CN111635802A - 一种长期脱水防锈油的制备方法 - Google Patents

一种长期脱水防锈油的制备方法 Download PDF

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CN111635802A
CN111635802A CN202010647726.XA CN202010647726A CN111635802A CN 111635802 A CN111635802 A CN 111635802A CN 202010647726 A CN202010647726 A CN 202010647726A CN 111635802 A CN111635802 A CN 111635802A
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additive
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李修喜
余杰
孙运强
杨春林
陈晓梅
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Shandong Shuoli New Material Technology Co ltd
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Abstract

本发明公开了一种长期脱水防锈油的制备方法，包括以下步骤：A、配置成膜助剂，B、配置防锈添加剂，C、称取脱水添加剂，D、称取抗氧化剂，E、成型：按重量分数称取上述备料成膜助剂6‑10份、防锈添加剂8‑12份、脱水添加剂2‑4份、抗氧化剂1‑2份以及矿物油75‑85份，将成膜助剂、防锈添加剂、脱水添加剂、抗氧化剂和矿物油放入搅拌釜内，加热至40‑50℃，搅拌40‑60分钟，至各组分充分分散溶解，取出后过滤杂质得成品。本发明与现有技术相比的优点在于：配置工艺简单易实施，成品使用效果好，长期有效。

Description

一种长期脱水防锈油的制备方法
技术领域
本发明涉及防锈油技术领域，具体是指一种长期脱水防锈油的制备方法。
背景技术
随着现在国防、汽车制造等行业的迅速发展，对金属板材的需求量越来越大，对板材的表面质量要求也越来越高，因为如何防腐，降低成产、运输、贮存成本的损失是重中之重，目前，防止金属腐蚀的普遍做饭是将工件表面涂上一层防锈油。
目前传统的防锈油大多成分简单，在某种或者几个特定的方面性能不错，但是综合性能不良，尤其是防锈期端，但金属制品必要经过长期的贮存、运输和使用，长期有效的防锈油才能保证金属板材的高质量。
发明内容
本发明要解决的技术问题是克服以上技术缺陷，提供一种配置工艺简单易实施，成品使用效果好，长期有效的一种长期脱水防锈油的制备方法。
为解决上述技术问题，本发明提供的技术方案为：一种长期脱水防锈油的制备方法，包括以下步骤：
A、配置成膜助剂：按重量份称取原料十二烯基丁二酸7-9份、虫胶树脂1-2份、双硬脂酸铝4-5份、丙二醇甲醚醋酸酯3-4份、乙二醇单乙醚0.1-0.2份、霍霍巴油0.15-0.25份；将双硬脂酸铝加热到75-85℃，加入丙二醇甲醚醋酸酯，充分搅拌后降低温度为62-68℃，加入乙二醇单乙醚，500-600转/分搅拌分散5分钟，得预混料；将十二烯基丁二酸与虫胶树脂在80-100℃下混合，搅拌均匀后加入到预混料中，充分搅拌后，加入霍霍巴油，冷却至常温，即得所述成膜助剂；
B、配置防锈添加剂：以矿物油为溶剂，按重量分数称取羊毛脂镁皂1-3份、二壬基萘磺酸鋇3-5份、油酸三乙醇铵3-5份、石蜡1-3份，加热混合搅拌至全部溶解后继续即热30-40分钟，冷却备用；
C、称取脱水添加剂：石油醚；
D、称取抗氧化剂：苯二酚；
E、成型：按重量分数称取上述备料成膜助剂6-10份、防锈添加剂8-12份、脱水添加剂2-4份、抗氧化剂1-2份以及矿物油75-85份，将成膜助剂、防锈添加剂、脱水添加剂、抗氧化剂和矿物油放入搅拌釜内，加热至40-50℃，搅拌40-60分钟，至各组分充分分散溶解，取出后过滤杂质得成品。
作为改进，所述矿物油为机械油、液压油、灯用煤油中的一种或多种混合。
本发明与现有技术相比的优点在于：添加脱水添加剂，具有脱水效果，简化金属板材浸油处理前期工艺；添加抗氧化剂，避免金属板材表面氧化，增加防锈油对金属板材的保护效果；可长期高效保持防锈效果；整体工艺步骤简单，生产加工制作方便。
具体实施方式
实施例一
一种长期脱水防锈油的制备方法，包括以下步骤：
A、配置成膜助剂：按重量份称取原料十二烯基丁二酸8份、虫胶树脂1.5份、双硬脂酸铝3份、丙二醇甲醚醋酸酯3.5份、乙二醇单乙醚0.15份、霍霍巴油0.2份；将双硬脂酸铝加热到80℃，加入丙二醇甲醚醋酸酯，充分搅拌后降低温度为66℃，加入乙二醇单乙醚，550转/分搅拌分散5分钟，得预混料；将十二烯基丁二酸与虫胶树脂在90℃下混合，搅拌均匀后加入到预混料中，充分搅拌后，加入霍霍巴油，冷却至常温，即得所述成膜助剂；
B、配置防锈添加剂：以矿物油为溶剂，按重量分数称取羊毛脂镁皂2份、二壬基萘磺酸鋇4份、油酸三乙醇铵4份、石蜡2份，加热混合搅拌至全部溶解后继续即热35分钟，冷却备用；
C、称取脱水添加剂：石油醚；
D、称取抗氧化剂：苯二酚；
E、成型：按重量分数称取上述备料成膜助剂8份、防锈添加剂10份、脱水添加剂3份、抗氧化剂1.5份以及矿物油80份，所述矿物油为机械油和液压油各站50％比例混合，将成膜助剂、防锈添加剂、脱水添加剂、抗氧化剂和矿物油放入搅拌釜内，加热至45℃，搅拌50分钟，至各组分充分分散溶解，取出后过滤杂质得成品。
实施例二
一种长期脱水防锈油的制备方法，包括以下步骤：
A、配置成膜助剂：按重量份称取原料十二烯基丁二酸7份、虫胶树脂1份、双硬脂酸铝4份、丙二醇甲醚醋酸酯3份、乙二醇单乙醚0.1份、霍霍巴油0.15份；将双硬脂酸铝加热到75℃，加入丙二醇甲醚醋酸酯，充分搅拌后降低温度为62℃，加入乙二醇单乙醚，500转/分搅拌分散5分钟，得预混料；将十二烯基丁二酸与虫胶树脂在80℃下混合，搅拌均匀后加入到预混料中，充分搅拌后，加入霍霍巴油，冷却至常温，即得所述成膜助剂；
B、配置防锈添加剂：以矿物油为溶剂，按重量分数称取羊毛脂镁皂1份、二壬基萘磺酸鋇3份、油酸三乙醇铵3份、石蜡1份，加热混合搅拌至全部溶解后继续即热30分钟，冷却备用；
C、称取脱水添加剂：石油醚；
D、称取抗氧化剂：苯二酚；
E、成型：按重量分数称取上述备料成膜助剂6份、防锈添加剂8份、脱水添加剂2份、抗氧化剂1份以及矿物油75份，所述矿物油为机械油，将成膜助剂、防锈添加剂、脱水添加剂、抗氧化剂和矿物油放入搅拌釜内，加热至40℃，搅拌40分钟，至各组分充分分散溶解，取出后过滤杂质得成品。
实施例三
一种长期脱水防锈油的制备方法，包括以下步骤：
A、配置成膜助剂：按重量份称取原料十二烯基丁二酸9份、虫胶树脂2份、双硬脂酸铝5份、丙二醇甲醚醋酸酯4份、乙二醇单乙醚0.2份、霍霍巴油0.25份；将双硬脂酸铝加热到85℃，加入丙二醇甲醚醋酸酯，充分搅拌后降低温度为68℃，加入乙二醇单乙醚，600转/分搅拌分散5分钟，得预混料；将十二烯基丁二酸与虫胶树脂在100℃下混合，搅拌均匀后加入到预混料中，充分搅拌后，加入霍霍巴油，冷却至常温，即得所述成膜助剂；
B、配置防锈添加剂：以矿物油为溶剂，按重量分数称取羊毛脂镁皂3份、二壬基萘磺酸鋇5份、油酸三乙醇铵5份、石蜡3份，加热混合搅拌至全部溶解后继续即热40分钟，冷却备用；
C、称取脱水添加剂：石油醚；
D、称取抗氧化剂：苯二酚；
E、成型：按重量分数称取上述备料成膜助剂10份、防锈添加剂12份、脱水添加剂4份、抗氧化剂2份以及矿物油85份，所述矿物油为液压油，将成膜助剂、防锈添加剂、脱水添加剂、抗氧化剂和矿物油放入搅拌釜内，加热至50℃，搅拌60分钟，至各组分充分分散溶解，取出后过滤杂质得成品。

Claims (2)

1.一种长期脱水防锈油的制备方法，其特征在于，包括以下步骤：
A、配置成膜助剂：按重量份称取原料十二烯基丁二酸7-9份、虫胶树脂1-2份、双硬脂酸铝4-5份、丙二醇甲醚醋酸酯3-4份、乙二醇单乙醚0.1-0.2份、霍霍巴油0.15-0.25份；将双硬脂酸铝加热到75-85℃，加入丙二醇甲醚醋酸酯，充分搅拌后降低温度为62-68℃，加入乙二醇单乙醚，500-600转/分搅拌分散5分钟，得预混料；将十二烯基丁二酸与虫胶树脂在80-100℃下混合，搅拌均匀后加入到预混料中，充分搅拌后，加入霍霍巴油，冷却至常温，即得所述成膜助剂；
B、配置防锈添加剂：以矿物油为溶剂，按重量分数称取羊毛脂镁皂1-3份、二壬基萘磺酸鋇3-5份、油酸三乙醇铵3-5份、石蜡1-3份，加热混合搅拌至全部溶解后继续即热30-40分钟，冷却备用；
C、称取脱水添加剂：石油醚；
D、称取抗氧化剂：苯二酚；
E、成型：按重量分数称取上述备料成膜助剂6-10份、防锈添加剂8-12份、脱水添加剂2-4份、抗氧化剂1-2份以及矿物油75-85份，将成膜助剂、防锈添加剂、脱水添加剂、抗氧化剂和矿物油放入搅拌釜内，加热至40-50℃，搅拌40-60分钟，至各组分充分分散溶解，取出后过滤杂质得成品。
2.根据权利要求1所述的一种长期脱水防锈油的制备方法，其特征在于，所述矿物油为机械油、液压油、灯用煤油中的一种或多种混合。
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1588246A (en) * 1976-12-16 1981-04-23 Chevron Res Lubricating oil additives and compositions containing the same
CN1353173A (zh) * 2001-11-21 2002-06-12 蔡毓英 新型脱水防锈油
CN103484215A (zh) * 2013-08-20 2014-01-01 安徽精一机械设备有限公司 一种脱水防锈油
CN104818082A (zh) * 2015-03-12 2015-08-05 浏阳市三鹰新材料有限责任公司 一种低粘度的长效脱水防锈油

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1588246A (en) * 1976-12-16 1981-04-23 Chevron Res Lubricating oil additives and compositions containing the same
CN1353173A (zh) * 2001-11-21 2002-06-12 蔡毓英 新型脱水防锈油
CN103484215A (zh) * 2013-08-20 2014-01-01 安徽精一机械设备有限公司 一种脱水防锈油
CN104818082A (zh) * 2015-03-12 2015-08-05 浏阳市三鹰新材料有限责任公司 一种低粘度的长效脱水防锈油

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