CN111643409A - Production process of wolfberry lipstick - Google Patents

Production process of wolfberry lipstick Download PDF

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Publication number
CN111643409A
CN111643409A CN202010444491.4A CN202010444491A CN111643409A CN 111643409 A CN111643409 A CN 111643409A CN 202010444491 A CN202010444491 A CN 202010444491A CN 111643409 A CN111643409 A CN 111643409A
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China
Prior art keywords
parts
heating
wolfberry
extract
raw materials
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CN202010444491.4A
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Chinese (zh)
Inventor
邓守毅
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Individual
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Individual
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Priority to CN202010444491.4A priority Critical patent/CN111643409A/en
Publication of CN111643409A publication Critical patent/CN111643409A/en
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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

Abstract

The invention relates to a production process of a wolfberry lipstick, which comprises the following components in parts by weight: 15-25 parts of color paste, 5-20 parts of ozokerite, 4-16 parts of polyethylene wax, 10-40 parts of tridecyl alcohol trimellitate, 7-30 parts of cetyl alcohol ethyl acetate, 2-6 parts of diisostearyl malate, 8-35 parts of a boxthorn fruit extract, 1-5 parts of a preservative and 4-10 parts of pearl powder. The invention has the beneficial effects that: the invention has certain traditional Chinese medicine curative effect, the medlar extract contains rich vitamins and trace elements, and can provide nutrition for lips and nourish skin; the medlar extract also contains flavonoid compounds, and the flavonoid compounds have the effects of resisting bacteria and diminishing inflammation and are beneficial to preventing lip skin allergy.

Description

Production process of wolfberry lipstick
Technical Field
The invention relates to the field of daily chemicals, in particular to a production process of a wolfberry lipstick.
Background
The lip balm is a necessary cosmetic in daily life, and has the functions of keeping lips soft and glossy and preventing lips from drying and cracking. The lipstick can brighten the color of the lips, so that the face color is more beautiful, if the traditional lipstick can endow the connotation of national culture, the lipstick can be more compliant with the tide of developing Chinese culture, therefore, the best lipstick can be combined with the traditional Chinese medicine, the medlar has the effects of tonifying deficiency, replenishing vital essence, clearing heat, relieving cough, nourishing liver, improving eyesight, delaying senility and the like, the extract of the medlar is rich in amino acid, vitamin, trace elements and other nutritional ingredients, and also contains flavonoid compounds, alkaloid and other active substances, thereby having very high nutritional and health-care effects, and the medlar fruit extract and the lipstick are not well combined in the prior art for use.
Disclosure of Invention
The invention aims to solve the problems in the prior art, and provides a production process of a medlar lipstick, which has a certain traditional Chinese medicine curative effect and can supplement nutrition for lip skin.
In order to solve the technical problems, the technical scheme provided by the invention is as follows: a production process of a wolfberry lipstick comprises the following components in parts by weight: 15-25 parts of color paste, 5-20 parts of ozokerite, 4-16 parts of polyethylene wax, 10-40 parts of tridecyl alcohol trimellitate, 7-30 parts of cetyl alcohol ethyl acetate, 2-6 parts of diisostearyl malate, 8-35 parts of a boxthorn fruit extract, 1-5 parts of a preservative and 4-10 parts of pearl powder.
Further, the method specifically comprises the following steps: 1) preparing materials: checking whether the raw materials are qualified;
2) grinding color paste: the color paste is dispersed uniformly;
3) and b, correcting the platform scale: correcting a platform scale to be weighed to realize accurate weighing;
4) weighing: accurately weighing 15-25 parts of color paste, 5-20 parts of ozokerite, 4-16 parts of polyethylene wax, 10-40 parts of tridecyl alcohol trimellitate, 7-30 parts of cetyl alcohol ethyl acetate, 2-6 parts of diisostearyl malate and 8-35 parts of a boxthorn fruit extract;
5) melting: adding the raw materials weighed in the step 4) into a heating pot, heating and stirring at a high speed for 1 hour, and heating to 80-95 ℃ until the raw materials are completely melted;
6) feeding: adding 1-5 parts of preservative and 4-10 parts of pearl powder into the raw materials melted in the step 5);
7) color matching: taking the material obtained in the step 6) to compare with a colorimetric card;
8) filling and forming: pouring the mixed materials into a mould, and controlling the temperature at 70-80 ℃.
Further, the preparation method of the wolfberry fruit extract comprises the following steps: A. pulverizing fructus Lycii into coarse powder;
B. respectively taking 15 times of water, 70% ethanol, 80% ethanol and 90% ethanol as extraction solvents, respectively adding the coarse powder obtained in the step A, heating, refluxing and extracting for 2 hours, and filtering;
C. b, respectively taking water as an extraction solvent for the filtrate in the step B, heating, refluxing and extracting twice, and filtering;
D. and D, combining the filtrate obtained in the step B and the filtrate obtained in the step C, concentrating the mixture at 50 ℃ under reduced pressure to obtain an extract with the relative density of 1.1-1.2 at room temperature, and drying the extract at the temperature below 50 ℃ in vacuum to obtain the wolfberry fruit extract.
Furthermore, the time of heating reflux extraction in the step C is 2 hours, 10 times of water is added during the first heating reflux extraction, and 8 times of water is added during the second heating reflux extraction.
The invention has the beneficial effects that: the invention has certain traditional Chinese medicine curative effect, the medlar extract contains rich vitamins and trace elements, and can provide nutrition for lips and nourish skin; the fructus Lycii extract also contains flavonoid compounds, which have antibacterial and anti-inflammatory effects and are helpful for preventing lip skin allergy. In addition, the lip balm has good moisturizing effect, can prevent the lips from drying and cracking, and can keep the health of the lips for a long time.
Detailed Description
The invention is illustrated below by means of specific examples, without being restricted thereto.
Example one
Pulverizing fructus Lycii into coarse powder, extracting with 15 times of water as extraction solvent, adding coarse powder of fructus Lycii, heating under reflux for 2 hr, and filtering; heating and refluxing the filtrate with water as extraction solvent for two times (2 hr), adding 10 times of water for the first heating and refluxing extraction, adding 8 times of water for the second heating and refluxing extraction, and filtering; mixing the three filtrates, concentrating at 50 deg.C under reduced pressure to obtain extract with relative density of 1.1-1.2 at room temperature, and vacuum drying at below 50 deg.C to obtain fructus Lycii extract;
checking whether the raw materials are qualified or not, grinding the color paste to enable the color paste to be uniformly dispersed, correcting a platform scale needing weighing to achieve accurate weighing, accurately weighing 15 parts of color paste, 5 parts of ozokerite, 4 parts of polyethylene wax, 10 parts of tridecyl alcohol trimellitate, 7 parts of cetyl alcohol ethyl acetate, 2 parts of diisostearyl malate and 8 parts of wolfberry fruit extract, adding the weighed raw materials into a heating pot, heating and stirring at a high speed for 1 hour, heating to 80-95 ℃ until the raw materials are completely melted, adding 1 part of preservative and 4 parts of pearl powder into the melted raw materials, taking the melted materials to contrast a color comparison card, filling the mixed materials into a mold, and controlling the temperature to be 70-80 ℃.
Example two
Pulverizing fructus Lycii into coarse powder, extracting with 70% ethanol as extraction solvent, adding coarse powder of fructus Lycii, heating under reflux for 2 hr, and filtering; heating and refluxing the filtrate with water as extraction solvent for two times (2 hr), adding 10 times of water for the first heating and refluxing extraction, adding 8 times of water for the second heating and refluxing extraction, and filtering; mixing the three filtrates, concentrating at 50 deg.C under reduced pressure to obtain extract with relative density of 1.1-1.2 at room temperature, and vacuum drying at below 50 deg.C to obtain fructus Lycii extract;
checking whether the raw materials are qualified or not, grinding the color paste to enable the color paste to be uniformly dispersed, correcting a platform scale needing weighing to achieve accurate weighing, accurately weighing 15 parts of color paste, 5 parts of ozokerite, 4 parts of polyethylene wax, 10 parts of tridecyl alcohol trimellitate, 7 parts of cetyl alcohol ethyl acetate, 2 parts of diisostearyl malate and 8 parts of wolfberry fruit extract, adding the weighed raw materials into a heating pot, heating and stirring at a high speed for 1 hour, heating to 80-95 ℃ until the raw materials are completely melted, adding 1 part of preservative and 4 parts of pearl powder into the melted raw materials, taking the melted materials to contrast a color comparison card, filling the mixed materials into a mold, and controlling the temperature to be 70-80 ℃.
EXAMPLE III
Pulverizing fructus Lycii into coarse powder, extracting with 80% ethanol as extraction solvent, adding coarse powder of fructus Lycii, heating under reflux for 2 hr, and filtering; heating and refluxing the filtrate with water as extraction solvent for two times (2 hr), adding 10 times of water for the first heating and refluxing extraction, adding 8 times of water for the second heating and refluxing extraction, and filtering; mixing the three filtrates, concentrating at 50 deg.C under reduced pressure to obtain extract with relative density of 1.1-1.2 at room temperature, and vacuum drying at below 50 deg.C to obtain fructus Lycii extract;
checking whether the raw materials are qualified or not, grinding the color paste to enable the color paste to be uniformly dispersed, correcting a platform scale needing weighing to achieve accurate weighing, accurately weighing 20 parts of color paste, 10 parts of ozokerite, 8 parts of polyethylene wax, 30 parts of tridecyl alcohol trimellitate, 15 parts of cetyl alcohol ethyl acetate, 4 parts of diisostearyl malate and 17 parts of wolfberry fruit extract, adding the weighed raw materials into a heating pot, heating and stirring at a high speed for 1 hour, heating to 80-95 ℃ until the raw materials are completely melted, adding 3 parts of preservative and 7 parts of pearl powder into the melted raw materials, taking the melted materials to contrast a color comparison card, filling the mixed materials into a mold, and controlling the temperature to be 70-80 ℃.
Example four
Pulverizing fructus Lycii into coarse powder, extracting with 90% ethanol as extraction solvent, adding coarse powder of fructus Lycii, heating under reflux for 2 hr, and filtering; heating and refluxing the filtrate with water as extraction solvent for two times (2 hr), adding 10 times of water for the first heating and refluxing extraction, adding 8 times of water for the second heating and refluxing extraction, and filtering; mixing the three filtrates, concentrating at 50 deg.C under reduced pressure to obtain extract with relative density of 1.1-1.2 at room temperature, and vacuum drying at below 50 deg.C to obtain fructus Lycii extract;
checking whether the raw materials are qualified or not, grinding the color paste to enable the color paste to be uniformly dispersed, correcting a platform scale needing weighing to achieve accurate weighing, accurately weighing 25 parts of color paste, 20 parts of ozokerite, 16 parts of polyethylene wax, 40 parts of tridecyl alcohol trimellitate, 30 parts of cetyl alcohol ethyl acetate, 6 parts of diisostearyl malate and 35 parts of wolfberry fruit extract, adding the weighed raw materials into a heating pot, heating and stirring at a high speed for 1 hour, heating to 80-95 ℃ until the raw materials are completely melted, adding 5 parts of preservative and 10 parts of pearl powder into the melted raw materials, taking the melted materials to contrast a color comparison card, filling the mixed materials into a mold, and controlling the temperature to be 70-80 ℃.
After the three examples, the contents of polysaccharide, total flavone and betaine in the product are detected, and a comparison table is prepared.
TABLE 1 comparison of results of different extraction processes
Extraction solvent Extraction yield (%) Lycium barbarum polysaccharides (%) Total Flavonoids (%) Betaine (%)
Water (W) 66.85 4.95 2.11 0.82
70% ethanol + water 73.94 4.74 2.83 0.85
80% ethanol + water 73.21 4.63 3.07 0.85
90% ethanol + water 74.66 4.59 3.07 0.86
The results show that: taking the extraction yield and the contents of lycium barbarum polysaccharides, total flavonoids and betaine in each extract into comprehensive consideration, determining the optimal process flow, namely crushing the lycium barbarum into coarse powder, taking 80% ethanol as an extraction solvent, adding the lycium barbarum coarse powder, heating, refluxing and extracting for 2 hours, and filtering; respectively heating and refluxing the filtrate for two times for 2 hours by using water as an extraction solvent, adding 10 times of water during the first heating and refluxing extraction, adding 8 times of water during the second heating and refluxing extraction, and filtering; mixing the three filtrates, concentrating at 50 deg.C under reduced pressure to obtain extract with relative density of 1.1-1.2 at room temperature, and vacuum drying at below 50 deg.C to obtain fructus Lycii extract;
checking whether the raw materials are qualified or not, grinding the color paste to enable the color paste to be uniformly dispersed, correcting a platform scale needing weighing to achieve accurate weighing, accurately weighing 20 parts of color paste, 10 parts of ozokerite, 8 parts of polyethylene wax, 30 parts of tridecyl alcohol trimellitate, 15 parts of cetyl alcohol ethyl acetate, 4 parts of diisostearyl malate and 17 parts of wolfberry fruit extract, adding the weighed raw materials into a heating pot, heating and stirring at a high speed for 1 hour, heating to 85 ℃ until the raw materials are completely melted, adding 3 parts of preservative and 7 parts of pearl powder into the melted raw materials, taking the melted materials to contrast a colorimetric card, filling the mixed materials into a mold, and controlling the temperature at 75 ℃.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (4)

1. The production process of the wolfberry lipstick is characterized by comprising the following components in parts by weight: 15-25 parts of color paste, 5-20 parts of ozokerite, 4-16 parts of polyethylene wax, 10-40 parts of tridecyl alcohol trimellitate, 7-30 parts of cetyl alcohol ethyl acetate, 2-6 parts of diisostearyl malate, 8-35 parts of a boxthorn fruit extract, 1-5 parts of a preservative and 4-10 parts of pearl powder.
2. The production process of the wolfberry lipstick according to claim 1, which is characterized by comprising the following steps: 1) preparing materials: checking whether the raw materials are qualified;
2) grinding color paste: the color paste is dispersed uniformly;
3) and b, correcting the platform scale: correcting a platform scale to be weighed to realize accurate weighing;
4) weighing: accurately weighing 15-25 parts of color paste, 5-20 parts of ozokerite, 4-16 parts of polyethylene wax, 10-40 parts of tridecyl alcohol trimellitate, 7-30 parts of cetyl alcohol ethyl acetate, 2-6 parts of diisostearyl malate and 8-35 parts of a boxthorn fruit extract;
5) melting: adding the raw materials weighed in the step 4) into a heating pot, heating and stirring at a high speed for 1 hour, and heating to 80-95 ℃ until the raw materials are completely melted;
6) feeding: adding 1-5 parts of preservative and 4-10 parts of pearl powder into the raw materials melted in the step 5);
7) color matching: taking the material obtained in the step 6) to compare with a colorimetric card;
8) filling and forming: pouring the mixed materials into a mould, and controlling the temperature at 70-80 ℃.
3. The process for producing wolfberry lipstick according to claim 1, wherein the wolfberry fruit extract is prepared by the following steps:
A. pulverizing fructus Lycii into coarse powder;
B. respectively taking 15 times of water, 70% ethanol, 80% ethanol and 90% ethanol as extraction solvents, respectively adding the coarse powder obtained in the step A, heating, refluxing and extracting for 2 hours, and filtering;
C. b, respectively taking water as an extraction solvent for the filtrate in the step B, heating, refluxing and extracting twice, and filtering;
D. and D, combining the filtrate obtained in the step B and the filtrate obtained in the step C, concentrating the mixture at 50 ℃ under reduced pressure to obtain an extract with the relative density of 1.1-1.2 at room temperature, and drying the extract at the temperature below 50 ℃ in vacuum to obtain the wolfberry fruit extract.
4. The process for producing the wolfberry lipstick according to claim 3, wherein the wolfberry lipstick comprises the following components in percentage by weight: and C, in the step C, the time for heating reflux extraction is 2 hours, 10 times of water is added in the first heating reflux extraction, and 8 times of water is added in the second heating reflux extraction.
CN202010444491.4A 2020-05-23 2020-05-23 Production process of wolfberry lipstick Pending CN111643409A (en)

Priority Applications (1)

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CN202010444491.4A CN111643409A (en) 2020-05-23 2020-05-23 Production process of wolfberry lipstick

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Application Number Priority Date Filing Date Title
CN202010444491.4A CN111643409A (en) 2020-05-23 2020-05-23 Production process of wolfberry lipstick

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112426389A (en) * 2020-12-15 2021-03-02 邓守毅 Production process of red cherry lipstick
CN114557936A (en) * 2022-03-24 2022-05-31 宁夏医科大学 Wolfberry lipstick and preparation method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103027879A (en) * 2011-09-29 2013-04-10 庞来祥 Wolfberry lipstick with moisturizing function and its preparation method
WO2014068190A2 (en) * 2012-11-01 2014-05-08 Lumene Oy Cosmetic compositions containing fractions of lingonberry extracts
CN105963166A (en) * 2016-04-11 2016-09-28 甘肃大禹黑枸杞农业科技有限公司 Lipstick prepared form lycium ruthenicum mill
CN107616942A (en) * 2017-10-26 2018-01-23 祝相长 A kind of lip gloss containing wolfberry fruit extract
CN107669501A (en) * 2017-11-15 2018-02-09 陈荷芬 A kind of anti-cracking type plant nourishes hand lotion
CN108938481A (en) * 2018-07-02 2018-12-07 广州艾蓓生物科技有限公司 A kind of discoloration lip gloss and preparation method thereof with maintenance effect

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103027879A (en) * 2011-09-29 2013-04-10 庞来祥 Wolfberry lipstick with moisturizing function and its preparation method
WO2014068190A2 (en) * 2012-11-01 2014-05-08 Lumene Oy Cosmetic compositions containing fractions of lingonberry extracts
CN105963166A (en) * 2016-04-11 2016-09-28 甘肃大禹黑枸杞农业科技有限公司 Lipstick prepared form lycium ruthenicum mill
CN107616942A (en) * 2017-10-26 2018-01-23 祝相长 A kind of lip gloss containing wolfberry fruit extract
CN107669501A (en) * 2017-11-15 2018-02-09 陈荷芬 A kind of anti-cracking type plant nourishes hand lotion
CN108938481A (en) * 2018-07-02 2018-12-07 广州艾蓓生物科技有限公司 A kind of discoloration lip gloss and preparation method thereof with maintenance effect

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112426389A (en) * 2020-12-15 2021-03-02 邓守毅 Production process of red cherry lipstick
CN114557936A (en) * 2022-03-24 2022-05-31 宁夏医科大学 Wolfberry lipstick and preparation method thereof

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Application publication date: 20200911

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