CN110623851B - Soothing and repairing essence and preparation method thereof - Google Patents

Abstract

The invention provides a soothing and repairing essence and a preparation method thereof, wherein the soothing and repairing essence comprises an A phase and a B phase, wherein the A phase comprises deionized water: 64.0-96.0 parts of EDTA disodium: 0.01-0.03 part, butanediol: 1.0-4.0 parts of glycerol: 1.0-4.0 parts and beta-glucan: 0.01-1.0 part; and the phase B comprises ceramide coated by lecithin: 0.31-1.5 parts of paeonol: 0.1-1.0 parts, fibronectin: 0.1-3.0 parts of Bulgaria rose water: 1.0-20 parts, 1, 2-hexanediol: 0.5-2.0 parts of purslane extract: 0.1-3.0 parts and flower root extract: 0.1-3.0 parts; and heating in water bath with the components in corresponding weight parts, stirring in vacuum, dissolving and mixing uniformly, standing, storing in an aseptic environment and filling to obtain the finished product.

Description

Soothing and repairing essence and preparation method thereof

Technical Field

The invention relates to the technical field of skin care cosmetics, and particularly relates to a soothing and repairing essence and a preparation method thereof.

Background

With the improvement of living standard, the types of skin care products are more and more, the skin care products are more and more widely used, the quality requirements on the products are higher and higher, but the quality of the skin care products is not uniform. In order to achieve a temporary effect, glucocorticoid can be added into some products, so that the skin health of consumers can be damaged after long-term use, and the skin is more susceptible to being sensitive; in addition, the change of the external environment, the rise of global temperature and environmental pollution, and the improper use of cosmetics and skin care products also cause the skin of the human body to be sensitive easily, which is mainly characterized in that the cuticle of the skin becomes thin, and the phenomena of redness, swelling, itching or small red rash appear.

The anti-allergy skin care product and the repair skin care product are produced according to the skin sensitivity phenomenon. The skin care product is mainly prepared by reducing stimulating components such as essence, pigment, alcohol and preservative, or adding some anti-inflammatory and relieving components, such as: the aloe powder, the chamomile extract and other raw materials achieve the anti-allergic effect; the other is the essence for repairing, which can play a certain role in relieving and repairing skin after the skin is sensitive, but has poor absorption effect and long repair period.

In addition, the anti-allergy skin care product or the repairing skin care product has relatively single function and limited effect. The repair capability of the anti-allergy type product is deficient, effective relieving and repairing effects cannot be generated during allergy, and the repair period is long due to the lack of the anti-allergy prevention effect in the repair process of the repair type skin care product, so that the dual effects of anti-allergy and repair cannot be achieved.

Disclosure of Invention

Aiming at the defects and shortcomings in the background technology, the invention provides the soothing and repairing essence, which can achieve the dual effects of anti-allergy and repairing for sensitive skin, and also has the effects of repairing skin barriers and relieving itching.

The second purpose of the invention is to provide a preparation method of the soothing and repairing essence, which can effectively protect the activity of each component, so that the raw materials can fully play a synergistic function, and the maximization of skin barrier repairing and relieving itching is achieved.

In order to realize the purpose, the invention adopts the following technical scheme to realize the purpose:

the soothing and repairing essence comprises an A phase and a B phase, wherein the A phase comprises the following components in parts by weight:

deionized water: 64.0 to 96.0 portions;

disodium EDTA: 0.01-0.03 part;

butanediol: 1.0-4.0 parts;

glycerol: 1.0-4.0 parts;

beta-glucan: 0.01-1.0 part;

the phase B comprises the following components in parts by weight:

lecithin-encapsulated ceramides: 0.31-1.5 parts;

paeonol: 0.1-1.0 part;

fibronectin: 0.1-3.0 parts;

bulgaria rose water: 1.0-20 parts;

1, 2-hexanediol: 0.5-2.0 parts;

and (3) purslane extract: 0.1-3.0 parts;

flower root extract: 0.1 to 3.0 portions.

Further measures taken are: the phase A comprises the following components in parts by weight:

deionized water: 79.69 parts of;

disodium EDTA: 0.01 part;

butanediol: 2.0 parts of (B);

glycerol: 3.0 parts of (B);

beta-glucan: 1.0 part;

the phase B comprises the following components in parts by weight:

hydrogenated lecithin: 0.3 part;

ceramide 3: 0.2 part;

paeonol: 1.0 part;

fibronectin: 1.5 parts;

bulgaria rose water: 5.0 parts of (B);

1, 2-hexanediol: 0.3 part;

and (3) purslane extract: 3.0 parts of (B);

peony root extract: 3.0 parts.

Further measures taken are: the lecithin-coated ceramide comprises hydrogenated lecithin and ceramide 3.

Further measures taken are: the hydrogenated lecithin comprises the following components in parts by weight: 0.35-1.0 part; the ceramide 3 comprises the following components in parts by weight: 0.01-0.5 portion.

Further measures taken are: the flower root extract is root extract of one or more of peony, rose and Chinese rose.

The ceramide wrapped by lecithin is one of important components of skin lipid, can effectively repair skin barriers, prevent water loss and stimulation of external adverse factors to skin, and slow down stress response; the paeonol has good effects of relieving pain, diminishing inflammation and relieving itching, and can immediately relieve skin discomfort; fibronectin is widely involved in the processes of cell migration, adhesion, proliferation, hemostasis, tissue repair and the like, mobilizes a mononuclear phagocyte system to remove harmful substances at the damaged tissue, and has the function of growth factors; the purslane plant extract and the root extracts of the peony, the rose and the Chinese rose have good skin conditioning effects of sterilization, inflammation diminishing, sedation and the like.

The invention also provides a preparation method of the soothing and repairing essence, which comprises the following steps:

1) adding the phase A components in parts by weight into a vacuum closed container, heating in a water bath to 83-86 ℃, and stirring in vacuum for 15-25 minutes until the phase A components are completely dissolved to obtain a mixture A;

2) stopping heating the mixture A, stopping stirring, and standing for a period of time until the temperature is reduced to 43-47 ℃;

3) adding the components of the phase B in parts by weight into the mixture A obtained in the step 2), and carrying out vacuum stirring until the components in the phase B are fully and uniformly mixed with the mixture A to obtain a semi-finished product B;

4) inspecting the semi-finished product B, discharging, and storing in a sterile environment;

5) and (4) carrying out vacuum filling on the semi-finished product B stored in the sterile environment, packaging and warehousing to obtain a finished product.

Through the technical scheme, compared with the prior art, the invention has the following beneficial effects:

(1) the invention fully considers all sensitization factors, all the selected components are natural and have no irritation, and the components are compatible according to the characteristics and the proportion of the components, so that the components supplement each other, the remarkable synergistic function is achieved, and the invention has remarkable effects of relieving, resisting allergy and repairing.

(2) According to the invention, the ceramide is coated by the lecithin to form a structure similar to a skin lipid component, so that the penetration and absorption of active ingredients are effectively promoted; meanwhile, the raw material composition of the plant extraction essences such as fibronectin, paeonol, purslane and the like is added, so that the effects of diminishing inflammation, relieving itching and repairing can be achieved, the effect is mild, and no stimulation is generated.

(3) The preparation method provided by the invention can effectively protect the activity of each component, so that the raw materials can fully play a synergistic function, and the maximization of the effects of repairing skin barriers and relieving itching is achieved.

Detailed Description

In order to clearly understand the technical solutions adopted by the present invention, the following description is made on the preferred embodiments of the present invention, and it should be understood that the embodiments described herein are only used for illustrating and explaining the present invention, and are not used to limit the present invention.

Example 1: the soothing and repairing essence comprises an A phase and a B phase, wherein the A phase comprises the following components in parts by weight:

deionized water: 89.49 parts of a binder;

disodium EDTA: 0.01 part;

butanediol: 1.0 part;

glycerol: 2.0 parts of (B);

beta-glucan: 0.5 part;

the phase B comprises the following components in parts by weight:

hydrogenated lecithin: 0.6 part;

ceramide 3: 0.4 part;

paeonol: 0.5 part;

fibronectin: 1 part;

bulgaria rose water: 2.0 parts of (B);

1, 2-hexanediol: 0.5 part;

and (3) purslane extract: 1.0 part;

peony root extract: 1.0 part.

And was prepared by the following experimental procedure:

1) adding the phase A components in parts by weight into a vacuum closed container, heating the mixture to 86 ℃ in a water bath, and stirring the mixture for 15 to 25 minutes in vacuum until the phase A components are completely dissolved to obtain a mixture A;

2) stopping heating the mixture A, stopping stirring, and standing for a period of time until the temperature is reduced to 47 ℃;

3) adding the components of the phase B in parts by weight into the mixture A obtained in the step 2), and carrying out vacuum stirring until the components in the phase B are fully and uniformly mixed with the mixture A to obtain a semi-finished product B;

4) inspecting the semi-finished product B, discharging, and storing in a sterile environment;

5) and (4) carrying out vacuum filling on the semi-finished product B stored in the sterile environment, and packaging and warehousing to obtain the finished product 1.

Example 2: the soothing and repairing essence comprises an A phase and a B phase, wherein the A phase comprises the following components in parts by weight:

deionized water: 79.69 parts of;

disodium EDTA: 0.01 part;

butanediol: 2.0 parts of (B);

glycerol: 3.0 parts of (B);

beta-glucan: 1.0 part;

the phase B comprises the following components in parts by weight:

hydrogenated lecithin: 0.3 part;

ceramide 3: 0.2 part;

paeonol: 1.0 part;

fibronectin: 1.5 parts;

bulgaria rose water: 5.0 parts of (B);

1, 2-hexanediol: 0.3 part;

and (3) purslane extract: 3.0 parts of (B);

peony root extract: 3.0 parts.

And was prepared by the following experimental procedure:

1) adding the phase A components in parts by weight into a vacuum closed container, heating the mixture to 85 ℃ in a water bath, and stirring the mixture for 15 to 25 minutes in vacuum until the phase A components are completely dissolved to obtain a mixture A;

2) stopping heating the mixture A, stopping stirring, and standing for a period of time until the temperature is reduced to 45 ℃;

3) adding the components of the phase B in parts by weight into the mixture A obtained in the step 2), and carrying out vacuum stirring until the components in the phase B are fully and uniformly mixed with the mixture A to obtain a semi-finished product B;

4) inspecting the semi-finished product B, discharging, and storing in a sterile environment;

5) and (4) carrying out vacuum filling on the semi-finished product B stored in the sterile environment, packaging and warehousing to obtain a finished product 2.

Example 3: the soothing and repairing essence comprises an A phase and a B phase, wherein the A phase comprises the following components in parts by weight:

deionized water: 78.17 parts;

disodium EDTA: 0.02 part;

butanediol: 4.0 parts of (B);

glycerol: 1.0 part;

beta-glucan: 0.01 part;

the phase B comprises the following components in parts by weight:

hydrogenated lecithin: 1.0 part;

ceramide 3: 0.5 part;

paeonol: 0.1 part;

fibronectin: 3.0 parts of (B);

bulgaria rose water: 10.0 parts;

1, 2-hexanediol: 2.0 parts of (B);

and (3) purslane extract: 0.1 part;

peony root extract: 0.1 part.

And was prepared by the following experimental procedure:

1) adding the phase A components in parts by weight into a vacuum closed container, heating the mixture to 83 ℃ in a water bath, and stirring the mixture for 15 to 25 minutes in vacuum until the phase A components are completely dissolved to obtain a mixture A;

2) stopping heating the mixture A, stopping stirring, and standing for a period of time until the temperature is reduced to 43 ℃;

3) adding the components of the phase B in parts by weight into the mixture A obtained in the step 2), and carrying out vacuum stirring until the components in the phase B are fully and uniformly mixed with the mixture A to obtain a semi-finished product B;

4) inspecting the semi-finished product B, discharging, and storing in a sterile environment;

5) and (4) carrying out vacuum filling on the semi-finished product B stored in the sterile environment, packaging and warehousing to obtain a finished product 3.

In addition, the following tests are performed by respectively preparing essence 1, essence 2 and essence 3 by adopting the technical schemes of example 1, example 2 and example 3, and purchasing two similar conventional essences on the market and respectively named as control essence 1 and control essence 2 for comparison.

The test method comprises the following steps: 150 healthy female volunteers 18-38 years old in the same area are collected as subjects, the faces of the subjects have slight inflammation or allergy, the subjects are sensitive skins, and the faces all have slight dry symptoms; volunteers were randomly assigned to 5 groups, 1 to 5, each of 30 people. Volunteer subjects used the corresponding serum samples of each group to be evenly smeared on the face every night and morning after the face was cleaned, and effect and feeling feedback was performed within 3 hours after use.

One month usage records were collected and analyzed for summary data, with the experimental results as shown in tables 1 and 2 below:

table 1: feedback result analysis of volunteer subject use effect

Table 2: improved repair cycle outcome analysis after use by volunteer subjects

Through the test feedback and data analysis results, it can be obviously seen that the essence prepared by the invention has obvious functions of relieving and repairing, has a shorter repairing period, and can meet the requirements of easy sensitivity and quick repair of modern female skin.

The above description is only for the purpose of illustrating the technical solutions of the present invention and not for the purpose of limiting the same, and other modifications or equivalent substitutions made by those skilled in the art to the technical solutions of the present invention should be covered within the scope of the claims of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (5)

1. The soothing and repairing essence is characterized by comprising an A phase and a B phase, wherein the A phase comprises the following components in parts by weight:

deionized water: 60.0-96.0 parts;

disodium EDTA: 0.01-0.03 part;

butanediol: 1.0-4.0 parts;

glycerol: 1.0-4.0 parts;

beta-glucan: 0.01-1.0 part;

the phase B comprises the following components in parts by weight:

lecithin-encapsulated ceramides: 0.31-1.5 parts;

paeonol: 0.1-1.0 part;

fibronectin: 0.1-3.0 parts;

bulgaria rose water: 1.0-20 parts;

1, 2-hexanediol: 0.5-2.0 parts;

and (3) purslane extract: 0.1-3.0 parts;

flower root extract: 0.1-3.0 parts;

the flower root extract is root extract of one or more of peony, rose and Chinese rose.

2. A soothing and repairing essence is characterized in that: the phase A comprises the following components in parts by weight:

deionized water: 79.69 parts of;

disodium EDTA: 0.01 part;

butanediol: 2.0 parts of (B);

glycerol: 3.0 parts of (B);

beta-glucan: 1.0 part;

the phase B comprises the following components in parts by weight:

lecithin-encapsulated ceramides, wherein the ratio of hydrogenated lecithin: 0.3 part; ceramide 3: 0.2 part;

paeonol: 1.0 part;

fibronectin: 1.5 parts;

bulgaria rose water: 5.0 parts of (B);

1, 2-hexanediol: 0.3 part;

and (3) purslane extract: 3.0 parts of (B);

peony root extract: 3.0 parts.

3. A soothing repair serum as claimed in claim 1, wherein: the lecithin-coated ceramide comprises hydrogenated lecithin and ceramide 3.

4. A soothing repair serum according to claim 3, wherein: the hydrogenated lecithin comprises the following components in parts by weight: 0.35-1.0 part; the ceramide 3 comprises the following components in parts by weight: 0.01-0.5 portion.

5. A process for preparing a soothing and rejuvenating serum as claimed in any one of claims 1 to 4, comprising the steps of:

1) adding the phase A components in parts by weight into a vacuum closed container, heating in a water bath to 83-86 ℃, and stirring in vacuum for 15-25 minutes until the phase A components are completely dissolved to obtain a mixture A;

2) stopping heating the mixture A, stopping stirring, and standing for a period of time until the temperature is reduced to 43-47 ℃;

3) adding the components of the phase B in parts by weight into the mixture A obtained in the step 2), and carrying out vacuum stirring until the components in the phase B are fully and uniformly mixed with the mixture A to obtain a semi-finished product B;

4) inspecting the semi-finished product B, discharging, and storing in a sterile environment;

5) and (4) carrying out vacuum filling on the semi-finished product B stored in the sterile environment, packaging and warehousing to obtain a finished product.