CN111329894A - Plant mint-flavored oral cavity atomized liquid and preparation method thereof - Google Patents
Plant mint-flavored oral cavity atomized liquid and preparation method thereof Download PDFInfo
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- CN111329894A CN111329894A CN202010360695.XA CN202010360695A CN111329894A CN 111329894 A CN111329894 A CN 111329894A CN 202010360695 A CN202010360695 A CN 202010360695A CN 111329894 A CN111329894 A CN 111329894A
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
- A61K31/047—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates having two or more hydroxy groups, e.g. sorbitol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/44—Oils, fats or waxes according to two or more groups of A61K47/02-A61K47/42; Natural or modified natural oils, fats or waxes, e.g. castor oil, polyethoxylated castor oil, montan wax, lignite, shellac, rosin, beeswax or lanolin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0053—Mouth and digestive tract, i.e. intraoral and peroral administration
- A61K9/006—Oral mucosa, e.g. mucoadhesive forms, sublingual droplets; Buccal patches or films; Buccal sprays
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The invention discloses a plant mint-flavored oral cavity atomized liquid and a preparation method thereof, wherein the plant mint-flavored oral cavity atomized liquid comprises the following components in percentage by mass: water: 50-57%, glycerol: 8-10%, peppermint oil: 10-12%, emulsifier: 3-5% and honeysuckle: 7-9%, menthol: 3-5%, xylitol: 6-7%, eucalyptol: 6 to 9 percent; the preparation method comprises the steps of raw material mixing, filtering and finished product liquid preparation. The mint-flavored oral cavity atomized liquid disclosed by the invention is convenient to accept by people, has more complex content, can stay in the oral cavity for a long time, reduces the spraying times, and is more convenient for people to use.
Description
Technical Field
The invention relates to the technical field of atomized liquid, in particular to plant mint-flavored oral atomized liquid and a preparation method thereof.
Background
Mint is widely used in chewing gum and spray as a raw material for regulating taste in daily life, and the mint-flavored spray can refresh breath, stimulate brain and keep the mind awake.
However, the currently marketed atomized liquid spray has a short stay time in the oral cavity due to its simple internal content, and needs to be frequently sprayed, so we propose a plant mint-flavored oral atomized liquid and a preparation method thereof.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a plant mint-flavored oral cavity atomized liquid and a preparation method thereof.
The invention provides a plant mint-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: water: 50-57%, glycerol: 8-10%, peppermint oil: 10-12%, emulsifier: 3-5% and honeysuckle: 7-9%, menthol: 3-5%, xylitol: 6-7%, eucalyptol: 6 to 9 percent.
Preferably, the composition comprises the following components in percentage by mass: water: 52%, glycerol: 10%, peppermint oil: 10.5%, emulsifier: 3% and honeysuckle: 7%, menthol: 3.5%, xylitol: 6.2%, eucalyptol: 7.8 percent.
The preparation method comprises the following steps:
r1: cleaning raw materials: cleaning the honeysuckle, and then putting the honeysuckle into a drying box for drying.
R2: weighing raw materials: preparing an electronic scale, and weighing raw materials such as water, glycerol, peppermint oil, an emulsifier, honeysuckle, menthol, xylitol and eucalyptol one by one according to a required proportion to ensure the accuracy of the used amount of the raw materials.
R3: preparing raw materials: preparing a mixing barrel and a stirrer, pouring the peppermint oil and the emulsifier into the mixing barrel to obtain stock solution A, and then stirring for a period of time by the stirrer.
R4: mixing raw materials: preparing a boiling pot, firstly adding water, the stock solution A and honeysuckle into the boiling pot, boiling for a period of time by using strong fire to obtain a stock solution B, then putting glycerol, menthol, xylitol and eucalyptol into the stock solution B, and then boiling for a period of time by using slow fire to obtain a stock solution C.
R5: filtering the stock solution: preparing a storage barrel, arranging a filter cloth in the storage barrel, filtering the boiled stock solution C through the filter cloth, and then feeding the stock solution C into the storage barrel to obtain atomized liquid.
R6: preparing a finished product liquid: naturally cooling the atomized liquid for 30-40min, transferring to a refrigerated cabinet, adjusting the temperature in the refrigerated cabinet to 5-10 deg.C, preparing multiple sterilized spray bottles, packaging the atomized liquid in the spray bottles, and storing the packaged spray bottles in shade at 20-30 deg.C.
R6: preparing a finished product liquid: naturally cooling the atomized liquid for 30-40min, transferring to a refrigerated cabinet, adjusting the temperature in the refrigerated cabinet to 5-10 deg.C, preparing multiple sterilized spray bottles, packaging the atomized liquid in the spray bottles, and storing the packaged spray bottles in shade at 20-30 deg.C.
Preferably, in the R2, the electronic scale is BH3-600, and the specification is 600g/0.1 g.
Preferably, in the R3, the stirrer is driven by a motor, and the rotating speed of the motor is adjusted to be 300-500R/min.
Preferably, in the R4, the temperature of strong fire is controlled to be 200-.
Preferably, in the R5, the filtering precision of the filter cloth is 3-5 um.
Discussion of the formulation:
water is used as a neutralizing medium; glycerin is used as a sweetener and can promote the fusion speed among various liquids; the peppermint oil is used for harmonizing peppermint flavor and refreshing; the emulsifier is used for blending the peppermint oil to ensure that the peppermint oil is better blended with water; the honeysuckle has the functions of antibiosis and antiphlogosis, so that the liquid is cleaner; menthol is used to improve the coolness of liquids; xylitol is used for protecting teeth and helping teeth to clean; eucalyptol is used to clean the oral cavity of teeth.
The invention has the beneficial effects that: the plant mint-flavored oral cavity atomized liquid disclosed by the invention is convenient to accept by people in taste, is more complex in content, can stay in an oral cavity for a long time, reduces the spraying times, and is more convenient for people to use.
Detailed Description
The present invention will be further illustrated with reference to the following specific examples.
Example one
The embodiment provides a plant mint-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: water: 50%, glycerin: 8.5%, peppermint oil: 10% of an emulsifier: 4.5% and honeysuckle: 8.5%, menthol: 4.5%, xylitol: 6%, eucalyptol: 8 percent;
the manufacturing method comprises the following steps:
r1: cleaning raw materials: cleaning the honeysuckle, and then putting the honeysuckle into a drying box for drying.
R2: weighing raw materials: preparing an electronic scale, and weighing raw materials such as water, glycerol, peppermint oil, an emulsifier, honeysuckle, menthol, xylitol and eucalyptol one by one according to a required proportion to ensure the accuracy of the used amount of the raw materials.
R3: preparing raw materials: preparing a mixing barrel and a stirrer, pouring the peppermint oil and the emulsifier into the mixing barrel to obtain stock solution A, and then stirring for a period of time by the stirrer.
R4: mixing raw materials: preparing a boiling pot, firstly adding water, the stock solution A and honeysuckle into the boiling pot, boiling for a period of time by using strong fire to obtain a stock solution B, then putting glycerol, menthol, xylitol and eucalyptol into the stock solution B, and then boiling for a period of time by using slow fire to obtain a stock solution C.
R5: filtering the stock solution: preparing a storage barrel, arranging a filter cloth in the storage barrel, filtering the boiled stock solution C through the filter cloth, and then feeding the stock solution C into the storage barrel to obtain atomized liquid.
R6: preparing a finished product liquid: naturally cooling the atomized liquid for 30-40min, transferring to a refrigerated cabinet, adjusting the temperature in the refrigerated cabinet to 5-10 deg.C, preparing multiple sterilized spray bottles, packaging the atomized liquid in the spray bottles, and storing the packaged spray bottles in shade at 20-30 deg.C.
In S2, the model of the electronic scale in R2 is BH3-600, and the specification is 600g/0.1 g; in the R3, the stirrer is driven by a motor, the rotating speed of the motor is adjusted to be 500R/min, and the stirring time is controlled to be 3 min; in the R4, the temperature of strong fire is controlled at 240 ℃, the boiling time of strong fire is controlled at 15min, the temperature of slow fire is controlled at 120 ℃, and the boiling time of slow fire is controlled at 40 min; in the R5, the filtering precision of the filter cloth is 3-5 um.
Example two
The embodiment provides a plant mint-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: water: 51%, glycerin: 8.5%, peppermint oil: 11% and an emulsifier: 4% and honeysuckle: 7%, menthol: 4% and xylitol: 6.5%, eucalyptol: 8 percent;
the manufacturing method comprises the following steps:
r1: cleaning raw materials: cleaning the honeysuckle, and then putting the honeysuckle into a drying box for drying.
R2: weighing raw materials: preparing an electronic scale, and weighing raw materials such as water, glycerol, peppermint oil, an emulsifier, honeysuckle, menthol, xylitol and eucalyptol one by one according to a required proportion to ensure the accuracy of the used amount of the raw materials.
R3: preparing raw materials: preparing a mixing barrel and a stirrer, pouring the peppermint oil and the emulsifier into the mixing barrel to obtain stock solution A, and then stirring for a period of time by the stirrer.
R4: mixing raw materials: preparing a boiling pot, firstly adding water, the stock solution A and honeysuckle into the boiling pot, boiling for a period of time by using strong fire to obtain a stock solution B, then putting glycerol, menthol, xylitol and eucalyptol into the stock solution B, and then boiling for a period of time by using slow fire to obtain a stock solution C.
R5: filtering the stock solution: preparing a storage barrel, arranging a filter cloth in the storage barrel, filtering the boiled stock solution C through the filter cloth, and then feeding the stock solution C into the storage barrel to obtain atomized liquid.
R6: preparing a finished product liquid: naturally cooling the atomized liquid for 30-40min, transferring to a refrigerated cabinet, adjusting the temperature in the refrigerated cabinet to 5-10 deg.C, preparing multiple sterilized spray bottles, packaging the atomized liquid in the spray bottles, and storing the packaged spray bottles in shade at 20-30 deg.C.
In S2, the model of the electronic scale in R2 is BH3-600, and the specification is 600g/0.1 g; in the R3, the stirrer is driven by a motor, the rotating speed of the motor is adjusted to 400R/min, and the stirring time is controlled to 4 min; in the R4, the temperature of strong fire is controlled at 220 ℃, the boiling time of the strong fire is controlled at 18min, the temperature of slow fire is controlled at 130 ℃, and the boiling time of the slow fire is controlled at 35 min; in the R5, the filtering precision of the filter cloth is 3-5 um.
EXAMPLE III
The embodiment provides a plant mint-flavored oral cavity atomized liquid which comprises the following components in percentage by mass: water: 51%, glycerin: 8.5%, peppermint oil: 11% and an emulsifier: 3.5% and honeysuckle: 8%, menthol: 3% and xylitol: 6%, eucalyptol: 9 percent;
the manufacturing method comprises the following steps:
r1: cleaning raw materials: cleaning the honeysuckle, and then putting the honeysuckle into a drying box for drying.
R2: weighing raw materials: preparing an electronic scale, and weighing raw materials such as water, glycerol, peppermint oil, an emulsifier, honeysuckle, menthol, xylitol and eucalyptol one by one according to a required proportion to ensure the accuracy of the used amount of the raw materials.
R3: preparing raw materials: preparing a mixing barrel and a stirrer, pouring the peppermint oil and the emulsifier into the mixing barrel to obtain stock solution A, and then stirring for a period of time by the stirrer.
R4: mixing raw materials: preparing a boiling pot, firstly adding water, the stock solution A and honeysuckle into the boiling pot, boiling for a period of time by using strong fire to obtain a stock solution B, then putting glycerol, menthol, xylitol and eucalyptol into the stock solution B, and then boiling for a period of time by using slow fire to obtain a stock solution C.
R5: filtering the stock solution: preparing a storage barrel, arranging a filter cloth in the storage barrel, filtering the boiled stock solution C through the filter cloth, and then feeding the stock solution C into the storage barrel to obtain atomized liquid.
R6: preparing a finished product liquid: naturally cooling the atomized liquid for 30-40min, transferring to a refrigerated cabinet, adjusting the temperature in the refrigerated cabinet to 5-10 deg.C, preparing multiple sterilized spray bottles, packaging the atomized liquid in the spray bottles, and storing the packaged spray bottles in shade at 20-30 deg.C.
In S2, the model of the electronic scale in R2 is BH3-600, and the specification is 600g/0.1 g; in the R3, the stirrer is driven by a motor, the rotating speed of the motor is adjusted to be 300R/min, and the stirring time is controlled to be 5 min; in the R4, the temperature of strong fire is controlled at 200 ℃, the boiling time of the strong fire is controlled at 20min, the temperature of slow fire is controlled at 120 ℃, and the boiling time of the slow fire is controlled at 40 min; in the R5, the filtering precision of the filter cloth is 3-5 um.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (7)
1. A plant mint-flavored oral cavity atomized liquid is characterized by comprising the following components in percentage by mass: water: 50-57%, glycerol: 8-10%, peppermint oil: 10-12%, emulsifier: 3-5% and honeysuckle: 7-9%, menthol: 3-5%, xylitol: 6-7%, eucalyptol: 6 to 9 percent.
2. The plant mint flavored oral cavity atomized liquid as claimed in claim 1, wherein the plant mint flavored oral cavity atomized liquid comprises the following components in percentage by mass: water: 52%, glycerol: 10%, peppermint oil: 10.5%, emulsifier: 3% and honeysuckle: 7%, menthol: 3.5%, xylitol: 6.2%, eucalyptol: 7.8 percent.
3. A preparation method of plant mint-flavored oral cavity atomized liquid is characterized by comprising the following steps:
r1: cleaning raw materials: cleaning honeysuckle, and then putting the honeysuckle into a drying box for drying;
r2: weighing raw materials: preparing an electronic scale, and weighing raw materials such as water, glycerol, peppermint oil, an emulsifier, honeysuckle, menthol, xylitol and eucalyptol one by one according to a required proportion to ensure the accuracy of the used amount of the raw materials;
r3: preparing raw materials: preparing a mixing barrel and a stirrer, pouring the peppermint oil and the emulsifier into the mixing barrel to obtain a stock solution A, and then stirring for a period of time by the stirrer;
r4: mixing raw materials: preparing a boiling pot, firstly adding water, the stock solution A and honeysuckle into the boiling pot, boiling for a period of time by using strong fire to obtain a stock solution B, then putting glycerol, menthol, xylitol and eucalyptol into the stock solution B, and then boiling for a period of time by using slow fire to obtain a stock solution C;
r5: filtering the stock solution: preparing a storage barrel, arranging a filter cloth in the storage barrel, filtering the boiled stock solution C through the filter cloth, and then feeding the stock solution C into the storage barrel to obtain atomized liquid;
r6: preparing a finished product liquid: naturally cooling the atomized liquid for 30-40min, transferring to a refrigerated cabinet, adjusting the temperature in the refrigerated cabinet to 5-10 deg.C, preparing multiple sterilized spray bottles, packaging the atomized liquid in the spray bottles, and storing the packaged spray bottles in shade at 20-30 deg.C.
4. The method for preparing the plant mint-flavored oral cavity atomized liquid as claimed in claim 3, wherein in R2, an electronic scale is BH3-600, and the specification is 600g/0.1 g.
5. The method as claimed in claim 3, wherein the R3 motor drives the stirrer, the rotation speed of the motor is adjusted to be 500R/min, and the stirring time is controlled to be 3-5 min.
6. The method for preparing the plant mint-flavored oral cavity atomized liquid as claimed in claim 3, wherein in R4, the temperature of strong fire is controlled to be 200-.
7. The method for preparing the plant mint-flavored oral cavity atomized liquid as claimed in claim 3, wherein in R5, the filtration precision of the filter cloth is 3-5 um.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010360695.XA CN111329894A (en) | 2020-04-30 | 2020-04-30 | Plant mint-flavored oral cavity atomized liquid and preparation method thereof |
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| CN202010360695.XA CN111329894A (en) | 2020-04-30 | 2020-04-30 | Plant mint-flavored oral cavity atomized liquid and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104173498A (en) * | 2013-05-24 | 2014-12-03 | 贵州益佰制药股份有限公司 | KEKE spray used for oral cavity cleaning and bacteriostasis and preparation method thereof |
| CN104352367A (en) * | 2014-09-30 | 2015-02-18 | 青岛叁鼎卫生制品有限公司 | Halitosis-proof toothpaste |
| CN105232781A (en) * | 2015-11-05 | 2016-01-13 | 周菊香 | Spray for removing bad breath, and preparation method thereof |
| CN107281038A (en) * | 2017-07-27 | 2017-10-24 | 西南医科大学附属中医医院 | It is a kind of for composition of oral care and preparation method thereof |
-
2020
- 2020-04-30 CN CN202010360695.XA patent/CN111329894A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104173498A (en) * | 2013-05-24 | 2014-12-03 | 贵州益佰制药股份有限公司 | KEKE spray used for oral cavity cleaning and bacteriostasis and preparation method thereof |
| CN104352367A (en) * | 2014-09-30 | 2015-02-18 | 青岛叁鼎卫生制品有限公司 | Halitosis-proof toothpaste |
| CN105232781A (en) * | 2015-11-05 | 2016-01-13 | 周菊香 | Spray for removing bad breath, and preparation method thereof |
| CN107281038A (en) * | 2017-07-27 | 2017-10-24 | 西南医科大学附属中医医院 | It is a kind of for composition of oral care and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 国家食品药品监督管理局执业药师资格认证中心: "《中药学专业知识（一）》", 30 April 2013, 中国医药科技出版社 * |
| 张文富等: "《49种实用化工产品制造技术》", 31 January 2002, 金盾出版社 * |
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Application publication date: 20200626 |