CN110403884A - A kind of lipstick and preparation method thereof containing iron rod yam ingredient - Google Patents
A kind of lipstick and preparation method thereof containing iron rod yam ingredient Download PDFInfo
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- CN110403884A CN110403884A CN201910857559.9A CN201910857559A CN110403884A CN 110403884 A CN110403884 A CN 110403884A CN 201910857559 A CN201910857559 A CN 201910857559A CN 110403884 A CN110403884 A CN 110403884A
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention belongs to cosmetic fields, particularly relate to a kind of lipstick and preparation method thereof containing iron rod yam ingredient.The raw material of lipstick includes iron rod yam polypeptide powder, iron rod yam saponin(e, iron rod yam polysaccharide, iron rod yam flavones, make iron rod yam Chinese medicine water extract by oneself, make iron rod yam Chinese medicine alcohol extracting thing by oneself, make iron rod yam herb fermenting extract by oneself, Natural Carnauba wax, bear ground lira wax, natural beeswax, rose floral wax, tuberose floral wax, acacia farnesiana floral wax, white orchid floral wax, Chilean hazel seed oil, lard fruit seed rouge, simple and unsophisticated A Su fruit oil, peony seed oil, Amygdalus pedunculata benevolence oil, iron rod yam essential oil, edible pigment and other additives.It is made of " high temperature consolute, the casting of middle low-temperature mixed " new process, the resulting more effect iron rod yam lipsticks of high nutrition have full of nutrition, anti-aging, and moisturizing repairs the multiple efficacies such as skin and prevention contact cheilitis.And effect is lasting, securely and reliably.
Description
Technical field
The invention belongs to cosmetic fields, particularly relate to a kind of lipstick and preparation method thereof containing iron rod yam ingredient.
Background technique
With the raising of human living standard, requirement of the people to lip treatment products especially lipstick class product is also more next
It is higher, aesthetics, modified are not only required, novelty it is also desirable to have trophism, maintenance, moisture retention, safety
Deng.Lipstick class product currently on the market is made a general survey of, although a great variety, but still have many defects, such as traditional mouth
Red, especially not viscous rim of a cup is red, due to having selected a large amount of chemically synthesized wax, film forming agent and pigment, essence etc., makes for a long time
It is easy for causing the drying of skin of lip after, the problems such as decortication and pigmentation.It is also easy to cause contact cheilitis.And it is many
" edibility lipstick " and the edibility due to excessively paying attention to lipstick, causes product to lose some due rhetorical functions.It is some
Water-soluble lip care product has a single function again, inconvenient for use etc..Therefore it develops not only safe and reliable but also traditional lipstick function can be taken into account
And the trophism and long-term effect of the multifunctional novel product with local characteristic, especially raising product will be the current and following mouth
Red developing direction.
Iron rod yam is one of " four-Huai medicine ", and is the model of integration of drinking and medicinal herbs, has very high skin care, health care and nutrition
Value.Iron rod yam is the yam variety for originating in the ground such as Henan Wuzhi, belongs to " superfine product " in RHIIZOMA DIOSCOREAE from Henan of China, and rhizome is cylindrical, long
60-80 centimetres, longest is up to 100 centimetres or more, and body is thin and hard, and moisture is few, and juice is denseer, delicious flavour, entrance " face and sweet tea ",
And with light numb taste.Main component is saponin(e, mucilaginous substance, choline, Chinese yam alkali, starch, glycoprotein, free amino acid, polyphenol
Oxidizing ferment, vitamin C, iodine matter, 16 kinds of amino acid, the various trace elements such as Yi Jitie, copper, zinc, manganese, calcium have invigorating the spleen, mend
Lung, reinforce the kidney, beneficial brain, intelligence development, beauty treatment, anti-aging, antitumor, antifatigue, anti-harmful substance stimulation, to adjust metabolism, enhancing immune
Function promotes growth, adjusts endocrine, adjusts renal function, excitement blood system processed, the function of adjusting nervous system, is RHIIZOMA DIOSCOREAE from Henan of China
Middle medical value highest, the optimal kind of tonic effect.It is often edible, constitution not only can be enhanced, nourishes rough skin delays to decline
Always, and to lumbago due to the kidney deficiency, dysmenorrhea, deficiency of kidney essence, loss of appetite, anorexia and loose stool, splenasthenic diarrhea, spleen deficiency chronic cough, obesity etc. quite
There is good effect.It is found after thering is scientific research personnel to compare the Chinese yam sampling of the produced iron rod yam in Jiaozhuo and other areas, Board Lot
Iron rod yam contained by various amino acid all far more than the nonlocal Chinese yam of same amount, wherein also belonging to it just like r- aminobutyric acid
Its Chinese yam does not have substantially and the exclusive amino acid of iron rod yam (RHIIZOMA DIOSCOREAE from Henan of China).It is tested through modern feasibility study means, institute in iron rod yam
The Chinese yam polysaccharide, allantoin, protein, saponin(e and the iron that contain, calcium, zinc content all far more than Chinese yam.
Application in relation to yam extract in lipstick and lip treatment products also has been reported that；Such as Patent publication No
CN101756859A discloses " a kind of lipstick for preventing lip chap ", wherein being added to the Succus Rhizoma Dioscoreae of 10-15%；Patent disclosure
Number CN109223616A discloses " a kind of moist repairing type lipstick formula and preparation method thereof ", wherein being added to 7-10 parts of mountain
Medicinal powder.But from the patent document announced as can be seen that in lip treatment products, the application of iron rod yam, which is also compared, to be had
Limit, or even is still in the primary stage, and is Succus Rhizoma Dioscoreae or yam flour to be added to aqueous lipstick, in lip film system or emulsifying mostly
Application in lipstick, lip film system, and in tubulose lipstick is not yet reported that.It is well known that every lipstick in general
Dosage there was only 3-5G, belong to the lip cosmetic of small volume, it is obvious that in lipstick with good iron rod yam this
Fine work in " four-Huai medicine ", really the essential ingredient " hanging on mouth " in iron rod yam, and balanced other effects of arranging in pairs or groups
Raw material invents qualified " the iron rod yam lipstick " based on iron rod yam ingredient, it is also necessary to go iron rod yam slightly
It takes essence or carries out deep processing.Meanwhile the iron rod yam lipstick of high quality, high nutrition is produced, traditional lipstick is matched
Side and preparation process are a big challenges.
Summary of the invention
To solve good application problem of the iron rod yam in lipstick, a kind of lipstick containing iron rod yam ingredient is disclosed
And preparation method thereof.
The technical scheme of the present invention is realized as follows:
A kind of lipstick containing iron rod yam ingredient, the raw material of the lipstick include iron rod yam polypeptide powder, iron rod yam saponin(e,
Iron rod yam polysaccharide, iron rod yam flavones, self-control iron rod yam Chinese medicine water extract, self-control iron rod yam Chinese medicine alcohol extracting thing,
Self-control iron rod yam herb fermenting extract, Natural Carnauba wax bear ground lira wax, natural beeswax, rose floral wax, tuberose
Floral wax, acacia farnesiana floral wax, white orchid floral wax, Chilean hazel seed oil, lard fruit seed rouge, simple and unsophisticated A Su fruit oil, peony seed oil, Amygdalus pedunculata
Benevolence oil, iron rod yam essential oil, phytosterols oletate, three isooctadecanol citrates, the smooth olive oleate of sorb, olea europaea fruit
The red 27# of oily Cer NP, olive oil hyaluronic acid, Nexbase 2004, tridecanol trimellitate, D & C, D & C Huang 6#,
Wheat-germ oil, VE oil, BHT, TBHQ, methyl p-hydroxybenzoate and propylparaben.
The parts by weight of each raw material in the lipstick are as follows: 0.1-5 parts of iron rod yam polypeptide powder, iron rod yam saponin(e 0.1-3
Part, 0.1-2 parts of iron rod yam polysaccharide, 0.05-2 parts of iron rod yam flavones, self-control 0.1-5 parts of iron rod yam Chinese medicine water extract,
Make 0.1-2 parts of iron rod yam Chinese medicine alcohol extracting thing, self-control 0.1-3 parts of iron rod yam herb fermenting extract, natural cohune by oneself
0.5-6 parts of palmitic acid wax bears ground 0.1-3 parts of lira wax, beeswax 0.5-8 parts natural, 0.1-1 parts of rose floral wax, tuberose floral wax 0.1-1
Part, 0.1-0.5 parts of acacia farnesiana floral wax, 0.1-0.5 parts of white orchid floral wax, Chilean 0.5-3 parts of hazel seed oil, 0.5-6 parts of lard fruit seed rouge,
0.5-5 parts of simple and unsophisticated A Su fruit oil, 0.5-3 parts of peony seed oil, 0.5-5 parts of Amygdalus pedunculata benevolence oil, 0.05-3 parts of iron rod yam essential oil,
0.5-5 parts of phytosterols oletate, 5-20 parts of three isooctadecanol citrate, 1-6 parts of sorb smooth olive oleate, olea europaea fruit
Oily Cer NP 0.1-2 parts, 0.5-2 parts of olive oil hyaluronic acid, 1-10 parts of Nexbase 2004, tridecanol trimellitate
5-25 parts, D & C is 27#0.5-3 parts red, 0.5-5 parts of D & C Huang 6#, 0.5-3 parts of wheat-germ oil, 0.5-2 parts of VE oil,
BHT0.01-0.1 parts, TBHQ0.01-0.1 parts, 0.1-0.5 parts of methyl p-hydroxybenzoate and propylparaben 0.1-
0.5 part.
It is described self-control iron rod yam water extract of TCM the preparation method comprises the following steps:
A, the raw material of following parts by weight, 40-60 parts of iron rod yam dry plate, 5-10 parts of radix polygonati officinalis, Radix Ophiopogonis 10-15 part, Huai Chrysanthemi are weighed
1-2 parts, 5-8 parts of Radix Glycyrrhizae, 5-10 parts of jujube, 1-5 parts of honeysuckle, 1-5 parts of fructus lycii, 1-3 parts of cape jasmine, 5-8 parts of mulberry leaf, radix scrophulariae 1-
3 parts, 1-2 parts of lily, 1-3 parts of semen coicis, 1-3 parts of rhizoma polygonati, 1-2 parts of peppermint；
B, by raw material each in step a according to material: water=1:10 ratio adds water, used after impregnating 8-10 hour traditional Chinese medicine extraction device in
It extracts 30-40 minutes at 100-105 DEG C, then filters, take filter vacuum to be concentrated and be spray-dried to get self-control iron rod yam is arrived
Water extract of TCM.
It is described self-control iron rod yam herb fermenting extract the preparation method comprises the following steps:
1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, sucrose 2-4 parts of addition is red
It is 4-6 parts sugared, 20-40 parts of iron rod yam dry plate, 400-500 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection
It 20-30 minutes, is then cooled to 28-32 DEG C and obtains fermentation material；
2) the Lu Shi Zygosaccharomyces bacterium strain of Angel dry ferment and 0.05-0.1% is added according to the 1-3% of fermentation material total amount, in 28-
It is passed through filtrated air aerobic fermentation at a temperature of 32 DEG C 1-2 days, system is then warming up to 35-37 DEG C, adds glucose 3-5
Part, 1-3 parts of Pidolidone list sodium, CaCl20.05-0.1 parts, 3-5 parts of yeast extract and access fermentation system quality 1-3%'s
Lactobacillus pentosus is simultaneously passed through filtrated air and ferments 2-4 days, the prebiotic bacterial content sum of the remnants in inspection system, when always count≤
When 500cfu/ml has no living contaminants, stop fermentation, filter out fermentation liquid, fermentation liquid is first crossed into 300 meshes, it is later that filtrate is dilute
After 600 meshes after releasing one times, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, by vacuum refrigeration
After drying, self-control iron rod yam herb fermenting extract is obtained.
The concrete operations of the alcohol extracting are as follows: the filter residue fetched water after mentioning crushed 20 meshes, press after weighing after being dried
Take care of: 75%-95% ethyl alcohol 1:(7-10) volume ratio, flow back alcohol extracting 2-3 hours at a temperature of 60-80 DEG C, be then obtained by filtration
Iron rod yam Chinese medicine alcohol extract arrives iron rod yam Chinese medicine alcohol extract using heating concentration, drying.
The preparation method of lipstick containing iron rod yam ingredient, steps are as follows:
(1) weigh the raw material of following parts by weight: 5-15 parts of tridecanol trimellitate, D & C are 27# 0.1-3 parts red, D & C is yellow
0.5-5 parts of 6#, 0.1-5 parts of iron rod yam polypeptide powder, 0.1-3 parts of iron rod yam saponin(e, 0.1-2 parts of iron rod yam polysaccharide, self-control
0.1-5 parts of iron rod yam Chinese medicine water extract, 0.1-2 parts of iron rod yam alcohol extracting thing of self-control, self-control iron rod yam herb fermenting
0.1-3 parts of extract；
(2) after mixing the raw material of each parts by weight in step (1), upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 0.5-6 parts of Natural Carnauba wax bears ground 0.1-3 parts of lira wax, natural beeswax
0.5-8 parts, 0.1-1 parts of rose floral wax, 0.1-1 parts of tuberose floral wax, 0.1-0.5 parts of acacia farnesiana floral wax, white orchid floral wax 0.1-0.5
Part, Chilean 0.5-3 parts of hazel seed oil, 0.5-6 parts of lard fruit seed rouge, 0.5-5 parts of simple and unsophisticated A Su fruit oil, 0.5-3 parts of peony seed oil, length
0.5-5 parts of handle almond oil, 0.5-5 parts of phytosterols oletate, 5-20 parts of three isooctadecanol citrate, the smooth olive oil of sorb
1-6 parts of acid esters, 0.1-2 parts of olive oil Cer NP, 0.5-2 parts of olive oil hyaluronic acid, 1-10 parts of Nexbase 2004,
5-10 parts of tridecanol trimellitate, 0.5-3 parts of wheat-germ oil, 0.5-2 parts of VE oil, 0.01-0.1 parts of BHT,
TBHQ0.01-0.1 parts, 0.1-0.5 parts of methyl p-hydroxybenzoate, 0.1-0.5 parts of propylparaben；
(4) each component raw material in step (1) is heated into consolute in stainless steel kettle, temperature controls between 85-95 DEG C, repeatedly
Melting is allowed to uniformly, cool at a temperature of 45-60 DEG C later, is added 0.05-2 parts of Chinese yam flavones, stirs evenly, obtain B component,
For use；
(5) component A is added in B component, is stirred evenly at a temperature of 45-60 DEG C, Rouge mold is cast in after froth in vacuum
In, after cooling and shaping, demoulding is examined, up to the lipstick containing iron rod yam ingredient after qualification.
The invention has the following advantages:
1, the present invention is using innovative thinking and new formula and new process: by the fine work iron rod yam of four-Huai medicine it is effective at
Point, applied in the common lip treatments lipstick of people to greatest extent, produce it is domestic first with iron rod yam series at
It is divided into the iron rod yam lipstick of main keynote, is really to realize the dream of " hanging over iron rod yam on mouth " and four big
The strategic structural that bosom medicine is applied in lipstick field.
2, contain unique amino acid -- r- aminobutyric acid in iron rod yam, this is that do not had in domestic other yam varieties
, show according to modern scientific research: r- aminobutyric acid has important physiological function, has the reactivity for promoting brain, brain tonic
Intelligence development promotes sleep, and beauty moisturizing delays senescence, and supplements human body inhibitory neurotransmitter, improves nervous function, blood pressure lowering, town
Jing'an mind, antianxiety improve hepatic and renal function, adjust immune function, prevent skin aging, eliminate body odor, improve lipid-metabolism etc.
Multiple efficacies.But the r- aminobutyric acid made from chemical synthesis due to higher cost, and contains residual harmful solvent, therefore not
It is suitble to use in cosmetics and food.The present invention is with iron rod yam, lily, jujube and plurality of Chinese, yeast extract, L-
Monosodium glutamate etc. is fermentation base-material, is fermented using dominant bacteria Lactobacillus pentosus and is enriched with r- aminobutyric acid, achieves breakthrough
Property achievement.After measured, the yield of r- aminobutyric acid has just reached 0.5 gram every liter or more, four days in the fermentation liquid after fermenting three days
It is even up to 1.0 grams every liter or more afterwards, this illustrates that iron rod yam is also the fine base-material for being enriched with r- aminobutyric acid, to iron rod yam
Carry out what deep processing was still well worth doing.
3, overturned the formula mentality of designing of traditional lipstick: conventional tube lipstick by hardness, is smeared due to being bar-like product
The limitation of physical and chemical indexes and the limitation of traditional fabrication equipment, manufacture craft such as property, uniformity, stability, generally on formula all
Make every effort to succinct, in effect also mostly based on decoration and beauty.Even a little moisturizings are added, nutrition skin-protection ingredient, and
Additive amount is very low.Therefore it's hard to say it is qualified trophism lipstick.The present invention has broken the formula thinking of traditional lipstick,
The iron rod yam essential ingredient of highest up to 20% or more is added in lip stick, this is rarely found in trophism lipstick
's.But the performance of trophism powder must not be equal to traditional titanium dioxide, zinc oxide, the inorganic material powders such as talcum powder, especially
It is some protein and peptide classes, amino acids, polysaccharide, vitamins, flavonoids etc., is easy to assemble in lipstick system blocking
Shape.The present invention in formula design sufficiently by way of composite diffusion, by traditional dispersed grease " inclined benzene three of tridecanol
Sour rouge " and the balanced collocation of novel emulsion dispersing agent " the smooth olive olein of sorb " use, and can reach dispersion well and contain iron rod
Nutritional ingredient in nutritional ingredient and other raw materials, the effect for preventing it from assembling in Chinese yam.A variety of antioxidants and preservative simultaneously
Compounding use, also solve the oxidation Anticorrosion of this high nutrition iron rod yam lipstick.
4, innovate and overturned traditional lipstick manufacture craft:
Traditional tubulose lipstick manufacture craft is generally the consolute under high temperature (85 to 100 DEG C), and at high temperature (80 to 95 DEG C)
Under be while hot poured.Because pouring temperature is higher, system liquidity is better, and pouring operation is easier.But in system of the invention
Containing a large amount of trophism pulvis, if then some nutriments will the coking in the cured body of oil using traditional manufacture craft
It agglomerates with aggregation, this is also the basic reason that nutritional substance is not added or added less in traditional lipstick.The use of the invention" (45 to 60 DEG C) mixing casting of the miscible and middle low temperature of part high temperature (80 to 95 DEG C)" new process, and nutriment with point
It makes great efforts in terms of the prior mixed grinding for dissipating property grease.This iron rod yam nutritional ingredient for just making to be ground into particulate and other
Nutritional ingredient in raw material under the conditions of optimal temperature by dispersed encapsulated in lipstick system, avoid conventional high-temperature pourer
The drawbacks of skill.
5, larger in view of the molecular weight of crude protein in iron rod yam, skin is not easy the fact that absorb, and the present invention selects enzymatic hydrolysis
Small molecule iron rod yam polypeptide (molecular weight is below 1000 dalton) powder afterwards, efficiently solves protein-based in iron rod yam
The absorption problem of substance, the deep processing and utilization for local speciality iron rod yam provide new model and new approaches.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical solution of the present invention is clearly and completely described, it is clear that institute
The embodiment of description is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention,
Those of ordinary skill in the art's every other embodiment obtained under that premise of not paying creative labor, belongs to this hair
The range of bright protection.
Raw material: the raw material of the application can bought in addition to homemade.
Embodiment 1
The present embodiment self-control iron rod yam water extract of TCM the preparation method comprises the following steps:
(1) raw material of following parts by weight is weighed: 40 parts of iron rod yam dry plate, 5 parts of radix polygonati officinalis, 15 parts of Radix Ophiopogonis, 1 part of Huai Chrysanthemi, Radix Glycyrrhizae 8
Part, 5 parts of jujube, 5 parts of honeysuckle, 1 part of fructus lycii, 3 parts of cape jasmine, 8 parts of mulberry leaf, 1 part of radix scrophulariae, 2 parts of lily, 1 part of semen coicis, rhizoma polygonati
3 parts, 2 parts of peppermint；
(2) by step (1) by each raw material according to material: water=1:10 ratio adds water, is existed after impregnating 8 hours with traditional Chinese medicine extraction device
It extracts 30 minutes at a temperature of 100 DEG C, then filters, filter vacuum is taken to be concentrated and be spray-dried to get into self-control iron rod yam
Liquid medicine extract.
Self-control iron rod yam Chinese medicine alcohol extract is made of following methods: the filter residue after water is mentioned crushed after being dried
20 meshes, according to material after weighing: ethyl alcohol (75%)=1:10 ratio flows back alcohol extracting 3 hours at a temperature of 60 DEG C, then filters
To iron rod yam Chinese medicine alcohol extract, iron rod yam Chinese medicine is arrived using heating concentration (recycling ethyl alcohol) and after being dried
Alcohol extract.
Make by oneself iron rod yam herb fermenting extract the preparation method comprises the following steps:
(1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, 2 parts of sucrose of addition is red
6 parts of sugar, 40 parts of iron rod yam dry plate, 400 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection 20 minutes, then
It is cooled to 28 DEG C；
(2) Angel dry ferment (strain be purchased from Angel Group company high glycoform) and 0.05% is added according to the 3% of fermentation material total amount
Lu Shi Zygosaccharomyces bacterium strain (strain is purchased from Beijing Yu Wei Science and Technology Ltd. bacterium numbering CICC1417), at a temperature of 28 DEG C
It is passed through filtrated air aerobic fermentation 1 day, system is then warming up to 35 DEG C, add 4 parts of glucose, 3 parts of Pidolidone list sodium,
CaCl20.07 part, 5 parts of yeast extract and access 3 parts Lactobacillus pentosus (strain be purchased from Beijing Yu Wei Science and Technology Ltd., bacterium
Kind number CICC23117), and be passed through filtrated air and ferment 4 days, the prebiotic bacterial content sum of the remnants in inspection system works as sum
≤ 500cfu/ml, when having no living contaminants, stops fermentation, filters out fermentation liquid, fermentation liquid is first crossed 300 meshes, later by filtrate
After 600 meshes after dilution half, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, it is cold by vacuum
Be lyophilized it is dry after, obtain self-control iron rod yam herb fermenting extract.
The preparation method of lipstick containing iron rod yam ingredient, preparation step are as follows:
(1) weigh the raw material of following parts by weight: 6 parts of tridecanol trimellitate, D & C is 27#0.3 parts red, and 6#3 parts of C Huang of D &,
3 parts of iron rod yam polypeptide powder, 2 parts of iron rod yam saponin(e, 2 parts of iron rod yam polysaccharide, self-control iron rod yam Chinese medicine water extract
3.39 parts, 2 parts 2 parts of iron rod yam Chinese medicine alcohol extracting thing of self-control, self-control of iron rod yam herb fermenting extract；
(2) after mixing the raw material of each parts by weight in step (1), upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 4 parts of Natural Carnauba wax bears 3 parts of ground lira wax, 2 parts of natural beeswax, rose
1 part of floral wax, 0.1 part of tuberose floral wax, 0.5 part of acacia farnesiana floral wax, 0.1 part of white orchid floral wax, Chilean hazel seed oily 2.6 parts, fat prok
It is 3.9 parts of seed rouge, 4 parts of simple and unsophisticated A Su fruit oil, 3 parts of peony seed oil, 3 parts of Amygdalus pedunculata benevolence oil, 5 parts of phytosterols oletate, three different
5 parts of the smooth olive oleate of 15.5 parts of stearyl alcohol citrate, sorb, 2 parts of olive oil Cer NP, olive oil hyalomitome
Acid 2 parts, 9 parts of Nexbase 2004,10 parts of tridecanol trimellitate, 3 parts of wheat-germ oil, VE oil 2 parts, 0.1 part of BHT,
TBHQ0.01 parts, 0.4 part of methyl p-hydroxybenzoate, 0.1 part of propylparaben.
(4) each component raw material in step (3) is heated into consolute in stainless steel kettle, temperature is controlled at 85 DEG C, melted repeatedly
Refining is allowed to uniform；45 DEG C of temperature are cooled to later, are added 2 parts of Chinese yam flavones, are stirred evenly, it is stand-by to obtain B component.
(5) component A is added in B component, is stirred evenly at a temperature of 45 DEG C.Rouge mold is cast in after froth in vacuum
In, casting is put into refrigerator freezing 10 minutes, and demoulding is examined, and qualified product packaging is finished product.
Embodiment 2
The present embodiment self-control iron rod yam water extract of TCM the preparation method comprises the following steps:
(1) raw material of following parts by weight is weighed: 50 parts of iron rod yam dry plate, 8 parts of radix polygonati officinalis, 4 parts of Radix Ophiopogonis, 2 parts of Huai Chrysanthemi, Radix Glycyrrhizae 6
Part, 7 parts of jujube, 3 parts of honeysuckle, 4 parts of fructus lycii, 1 part of cape jasmine, 6 parts of mulberry leaf, 2 parts of radix scrophulariae, 2 parts of lily, 2 parts of semen coicis, rhizoma polygonati
1 part, 2 parts of peppermint；
(2) by step (1) by each raw material according to material: water=1:10 ratio adds water, uses traditional Chinese medicine extraction device after impregnating 8.5 hours
It extracts 35 minutes at a temperature of 101 DEG C, then filters, take filter vacuum to be concentrated and be spray-dried to get self-control iron rod yam is arrived
Water extract of TCM.
Make by oneself iron rod yam Chinese medicine alcohol extract the preparation method comprises the following steps:
Filter residue after water is mentioned crushed 20 meshes after being dried, according to material after weighing: ethyl alcohol (80%)=1:9 ratio exists
It flows back alcohol extracting 2.5 hours at a temperature of 65 DEG C, iron rod yam Chinese medicine alcohol extract is then obtained by filtration, using heating concentration (recycling
Ethyl alcohol) and be dried after to get arrive iron rod yam Chinese medicine alcohol extract；
Make by oneself iron rod yam herb fermenting extract the preparation method comprises the following steps:
(1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, 3 parts of sucrose of addition is red
4 parts of sugar, 30 parts of iron rod yam dry plate, 500 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection 25 minutes, then
It is cooled to 30 DEG C；
(2) Shandong that Angel dry ferment (strain is purchased from Angel Group company high glycoform) and 0.1% is added according to the 3% of fermentation material total amount
Family name Zygosaccharomyces bacterium strain (strain is purchased from Beijing Yu Wei Science and Technology Ltd. bacterium numbering CICC1417), leads at a temperature of 30 DEG C
Enter filtrated air aerobic fermentation 1.5 days, system is then warming up to 36 DEG C, adds 4 parts of glucose, 2 parts of Pidolidone list sodium,
CaCl20.06 part, 5 parts of yeast extract simultaneously accesses 1.94 parts of Lactobacillus pentosus (strain is purchased from the limited public affairs of Beijing Henan dimension science and technology
Department, bacterium numbering CICC23117), and be passed through filtrated air and ferment 3.5 days, the prebiotic bacterial content sum of the remnants in inspection system,
As Zong Shuo≤500cfu/ml, when having no living contaminants, stop fermentation, filter out fermentation liquid, fermentation liquid is first crossed into 300 meshes, later
After 600 meshes after filtrate is diluted one times, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, is passed through
After vacuum freeze drying, self-control iron rod yam herb fermenting extract is obtained.
The preparation method of lipstick containing iron rod yam ingredient, preparation step are as follows:
(1) weigh the raw material of following parts by weight: 13 parts of tridecanol trimellitate, D & C is 27#0.5 parts red, D & C Huang 6#0.5
Part, 2 parts of iron rod yam polypeptide powder, 2 parts of iron rod yam saponin(e, 0.19 part of iron rod yam polysaccharide, self-control iron rod yam in liquid medicine mention
Take 5 parts 4.5 parts of object, 2 parts of iron rod yam Chinese medicine alcohol extracting thing of self-control, self-control of iron rod yam herb fermenting extract；
(2) after mixing the raw material of each parts by weight in step (1), upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 6 parts of Natural Carnauba wax bears 2 parts of ground lira wax, 4 parts of natural beeswax, rose
0.5 part of floral wax, 0.1 part of tuberose floral wax, 0.4 part of acacia farnesiana floral wax, 0.3 part of white orchid floral wax, Chilean hazel seed oily 1 part, fat prok
It is 4 parts of seed rouge, 3 parts of simple and unsophisticated A Su fruit oil, 2.2 parts of peony seed oil, 4 parts of Amygdalus pedunculata benevolence oil, 3 parts of phytosterols oletate, three different
5 parts of the smooth olive oleate of 14.4 parts of stearyl alcohol citrate, sorb, 1 part of olive oil Cer NP, olive oil hyalomitome
Sour 1.5 parts, 8 parts of Nexbase 2004,6 parts of tridecanol trimellitate, 2 parts of wheat-germ oil, VE oil 1.2 parts, BHT 0.06
Part, TBHQ0.05 parts, 0.4 part of methyl p-hydroxybenzoate, 0.2 part of propylparaben；
(4) each component raw material in step (3) is heated into consolute in stainless steel kettle, temperature is controlled at 90 DEG C, and melt back makes
It is uniform；It is cooled at a temperature of 50 DEG C later, is added 1.5 parts of Chinese yam flavones, stirs evenly, it is stand-by to obtain B component；
(5) component A is added in B component, is stirred evenly at 50 °C.It is cast in Rouge mold after froth in vacuum,
Casting is put into refrigerator freezing 10 minutes, and demoulding is examined, and qualified product packaging is finished product.
Embodiment 3
The present embodiment self-control iron rod yam water extract of TCM the preparation method comprises the following steps:
(1) raw material of following parts by weight is weighed: 45 parts of iron rod yam dry plate, 4 parts of radix polygonati officinalis, 10 parts of Radix Ophiopogonis, 1.5 parts of Huai Chrysanthemi, sweet
7 parts of grass, 6 parts of jujube, 4 parts of honeysuckle, 5 parts of fructus lycii, 2.5 parts of cape jasmine, 7 parts of mulberry leaf, 3 parts of radix scrophulariae, 1 part of lily, semen coicis 2
Part, 1 part of rhizoma polygonati, 1 part of peppermint；
(2) by step (1) by each raw material according to material: water=1:10 ratio adds water, is existed after impregnating 9 hours with traditional Chinese medicine extraction device
It extracts 40 minutes at a temperature of 102 DEG C, then filters, filter vacuum is taken to be concentrated and be spray-dried to get into self-control iron rod yam
Liquid medicine extract.
Make by oneself iron rod yam Chinese medicine alcohol extract the preparation method comprises the following steps:
Filter residue after water is mentioned crushed 20 meshes after being dried, according to material after weighing: ethyl alcohol (85%)=1:8 ratio exists
It flows back alcohol extracting 2.5 hours at a temperature of 70 DEG C, iron rod yam Chinese medicine alcohol extract is then obtained by filtration, using heating concentration (recycling
Ethyl alcohol) and be dried after to get arrive iron rod yam Chinese medicine alcohol extract.
Make by oneself iron rod yam herb fermenting extract the preparation method comprises the following steps:
(1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, 4 parts of sucrose of addition is red
5 parts of sugar, 20 parts of iron rod yam dry plate, 500 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection 30 minutes, then
It is cooled to 32 DEG C；
(2) Angel dry ferment (strain be purchased from Angel Group company high glycoform) and 0.07% is added according to the 1% of fermentation material total amount
Lu Shi Zygosaccharomyces bacterium strain (strain is purchased from Beijing Yu Wei Science and Technology Ltd. bacterium numbering CICC1417), at a temperature of 32 DEG C
It is passed through filtrated air aerobic fermentation 1 day, system is then warming up to 37 DEG C, add 3 parts of glucose, 1 part of Pidolidone list sodium,
CaCl20.1 part, 3 parts of yeast extract and access 1.5 parts Lactobacillus pentosus (strain be purchased from Beijing Yu Wei Science and Technology Ltd.,
Bacterium numbering CICC23117), and be passed through filtrated air and ferment 3.5 days, the prebiotic bacterial content sum of the remnants in inspection system, when
Zong Shuo≤500cfu/ml, when having no living contaminants, stops fermentation, filters out fermentation liquid, and fermentation liquid is first crossed 300 meshes, later will
After 600 meshes after one times of filtrate dilution, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, by true
After vacuum freecing-dry, self-control iron rod yam herb fermenting extract is obtained.
A kind of preparation method of the lipstick containing iron rod yam ingredient, steps are as follows:
(1) weigh the raw material of following parts by weight: 5 parts of tridecanol trimellitate, D & C is 27#2 parts red, and 6#0.5 parts of C Huang of D &,
4.5 parts of iron rod yam polypeptide powder, 0.1 part of iron rod yam saponin(e, 0.1 part of iron rod yam polysaccharide, self-control iron rod yam in liquid medicine mention
Take 4 parts 5 parts of object, 1 part of iron rod yam Chinese medicine alcohol extracting thing of self-control, self-control of iron rod yam herb fermenting extract；
(2) after mixing the raw material of each parts by weight in step (1), upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 0.5 part of Natural Carnauba wax bears 3 parts of ground lira wax, 8 parts of natural beeswax, rose
1 part of rare floral wax, 0.5 part of tuberose floral wax, 0.4 part of acacia farnesiana floral wax, 0.4 part of white orchid floral wax, Chilean hazel seed oily 3 parts, fat prok
It is 4 parts of seed rouge, 5 parts of simple and unsophisticated A Su fruit oil, 2.5 parts of peony seed oil, 5 parts of Amygdalus pedunculata benevolence oil, 4 parts of phytosterols oletate, three different
6 parts of the smooth olive oleate of 18 parts of stearyl alcohol citrate, sorb, 0.5 part of olive oil Cer NP, olive oil hyalomitome
Sour 1 part, 4 parts of Nexbase 2004,7 parts of tridecanol trimellitate, 2.5 parts of wheat-germ oil, VE oil 0.5 part, BHT 0.1
Part, TBHQ0.1 parts, 0.3 part of methyl p-hydroxybenzoate, 0.2 part of propylparaben；
(4) each component raw material in step (3) is heated into consolute in stainless steel kettle, temperature is controlled at 95 DEG C, and melt back makes
It is uniform；It is cooled at a temperature of 55 DEG C later, is added 1.0 parts of Chinese yam flavones, stirs evenly, it is stand-by to obtain B component；
(5) component A is added in B component, stirs evenly at a temperature of 55 DEG C, is cast in Rouge mold after froth in vacuum,
Casting is put into refrigerator freezing 10 minutes, and demoulding is examined, and qualified product packaging is finished product.
Embodiment 4
The present embodiment self-control iron rod yam water extract of TCM the preparation method comprises the following steps:
(1) raw material of following parts by weight is weighed: 52 parts of iron rod yam dry plate, 6 parts of radix polygonati officinalis, 11 parts of Radix Ophiopogonis, 2 parts of Huai Chrysanthemi, Radix Glycyrrhizae 5
Part, 5 parts of jujube, 2 parts of honeysuckle, 2 parts of fructus lycii, 2 parts of cape jasmine, 6 parts of mulberry leaf, 1.5 parts of radix scrophulariae, 1 part of lily, 1.5 parts of semen coicis,
2 parts of rhizoma polygonati, 1.5 parts of peppermint；
(2) by step (1) by each raw material according to material: water=1:10 ratio adds water, is existed after impregnating 10 hours with traditional Chinese medicine extraction device
It extracts 30 minutes at a temperature of 104 DEG C, then filters, filter vacuum is taken to be concentrated and be spray-dried to get into self-control iron rod yam
Liquid medicine extract；
Make by oneself iron rod yam Chinese medicine alcohol extract the preparation method comprises the following steps:
Filter residue after water is mentioned crushed 20 meshes after being dried, according to material after weighing: ethyl alcohol (90%)=1:8.5 ratio
It flows back alcohol extracting 3 hours at a temperature of 65 DEG C, iron rod yam Chinese medicine alcohol extract is then obtained by filtration, using heating concentration (recycling
Ethyl alcohol) and be dried after to get arrive iron rod yam Chinese medicine alcohol extract.
Make by oneself iron rod yam herb fermenting extract the preparation method comprises the following steps:
(1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, 3 parts of sucrose of addition is red
4.5 parts of sugar, 35 parts of iron rod yam dry plate, 500 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection 30 minutes, so
After be cooled to 32 DEG C；
(2) Angel dry ferment (strain is purchased from Angel Group company high glycoform) and 0.09% is added according to the 2.5% of fermentation material total amount
Lu Shi Zygosaccharomyces bacterium strain (strain be purchased from Beijing Yu Wei Science and Technology Ltd. bacterium numbering CICC1417), in 32 DEG C of temperature
Under be passed through filtrated air aerobic fermentation 2 days, system is then warming up to 36 DEG C, adds 5 parts of glucose, Pidolidone list sodium 2
Part, CaCl20.08 part, 4 parts of yeast extract simultaneously accesses 2 parts of Lactobacillus pentosus (strain is purchased from the limited public affairs of Beijing Henan dimension science and technology
Department, bacterium numbering CICC23117), and be passed through filtrated air and ferment 3 days, the prebiotic bacterial content sum of the remnants in inspection system, when
Zong Shuo≤500cfu/ml, when having no living contaminants, stops fermentation, filters out fermentation liquid, and fermentation liquid is first crossed 300 meshes, later will
After 600 meshes after one times of filtrate dilution, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, by true
After vacuum freecing-dry, self-control iron rod yam herb fermenting extract is obtained.
The preparation method of lipstick containing iron rod yam ingredient, steps are as follows:
(1) raw material of following parts by weight is weighed: 15 parts of tridecanol trimellitate, 0.1 part of the red 27# of D & C, D & C Huang 6#3
4 parts of part iron rod yam polypeptide powder, 2 parts of iron rod yam polysaccharide, makes liquid medicine extraction in iron rod yam by oneself at 2.5 parts of iron rod yam saponin(e
3 parts 3 parts of object, 1.5 parts of iron rod yam Chinese medicine alcohol extracting thing of self-control, self-control of iron rod yam herb fermenting extract；
(2) after mixing the raw material of each parts by weight in step (1), upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 2 parts of Natural Carnauba wax, bear 0.1 part of ground lira wax, 6.5 parts of natural beeswax,
0.1 part of rose floral wax, 0.4 part of tuberose floral wax, 0.3 part of acacia farnesiana floral wax, 0.1 part of white orchid floral wax, Chilean hazel seed oily 2 parts, pig
2 parts of oily fruit seed rouge, 2 parts of simple and unsophisticated A Su fruit oil, 2 parts of peony seed oil, Amygdalus pedunculata benevolence oily 2 parts, 2 parts of phytosterols oletate, three
4.59 parts of the smooth olive oleate of 14 parts of isooctadecanol citrate, sorb, 1.4 parts of olive oil Cer NP, olive oil
1.5 parts of hyaluronic acid, 10 parts of Nexbase 2004,8 parts of tridecanol trimellitate, 0.5 part of wheat-germ oil, VE oil 1 part,
0.01 part of BHT, TBHQ0.1 parts, methyl p-hydroxybenzoate 0.2,0.2 part of propylparaben；
(4) each component raw material in step (3) is heated into consolute in stainless steel kettle, temperature is controlled at 85 DEG C, and melt back makes
It is uniform；It is cooled at a temperature of 55 DEG C later, is added 0.5 part of Chinese yam flavones, stirs evenly, it is stand-by to obtain B component；
(5) component A is added in B component, stirs evenly at a temperature of 45 DEG C, is cast in Rouge mold after froth in vacuum,
Casting is put into refrigerator freezing 10 minutes, and demoulding is examined, and qualified product packaging is finished product.
Embodiment 5
The present embodiment self-control iron rod yam water extract of TCM the preparation method comprises the following steps:
(1) raw material of following parts by weight is weighed: 59 parts of iron rod yam dry plate, 5 parts of radix polygonati officinalis, 12 parts of Radix Ophiopogonis, 1 part of Huai Chrysanthemi, Radix Glycyrrhizae 5
Part, 5 parts of jujube, 1 part of honeysuckle, 1 part of fructus lycii, 1 part of cape jasmine, 5 parts of mulberry leaf, 1 part of radix scrophulariae, 1 part of lily, 1 part of semen coicis, rhizoma polygonati
1 part, 1 part of peppermint；
(2) by step (1) by each raw material according to material: water=1:10 ratio adds water, is existed after impregnating 10 hours with traditional Chinese medicine extraction device
It extracts 30 minutes at a temperature of 105 DEG C, then filters, filter vacuum is taken to be concentrated and be spray-dried to get into self-control iron rod yam
Liquid medicine extract.
Make by oneself iron rod yam Chinese medicine alcohol extract the preparation method comprises the following steps:
Filter residue after water is mentioned crushed 20 meshes after being dried, according to material after weighing: ethyl alcohol (95%)=1:7 ratio exists
It flows back alcohol extracting 2 hours at a temperature of 80 DEG C, iron rod yam Chinese medicine alcohol extract is then obtained by filtration, using heating concentration (recycling second
Alcohol) and be dried after to get arrive iron rod yam Chinese medicine alcohol extract.
Make the preparation step of iron rod yam herb fermenting extract by oneself are as follows:
(1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, 4 parts of sucrose of addition is red
4 parts of sugar, 25 parts of iron rod yam dry plate, 500 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection 20 minutes, then
It is 30 DEG C cooling；
(2) Angel dry ferment (strain be purchased from Angel Group company high glycoform) and 0.08% is added according to the 2% of fermentation material total amount
Lu Shi Zygosaccharomyces bacterium strain (strain is purchased from Beijing Yu Wei Science and Technology Ltd. bacterium numbering CICC1417), at a temperature of 29 DEG C
It is passed through filtrated air aerobic fermentation 1.5 days, system is then warming up to 36 DEG C, add 3 parts of glucose, Pidolidone list sodium 3
Part, CaCl20.09 part, 3 parts of yeast extract simultaneously accesses 2.5 parts of Lactobacillus pentosus (strain is purchased from the limited public affairs of Beijing Henan dimension science and technology
Department, bacterium numbering CICC23117), and be passed through filtrated air and ferment 2 days, the prebiotic bacterial content sum of the remnants in inspection system, when
Zong Shuo≤500cfu/ml, when having no living contaminants, stops fermentation, filters out fermentation liquid, and fermentation liquid is first crossed 300 meshes, later will
After 600 meshes after one times of filtrate dilution, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, by true
After vacuum freecing-dry, self-control iron rod yam herb fermenting extract is obtained.
The preparation method of lipstick containing iron rod yam ingredient, steps are as follows
(1), weigh the raw material of following parts by weight: 11.45 parts of tridecanol trimellitate, D & C is 27#2.5 parts red, and D & C is yellow
6#2.5 parts, 2.5 parts of iron rod yam polypeptide powder, 1.5 parts of iron rod yam polysaccharide, is made by oneself in iron rod yam 3 parts of iron rod yam saponin(e
4 parts 4 parts of liquid medicine extract, 2 parts of iron rod yam Chinese medicine alcohol extracting thing of self-control, self-control of iron rod yam herb fermenting extract；
(2) by step, (after the raw material of each parts by weight mixes in 10, upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 5 parts of Natural Carnauba wax bears 1 part of ground lira wax, 8 parts of natural beeswax, rose
0.4 part of floral wax, 0.1 part of tuberose floral wax, 0.2 part of acacia farnesiana floral wax, 0.5 part of white orchid floral wax, Chilean hazel seed oily 2.4 parts, lard
It is 6 parts of fruit seed rouge, 4 parts of simple and unsophisticated A Su fruit oil, 1 part of peony seed oil, 4 parts of Amygdalus pedunculata benevolence oil, 1 part of phytosterols oletate, three different
2 parts of the smooth olive oleate of 19.3 parts of stearyl alcohol citrate, sorb, 0.1 part of olive oil Cer NP, olive oil are transparent
Matter acid 1.3 parts, 3 parts of Nexbase 2004,5 parts of tridecanol trimellitate, 1 part of wheat-germ oil, VE oil 0.4 part, BHT 0.1
Part, TBHQ0.05 parts, 0.5 part of methyl p-hydroxybenzoate, 0.2 part of propylparaben；
(4) each component raw material in step (3) is heated into consolute in stainless steel kettle, temperature controls between 85-95 DEG C, repeatedly
Melting is allowed to uniform；It is cooled at a temperature of 60 DEG C later, is added 0.05 part of Chinese yam flavones, stirs evenly, it is stand-by to obtain B component.
(5) component A is added in B component, is stirred evenly at a temperature of 60 DEG C.Rouge mold is cast in after froth in vacuum
In, casting is put into refrigerator freezing 10 minutes, and demoulding is examined, and qualified product packaging is finished product.
Implementation result example
Product prepared by the embodiment of the present invention 1 is through inspection institute's testing result table:
As seen from the above table lipstick disclosed by the invention better than the Ministry of Public Health " cosmetics safety technical specification " 2015 editions, " cosmetics have
Noxious material limitation ", arsenic, cadmium, excrement colibacillus group, staphylococcus aureus, Pseudomonas aeruginosa are not detected in lipstick of the present invention.
Product stability data
Product stability experimental result is shown in Table one, wherein 1,2,3,4, No. 5 sample respectively corresponds embodiment 1,2,3,4,5.
One product stability experimental result of table
Table one the result shows that, the lipstick that the application prepares has good hot cold stability, meets national QB/T1977-2004
Standard.
Product using effect:
By women of 369 ages between 18 to 65 years old, effect is used using the lipstick product in table one daily in three months
Fruit feedback is: 79.6% women states that their lip whole day wetability is fine.Indicating after 92.3% women is on probation should
Lipstick formulations use skin sense fine, and can be persistently comfortable and moist.The lipstick unlike is easy that stiff or effect is lasting like that
Property it is poor, but more with better.Effect after two months be superior to one month after effect, the effect after three months is superior to two
Effect after month, this illustrates that high nutrition lipstick of the invention can actually continue maintenance lip skin.86.5% women indicates examination
After one month, lip skin just makes moderate progress.Seem healthier after two months, natural and young, improvement is obvious.
After three months significant effect and stablize persistently, 88.9% women indicates the lipstick, either in appearance, smell, color, smearing
Property, dicoration etc., or moisture retention, moistness, trophism, prosthetic, in terms of it is pretty good, especially
It is that trophism and anti-aging are best.People can be allowed the more to use the more young, and use and trust, there is the feeling after eating iron rod yam.It is overall
On say, young woman is better than to the effect of female middle-aged and old women；But the using effect of young woman is also significantly better than city
The effect of general lipstick product on field.It is strictly a high-end efficient lip treatments to verify the lipstick.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (6)
1. a kind of lipstick containing iron rod yam ingredient, it is characterised in that: the raw material of the lipstick include iron rod yam polypeptide powder,
Iron rod yam saponin(e, iron rod yam polysaccharide, iron rod yam flavones, self-control iron rod yam Chinese medicine water extract, self-control iron rod yam
Chinese medicine alcohol extracting thing, bears ground lira wax, natural beeswax, rose at self-control iron rod yam herb fermenting extract, Natural Carnauba wax
Rare floral wax, tuberose floral wax, acacia farnesiana floral wax, white orchid floral wax, Chilean hazel seed oil, lard fruit seed rouge, simple and unsophisticated A Su fruit oil, tree peony
Seed oil, Amygdalus pedunculata benevolence oil, iron rod yam essential oil, phytosterols oletate, three isooctadecanol citrates, the smooth olive oil of sorb
Acid esters, olive oil Cer NP, olive oil hyaluronic acid, Nexbase 2004, tridecanol trimellitate, D & C are red
27#, D & C Huang 6#, wheat-germ oil, VE oil, BHT, TBHQ, methyl p-hydroxybenzoate and propylparaben.
2. the lipstick according to claim 1 containing iron rod yam ingredient, which is characterized in that each raw material in the lipstick
Parts by weight are as follows: 0.1-5 parts of iron rod yam polypeptide powder, 0.1-3 parts of iron rod yam saponin(e, 0.1-2 parts of iron rod yam polysaccharide, iron rod
0.05-2 parts of Chinese yam flavones, 0.1-5 parts of iron rod yam Chinese medicine water extract of self-control, self-control iron rod yam Chinese medicine alcohol extracting thing 0.1-
2 parts, self-control 0.1-3 part of iron rod yam herb fermenting extract, 0.5-6 parts of Natural Carnauba wax, bear lira wax 0.1-3
Part, beeswax 0.5-8 parts natural, 0.1-1 parts of rose floral wax, 0.1-1 parts of tuberose floral wax, 0.1-0.5 parts of acacia farnesiana floral wax, white orchid
0.1-0.5 parts of floral wax, Chilean 0.5-3 parts of hazel seed oil, 0.5-6 parts of lard fruit seed rouge, 0.5-5 parts of simple and unsophisticated A Su fruit oil, peony seeds
It is 0.5-3 parts oily, 0.5-5 parts of Amygdalus pedunculata benevolence oil, 0.05-3 parts of iron rod yam essential oil, 0.5-5 parts of phytosterols oletate, three different
1-6 parts of 5-20 parts of stearyl alcohol citrate, sorb smooth olive oleate, 0.1-2 parts of olive oil Cer NP, olive oil
0.5-2 parts of hyaluronic acid, 1-10 parts of Nexbase 2004,5-25 parts of tridecanol trimellitate, D & C be 27#0.1-3 parts red,
0.5-5 parts of D & C Huang 6#, 0.5-3 parts of wheat-germ oil, 0.5-2 parts of VE oil, BHT0.01-0.1 parts, 0.01-0.1 parts of TBHQ,
0.1-0.5 parts and propylparaben 0.1-0.5 parts of methyl p-hydroxybenzoate.
3. the lipstick according to claim 1 or 2 containing iron rod yam ingredient, which is characterized in that the self-control iron rod mountain
Medicine water extract of TCM the preparation method comprises the following steps:
A, the raw material of following parts by weight, 40-60 parts of iron rod yam dry plate, 0 part of radix polygonati officinalis 5-1, Radix Ophiopogonis 10-15 part, Huai Chrysanthemi are weighed
1-2 parts, 5-8 parts of Radix Glycyrrhizae, 5-10 parts of jujube, 1-5 parts of honeysuckle, 1-5 parts of fructus lycii, 1-3 parts of cape jasmine, 5-8 parts of mulberry leaf, radix scrophulariae 1-
3 parts, 1-2 parts of lily, 1-3 parts of semen coicis, 1-3 parts of rhizoma polygonati, 1-2 parts of peppermint；
B, by raw material each in step a according to material: water=1:10 ratio adds water, used after impregnating 8-10 hour traditional Chinese medicine extraction device in
Extracted 30-40 minutes at 100-105 DEG C, then filter, obtain filter residue and filtrate, take filter vacuum be concentrated and be spray-dried to get
To self-control iron rod yam water extract of TCM.
4. the lipstick according to claim 3 containing iron rod yam ingredient, which is characterized in that in the self-control iron rod yam
Medicine extractive from fermentative the preparation method comprises the following steps:
1) it will mention by water and being added in enamel fermentor with the iron rod yam Chinese medicine filter residue after alcohol extracting, sucrose 2-4 parts of addition is red
It is 4-6 parts sugared, 20-40 parts of iron rod yam dry plate, 400-500 parts of water, after system is heated to boiling under stirring, then constant temperature disinfection
It 20-30 minutes, is then cooled to 28-32 DEG C and obtains fermentation material；
2) the Lu Shi Zygosaccharomyces bacterium strain of Angel dry ferment and 0.05-0.1% is added according to the 1-3% of fermentation material total amount, in 28-
It is passed through filtrated air aerobic fermentation at a temperature of 32 DEG C 1-2 days, system is then warming up to 35-37 DEG C, adds glucose 3-5
Part, 1-3 parts of Pidolidone list sodium, CaCl20.05-0.1 parts, 3-5 parts of yeast extract and access fermentation system quality 1-3%'s
Lactobacillus pentosus is simultaneously passed through filtrated air and ferments 2-4 days, the prebiotic bacterial content sum of the remnants in inspection system, when always count≤
When 500cfu/ml has no living contaminants, stop fermentation, filter out fermentation liquid, fermentation liquid is first crossed into 300 meshes, it is later that filtrate is dilute
After 600 meshes after releasing one times, then fermentation liquid is build-up ice under the conditions of -60 DEG C, then subliming water, by vacuum refrigeration
After drying, self-control iron rod yam herb fermenting extract is obtained.
5. the lipstick as claimed in claim 4 containing iron rod yam ingredient, which is characterized in that the concrete operations of the alcohol extracting are as follows:
Water intaking mention after filter residue after being dried, crushed 20 meshes, according to material after weighing: 75%-95% ethyl alcohol 1:(7-10) body
Product ratio, flows back alcohol extracting 2-3 hours at a temperature of 60-80 DEG C, iron rod yam Chinese medicine alcohol extract is then obtained by filtration, using heating
Concentration is dried to get iron rod yam Chinese medicine alcohol extract is arrived.
6. the preparation method of the lipstick containing iron rod yam ingredient described in claim 5, which is characterized in that steps are as follows:
(1) weigh the raw material of following parts by weight: 5-15 parts of tridecanol trimellitate, D & C are 27# 0.1-3 parts red, D & C is yellow
0.5-5 parts of 6#, 0.1-5 parts of iron rod yam polypeptide powder, 0.1-3 parts of iron rod yam saponin(e, 0.1-2 parts of iron rod yam polysaccharide, self-control
0.1-5 parts of iron rod yam Chinese medicine water extract, 0.1-2 parts of iron rod yam alcohol extracting thing of self-control, self-control iron rod yam herb fermenting
0.1-3 parts of extract；
(2) after mixing the raw material of each parts by weight in step (1), upper three-roll grinder is adequately ground, and obtains A after uniform
Component, for use；
(3) weigh the raw material of following parts by weight: 0.5-6 parts of Natural Carnauba wax bears ground 0.1-3 parts of lira wax, natural beeswax
0.5-8 parts, 0.1-1 parts of rose floral wax, 0.1-1 parts of tuberose floral wax, 0.1-0.5 parts of acacia farnesiana floral wax, white orchid floral wax 0.1-0.5
Part, Chilean 0.5-3 parts of hazel seed oil, 0.5-6 parts of lard fruit seed rouge, 0.5-5 parts of simple and unsophisticated A Su fruit oil, 0.5-3 parts of peony seed oil, length
0.5-5 parts of handle almond oil, 0.5-5 parts of phytosterols oletate, 5-20 parts of three isooctadecanol citrate, the smooth olive oil of sorb
1-6 parts of acid esters, 0.1-2 parts of olive oil Cer NP, 0.5-2 parts of olive oil hyaluronic acid, 1-10 parts of Nexbase 2004,
5-10 parts of tridecanol trimellitate, 0.5-3 parts of wheat-germ oil, 0.5-2 parts of VE oil, 0.01-0.1 parts of BHT,
TBHQ0.01-0.1 parts, 0.1-0.5 parts of methyl p-hydroxybenzoate, 0.1-0.5 parts of propylparaben；
(4) each component raw material in step (1) is heated into consolute in stainless steel kettle, temperature controls between 85-95 DEG C, repeatedly
Melting is allowed to uniformly, cool at a temperature of 45-60 DEG C later, is added 0.05-2 parts of Chinese yam flavones, stirs evenly, obtain B component,
For use；
(5) component A is added in B component, is stirred evenly at a temperature of 45-60 DEG C, Rouge mold is cast in after froth in vacuum
In, after cooling and shaping, demoulding is examined, up to the lipstick containing iron rod yam ingredient after qualification.
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| CN110897991A (en) * | 2019-12-26 | 2020-03-24 | 上海新如生物科技有限公司 | Lip gloss with skin care function and preparation method thereof |
| CN116035994A (en) * | 2023-02-08 | 2023-05-02 | 上海侬本雅生物科技有限公司 | Method for preparing polygonatum odoratum extract by adopting probiotics fermentation |
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Application publication date: 20191105 |