CN111534387A - Cleaning agent and preparation method and application thereof - Google Patents
Cleaning agent and preparation method and application thereof Download PDFInfo
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- CN111534387A CN111534387A CN202010427828.0A CN202010427828A CN111534387A CN 111534387 A CN111534387 A CN 111534387A CN 202010427828 A CN202010427828 A CN 202010427828A CN 111534387 A CN111534387 A CN 111534387A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/06—Hydroxides
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/26—Chlorine; Compounds thereof
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Agronomy & Crop Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Detergent Compositions (AREA)
Abstract
The invention is suitable for the technical field of washing products, and provides a detergent, a preparation method and application thereof, wherein the preparation method of the detergent comprises the following steps: adding electrolyte into the electrolytic cell; the electrolyte comprises edible salt and water; applying voltage to the electrolyte to perform electrolytic treatment on the electrolyte to obtain an electrolytic product; separating the electrolysis product to obtain an acidic product and an alkaline product; and filtering and screening the alkaline product, and purifying to obtain the cleaning agent. The invention adopts the method of electrolyzing the salt solution and carries out bidirectional treatment on the electrolyzed product, thereby not only being capable of preparing the inorganic substance type cleaning agent with strong alkalinity, good cleaning effect and no harmful organic substance residue for washing and cleaning kitchen utensils and fruits and vegetables, but also being capable of carrying out oxidation treatment on the by-product to prepare the product with disinfection performance, thereby achieving the purpose of maximizing the utilization of resources.
Description
Technical Field
The invention belongs to the technical field of washing products, and particularly relates to a cleaning agent as well as a preparation method and application thereof.
Background
In recent years, the production of detergents has been rapidly developed due to the continuous progress of scientific technology and the rapid development of petroleum and chemical industries and urgent needs of people for washing products. At present, various high-quality, multi-effect and safe detergents, such as soap, shampoo, cleanser and the like, appear in domestic commodity markets.
The main component of the conventional detergents such as soap, shampoo and detergent is a surfactant, and the surfactant is an organic compound having a hydrophilic group and a lipophilic group in a molecular structure. Generally, surfactants are classified into two major classes, i.e., ionic surfactants and nonionic surfactants, according to whether the surfactants can be decomposed into ions in an aqueous solution. The ionic surfactant may be further classified into a cationic surfactant, an anionic surfactant and a zwitterionic surfactant. The ionic surfactant is synthesized by ring-opening polymerization of ethylene oxide to form a high molecular polymer with a certain molecular weight.
The surfactant is synthesized into a high molecular compound formed by ring-opening polymerization of ethylene oxide, and a product with a specific HLB value is designed according to a certain proportion of compounding, however, most of organic synthesis is reversible reaction and is generated along with side reaction, and the product contains certain micromolecule residues and byproducts, is used for daily necessities and has certain influence on human bodies. Therefore, in view of the above disadvantages, there is a need to develop an inorganic cleaning agent with good cleaning effect and no organic compound residue to avoid negative effects on human body.
Disclosure of Invention
The embodiment of the invention aims to provide a preparation method of a cleaning agent, and aims to solve the problems in the background technology.
The embodiment of the invention is realized in such a way that the preparation method of the cleaning agent comprises the following steps:
adding electrolyte into the electrolytic cell; the electrolyte comprises edible salt and water; the mass ratio of the edible salt to the water is 1 (800-1200);
applying voltage to the electrolyte to perform electrolytic treatment on the electrolyte to obtain an electrolytic product;
separating the electrolysis product to obtain an acidic product and an alkaline product;
and filtering and screening the alkaline product, and purifying to obtain the cleaning agent.
In a preferred embodiment of the present invention, the mass ratio of the edible salt to the water is 1 (900 to 1100).
In another preferable embodiment of the present invention, in the step, the voltage applied to the electrolyte is 1 to 5V.
In another preferable embodiment of the present invention, in the step, the current density of the electrolytic treatment is 3 to 6kA/m2。
As another preferable embodiment of the present invention, the step of separating the electrolysis product to obtain an acidic product and an alkaline product specifically includes:
and separating the electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product.
As another preferable scheme of the embodiment of the present invention, the step of filtering and screening the alkaline product specifically includes:
and filtering and screening the alkaline product through ion exchange resin.
As another preferable aspect of the embodiment of the present invention, the preparation method further includes the steps of:
adding a salt solution to the acidic product to subject the acidic product to an oxidation treatment.
Another object of the embodiments of the present invention is to provide a detergent prepared by the above preparation method.
As another preferable scheme of the embodiment of the invention, the pH value of the cleaning agent is 11-12.
Another object of the embodiments of the present invention is to provide an application of the above cleaning agent in cleaning kitchen utensils and/or fruits and vegetables.
According to the preparation method of the detergent provided by the embodiment of the invention, by adopting a method of electrolyzing the salt solution and performing bidirectional treatment on the electrolyzed product, the inorganic detergent with strong alkalinity, good cleaning effect and no harmful organic matter residue can be prepared for washing and cleaning kitchen utensils and fruits and vegetables, and the byproduct can be subjected to oxidation treatment to prepare a product with disinfection performance, so that the aim of maximally utilizing resources can be achieved.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 1/3 of the volume of the electrolytic cell; the electrolyte is obtained by mixing edible salt and water in a mass ratio of 1: 1000.
S2, arranging an anode and a cathode in the electrolyte, applying a voltage of 2.7V to the two ends of the anode and the cathode to perform electrolytic treatment on the electrolyte, and controlling the current density in the electrolytic treatment process to be 4.5kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
Example 2
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 1/3 of the volume of the electrolytic cell; the electrolyte is obtained by mixing edible salt and water at a mass ratio of 1: 800.
S2, arranging an anode and a cathode in the electrolyte, applying a voltage of 1V to the two ends of the anode and the cathode to perform electrolytic treatment on the electrolyte, and controlling the current density in the electrolytic treatment process to be 3kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
Example 3
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 2/3 of the volume of the electrolytic cell; the electrolyte is obtained by mixing edible salt and water at a mass ratio of 1: 1200.
S2, setting anode anda cathode, and applying a voltage of 5V across the anode and the cathode to electrolyze the electrolyte, and controlling the current density during the electrolysis to be 6kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
Example 4
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 1/3 of the volume of the electrolytic cell; the electrolyte is obtained by mixing edible salt and water at a mass ratio of 1: 900.
S2, arranging an anode and a cathode in the electrolyte, applying a voltage of 2V to the two ends of the anode and the cathode to perform electrolytic treatment on the electrolyte, and controlling the current density in the electrolytic treatment process to be 3.5kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
Example 5
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 2/3 of the volume of the electrolytic cell; the electrolyte was prepared by mixing edible salt and water at a mass ratio of 1: 1100.
S2, arranging an anode and a cathode in the electrolyte, applying a voltage of 4V to the two ends of the anode and the cathode to perform electrolytic treatment on the electrolyte, and controlling the current density in the electrolytic treatment process to be 5kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
Example 6
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 2/3 of the volume of the electrolytic cell; the electrolyte is obtained by mixing edible salt and water in a mass ratio of 1: 950.
S2, arranging an anode and a cathode in the electrolyte, applying a voltage of 3V at two ends of the anode and the cathode to perform electrolytic treatment on the electrolyte, and controlling the current density in the electrolytic treatment process to be 4kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
Example 7
This embodiment provides a method of preparing a detergent, comprising the steps of:
s1, adding electrolyte into the electrolytic cell; wherein the volume of the electrolyte added is 2/3 of the volume of the electrolytic cell; the electrolyte is obtained by mixing edible salt and water in a mass ratio of 1: 1050.
S2, arranging an anode and a cathode in the electrolyte, applying a voltage of 2.5V to the two ends of the anode and the cathode to perform electrolytic treatment on the electrolyte, and controlling the current density in the electrolytic treatment process to be 4kA/m2And obtaining an electrolysis product. Meanwhile, in the electrolysis process, raw materials such as edible salt, water and the like can be continuously supplemented at the anode, and the amount of the raw materials is measured by a flowmeter.
S3, separating the obtained electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product, and enabling the acidic product to enter an acidic tank and the alkaline product to enter an alkaline tank.
And S4, continuously dripping salt solution into the acid tank according to the liquid level change in the acid tank to oxidize the acid product in the acid tank, thereby preparing the chloric acid/perchloric acid disinfectant.
S5, filtering and screening the alkaline product in the alkaline tank through ion exchange resin, and purifying to obtain the cleaning agent.
Wherein the ion diaphragm can be selected from CHF-Wk-1 available from Nippon environmental engineering of Japan; the salt solution can adopt sodium chloride solution; the purification method can adopt an electrolysis method, and alkaline products are purified and separated through processing links such as electrode reaction, an isolating membrane and the like in electrolysis equipment.
The acidic product and the detergent obtained in example 1 were subjected to pH measurement and component analysis, and the measurement and analysis results are shown in table 1 below.
TABLE 1
Product of | pH value | Chlorine content (mg/L) | Lead content (mg/L) | Mercury content (mg/L) |
Acidic products | 2.1 | 1.44 | <0.0007 | <0.0001 |
Cleaning agent | 11.5 | 0 | - | - |
As can be seen from Table 1 above, the detergent prepared by the embodiment of the present invention has strong alkalinity, and can be effectively used for cleaning kitchenware, fruits, vegetables, etc.
In practical application, the surface of the tableware before being cleaned is provided with a layer of oil stain, and the oil stain can be quickly dissolved under the action of the cleaning agent prepared by the embodiment of the invention, so that the cleaning agent has strong alkali-containing property and has the properties of a surfactant and emulsification. The oil is permeated and emulsified to increase the dissolving effect, so that the oil stain is washed away, and the tableware becomes bright and clean, and has no odor and oil stain. At present, tableware detergent on the market is formed by combining a plurality of chemical products, contains polyhydroxy fatty acid, foam reinforcing agent and other chemical products, and if the detergent is not washed by a large amount of clear water after being degreased, certain chemical residues can be left on tableware and fruits and vegetables, so that the detergent can be eaten by people for a long time and can directly harm human health. Meanwhile, due to the discharge of a large amount of chemical liquid, the environment can be polluted, and limited water resources are wasted. The cleaning agent prepared by the embodiment of the invention is a strong-alkaline cleaning agent without any chemical residues, and has strong cleaning property, no toxicity and no pollution.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the present invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (10)
1. The preparation method of the cleaning agent is characterized by comprising the following steps:
adding electrolyte into the electrolytic cell; the electrolyte comprises edible salt and water; the mass ratio of the edible salt to the water is 1 (800-1200);
applying voltage to the electrolyte to perform electrolytic treatment on the electrolyte to obtain an electrolytic product;
separating the electrolysis product to obtain an acidic product and an alkaline product;
and filtering and screening the alkaline product, and purifying to obtain the cleaning agent.
2. The preparation method of the detergent according to claim 1, wherein the mass ratio of the edible salt to the water is 1 (900-1100).
3. The method for preparing a cleaning agent according to claim 1, wherein in the step, the voltage applied to the electrolyte is 1-5V.
4. The method for preparing a cleaning agent according to claim 1, wherein in the step (A), the current density of the electrolysis treatment is 3-6 kA/m2。
5. The method for preparing a cleaning agent according to claim 1, wherein the step of separating the electrolysis product to obtain an acidic product and an alkaline product specifically comprises:
and separating the electrolysis product through an ion diaphragm to obtain an acidic product and an alkaline product.
6. The method for preparing the cleaning agent according to claim 1, wherein the step of filtering and screening the alkaline product specifically comprises:
and filtering and screening the alkaline product through ion exchange resin.
7. The preparation method of the cleaning agent as claimed in any one of claims 1 to 6, wherein the preparation method further comprises the following steps:
adding a salt solution to the acidic product to subject the acidic product to an oxidation treatment.
8. A cleaning agent prepared by the preparation method of any one of claims 1 to 7.
9. The cleaning agent according to claim 8, wherein the pH of the cleaning agent is 11 to 12.
10. Use of a cleaning agent according to any one of claims 8 to 9 for cleaning kitchen utensils and/or fruit and vegetables.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112603928A (en) * | 2020-12-15 | 2021-04-06 | 上海安法生物科技有限公司 | Disinfectant and detergent co-production method and disinfectant |
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US6743351B1 (en) * | 1998-10-05 | 2004-06-01 | Miz Co., Ltd. | Method and apparatus for producing cleaning agent |
CN103058332A (en) * | 2012-12-26 | 2013-04-24 | 王玉华 | Household electrically functional acidic ionized water generator and control method |
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