CN111544341A - Blackhead-removing essential oil and preparation method thereof - Google Patents
Blackhead-removing essential oil and preparation method thereof Download PDFInfo
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- CN111544341A CN111544341A CN201911194984.0A CN201911194984A CN111544341A CN 111544341 A CN111544341 A CN 111544341A CN 201911194984 A CN201911194984 A CN 201911194984A CN 111544341 A CN111544341 A CN 111544341A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses blackhead-removing essential oil which comprises, by mass, 2-5 parts of clary sage essential oil, 2-5 parts of sage essential oil, 4-10 parts of verbena rosemary essential oil, 2-5 parts of cajeput essential oil and 900-990 parts of jojoba oil. The compound essential oil composed of 5 kinds of essential oil with different functions can not only keep the inherent efficacy of the single essential oil, but also generate synergistic effect to build the effect of 1+1> 2. The essential oil has extremely small molecular structure and 70 times of the permeability of common skin care products, so the essential oil can quickly enter the deep layer of the skin, dissolve redundant lipid and dead cells in pores, deeply clean the skin, fundamentally remove blackheads and acnes, and can also eliminate skin inflammation and rebuild the skin structure.
Description
Technical Field
The invention relates to compound essential oil for blackhead acne, and further relates to blackhead-removing essential oil and a preparation method thereof.
Background
The essential oil is extracted from leaves, flowers, seeds, fruits, roots, barks, resins, hearts and other parts of plants by steam distillation, cold pressing, fat absorption, solvent extraction and the like, and has high-concentration fragrance and volatility. In addition to essential oils extracted from a part of a plant, some plants extract essential oils from several parts, for example, bitter oranges extract essential oils from 3 parts of the buds, leaves and fruits. However, not all plants produce essential oils, and only plants containing the sebaceous glands are likely to produce essential oils.
Essential oils contain many different components, such as rose essential oil, which can be made up of more than 250 different molecules. Essential oils are lipophilic and readily soluble in oils and fats because the molecular chains of essential oils are usually relatively short, which makes them highly permeable to the skin and enter the body via the abundant capillary vessels beneath the subcutaneous fat. Essential oils are composed of a number of very small molecules that pass through the skin or other tissues into the body to regulate physical and mental functions.
Acne is an inflammatory disease of skin appendages, and comedones are one manifestation of acne. At present, the blackhead removing products on the market are mainly of the following two types:
(1) tearing the mask: although blackheads, aged keratin and oils on the skin can be removed, improper use can easily lead to loose skin, large pores and some skin allergy problems. Not only can damage the deep structure of the skin, but also can cause the situation that the blackheads are not completely removed and are repeated.
(2) Black spot cleaning beauty instrument: although effective, excessive use of blackheads can cause the skin to become loose, fine lines on the face to appear, and the blackheads to reappear.
The search application document CN105560101A discloses blackhead-removing essential oil, and the technical scheme disclosed by the essential oil can only dissipate wind and dampness, reduce swelling and expel pus and improve acne; according to the scheme, the proportioning components can generate a synergistic effect, the permeability is better, and the skin can quickly enter the deep layer of the skin.
Disclosure of Invention
The technical scheme adopted by the invention for solving the technical problems is to provide the compound essential oil, solve the problems of poor effect and easy repeatability of the existing blackhead removing product, have low irritation to a human body, cannot cause the loosening and enlargement of hair holes, and has excellent blackhead removing effect.
The specific technical scheme is as follows:
the blackhead-removing essential oil comprises, by mass, 2-5 parts of clary sage (salvia miltiorrhiza) essential oil, 2-5 parts of sage essential oil, 4-10 parts of verbena rosemary essential oil, 2-5 parts of cajeput essential oil and 900-990 parts of jojoba oil.
The application also comprises a preparation method of the blackhead removing essential oil, which comprises the following steps:
the Salvia miltiorrhiza essential oil adopts a microwave extraction mode: cyclohexane is used as an extracting agent, the microwave power is 329W, the microwave time is 80s, the material-liquid ratio is 1: 6, the soaking time is 56min, and the actual yield is 1.783%.
Supercritical CO2 extraction method of sage essential oil: pulverizing herba Salvia officinalis particles to 40-60 mesh, extracting at 50 deg.C under 15MPa for 120min with carbon dioxide flow rate of 20L/h, and separating at 40 deg.C. The extraction rate of the sage essential oil extracted by the supercritical CO2 fluid is 6.01 +/-0.13%.
Extracting the verbena officinalis essential oil by using supercritical CO 2: drying at 60 deg.C to constant weight, and pulverizing to 40-60 mesh; the extraction temperature is 50 ℃, the extraction pressure is 15MPa, the carbon dioxide flow is 20L/h, the extraction time is 4h, and the separation temperature is 40 ℃. The extraction rate of the rosemary essential oil extracted by the supercritical CO2 fluid is 7.12 +/-0.11 percent.
Extracting the cajeput essential oil by adopting steam distillation: the pressure of the boiler is 30kg/cm2, the evaporation capacity is 30kg/h, the extraction temperature is 214 ℃, the extraction pressure is 2.1MPa, the distillate is recovered for 40min, and the waste liquid is finally recovered for 5min, wherein the extraction rate is 1.1 +/-0.03%.
The jojoba oil is extracted by adopting a cold pressing method: squeezing at room temperature to obtain oil yield of 32.36 + -0.12%.
Compared with the prior art, the invention has the following beneficial effects:
the Salvia miltiorrhiza essential oil comprises the following specific components: linalool (20.3%), linalyl acetate (42.7%), D-limonene, alpha-terpineol, nerol, citral, neryl acetate, geranyl acetate, caryophyllene, nerolidol. It can regulate skin oil secretion, repair skin cell tissue, relieve inflammation, and improve skin problems such as oil, acne, etc.
The sage essential oil comprises the following specific components: 3, 7-dimethyl-2.6-octadiene (22.39%), 3, 7-dimethyl-2, 6-octadiene (11.91%), 6-methyl-1, 5-heptadiene (7.11%), 3-methyl-2-pentene (6.74%), thujone (5.74%), alpha-thujone, beta-thujone, camphor, 1, 8-cineole, humulene, pinene, camphene, limonene, bornyl acetate, etc. It has excellent antioxidant and antibacterial activity, and can promote skin regeneration, and effectively improve skin pore and skin ulcer.
The verbena-mefone rosemary essential oil comprises the following specific components: 1, 8-eucalyptol (19.520%), alpha-pinene (28.540%), camphor (8.01%), verbenone (1.56%), abietinone (0.13%), etc. Not only can resist bacteria and oxidation (terpenes, phenols and acids), but also can kill bacteria, kill insects, diminish inflammation, dissolve fat and the like.
The cajeput essential oil comprises the following specific components: alpha-terpinene (5-13%), terpadiene (0.5-4%), m-isopropylbenzene (0.5-12%), 1,8 cineole (15%), gamma-terpinene (10-28%), terpinolene (1.5-5%), terpinen-4-ol (> 30%), alpha-terpineol (1.5-8%), vanillin (7%), trumpet tea terpene (0.5-6.5%), -juniperberry sesquiterpene (8%), eudesmol (3%), Viridiflorol (1.5%), etc. It can rapidly kill intractable bacteria, and has obvious effect in inhibiting Staphylococcus aureus, Propionibacterium acnes, and Staphylococcus epidermidis. The cajeput essential oil also has the properties of diminishing inflammation, relieving pain and promoting wound healing.
Jojoba oil is in fact a vegetable wax structure. Similar to the structure of the grease secreted by sebaceous glands of human skin, the triangular structure on the molecular configuration is beneficial to the jojoba oil molecules to enter the skin to be blended with the fat in the skin, and the garbage in the skin is taken away. Can inhibit oxidation of oil and fat and prevent blackhead generation.
The essential oils of the present invention are all extracted from the world plants, for example rosemary essential oil is extracted from the Italy verbolone rosemary and cajeput essential oil is extracted from the cajeput of Calcega. The extraction mode of the essential oil is diversified, and the beneficial components contained in the natural plants can be extracted to the maximum extent.
This kind can not only keep the inherent efficiency of folk prescription essential oil by the compound essential oil that 5 kinds of essential oils that have different functions constitute, more can produce the synergism, builds the effect that 1+1>2, specifically is:
the similar components of different essential oils have a synergistic promoting effect:
different essential oils contain different ketone components, such as verbena, rosemary, sage, thujone, etc. The ketone component can dissolve fat, and can remove blackhead. In addition, the ketones also have the characteristic of promoting cell regeneration, and can fundamentally reduce blackhead generation and meticulous hair pores.
② different components of different essential oils have synergistic effect:
the ketones in the essential oil can decompose blackheads and promote cell regeneration, and the oxide in the cajeput can help to dredge pores and reduce blackheads. The ketone substance and the oxide substance act simultaneously, so that pores can be unblocked, clean and fine from inside to outside.
③ mutual synergy of the effects of the essential oil and the vegetable oil:
because the jojoba oil and the sebum are similar, various plants are refined together to play a stronger role in dissolving blackheads by utilizing the principle of similarity and intermiscibility.
The essential oil has extremely small molecular structure and 70 times of the permeability of common skin care products, so the essential oil can quickly enter the deep layer of the skin, dissolve redundant lipid and dead cells in pores, deeply clean the skin, fundamentally remove blackheads and acnes, and can also eliminate skin inflammation and rebuild the skin structure.
Detailed Description
The present invention will be further described with reference to the following examples.
Example 1: the blackhead-removing essential oil in the test mode comprises the following components in parts by weight: 2 parts of clary sage essential oil, 2 parts of sage essential oil, 4 parts of verbena rosemary essential oil, 2 parts of cajeput essential oil and 970 parts of jojoba oil.
Example 2: the blackhead removing essential oil in the test mode comprises the following components in parts by weight: 3 parts of clary sage essential oil, 3 parts of sage essential oil, 6 parts of verbena essential oil and rosemary essential oil, 3 parts of cajeput essential oil and 950 parts of jojoba oil.
Example 3: the blackhead-removing essential oil in the test mode comprises the following components in parts by weight: 3 parts of clary sage essential oil, 3 parts of sage essential oil, 7 parts of verbena rosemary essential oil, 4 parts of cajeput essential oil and 900 parts of jojoba oil.
Example 4: the blackhead-removing essential oil in the test mode comprises the following components in parts by weight: 4 parts of clary sage essential oil, 4 parts of sage essential oil, 8 parts of verbena rosemary essential oil, 4 parts of cajeput essential oil and 900 parts of jojoba oil.
The essential oil of the components is uniformly mixed according to a proportion, and then is mixed with jojoba oil to obtain the essential oil for removing blackheads and acnes.
Although the present invention has been described with respect to the preferred embodiments, it will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (6)
1. The blackhead removing essential oil is characterized in that: the blackhead-removing essential oil comprises, by mass, 2-5 parts of clary sage essential oil, 2-5 parts of sage essential oil, 4-10 parts of verbena rosemary essential oil, 2-5 parts of cajeput essential oil and 900-990 parts of jojoba oil.
2. A preparation method of blackhead-removing essential oil is characterized by comprising the following steps: the Salvia miltiorrhiza essential oil adopts a microwave extraction mode: cyclohexane is used as an extracting agent, the microwave power is 329W, the microwave time is 80s, the material-liquid ratio is 1: 6, the soaking time is 56min, and the actual yield is 1.783%.
3. The method for preparing the blackhead-removing essential oil as claimed in claim 2, wherein: supercritical CO2 extraction method of sage essential oil: pulverizing herba Salvia officinalis particles to 40-60 mesh, extracting at 50 deg.C under 15MPa for 120min with carbon dioxide flow rate of 20L/h, and separating at 40 deg.C. The extraction rate of the sage essential oil extracted by the supercritical CO2 fluid is 6.01 +/-0.13%.
4. The method for preparing the blackhead-removing essential oil as claimed in claim 2, wherein: extracting the verbena rosemary essential oil by using supercritical CO 2: drying at 60 deg.C to constant weight, and pulverizing to 40-60 mesh; the extraction temperature is 50 ℃, the extraction pressure is 15MPa, the carbon dioxide flow is 20L/h, the extraction time is 4h, and the separation temperature is 40 ℃. The extraction rate of the rosemary essential oil extracted by the supercritical CO2 fluid is 7.12 +/-0.11 percent.
5. The method for preparing the blackhead-removing essential oil as claimed in claim 2, wherein: extracting the cajeput essential oil by adopting steam distillation: the pressure of the boiler was 30kg/cm2The evaporation capacity is 30kg/h, the extraction temperature is 214 ℃, the extraction pressure is 2.1MPa, the distillate is recovered for 40min, and finally the waste liquid is recovered for 5min, and the extraction rate is 1.1 +/-0.03%.
6. The method for preparing the blackhead-removing essential oil as claimed in claim 2, wherein: the jojoba oil is extracted by adopting a cold pressing method: squeezing at room temperature to obtain oil yield of 32.36 + -0.12%.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115363030A (en) * | 2022-09-14 | 2022-11-22 | 河南科技大学 | Bactrocera dorsalis male and female attractant and application thereof |
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Non-Patent Citations (3)
Title |
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南京阿奴生物科技有限公司: "ANU祛黑头按摩精油", 《HTTPS://HZPBA.NMPA.GOV.CN/GCCX/CHAKANHIS.HTML?PRODID=201808071159498AB7B&GB=G》 * |
张语庭等: "《精油生活秘笈》", 31 July 2017, 华中科技大学出版社 * |
高锦明等: "《天然产品加工工艺学》", 31 March 2018, 西北农林科技大学出版社 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115363030A (en) * | 2022-09-14 | 2022-11-22 | 河南科技大学 | Bactrocera dorsalis male and female attractant and application thereof |
CN115363030B (en) * | 2022-09-14 | 2023-08-18 | 河南科技大学 | Bactrocera dorsalis male and female double-attraction attractant and application thereof |
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