CN105796444A - Method for extracting kohlrabi extract from kohlrabi fruits and application of kohlrabi extract - Google Patents
Method for extracting kohlrabi extract from kohlrabi fruits and application of kohlrabi extract Download PDFInfo
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- CN105796444A CN105796444A CN201610345990.1A CN201610345990A CN105796444A CN 105796444 A CN105796444 A CN 105796444A CN 201610345990 A CN201610345990 A CN 201610345990A CN 105796444 A CN105796444 A CN 105796444A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention relates to the field of plant application research, in particular a method for extracting a kohlrabi extract from kohlrabi fruits and an application of the kohlrabi extract. By virtue of an atomizing extraction and separation technology, the kohlrabi extract is extracted from kohlrabi corms, and the kohlrabi extract, as an accessory, can be added to cosmetics so as to prepare such products as a facial mask, a facial cleanser, a shampoo, a skin lotion, a moisturizer, a whitening cream, an essence and the like specifically. The extracting method disclosed by the invention has the beneficial effects that by atomizing raw material liquid, dynamic continuity of a production process is achieved, so that a production production is increased by several times; by virtue of atomizing, a mass transfer process between materials and a solvent is improved and limitation on mass transfer conditions is reduced, so that energy consumption and solvent consumption are greatly reduced and production cost is reduced; and meanwhile, a leaching rate of active ingredients is improved, so that the full utilization of medicinal raw materials is achieved and income is increased; and the kohlrabi extract, which contains organism immunity enhancing ingredients and various nutrient ingredients, is applicable to cosmetics, so that the application scope of the kohlrabi extract is widened.
Description
Technical field
The present invention relates to plant application research field, be specially a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit and application thereof.
Background technology
Corm Brassicae caulorapae is the one of Caulis et Folium Brassicae capitatae, and formal name used at school is kohlrabi.Corm Brassicae caulorapae is the vegetable between root-mustard and cabbage, it is possible to bringing steams in clear soup is used as pickles, or cold and dressed with sauce salad is made in shredding.Its Vitamin C content is high, and one glass of Corm Brassicae caulorapae boiled contains 1.5 times of " every day advises intake ".It is also containing substantial amounts of potassium, and the content of vitamin E also above " every day advises intake " 10%.According to nutritionist analysis, containing 5.9 grams of protein in every 500 grams of Corm Brassicae caulorapaes. sugar 11 grams, crude fibre 4.1 grams, ash 3.3 grams, calcium 81 milligrams, 122 milligrams of phosphorus, ferrum 1.1 milligrams, carotene trace, thiamine 0.19 milligram, 0.07 milligram of riboflavin, nicotinic acid 1.5 milligrams, vitamin C 152 milligrams.Corm Brassicae caulorapae vitamin content is very abundant, and especially fresh goods strand juice is taken, and gastropathy has treatment make.The signboard nutrients such as its contained vitamin C, have the effect of pain relieving granulation promoting, can promote the healing of gastroduodenal ulcer.Include large quantity of moisture and dietary fiber, can wide intestinal relieving constipation, anti-treat constipation, get rid of toxin.Corm Brassicae caulorapae, possibly together with abundant vitamin E, has the effect strengthening immune function of human body.Contained trace element molybdenum, can suppress the synthesis of inferior ammonium nitrate, thus have certain anti-cancer and kill cancer action.
A kind of Corm Brassicae caulorapae crystal dry (CN201310270890.3) disclosed in Chinese patent storehouse, by Corm Brassicae caulorapae screened stock, 1.5% carrageenan, 3% glucose, 4% white sugar, 30% maltose syrup, 0.15% ethylenediaminetetraacetic acid two is received, 0.25% sodium pyrosulfite, after cooling molding, baking forms, and finished product water content is between 8-10%.Its preparation method is: Corm Brassicae caulorapae is removed the peel, clean after add 0.25% citric acid and boil in the steam jacket of 100-110 degree, screened stock worn into by well-done Corm Brassicae caulorapae colloid mill, add carrageenan, glucose, white sugar, maltose syrup stirs, and boils to 97-100 degree, Corm Brassicae caulorapae slurry balanced for cooked stirring is poured in mould and cools down 15-20 minute: remove mould, after 50-73 degree temperature is toasted 15 to 16 hours and edible.Raw material utilization ratio is high, its product is faint yellow or yellow, has vivid natural colored and strong Corm Brassicae caulorapae fragrance.
A kind of compound recipe Corm Brassicae caulorapae sub-QI invigorating drug for controlling intestinal function thing and its preparation method and application (CN201510707215.1) disclosed in Chinese patent storehouse, this medicine is made up of Chinese medicine ingredients, western medicine composition and adjuvant;Described Chinese medicine ingredients includes: Corm Brassicae caulorapae, son, Castanopsis delavayi Franch, Shi Shi, Rhizoma nupharis pumili, Amylum Metroxyli sagu, Bos taurus domesticus Gmelin, Mulberry, Crop Gallus domesticus daughter root, Radix Helwingiae, Herba polygoni senticosi, Galeola faberi Rolfe., floating and thready pulse LIUYECAI, Fructus Pruni persicae immaturus, and described western medicine composition includes: furazolidone, antibacterial peptide, polymyxin, probiotic bacteria.This compound recipe Corm Brassicae caulorapae sub-QI invigorating selected Chinese medicine medicines of drug for controlling intestinal function thing, cooperation has antibacterial, the Western medicine of antiinflammation; and the beneficial bacteria of intestinal tract of conditioning intestinal normal function, it is possible to invigorating spleen and reinforcing stomach, qi-restoratives stops blooding; astringing to arrest diarrhea, heat-clearing and toxic substances removing, regulating QI to relieve pain; effectively eliminate pathogenic bacterium, protection intestinal mucosa secretion, not stimulating intestine and stomach mucosa; increase diseased region rehabilitation; enhancing human body immunity function, comes off evident in efficacy to treatment intestinal mucosa, and safely and effectively.
The method of plant extract has a lot; plant extract is applied primarily to the fields such as food, chemical industry, cosmetics; but extracting method and plant extract species have very big limitation; how simply, plant safely, effectively is extracted; select which kind of plant; and its safety is applied in cosmetics, protect sensitive skin, be problem demanding prompt solution.
Summary of the invention
For the problems referred to above, it is an object of the invention to provide a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit and application thereof, atomization extraction and separation technology is adopted to extract Corm Brassicae caulorapae extract from Corm Brassicae caulorapae bulb, Corm Brassicae caulorapae extract can add in cosmetics as dispensing, specifically can be made into the products such as facial film, cleansing milk, leaves shampoo, bath gel, surfactant, emollient cream, skin whitener, essence.
To achieve these goals, the present invention adopts below scheme
According to the first aspect of the invention, a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit, it comprises the following steps:
(1) pulverizing, use pulverizer to be pulverized by Corm Brassicae caulorapae fruit, make Corm Brassicae caulorapae microgranule, particle diameter is 20-50 sieve mesh;
(2) suspension processed, is mixed and made into suspension by Corm Brassicae caulorapae microgranule and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:8-15, and temperature is 18-30 DEG C;
(3) atomization lixiviate, uses nebulizer be atomized by suspension and spray away, and liquid mist natural subsidence reverts to suspension, collects suspension, keeps temperature to be 18-50 DEG C;
(4) isolated by filtration, obtains suspension by step (3) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(5) secondary lixiviate, is mixed and made into suspension by Corm Brassicae caulorapae residue and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:5-8, and temperature is 18-30 DEG C;Using nebulizer be atomized by suspension and spray away, liquid mist natural subsidence reverts to suspension, collects suspension, keeps temperature to be 18-50 DEG C;
(6) secondary separation, obtains suspension by step (5) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(7) separating solvent, clear liquid step (4) and step (6) obtained enters heating, isolates solvent, obtains Corm Brassicae caulorapae extracting solution;
(8) extracting solution concentration, concentrates Corm Brassicae caulorapae extracting solution, obtains Corm Brassicae caulorapae extract, and the water content of Corm Brassicae caulorapae extract is 30%-40%;
(9) decolorising agent or toner is selected to make required color according to the final color of Corm Brassicae caulorapae fruit extract.
Preferably, in step (2), the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:12, and temperature is 24 DEG C.
Preferably, in step (2), solvent is ethanol, butanol, butyl ester, ethyl acetate or pentyl acetate.
Preferably, in step (2), solvent is ethanol.
Preferably, in step (3), temperature is 35-50 DEG C.
Preferably, in step (5), the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:6.
Preferably, step (7) adopts vacuum concentration technique.
According to the second aspect of the invention, it is provided that the application of a kind of Corm Brassicae caulorapae extract, described Corm Brassicae caulorapae extract adds in cosmetics as a kind of dispensing.
Preferably, Corm Brassicae caulorapae extract is applied in the cosmetics of skin moistening, moisturizing, face cleaning, shower, defying age class.
Preferably, a kind of skin moistening class cosmetic combinations containing Corm Brassicae caulorapae extract, by weight, including following components: Corm Brassicae caulorapae extract 8-12 part, moisturizing agent 1-3 part, antioxidant 0.5-2 part, crease-resistant activating agent 1-2.5 part, anti-sensitizer 0.2-0.6 part, whitening agent 1.5-3 part, potassium hydroxide 0.03-0.1 part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-4 part, preservative 0.2-0.6 part, deionized water 40-80 part.
The invention has the beneficial effects as follows: by being atomized by material liquid so that the dynamic serialization of production process, production efficiency improves several times;Atomization improves the mass transport process between material and solvent, reduces mass transfer condition restriction, makes energy resource consumption, solvent consumption be greatly saved, reduces production cost, improves effective ingredient leaching rate simultaneously, makes full use of raw medicinal material, additional income;Containing enhancing human body immunity power composition and multiple nutritional components in Corm Brassicae caulorapae extract, Corm Brassicae caulorapae extract is applied in cosmetics, expands range of application.
Detailed description of the invention
For the problems referred to above, it is an object of the invention to provide a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit and application thereof, atomization extraction and separation technology is adopted to extract Corm Brassicae caulorapae extract from Corm Brassicae caulorapae bulb, Corm Brassicae caulorapae extract can add in cosmetics as dispensing, specifically can be made into the products such as facial film, cleansing milk, leaves shampoo, bath gel, surfactant, emollient cream, skin whitener, essence.
To achieve these goals, the present invention adopts below scheme
According to the first aspect of the invention, a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit, it comprises the following steps:
(1) pulverizing, use pulverizer to be pulverized by Corm Brassicae caulorapae fruit, make Corm Brassicae caulorapae microgranule, particle diameter is 20-50 sieve mesh;
(2) suspension processed, is mixed and made into suspension by Corm Brassicae caulorapae microgranule and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:8-15, and temperature is 18-30 DEG C;
(3) atomization lixiviate, uses nebulizer be atomized by suspension and spray away, and liquid mist natural subsidence reverts to suspension, collects suspension, keeps temperature to be 18-50 DEG C;
(4) isolated by filtration, obtains suspension by step (3) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(5) secondary lixiviate, is mixed and made into suspension by Corm Brassicae caulorapae residue and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:5-8, and temperature is 18-30 DEG C;Using nebulizer be atomized by suspension and spray away, liquid mist natural subsidence reverts to suspension, collects suspension, keeps temperature to be 18-50 DEG C;
(6) secondary separation, obtains suspension by step (5) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(7) separating solvent, clear liquid step (4) and step (6) obtained enters heating, isolates solvent, obtains Corm Brassicae caulorapae extracting solution;
(8) extracting solution concentration, concentrates Corm Brassicae caulorapae extracting solution, obtains Corm Brassicae caulorapae extract, and the water content of Corm Brassicae caulorapae extract is 30%-40%;
(9) decolorising agent or toner is selected to make required color according to the final color of Corm Brassicae caulorapae fruit extract.
Preferably, in step (2), the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:12, and temperature is 24 DEG C.
Preferably, in step (2), solvent is ethanol, butanol, butyl ester, ethyl acetate or pentyl acetate.
Preferably, in step (2), solvent is ethanol.
Preferably, in step (3), temperature is 35-50 DEG C.
Preferably, in step (5), the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:6.
Preferably, step (7) adopts vacuum concentration technique.
According to the second aspect of the invention, it is provided that the application of a kind of Corm Brassicae caulorapae extract, described Corm Brassicae caulorapae extract adds in cosmetics as a kind of dispensing.
Preferably, Corm Brassicae caulorapae extract is applied in the cosmetics of skin moistening, moisturizing, face cleaning, shower, defying age class.
Preferably, a kind of skin moistening class cosmetic combinations containing Corm Brassicae caulorapae extract, by weight, including following components: Corm Brassicae caulorapae extract 8-12 part, moisturizing agent 1-3 part, antioxidant 0.5-2 part, crease-resistant activating agent 1-2.5 part, anti-sensitizer 0.2-0.6 part, whitening agent 1.5-3 part, potassium hydroxide 0.03-0.1 part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-4 part, preservative 0.2-0.6 part, deionized water 40-80 part.
Spray extraction principle, is atomized into superfine little droplet by material liquid by nebulizer, the surface area of feed liquid is increased 10000 times, after contacting with extraction phase, completes extraction process, reach extraction equilibrium within the several seconds.Being atomized and self produce impulsive force and eddy current effect and may also function as the effect of stirring, auxiliary extraction operates.Spray extraction flow process can realize single-stage extraction also can realize multistage cross flow, counter-current extraction, back extraction.Nebulizer also can produce eddy current effect, produces the effect of high-speed stirred, Accelerative mass transfer in local.Coordinate solvent adverse current again, droplet both can have been made constantly to move in adverse current gradient, continue replacement process, the dissolubility of solvent can be made full use of again, reaching to save solvent and make the effect of consumption, when droplet moves to bottom extraction pot, most target components of cell interior are replaced out.Atomization is extracted at 25 DEG C and just can have normal extraction effect, and with little need for extra heat supplement, this is that conventional thermal reflux technique can not be compared.
In order to make those skilled in the art be better understood from the technical scheme in the application; below in conjunction with embodiment, technical scheme is clearly and completely described; obviously; described embodiment is only a part of embodiment of the application; based on the embodiment in the application; the every other embodiment that those of ordinary skill in the art obtain under not making creative work premise, all should belong to the scope of the application protection.
Embodiment 1
A kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit, it comprises the following steps:
Corm Brassicae caulorapae fruit weight: 10KG, solvent is ethanol;
(1) pulverizing, use pulverizer to be pulverized by Corm Brassicae caulorapae fruit, make Corm Brassicae caulorapae microgranule, particle diameter is 30 sieve meshes;
(2) suspension processed, is mixed and made into suspension by Corm Brassicae caulorapae microgranule and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:12, and temperature is 24 DEG C;
(3) atomization lixiviate, uses nebulizer be atomized by suspension and spray away, and liquid mist natural subsidence reverts to suspension, collects suspension, and keeping temperature is 35 DEG C;
(4) isolated by filtration, obtains suspension by step (3) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(5) secondary lixiviate, is mixed and made into suspension by Corm Brassicae caulorapae residue and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:5, and temperature is 24 DEG C;Using nebulizer be atomized by suspension and spray away, liquid mist natural subsidence reverts to suspension, collects suspension, and keeping temperature is 35 DEG C;
(6) secondary separation, obtains suspension by step (5) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(7) separating solvent, clear liquid step (4) and step (6) obtained enters heating, isolates solvent, obtains Corm Brassicae caulorapae extracting solution;
(8) extracting solution concentration, concentrates Corm Brassicae caulorapae extracting solution, obtains Corm Brassicae caulorapae extract, and the water content of Corm Brassicae caulorapae extract is 32%;
(9) decolorising agent or toner is selected to make required color according to the final color of Corm Brassicae caulorapae fruit extract.
Embodiment 2
A kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit, it comprises the following steps:
Corm Brassicae caulorapae fruit weight: 50KG, solvent is butanol;
(1) pulverizing, use pulverizer to be pulverized by Corm Brassicae caulorapae fruit, make Corm Brassicae caulorapae microgranule, particle diameter is 40 sieve meshes;
(2) suspension processed, is mixed and made into suspension by Corm Brassicae caulorapae microgranule and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:10, and temperature is 24 DEG C;
(3) atomization lixiviate, uses nebulizer be atomized by suspension and spray away, and liquid mist natural subsidence reverts to suspension, collects suspension, and keeping temperature is 40 DEG C;
(4) isolated by filtration, obtains suspension by step (3) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(5) secondary lixiviate, is mixed and made into suspension by Corm Brassicae caulorapae residue and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:6, and temperature is 24 DEG C;Using nebulizer be atomized by suspension and spray away, liquid mist natural subsidence reverts to suspension, collects suspension, and keeping temperature is 40 DEG C;
(6) secondary separation, obtains suspension by step (5) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(7) separating solvent, clear liquid step (4) and step (6) obtained enters heating, isolates solvent, obtains Corm Brassicae caulorapae extracting solution;
(8) extracting solution concentration, concentrates Corm Brassicae caulorapae extracting solution, obtains Corm Brassicae caulorapae extract, and the water content of Corm Brassicae caulorapae extract is 33%;
(9) decolorising agent or toner is selected to make required color according to the final color of Corm Brassicae caulorapae fruit extract.
Embodiment 3
A kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit, it comprises the following steps:
Corm Brassicae caulorapae fruit weight: 100KG, solvent is pentyl acetate;
(1) pulverizing, use pulverizer to be pulverized by Corm Brassicae caulorapae fruit, make Corm Brassicae caulorapae microgranule, particle diameter is 50 sieve meshes;
(2) suspension processed, is mixed and made into suspension by Corm Brassicae caulorapae microgranule and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:15, and temperature is 24 DEG C;
(3) atomization lixiviate, uses nebulizer be atomized by suspension and spray away, and liquid mist natural subsidence reverts to suspension, collects suspension, and keeping temperature is 45 DEG C;
(4) isolated by filtration, obtains suspension by step (3) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(5) secondary lixiviate, is mixed and made into suspension by Corm Brassicae caulorapae residue and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:7, and temperature is 24 DEG C;Using nebulizer be atomized by suspension and spray away, liquid mist natural subsidence reverts to suspension, collects suspension, and keeping temperature is 45 DEG C;
(6) secondary separation, obtains suspension by step (5) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(7) separating solvent, clear liquid step (4) and step (6) obtained enters heating, isolates solvent, obtains Corm Brassicae caulorapae extracting solution;
(8) extracting solution concentration, concentrates Corm Brassicae caulorapae extracting solution, obtains Corm Brassicae caulorapae extract, and the water content of Corm Brassicae caulorapae extract is 30%;
(9) decolorising agent or toner is selected to make required color according to the final color of Corm Brassicae caulorapae fruit extract.
What finally illustrate is, above example is only in order to illustrate technical scheme and unrestricted, other amendments that technical scheme is made by those of ordinary skill in the art or equivalent replace, without departing from the spirit and scope of technical solution of the present invention, all should be encompassed in the middle of scope of the presently claimed invention.
Claims (10)
1. the method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit, it is characterised in that it comprises the following steps:
(1) pulverizing, use pulverizer to be pulverized by Corm Brassicae caulorapae fruit, make Corm Brassicae caulorapae microgranule, particle diameter is 20-50 sieve mesh;
(2) suspension processed, is mixed and made into suspension by Corm Brassicae caulorapae microgranule and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:8-15, and temperature is 18-30 DEG C;
(3) atomization lixiviate, uses nebulizer be atomized by suspension and spray away, and liquid mist natural subsidence reverts to suspension, collects suspension, keeps temperature to be 18-50 DEG C;
(4) isolated by filtration, obtains suspension by step (3) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(5) secondary lixiviate, is mixed and made into suspension by Corm Brassicae caulorapae residue and solvent, and the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:5-8, and temperature is 18-30 DEG C;Using nebulizer be atomized by suspension and spray away, liquid mist natural subsidence reverts to suspension, collects suspension, keeps temperature to be 18-50 DEG C;
(6) secondary separation, obtains suspension by step (5) and is filtered, and obtains clear liquid and Corm Brassicae caulorapae residue;
(7) separating solvent, clear liquid step (4) and step (6) obtained enters heating, isolates solvent, obtains Corm Brassicae caulorapae extracting solution;
(8) extracting solution concentration, concentrates Corm Brassicae caulorapae extracting solution, obtains Corm Brassicae caulorapae extract, and the water content of Corm Brassicae caulorapae extract is 30%-40%;
(9) decolorising agent or toner is selected to make required color according to the final color of Corm Brassicae caulorapae fruit extract.
2. a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit according to claim 1, it is characterised in that in step (2), the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:12, and temperature is 24 DEG C.
3. a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit according to claim 1, it is characterised in that in step (2), solvent is ethanol, butanol, butyl ester, ethyl acetate or pentyl acetate.
4. a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit according to claim 1, it is characterised in that in step (2), solvent is ethanol.
5. a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit according to claim 1, it is characterised in that in step (3), temperature is 35-50 DEG C.
6. a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit according to claim 1, it is characterised in that in step (5), the mass ratio of Corm Brassicae caulorapae microgranule and solvent is 1:6.
7. a kind of method extracting Corm Brassicae caulorapae extract from Corm Brassicae caulorapae fruit according to claim 1, it is characterised in that adopt vacuum concentration technique in step (7).
8. the application of a Corm Brassicae caulorapae extract, it is characterised in that described Corm Brassicae caulorapae extract adds in cosmetics as a kind of dispensing.
9. the application of a kind of Corm Brassicae caulorapae extract according to claim 8, it is characterised in that Corm Brassicae caulorapae extract is applied in the cosmetics of skin moistening, moisturizing, face cleaning, shower, defying age class.
10. the application of a kind of Corm Brassicae caulorapae extract according to claim 8 or claim 9, it is characterized in that, a kind of skin moistening class cosmetic combinations containing Corm Brassicae caulorapae extract, by weight, including following components: Corm Brassicae caulorapae extract 8-12 part, moisturizing agent 1-3 part, antioxidant 0.5-2 part, crease-resistant activating agent 1-2.5 part, anti-sensitizer 0.2-0.6 part, whitening agent 1.5-3 part, potassium hydroxide 0.03-0.1 part, thickening agent 0.1-0.3 part, emulsifying agent 1.5-4 part, preservative 0.2-0.6 part, deionized water 40-80 part.
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CN110559236A (en) * | 2019-10-10 | 2019-12-13 | 恩平市嘉鑫日用品有限公司 | Preparation method and application of micromolecule Acanthopanax trifoliatus extract |
CN111568783A (en) * | 2020-06-23 | 2020-08-25 | 昆仑技术研究(广州)有限公司 | Preparation method and application of white tomato extract liposome freeze-dried powder |
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CN102772912A (en) * | 2012-07-05 | 2012-11-14 | 西安鸿生生物技术有限公司 | Device and method for extracting effective components from natural plant by high-pressure spraying reverse-flow process |
CN104941551A (en) * | 2015-06-22 | 2015-09-30 | 江阴市苏新干燥设备有限公司 | Ultrasonic atomization extracting tank |
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CN102772912A (en) * | 2012-07-05 | 2012-11-14 | 西安鸿生生物技术有限公司 | Device and method for extracting effective components from natural plant by high-pressure spraying reverse-flow process |
CN104941551A (en) * | 2015-06-22 | 2015-09-30 | 江阴市苏新干燥设备有限公司 | Ultrasonic atomization extracting tank |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110559236A (en) * | 2019-10-10 | 2019-12-13 | 恩平市嘉鑫日用品有限公司 | Preparation method and application of micromolecule Acanthopanax trifoliatus extract |
CN111568783A (en) * | 2020-06-23 | 2020-08-25 | 昆仑技术研究(广州)有限公司 | Preparation method and application of white tomato extract liposome freeze-dried powder |
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