening-preventing agent comprises methylchlorosilane, modified water-soluble polyacrylonitrile, organotin catalysts and fluorocarbon siloxane polyethers.
4. The preparation process of the emulsified oil complexing agent for the hydraulic bracket according to claim 1, wherein the odor-resistant agent comprises one or more of sodium hypochlorite, ferrous ion salts, ferric iron derivatives and ligands of metal complexes.
5. The preparation process of the emulsified oil complexing agent for the hydraulic bracket according to claim 1, wherein the bactericide is one or more of chlorophenols, quaternary ammonium salts, chloramines and allicin.
6. The preparation process of the emulsified oil complexing agent for the hydraulic bracket according to claim 1, wherein the antirust agent is one or more of sodium sulfite, sodium carbonate and borax of inorganic salt.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010726107.XA CN111718784A (en) | 2020-07-25 | 2020-07-25 | Preparation process of emulsified oil complexing agent for hydraulic support |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010726107.XA CN111718784A (en) | 2020-07-25 | 2020-07-25 | Preparation process of emulsified oil complexing agent for hydraulic support |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1350047A (en) * | 2000-10-25 | 2002-05-22 | 宋福如 | High-temperature viscosity reducer for drilling fluid and its production process |
| CN105838494A (en) * | 2016-04-29 | 2016-08-10 | 榆林市金世源矿用油品有限公司 | Environment-friendly concentrated solution for hydraulic support and preparation method of environment-friendly concentrated solution |
| CN107057821A (en) * | 2017-05-24 | 2017-08-18 | 榆林市金世源矿用油品有限公司 | A kind of hydraulic support oil emulsion and preparation method thereof |
| CN108658250A (en) * | 2018-07-02 | 2018-10-16 | 安庆丰源化工有限公司 | A kind of fine chemistry industry sewage deodorizing agent and preparation method thereof |
-
2020
- 2020-07-25 CN CN202010726107.XA patent/CN111718784A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1350047A (en) * | 2000-10-25 | 2002-05-22 | 宋福如 | High-temperature viscosity reducer for drilling fluid and its production process |
| CN105838494A (en) * | 2016-04-29 | 2016-08-10 | 榆林市金世源矿用油品有限公司 | Environment-friendly concentrated solution for hydraulic support and preparation method of environment-friendly concentrated solution |
| CN107057821A (en) * | 2017-05-24 | 2017-08-18 | 榆林市金世源矿用油品有限公司 | A kind of hydraulic support oil emulsion and preparation method thereof |
| CN108658250A (en) * | 2018-07-02 | 2018-10-16 | 安庆丰源化工有限公司 | A kind of fine chemistry industry sewage deodorizing agent and preparation method thereof |
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Application publication date: 20200929 |
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