CN111450032B - Face mask for whitening skin, fading spots and repairing skin of gorgonia and preparation method thereof - Google Patents
Face mask for whitening skin, fading spots and repairing skin of gorgonia and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a pseudopterogorgia elisahethae whitening spot-fading repairing mask and a preparation method thereof. The facial mask is prepared from the following raw materials in parts by weight: 0.01-0.1 part of hyaluronic acid, 0.01-0.5 part of sclerotium rolfsii gum, 0.01-0.5 part of liquorice extract, 1-10 parts of glycerol, 1-5 parts of propylene glycol, 1-5 parts of butanediol, 0.01-0.5 part of gorgonia pseudopteropilea extract, 0.01-0.1 part of triethanolamine and the balance of water to 100 parts by weight. Human body experiments prove that the mask product has remarkable whitening, spot-lightening and repairing functions, and is safe and non-irritant.
Description
Technical Field
The invention relates to a mask and a preparation method thereof, in particular to a whitening spot-fading repairing mask containing an aucuba japonica extract and a preparation method thereof. The invention belongs to the technical field of cosmetics.
Background
Modern people pursue high-quality life and pay attention to maintenance and health preservation, but the rhythm of life becomes fast, the working pressure increases, and the long-term diet that produces from this is improper, and the life is unusual, leads to qi deficiency, weak blood, spleen transport is not healthy, gathers damp and produces phlegm, phlegm stagnation and transformation heat, evaporates on the face and sees admittedly: sallow complexion, tarnish, oily complexion, gradual appearance of acne and stain deposition. Especially for women, the skin problem caused by overtime stay up is more obvious. The whitening skin care products are good for all people, however, the whitening skin care products on the market are different in quality, most whitening skin care products contain lead and other components which are not good for human health, and even various additives in the skin care products can bring invisible side effects to the skin.
The facial mask is a carrier of facial skin care or beauty care products, is coated or stuck on the face for a certain time, and is removed by cleaning or stripping after beneficial substances in the care or beauty care products are absorbed by the skin or substances harmful to the health of the skin in the surface of the skin are absorbed by the facial mask, so that the purposes of facial skin care or beauty are achieved, such as moisturizing, whitening, anti-aging and oil balancing. However, most of the active ingredients of the existing facial mask are chemical synthesis preparations, and although the facial mask has the effects of moistening skin, whitening skin, beautifying, removing wrinkles and the like, the facial mask contains various chemical additives, belongs to strong drug irritation treatment and has toxic and side effects of stimulating skin and the like; the skin is caused to generate drug dependence, and the drug resistance is generated after long-term use.
Therefore, a mask product which can effectively relieve various symptoms of the skin and has higher safety is urgently needed in the market at present.
Disclosure of Invention
The invention aims to provide a mask product with whitening, spot lightening and repairing functions.
In order to achieve the purpose, the invention adopts the following technical means:
the invention relates to a gorgonia skin-whitening speckle-lightening repair mask which is prepared from the following raw materials in parts by weight:
0.01-0.1 part of hyaluronic acid, 0.01-0.5 part of sclerotium rolfsii gum, 0.01-0.5 part of liquorice extract, 1-10 parts of glycerol, 1-5 parts of propylene glycol, 1-5 parts of butanediol, 0.01-0.5 part of gorgonia pseudopteropilea extract, 0.01-0.1 part of triethanolamine and the balance of water to 100 parts by weight.
Wherein, preferably, the licorice extract contains 98wt% of dipotassium glycyrrhizinate.
Among them, preferably, the hyaluronic acid contains three kinds of molecular weight hyaluronic acid, namely macromolecular hyaluronic acid, medium molecular hyaluronic acid and small molecular hyaluronic acid.
Wherein: macromolecular hyaluronic acid (with the molecular weight range of 1800000-2200000) can form a breathable film on the surface of skin, so that the skin is smooth and moist, the invasion of external bacteria, dust and ultraviolet rays can be blocked, and the skin is protected from being damaged; the medium molecular hyaluronic acid (with the molecular weight range of 1000000-1800000) can tighten the skin and moisturize the skin for a long time; the small molecular hyaluronic acid (the molecular weight is 400000-1000000) can permeate into dermis, has the effects of slightly expanding capillary vessels, increasing blood circulation, improving middle metabolism, promoting skin nutrition absorption, has a strong wrinkle removing function, can increase skin elasticity and delay skin aging.
Wherein, the weight ratio of the three molecular weight (large: medium: small) hyaluronic acids is preferably 1: 1-5: 1-5.
Preferably, the gorgonian extract is prepared by the following method:
1) extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 50-70 mesh fine granules, and extracting with deionized water at 55-60 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.11-1.13, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by adopting a macroporous adsorption resin column, wherein the sample loading amount is 2 column volumes, eluting by using 16-20 vol% low-concentration ethanol, the elution volume is 3-5 column volumes, then eluting by using 95vol% high-concentration ethanol, the elution volume is 2-2.5 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high concentration ethanol solution collected by the resin at low temperature by an MVR evaporator to one fifth of the volume of the solution, discharging, standing the discharged solution in a cold storage for precipitation, controlling the temperature at-3 to-5 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
Wherein, preferably, the macroporous absorption resin column is nonpolar macroporous absorption resin, and comprises one or more of HP20, HPD100, HPD300 and D101 macroporous absorption resin.
Furthermore, the invention also provides application of the mask in preparing skin care products with whitening, spot-lightening and repairing functions.
Compared with the prior art, the invention has the beneficial effects that:
the invention provides a mask product with whitening, spot-lightening and repairing functions, wherein the mask contains an gorgonian extract component, and the gorgonian extract is a natural extract of pseudopterogorgia (also called verbena) and is an antiallergic component which is safe, efficient and environmentally-friendly. Pseudopterogorgia, collected from the 70 feet deep atlantic, in which polar lipid metabolites, pseudopterosin, were shown to be an anti-allergic active ingredient. The invention uses the gorgonia extract, hyaluronic acid, sclerotium rolfsii gum, licorice extract, glycerin, propylene glycol, butanediol and triethanolamine in a matching way, and the dosage of the glycerin, the propylene glycol, the butanediol and the triethanolamine is determined, so that the mask product is finally prepared.
Detailed Description
The invention will be further described with reference to specific embodiments, and the advantages and features of the invention will become apparent as the description proceeds. These examples are illustrative only and do not limit the scope of the present invention in any way. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.
Example 1 preparation of an extract of gorgonian
1) Extraction of
(1) Pulverizing and sieving the raw materials of the gorgonia pseudopterodonta to obtain fine particles of 60 meshes, and extracting the fine particles by using deionized water with the temperature controlled at 55 ℃; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.12, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by using a macroporous adsorption resin column HP20, wherein the sample loading amount is 2 column volumes, eluting by using 20vol% low-concentration ethanol, the elution volume is 4 column volumes, then eluting by using 95vol% high-concentration ethanol, the elution volume is 2 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high-concentration ethanol solution collected by the resin at low temperature by using an MVR evaporator to one fifth of the volume of the feed liquid, discharging, standing the discharged feed liquid in a cold storage for precipitation, controlling the temperature at-4 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
HPLC high performance liquid chromatography detection shows that the content of gorgonian acid is 1% and the content of methyl ester of gorgonian is 2%.
Example 2 preparation of an extract of Pseudopterogorgia elisahethae
1) Extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 50 mesh fine granules, and extracting with deionized water at 60 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.11, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by using a macroporous adsorption resin column D101, wherein the sample loading amount is 2 column volumes, eluting by using 16vol% low-concentration ethanol, the elution volume is 3 column volumes, then eluting by using 95vol% high-concentration ethanol, the elution volume is 2.5 column volumes, and collecting the eluate;
3) concentrating
Concentrating the high-concentration ethanol solution collected by the resin at low temperature by using an MVR evaporator to one fifth of the volume of the feed liquid, discharging, standing the discharged feed liquid in a cold storage for precipitation, controlling the temperature at-3 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
Example 3 preparation of an extract of Elaeagnus angustifolia
1) Extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 70 mesh fine granules, and extracting with deionized water at 55 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.13, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by using a macroporous adsorption resin column HPD300, wherein the sample loading amount is 2 column volumes, eluting by using low-concentration ethanol with the concentration of 20vol% firstly, the elution volume is 5 column volumes, then eluting by using high-concentration ethanol with the concentration of 95vol%, the elution volume is 2 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high-concentration ethanol solution collected by the resin at low temperature by using an MVR evaporator to one fifth of the volume of the feed liquid, discharging, standing the discharged feed liquid in a cold storage for precipitation, controlling the temperature at-5 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
Example 4 preparation of a Pseudopterogorgia elisahethae whitening and speckle-lightening repair mask
The facial mask is prepared from the following raw materials in parts by weight: hyaluronic acid 0.05 parts by weight, sclerotium rolfsii gum 0.3 parts by weight, licorice extract (containing 98wt% dipotassium glycyrrhizinate) 0.3 parts by weight, glycerin 5 parts by weight, propylene glycol 3 parts by weight, butylene glycol 3 parts by weight, pseudopterogorgia elisahethae extract (prepared in example 1) 0.3 parts by weight, triethanolamine 0.05 parts by weight, and water to 100 parts by weight.
The hyaluronic acid contains three kinds of hyaluronic acid with molecular weights, namely macromolecular hyaluronic acid, medium molecular hyaluronic acid and small molecular hyaluronic acid, wherein the weight ratio of the three kinds of hyaluronic acid with molecular weights is 1: 1: 1.
Detecting according to standards such as technical Specification for cosmetic safety (2015 edition), QB/T2872-2017, and bottling after qualification.
Example 5 preparation of a Pseudopterogorgia elisahethae whitening and speckle-lightening repair mask
The facial mask is prepared from the following raw materials in parts by weight: hyaluronic acid 0.1 parts by weight, sclerotium rolfsii gum 0.05 parts by weight, licorice extract (containing 98wt% dipotassium glycyrrhizinate) 0.1 parts by weight, glycerin 10 parts by weight, propylene glycol 5 parts by weight, butylene glycol 1 part by weight, pseudopterogorgia elisahethae extract (prepared in example 2) 0.5 parts by weight, triethanolamine 0.1 parts by weight, and water to 100 parts by weight.
The hyaluronic acid contains three kinds of hyaluronic acid with molecular weights, namely macromolecular hyaluronic acid, medium molecular hyaluronic acid and small molecular hyaluronic acid, wherein the weight ratio of the three kinds of hyaluronic acid with molecular weights is 1: 3: 4.
Detecting according to standards such as technical Specification for cosmetic safety (2015 edition), QB/T2872-2017, and bottling after qualification.
Example 6 preparation of a Pseudopterogorgia elisahethae whitening and speckle-lightening repair mask
The facial mask is prepared from the following raw materials in parts by weight: hyaluronic acid 0.01 parts by weight, sclerotium rolfsii gum 0.5 parts by weight, licorice extract (containing 98wt% dipotassium glycyrrhizinate) 0.5 parts by weight, glycerin 8 parts by weight, propylene glycol 3 parts by weight, butylene glycol 5 parts by weight, pseudopterogorgia elisahethae extract (prepared in example 3) 0.05 parts by weight, triethanolamine 0.08 parts by weight, and water to 100 parts by weight.
The hyaluronic acid contains three kinds of hyaluronic acid with molecular weights, namely macromolecular hyaluronic acid, medium molecular hyaluronic acid and small molecular hyaluronic acid, wherein the weight ratio of the three kinds of hyaluronic acid with molecular weights is 1: 4: 5.
Detecting according to standards such as technical Specification for cosmetic safety (2015 edition), QB/T2872-2017, and bottling after qualification.
Clinical test example 1 evaluation of spot-fading effect of Pseudopterogorgia elisahethae whitening and spot-fading repairing mask
The whitening and spot-lightening efficacy of the coral whitening and spot-lightening repair mask with the specific coral extract content in example 4 was evaluated by selecting 20 persons with different ages and sexes and having basic knowledge of cosmetics, each evaluator was applied twice a day, and the evaluation of each person was summarized after 28 days, wherein the number of spots on the face before the test, and the ratio of the area of the spots on the face after the test to the area before the test were provided for the testers. The results are shown in table 1 below:
TABLE 1 number of spots on face and area change of persons participating in the test
As can be seen from the results of table 1, the mask of the present invention has a significant spot-lightening effect.
Clinical test example 2 evaluation of whitening and speckle-reducing repair efficacy of gorgonian whitening and speckle-reducing repair mask
The whitening and spot-lightening repair efficacy of the coral whitening and spot-lightening repair facial mask (other components of the facial mask are the same as in example 4) with different coral extract contents is evaluated by selecting 20 persons with different ages and sexes and cosmetic basic knowledge, each evaluator is applied twice a day, and the evaluation of each person is summarized after 28 days. The number of persons in each evaluation level is shown in Table 2.
TABLE 2 number of people in each evaluation level
The results in table 2 show that the mask of the present invention has good whitening, spot-lightening and repairing effects, and the whitening, spot-lightening and repairing effects are improved with the increase of the content of the pseudopterogorgia elisabethae extract.
Claims (4)
1. The gorgonia skin-whitening spot-fading repair mask is characterized by comprising the following raw materials in parts by weight:
0.01-0.1 part of hyaluronic acid, 0.01-0.5 part of sclerotium rolfsii gum, 0.01-0.5 part of liquorice extract, 1-10 parts of glycerol, 1-5 parts of propylene glycol, 1-5 parts of butanediol, 0.01-0.5 part of gorgonia pseudopteropilea extract, 0.01-0.1 part of triethanolamine and the balance of water to 100 parts by weight;
the hyaluronic acid contains hyaluronic acid with three molecular weights, namely macromolecular hyaluronic acid, medium molecular hyaluronic acid and small molecular hyaluronic acid, wherein the weight ratio of the hyaluronic acid with the three molecular weights is 1: 1-5: 1-5;
the gorgonia pseudocerana extract is prepared by the following method:
1) extraction of
(1) Pulverizing and sieving herba Salicornia Herbacea raw material to obtain 50-70 mesh fine granules, and extracting with deionized water at 55-60 deg.C; extracting for three times, wherein the ratio of the first material to the liquid is 1: 6, 1 for the second time: 4, third time is 1: 3, 2 hours each time;
(2) after extraction, combining the three filtrates, concentrating at low temperature by using an MVR evaporator to obtain a feed liquid with a specific gravity of 1.11-1.13, and discharging the feed liquid for later use;
2) per resin
Purifying the extracted and concentrated feed liquid by adopting a macroporous adsorption resin column, wherein the sample loading amount is 2 column volumes, eluting by using 16-20 vol% low-concentration ethanol, the elution volume is 3-5 column volumes, then eluting by using 95vol% high-concentration ethanol, the elution volume is 2-2.5 column volumes, and collecting the eluent at this time;
3) concentrating
Concentrating the high concentration ethanol solution collected by the resin at low temperature by an MVR evaporator to one fifth of the volume of the solution, discharging, standing the discharged solution in a cold storage for precipitation, controlling the temperature at-3 to-5 ℃, standing for 8 hours, and filtering;
4) drying
Drying the filtered precipitate in an oven at 50 deg.C for 5 hr to obtain the final product.
2. The mask of claim 1, wherein said licorice extract comprises 98% by weight of dipotassium glycyrrhizinate.
3. The mask pack of claim 1, wherein the macroporous adsorbent resin column is a non-polar macroporous adsorbent resin comprising one or more of HP20, HPD100, HPD300, and D101 macroporous adsorbent resins.
4. Use of the mask pack according to any one of claims 1 to 3 for the preparation of a skin care product having whitening, spot lightening and repairing functions.
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| CN107334691A (en) * | 2017-09-08 | 2017-11-10 | 深圳市仙迪化妆品有限公司 | A kind of whitening cosmetic compound |
| CN108670973A (en) * | 2018-05-07 | 2018-10-19 | 福建中医药大学 | A kind of Chloranthus glaber anti-influenza virus activity extract and preparation method thereof |
| CN109966231A (en) * | 2019-04-11 | 2019-07-05 | 冯江 | A kind of bright face skin beautifying cream and preparation method thereof |
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| CN111053704A (en) * | 2018-10-17 | 2020-04-24 | 东莞市维康医疗投资有限公司 | Earthworm protein and anthocyanin repair beauty mask and preparation method thereof |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107334691A (en) * | 2017-09-08 | 2017-11-10 | 深圳市仙迪化妆品有限公司 | A kind of whitening cosmetic compound |
| CN108670973A (en) * | 2018-05-07 | 2018-10-19 | 福建中医药大学 | A kind of Chloranthus glaber anti-influenza virus activity extract and preparation method thereof |
| CN109966231A (en) * | 2019-04-11 | 2019-07-05 | 冯江 | A kind of bright face skin beautifying cream and preparation method thereof |
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