CN111450040A - Aquilaria agallocha wash-free sleeping mask and preparation method thereof - Google Patents
Aquilaria agallocha wash-free sleeping mask and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention provides an agilawood no-wash sleeping mask and a preparation method thereof, the agilawood no-wash sleeping mask comprises, by mass, 66-68% of water, 9-11% of butanediol, 4-6% of propylene glycol, 4-6% of isopropyl myristate, 1-3% of nicotinamide, 1-3% of trehalose, 1.4-1.6% of polyacrylamide/C13-14 isoparaffin/laureth-7, 0.5-1.5% of radix stephaniae tetrandrae extract, 0.4-0.6% of agilawood extract, 0.04-0.06% of leuconostoc/radish (RAPHANUSI VUS) root fermentation product filtrate, 1.4-1.6% of tripeptide-1 copper, 0.4-0.6% of yeast extract, 0.1-0.3% of β -glucan, 0.05-0.15% of allantoin, 0.05-0.15% of xanthan gum, 0.05-0.15% of carbomer, 0.2-0.2% of carbomer, 0.3% of triethanolamine, 0.2% of transparent moisturizing and 0.05-0.15% of xanthan gum, and the effects of skin repairing through moisturizing, and the effects of skin repairing through skin conditioning are improved, and the effects of effective conditioning effects of skin repairing through skin conditioning are achieved during the skin conditioning, the skin conditioning is overcome the defects of insufficient in skin repairing effect of skin repairing through skin moistening, the effects of skin repairing through skin repairing, the skin conditioning effect of the skin conditioning, the skin conditioning effect of the.
Description
Technical Field
The invention relates to the technical field of skin care products, and in particular relates to a agilawood wash-free sleep mask and a preparation method thereof.
Background
With the gradual acceleration of the pace of life of people, in recent years, the wash-free sleeping mask is popular with consumers because of the characteristic of being wash-free at night. However, the existing wash-free sleep mask mainly tends to have simple moisturizing and moisture-keeping functions, the high-concentration colloid component has film-forming property and prevents water in the horny layer from volatilizing, when the wash-free sleep mask is required to be endowed with the functions of nourishing and firming the skin, the wash-free sleep mask has poor stability and is not beneficial to skin absorption, the effective components are difficult to be in close contact with and permeate through skin tissues, the skin conditioning and repairing effects are poor, the effective components are easy to remain on the surface layer of the skin due to insufficient absorption of the effective components by the skin at night and influence the sebum metabolism of the skin, particularly for people with sensitive muscles, the percutaneous absorption rate of the nutrient components is low, the hair follicles of the skin are easy to be blocked and cause skin problems such as skin redness, acne, inflammation and the like, so that the wash-free sleep mask which has high stability and easy absorption and can effectively condition, repair and nourish the skin is prepared, and enhance the skin conditioning, promotes the wider application of the wash-free sleep mask and has important significance for the development and application of the wash-free sleep mask product.
Disclosure of Invention
In view of the above, the invention provides the agilawood no-clean sleep mask and the preparation method thereof, which effectively overcome the defects that the existing no-clean sleep mask is difficult to effectively realize poor skin permeation effect and low transdermal absorption rate of nutrient components and poor skin conditioning and repairing effects during sleep, and the agilawood no-clean sleep mask has good stability and easy absorption, can effectively condition, repair, nourish and tighten skin, enhances the absorption of the skin on the active components, and improves the skin conditioning, repairing, moisturizing and moisturizing functions.
The technical scheme of the invention is realized as follows:
the invention provides an agilawood leave-on sleep mask, which comprises, by mass, 66-68% of water, 9-11% of butanediol, 4-6% of propylene glycol, 4-6% of isopropyl myristate, 1-3% of nicotinamide, 1-3% of trehalose, 1.4-1.6% of polyacrylamide/C13-14% of isoparaffin/laureth-7, 0.5-1.5% of radix stephaniae tetrandrae extract, 0.4-0.6% of agilawood extract, 0.04-0.06% of leuconostoc/radish root fermentation product filtrate, 1.4-1.6% of tripeptide-1 copper, 0.4-0.6% of yeast extract, 0.1-0.3% of β -glucan, 0.05-0.15% of allantoin, 0.05-0.15% of xanthan gum, 0.2-0.4% of carbomer, 0.2-0.3% of triethanolamine, 0.2-0.4% of allantoin, 0.15% of allantoin, 0.05-0.15% of carrageenan, and 0.7.7% of a moisturizing skin-2 skin-2, and a moisturizing skin repairing skin by using a moisturizing skin-activating skin-skin.
Further, the plant extract includes any one or more of centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract.
Further, the composition comprises, by mass, 67.75% of water, 10% of butanediol, 5% of propylene glycol, 5% of isopropyl myristate, 2% of nicotinamide, 2% of trehalose, 1.5% of polyacrylamide/C13-14 isoparaffin/laureth-7, 1% of radix stephaniae tetrandrae extract, 0.5% of agilawood extract, 0.05% of a filtrate of a fermentation product of deinococcus tenuissimae/radish root, 1.5% of tripeptide-1 copper, 0.5% of a yeast extract, 0.2% of β -glucan, 0.1% of allantoin, 0.1% of xanthan gum, 0.3% of carbomer, 0.25% of triethanolamine, 0.3% of p-hydroxyacetophenone, 1% of 1, 2-hexanediol, 0.15% of hyaluronic acid and 0.8% of a plant extract.
A preparation method of the agilawood leave-on sleep mask comprises the following steps:
(1) oil phase mixture: weighing isopropyl myristate, polyacrylamide/C13-14 isoparaffin/laureth-7 according to the proportion, heating to dissolve at 80-90 ℃, and stirring for 3-5 min to mix uniformly to obtain an oil phase mixture for later use;
(2) aqueous phase mixture: weighing water, butanediol, propylene glycol, allantoin, xanthan gum, carbomer and hyaluronic acid according to a proportion, heating and dissolving at 80-90 ℃, and stirring for 5-8 min to uniformly mix to obtain a water phase mixture for later use;
(3) homogenizing and emulsifying: slowly stirring the oil phase mixture and the water phase mixture for 10-13 min at a speed of 20-25 r/min in a homogenizing and emulsifying pot, and then homogenizing and emulsifying for 7-10 min to obtain a water-oil mixture;
(4) sequentially adding nicotinamide, trehalose, tripeptide-1 copper, β -glucan and triethanolamine into the water-oil mixture under the continuous stirring state of 35-40 r/min, sequentially adding a radix stephaniae tetrandrae extract, an agilawood extract, a fermentation product filtrate of the roots of streptococcus pyogenes/radish (RAPHANU SSATIVUS), a yeast extract and a plant extract under the continuous stirring state of 70-80 r/min after the addition is finished, stirring for 3-5 min at 25-30 r/min after the addition is finished, and performing secondary high-pressure homogenizing emulsification for 5-8 min to obtain an agilawood washing-free sleep mask preform;
(5) adding p-hydroxyacetophenone and 1, 2-hexanediol, mixing and stirring uniformly to obtain the finished product of the agilawood wash-free sleeping mask. The invention respectively homogenizes and preliminarily emulsifies part of oil phase mixture and water phase mixture under certain conditions to form a preliminarily stable and uniform water-oil mixed system, then adds and mixes active ingredients such as nicotinamide, trehalose, tripeptide-1 copper, radix stephaniae tetrandrae extract, agilawood extract, staphylococcus aureus/radish (RAPHANU SSATIVUS) root fermentation product filtrate and the like and a composite skin activator step by step, improves the mixing uniformity among all the components under the action of secondary high-pressure homogenizing and emulsifying, and is beneficial to improving the dispersion and the use stability of the whole emulsifying mixed system.
Further, in the step (1), the mixing and stirring speed of the water phase mixture is 25-30 r/min.
Further, in the step (2), the mixing and stirring speed of the water phase mixture is 15-20 r/min.
Further, in the step (3), the oil phase mixture and the water phase mixture are mixed and stirred uniformly, and then the mixture is homogenized and emulsified at the temperature of 70-80 ℃ and the homogenization speed of 7500-8500 r/min. The oil phase mixture and the water phase mixture are homogenized and emulsified at high speed and high temperature, which is favorable for improving the dispersion stability of a mixed system.
Further, in the step (4), the second high-pressure homogenizing and emulsifying is to homogenize and emulsify under the conditions of 45-60 ℃, the homogenizing pressure of 120-300 MPa, and the homogenizing speed of 9000-12000 r/min. The secondary high-pressure homogenization treatment is favorable for the dispersion of fat-soluble components of the plant extract.
Further explaining, in the step (5), after the agilawood leave-in sleep mask preform subjected to secondary high-pressure homogenizing and emulsifying is kept at normal pressure for 10-15 min, p-hydroxyacetophenone and 1, 2-hexanediol are added, and the mixture is mixed and stirred uniformly, so that an agilawood leave-in sleep mask finished product is obtained.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, the agilawood extract and the natural plant extract are mainly used as active ingredients to enhance the barrier function of an epidermal cell membrane structure and improve the tolerance and conditioning and repairing effects of skin, and the tetrandra root extract, the leuconostoc/radish root fermentation product filtrate and the tripeptide-1 copper are preferably compounded to be used as a composite skin activator, so that the synergistic effect of good convergence and tightness on pores and anti-inflammatory and antioxidant reactions of skin is achieved, the balance state of the skin is further improved, the effects of promoting the remodeling and activation of skin tissue cells are jointly achieved, a deep penetration channel is opened for the skin, the deep penetration and absorption of nutrient substances and functional substances are promoted, and polyacrylamide/C13-14 isoparaffin/laureth-7, carbomer and triethanolamine are selected for thickening, Emulsifying to form a more stable macromolecular structure, and compounding with a humectant to achieve more stable moisturizing and skin moistening effects, so that the agilawood wash-free sleep mask is good in stability, easy to absorb, capable of effectively conditioning, repairing and nourishing and tightening skin, capable of enhancing the absorption of the skin to effective components, capable of effectively nourishing, tightening and brightening the skin, capable of improving the skin conditioning, repairing and moisturizing functions at night, and capable of moistening and moistening the skin, and enabling the skin to be moist and elastic, and continuous use enables the skin to be more tender, bright, smooth and glossy, and more extensive application of the wash-free sleep mask is promoted.
Detailed Description
In order to better understand the technical content of the invention, specific examples are provided below to further illustrate the invention.
The experimental methods used in the examples of the present invention are all conventional methods unless otherwise specified.
The materials, reagents and the like used in the examples of the present invention can be obtained commercially without specific description.
Example-preparation of a leave-in eaglewood sleeping mask according to the following method, comprising the steps of:
(1) oil phase mixture: weighing isopropyl myristate, polyacrylamide/C13-14 isoparaffin/laureth-7 at a certain ratio, dissolving at 85 deg.C under heating, stirring at 28r/min for 4min, and mixing to obtain oil phase mixture; wherein, polyacrylamide/C13-14 isoparaffin/laureth-7 is the existing commercial product Repoly 415;
(2) aqueous phase mixture: weighing water, butanediol, propylene glycol, allantoin, xanthan gum, carbomer and hyaluronic acid according to a certain proportion, heating and dissolving at 85 deg.C, and stirring at 16r/min for 7min to obtain water phase mixture;
(3) homogenizing and emulsifying: slowly stirring the oil phase mixture and the water phase mixture for 12min at 23r/min in a homogenizing and emulsifying pot, and homogenizing and emulsifying at 75 deg.C and 8000r/min for 8min to obtain water-oil mixture;
(4) sequentially adding nicotinamide, trehalose, tripeptide-1 copper, β -glucan and triethanolamine into the water-oil mixture under the continuous stirring state of 38r/min, sequentially adding a tetrandra root extract, an agilawood extract, a fermentation product filtrate of staphylococcus aureus/radish (RAPHANU SSATIVUS), a yeast extract and a plant extract under the continuous stirring state of 75r/min after the addition is finished, stirring for 4min at 28r/min after the addition is finished, performing secondary high-pressure homogenizing and emulsifying, and homogenizing and emulsifying for 6min at 55 ℃, the homogenizing pressure of 200MPa and the homogenizing speed of 11000r/min to obtain an agilawood washing-free mask preform;
(5) keeping the temperature at normal pressure for 13min, adding p-hydroxyacetophenone and 1, 2-hexanediol, mixing and stirring uniformly to obtain the finished product of the agilawood leave-in sleep mask.
Wherein, the proportion of each component is as follows:
wherein the plant extract is prepared by combining asiatic centella root extract, giant knotweed rhizome extract, baical skullcap root extract, tea leaf extract, glabrous greenbrier rhizome extract, chamomile flower extract and rosemary leaf extract according to the mass ratio of 1:1:1:1:2: 2; comparative example 1 tripeptide-1 copper was replaced with 1.5% oligopeptide-1 and used in combination with tetrandra root extract, leuconostoc/radish root fermentation product filtrate as a composite skin activator, and the rest was the same as in example 4.
In order to test the moisturizing, conditioning and repairing effects of the agilawood leave-in sleep mask, a trial investigation experiment is carried out, the agilawood leave-in sleep mask sample prepared in the embodiment 4 of the invention and the agilawood leave-in sleep mask sample prepared in the comparative example 1 are subjected to standard detection of the mask (QB/T2872-plus 2017) standard, and the trial investigation experiment is carried out after the results show that all indexes meet the corresponding standards.
1. Test objects: selecting 45 volunteer testers, dividing the testers into 3 groups, and respectively carrying out trial condition comparison investigation on the agilawood leave-free sleep mask samples obtained in the example 4 and the comparative example 1 and the existing commercially available leave-free sleep mask (a Bailinglingnighttime repairing sleep mask);
2. the test method comprises the following steps: after a tester cleans the skin, respectively taking a proper amount of different samples to coat the skin on the face, gently massaging the skin until the skin is absorbed, using the skin once every day at night for 1 month, observing and counting trial effect feedback conditions (according to the number of people) as shown in the following tables 1-3;
TABLE 1-feedback Table of trial effect of Aquilaria agallocha leave-on sleep mask of example 4
TABLE 2 trial effect feedback chart of the existing commercial no-clean sleeping mask
TABLE 3-feedback Table of trial effect of Aquilaria agallocha leave-on sleep mask of comparative example 1
The above tables 1-3 show that compared with the existing commercial products, the no-wash sleep mask obtained by the invention can achieve good moisturizing effect, effectively enhance the barrier function of the epidermal cell membrane structure, improve the tolerance and conditioning and repairing effects of the skin, improve the nourishing and tightening effects of the skin, enhance the anti-inflammatory and antioxidant functions of the skin, is fresh and cool, and reduces the thick and sticky feeling of the skin. Through comparison of trial effect feedback conditions of the embodiment 4 and the comparative example 1, the compound skin activator is prepared by preferably compounding the tetrandra root extract, the staphylococcus aureus/radish root fermentation product filtrate and the tripeptide-1 copper, so that the compound skin activator has the synergistic effects of good convergence and tightness on pores and enhancement of anti-inflammatory and antioxidant reactions of skin, further improves the balance state of skin, plays a role in promoting the remodeling and activation of skin tissue cells, opens a deep penetration channel for the skin, promotes the deep penetration and absorption of nutrient substances and functional substances, can effectively improve the effects of nourishing and pore tightening, improves the transdermal absorption rate of nutrient components of the skin at night, improves the skin conditioning and repairing and moisturizing functions, has no irritation on the skin, has allergic phenomena such as redness, swelling, peeling and the like, and long-term use of the nourishing and pore tightening, The firming effect is obviously better than that of the comparative example 1, and the firming agent has no greasy and thick feeling.
Example 5-according to the component formulation of example 4, a leave-in eaglewood sleeping mask was prepared by the following method, including the steps of:
(1) oil phase mixture: weighing isopropyl myristate, polyacrylamide/C13-14 isoparaffin/laureth-7 at a certain ratio, dissolving at 80 deg.C under heating, stirring at 25r/min for 3min, and mixing to obtain oil phase mixture;
(2) aqueous phase mixture: weighing water, butanediol, propylene glycol, allantoin, xanthan gum, carbomer and hyaluronic acid at a certain proportion, heating at 80 deg.C for dissolving, and stirring at 15r/min for 5min for mixing to obtain water phase mixture;
(3) homogenizing and emulsifying: slowly stirring the oil phase mixture and the water phase mixture for 10-13 min at 20r/min in a homogenizing and emulsifying pot, and then homogenizing and emulsifying for 7min at 70 ℃ and the homogenizing speed of 7500r/min to obtain a water-oil mixture;
(4) sequentially adding nicotinamide, trehalose, tripeptide-1 copper, β -glucan and triethanolamine into the water-oil mixture under the continuous stirring state of 35r/min, sequentially adding a tetrandra root extract, an agilawood extract, a fermentation product filtrate of staphylococcus aureus/radish (RAPHANU SSATIVUS) root, a yeast extract and a plant extract under the continuous stirring state of 70r/min after the addition is finished, stirring for 3min at 25r/min after the addition is finished, performing secondary high-pressure homogenizing and emulsifying, and homogenizing and emulsifying for 5min at 45 ℃, the homogenizing pressure of 120MPa and the homogenizing speed of 9000r/min to obtain an agilawood washing-free mask preform;
(5) keeping the temperature for 15min under normal pressure, adding p-hydroxyacetophenone and 1, 2-hexanediol, mixing and stirring uniformly to obtain the finished product of the agilawood leave-in sleep mask.
Comparative example 2-according to the component formulation of example 4, a leave-in eaglewood sleeping mask was prepared by a conventional preparation method, comprising the following steps:
(1) weighing water, butanediol, propylene glycol, allantoin, xanthan gum, carbomer, hyaluronic acid, isopropyl myristate, polyacrylamide/C13-14 isoparaffin/laureth-7 at a certain proportion, sequentially adding into a homogenizing emulsifying pot, stirring at 25r/min for 13min, and mixing;
(2) sequentially adding nicotinamide, trehalose, tripeptide-1 copper, β -glucan, triethanolamine, radix Stephaniae Tetrandrae extract, lignum Aquilariae Resinatum extract, Leuconostoc/radish (RAPHANU SSATIVUS) root fermentation product filtrate, yeast extract and plant extract under continuously stirring at 40r/min, and homogenizing and emulsifying at 80 deg.C and homogenizing speed of 10000r/min for 10min to obtain lignum Aquilariae Resinatum wash-free sleep mask preform;
(3) keeping the temperature for 15min under normal pressure, adding p-hydroxyacetophenone and 1, 2-hexanediol, mixing and stirring uniformly to obtain the finished product of the agilawood leave-in sleep mask.
The agilawood leave-in sleep mask prepared in the example 4, the example 5 and the comparative example 2 is subjected to a stability test and a viscosity test, wherein equal amounts of samples are respectively placed in cosmetic bottles and are kept standing for 3 months at room temperature, no layering phenomenon occurs, and the smell is unchanged; and the viscosity values of the samples are respectively measured by adopting a digital display viscometer, and the results are shown in the following table, so that the viscosity of the agilawood leave-on sleep mask in the comparative example 2 is lower than that of the examples 4 and 5, which shows that the invention firstly carries out homogenization and preliminary emulsification on part of oil phase mixture and water phase mixture, then further carries out step-by-step addition and mixing on effective active ingredients and a composite skin activator, and finally enhances the dispersion stability of an emulsification mixing system through secondary high-pressure homogenization and emulsification, thereby being beneficial to improving the mixing uniformity and emulsification dispersion effect among the components.
| Item | Example 4 | Example 5 | Comparative example 2 |
| Viscosity/(mpa.s) | 20151 | 20094 | 16532 |
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (9)
1. The agilawood leave-on sleeping mask is characterized by comprising, by mass, 66-68% of water, 9-11% of butanediol, 4-6% of propylene glycol, 4-6% of isopropyl myristate, 1-3% of nicotinamide, 1-3% of trehalose, 1.4-1.6% of polyacrylamide/C13-14 isoparaffin/laureth-7, 0.5-1.5% of radix stephaniae tetrandrae extract, 0.4-0.6% of agilawood extract, 0.04-0.06% of leuconostoc/radish root fermentation product filtrate, 1.4-1.6% of tripeptide-1 copper, 0.4-0.6% of yeast extract, 0.1-0.3% of β -glucan, 0.05-0.15% of allantoin, 0.05-0.15% of xanthan gum, 0.2-0.4% of carbomer, 0.2-0.3% of triethanolamine, 0.2-0.4% of acetophenone, 0.05-0.15% of p-hydroxy-hydroxybenzene glycol, and 0.9-1.7% of plant hyaluronic acid.
2. The agilawood leave-on sleep mask as claimed in claim 1, which is characterized in that: the plant extract comprises one or more of centella asiatica root extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea leaf extract, glycyrrhiza glabra root extract, chamomile flower extract and rosemary leaf extract.
3. The agilawood leave-on sleep mask as claimed in claim 1, which comprises, by mass, 67.75% of water, 10% of butylene glycol, 5% of propylene glycol, 5% of isopropyl myristate, 2% of nicotinamide, 2% of trehalose, 1.5% of polyacrylamide/C13-14 isoparaffin/laureth-7, 1% of radix stephaniae tetrandrae extract, 0.5% of agilawood extract, 0.05% of leuconostoc/radish root fermentation product filtrate, 1.5% of tripeptide-1 copper, 0.5% of yeast extract, 0.2% of β -glucan, 0.1% of allantoin, 0.1% of xanthan gum, 0.3% of carbomer, 0.25% of triethanolamine, 0.3% of p-hydroxyacetophenone, 1% of 1, 2-hexanediol, 0.15% of hyaluronic acid and 0.8% of plant extract.
4. A preparation method of the agilawood leave-on sleep mask as claimed in any one of claims 1 to 3, which is characterized in that: the method comprises the following steps:
(1) oil phase mixture: weighing isopropyl myristate, polyacrylamide/C13-14 isoparaffin/laureth-7 according to the proportion, heating to dissolve at 80-90 ℃, and stirring for 3-5 min to mix uniformly to obtain an oil phase mixture for later use;
(2) aqueous phase mixture: weighing water, butanediol, propylene glycol, allantoin, xanthan gum, carbomer and hyaluronic acid according to a proportion, heating and dissolving at 80-90 ℃, and stirring for 5-8 min to uniformly mix to obtain a water phase mixture for later use;
(3) homogenizing and emulsifying: slowly stirring the oil phase mixture and the water phase mixture for 10-13 min at a speed of 20-25 r/min in a homogenizing and emulsifying pot, and then homogenizing and emulsifying for 7-10 min to obtain a water-oil mixture;
(4) sequentially adding nicotinamide, trehalose, tripeptide-1 copper, β -glucan and triethanolamine into the water-oil mixture under the continuous stirring state of 35-40 r/min, sequentially adding a radix stephaniae tetrandrae extract, an agilawood extract, a fermentation product filtrate of the roots of streptococcus pyogenes/radish (RAPHANU SSATIVUS), a yeast extract and a plant extract under the continuous stirring state of 70-80 r/min after the addition is finished, stirring for 3-5 min at 25-30 r/min after the addition is finished, and performing secondary high-pressure homogenizing emulsification for 5-8 min to obtain an agilawood washing-free sleep mask preform;
(5) adding p-hydroxyacetophenone and 1, 2-hexanediol, mixing and stirring uniformly to obtain the finished product of the agilawood wash-free sleeping mask.
5. The preparation method of the agilawood leave-on sleep mask as claimed in claim 4, wherein the preparation method comprises the following steps: in the step (1), the mixing and stirring speed of the water phase mixture is 25-30 r/min.
6. The preparation method of the agilawood leave-on sleep mask as claimed in claim 4, wherein the preparation method comprises the following steps: in the step (2), the mixing and stirring speed of the water phase mixture is 15-20 r/min.
7. The preparation method of the agilawood leave-on sleep mask as claimed in claim 4, wherein the preparation method comprises the following steps: in the step (3), the oil phase mixture and the water phase mixture are mixed and stirred uniformly, and then homogenized and emulsified at the temperature of 70-80 ℃ and the homogenization speed of 7500-8500 r/min.
8. The preparation method of the agilawood leave-on sleep mask as claimed in claim 4, wherein the preparation method comprises the following steps: in the step (4), the secondary high-pressure homogenizing and emulsifying is to homogenize and emulsify under the conditions of 45-60 ℃, the homogenizing pressure of 120-300 MPa and the homogenizing speed of 9000-12000 r/min.
9. The preparation method of the agilawood leave-on sleep mask as claimed in claim 4, wherein the preparation method comprises the following steps: and (5) preserving the heat of the preformed agilawood leave-in sleep mask subjected to secondary high-pressure homogenizing and emulsifying for 10-15 min at normal pressure, adding p-hydroxyacetophenone and 1, 2-hexanediol, and mixing and stirring uniformly to obtain a finished agilawood leave-in sleep mask product.
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| CN114306154A (en) * | 2021-12-14 | 2022-04-12 | 中国热带农业科学院热带作物品种资源研究所 | Composite micro-emulsion mask liquid containing valerian oil and blumea balsamifera oil and preparation method thereof |
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