CN102415974A - Rose-water-containing astringent and preparation method thereof - Google Patents
Rose-water-containing astringent and preparation method thereof Download PDFInfo
- Publication number
- CN102415974A CN102415974A CN2011104108647A CN201110410864A CN102415974A CN 102415974 A CN102415974 A CN 102415974A CN 2011104108647 A CN2011104108647 A CN 2011104108647A CN 201110410864 A CN201110410864 A CN 201110410864A CN 102415974 A CN102415974 A CN 102415974A
- Authority
- CN
- China
- Prior art keywords
- astringent
- water
- vitamin
- rose water
- flos rosae
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000008132 rose water Substances 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title abstract description 7
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 35
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims abstract description 34
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims abstract description 17
- 229960000458 allantoin Drugs 0.000 claims abstract description 17
- 150000001413 amino acids Chemical class 0.000 claims abstract description 17
- 238000004821 distillation Methods 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 12
- 241000628997 Flos Species 0.000 claims description 24
- 235000001014 amino acid Nutrition 0.000 claims description 16
- 235000011187 glycerol Nutrition 0.000 claims description 16
- 229940088594 vitamin Drugs 0.000 claims description 16
- 229930003231 vitamin Natural products 0.000 claims description 16
- 235000013343 vitamin Nutrition 0.000 claims description 16
- 239000011782 vitamin Substances 0.000 claims description 16
- 150000003722 vitamin derivatives Chemical class 0.000 claims description 16
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims description 15
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims description 15
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims description 15
- 235000019155 vitamin A Nutrition 0.000 claims description 15
- 239000011719 vitamin A Substances 0.000 claims description 15
- 229940045997 vitamin a Drugs 0.000 claims description 15
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 10
- 238000010025 steaming Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 239000000470 constituent Substances 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 239000011780 sodium chloride Substances 0.000 claims description 5
- 230000003068 static effect Effects 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 4
- 238000012856 packing Methods 0.000 claims description 4
- 241001573881 Corolla Species 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 2
- 241000109329 Rosa xanthina Species 0.000 abstract 6
- 235000004789 Rosa xanthina Nutrition 0.000 abstract 6
- 206010020751 Hypersensitivity Diseases 0.000 abstract 1
- 208000003351 Melanosis Diseases 0.000 abstract 1
- 208000026935 allergic disease Diseases 0.000 abstract 1
- 230000007815 allergy Effects 0.000 abstract 1
- 235000009508 confectionery Nutrition 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 230000003020 moisturizing effect Effects 0.000 abstract 1
- 239000003755 preservative agent Substances 0.000 abstract 1
- 230000002335 preservative effect Effects 0.000 abstract 1
- 230000002087 whitening effect Effects 0.000 abstract 1
- 239000002537 cosmetic Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- 230000036555 skin type Effects 0.000 description 3
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 210000004877 mucosa Anatomy 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000037384 skin absorption Effects 0.000 description 1
- 231100000274 skin absorption Toxicity 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000019640 taste Nutrition 0.000 description 1
Abstract
The invention discloses rose-water-containing astringent and a preparation method thereof. The rose water in the astringent is prepared by distilling roses and water, wherein the weight of water added into the roses is 8 to 10 times the weight of the roses, the distillation speed based on ratio of liquid distilled out per hour to total water weight is 10 to 20 percent, distillation is performed until the liquid distilled out finally is equal to the weight of the roses, and thus, the rose water is obtained. The astringent is added with natural glycerol, allantoin, complex amino acid and other natural components, so the whitening, moisturizing, skin softening, freckle-lightening effects of the astringent are much obvious. The astringent does not contain any materials that may cause allergy to skin, such as alcohol and preservative, retains the sweet, moist, fresh and elegant fragrance of natural roses and provides a new approach for developing and utilizing roses.
Description
Technical field
The present invention relates to a kind of astringent that contains rose water and preparation method thereof, belong to the cosmetics technical field.
Background technology
Improving constantly of Along with people's living standard, the market demand of cosmetics continue to rise, numerous people, and especially the women extremely pays close attention to skin cosmetic, and this just lays a solid foundation for developing rapidly of beauty services industry.Astringent is a kind of cosmetics that receive consumer's favor for a long time deeply, and it can fully replenish the moisture in the skin horny layer, the health that can be used to clean skin, keeps skin.Simultaneously, astringent also has the effect of adjustment ph value, can adjust the pH-value of skin.
But several kinds of primary raw materials of existing commercially available astringent are all from mineral; Like hydro carbons, alcohols etc.; Cooperating raw material is chemical products coloring agent, odorant etc., and these compositions more or less contain the deleterious composition of application on human skin, and life-time service can infiltrate human body through skin; And, can produce harmful effect to people's skin of face mucosa by skin absorption in various degree.How many tastes of skin care item at present mainly deciding by contained natural component; What the skin-protection product of states such as skin-protection product more and more tends to naturalization, and is American-European-Japanese contained natural plants accounts for 80%, but that China market contains the cosmetics of natural plants is less; Especially composition is single; Can not be fit to the various skin type, and numerous astringent contains some skin is had the organic principle of stimulation, for example ethanol etc.
Summary of the invention
The objective of the invention is to overcome the deficiency of present technology; A kind of astringent that contains rose water of suitable different skin type is provided, and its constituent and mass percent are: rose water 93.5%～98.2%, natural glycerin 1%～3%, Vitamin A 0.1%～0.5%, vitamin e 0.1%～0.5%, aminoacids complex 0.5%～2%, allantoin 0.1%～0.5%.
Another purpose of the present invention provides a kind of method for preparing that contains the astringent of rose water, and its concrete operations step is following:
(1) Flos Rosae Rugosae is cleaned, roguing;
(2) in Flos Rosae Rugosae, add the deionized water of 8～10 times of Flos Rosae Rugosae weight; Add the NaCl of water weight 10～20% simultaneously; Mix the back distillation; Distillation speed is 10%～20% of a Total Water for per hour steaming liquid, stops distillation when liquid weight and used Flos Rosae Rugosae are equal in weight to steaming, and promptly gets rose water;
(3) press the mixed proportion of rose water 93.5%～98.2%, natural glycerin 1%～3%, Vitamin A 0.1%～0.5%, vitamin e 0.1%～0.5%, aminoacids complex 0.5%～2%, allantoin 0.1%～0.5%; When rose water is heated to 50～55 ℃; Add allantoin and aminoacids complex, stir, add Vitamin A, vitamin e, natural glycerin when reducing to 25～30 ℃; Stir, promptly get the astringent that contains rose water;
(4) will contain the astringent of rose water, and be positioned over 4 ℃, and be taken out to room temperature after static 48 hours, and filter, packing promptly gets the astringent finished product.
Flos Rosae Rugosae described in the present invention is Damascus Flos Rosae Rugosae, rich colored Flos Rosae Rugosae, Corolla Flos Rosae Rugosae etc.
Compare with the astringent on the existing market, remarkable result of the present invention embodies and is:
1, the key component of astringent is from natural plant, and the Flos Rosae Rugosae quintessence oil that it comprises has calmness, soothes the spirit, effect with all worries set aside, not only level and smooth skin effect, and the clean skin of feeling well, effects such as unobstructed pore.
2, contain multivitamin and plant nutrient ingredient in the rose water that Flos Rosae Rugosae distillation obtains, can replenish the nutrition and the moisture of skin, can regulate the pH-value of skin, and the allantoin in the composite composition has antioxidation, can make skin maintenance moisture; Natural glycerin then has the effect of preserving moisture, and aminoacids complex and vitamin then can provide nutrition and have effects such as antioxidation for skin.
3, being applicable to any skin type, is a kind of novel natural astringent.
The practical implementation method
Through embodiment the present invention is done further explain below, but protection domain of the present invention is not limited to said content.
Embodiment 1: the constituent and the mass percent that originally contain the astringent of rose water are: rose water 93.5%, natural glycerin 3%, Vitamin A 0.5%, vitamin e 0.5%, aminoacids complex 2%, allantoin 0.5%.
During preparation, the fresh Damascus Flos Rosae Rugosae flower of 1kg is cleaned roguing; Add the 8kg deionized water, add 800g NaCl simultaneously, put into boiler and distill, the control distillation speed is 10% of a Total Water for per hour steaming liquid, stops distillation when liquid and used Flos Rosae Rugosae are equal in weight to steaming, and promptly gets rose water; Press the mixed proportion of rose water 93.5%, natural glycerin 3%, Vitamin A 0.5%, vitamin e 0.5%, aminoacids complex 2%, allantoin 0.5% then; When rose water is heated to 50 ℃; Add allantoin and aminoacids complex, stir, add Vitamin A, vitamin e, natural glycerin when reducing to 25 ℃; Stir, promptly get the astringent that contains rose water; The astringent that will contain rose water is positioned over 4 ℃, is taken out to room temperature after static 48 hours, filters, and packing promptly gets the astringent finished product.
Embodiment 2: the constituent and the mass percent that originally contain the astringent of rose water are: rose water 95.4%, natural glycerin 2%, Vitamin A 0.4%, vitamin e 0.4%, aminoacids complex 1.4%, allantoin 0.4%.
During preparation, the fresh Flos Rosae Rugosae of 1kg is cleaned roguing; Add the 10kg deionized water, add 2kg NaCl simultaneously, put into boiler and distill, the control distillation speed is 15% of a Total Water for per hour steaming liquid, stops distillation when liquid and used Flos Rosae Rugosae are equal in weight to steaming, and promptly gets rose water; Press the mixed proportion of rose water 95.4%, natural glycerin 2%, Vitamin A 0.4%, vitamin e 0.4%, aminoacids complex 1.4%, allantoin 0.4% then; When rose water is heated to 55 ℃; Add allantoin and aminoacids complex, stir, add Vitamin A, vitamin e, natural glycerin when reducing to 30 ℃; Stir, promptly get the astringent that contains rose water; The astringent that will contain rose water is positioned over 4 ℃, is taken out to room temperature after static 48 hours, filters, and packing promptly gets the astringent finished product.
Embodiment 3: the constituent and the mass percent that originally contain the astringent of rose water are: rose water 98.2%, natural glycerin 1%, Vitamin A 0.1%, vitamin e 0.1%, aminoacids complex 0.5%, allantoin 0.1%.
During preparation, the fresh Corolla Flos Rosae Rugosae of 1kg is cleaned roguing; Add the 9kg deionized water, add 1350g NaCl simultaneously, put into boiler and distill, the control distillation speed is 15% of a Total Water for per hour steaming liquid, stops distillation when liquid and used Flos Rosae Rugosae are equal in weight to steaming, and promptly gets rose water; Press the mixed proportion of rose water 98.2%, natural glycerin 1%, Vitamin A 0.1%, vitamin e 0.1%, aminoacids complex 0.5%, allantoin 0.1% then; When rose water is heated to 53 ℃; Add allantoin and aminoacids complex, stir, add Vitamin A, vitamin e, natural glycerin when reducing to 27 ℃; Stir, promptly get the astringent that contains rose water; The astringent that will contain rose water is positioned over 4 ℃, is taken out to room temperature after static 48 hours, filters, and divides to install in the 200ml spray bottle, promptly gets the astringent finished product.
Claims (3)
1. an astringent that contains rose water is characterized in that constituent and mass percent are: rose water 93.5%～98.2%, natural glycerin 1%～3%, Vitamin A 0.1%～0.5%, vitamin e 0.1%～0.5%, aminoacids complex 0.5%～2%, allantoin 0.1%～0.5%.
2. the said method for preparing that contains the astringent of rose water of claim 1 is characterized in that carrying out as follows:
(1) Flos Rosae Rugosae is cleaned, roguing;
(2) in Flos Rosae Rugosae, add the deionized water of 8～10 times of Flos Rosae Rugosae weight; Add the NaCl of water weight 10～20% simultaneously; Mix the back distillation; Distillation speed is 10%～20% of a Total Water for per hour steaming liquid, stops distillation when liquid weight and used Flos Rosae Rugosae are equal in weight to steaming, and promptly gets rose water;
(3) press the mixed proportion of rose water 93.5%～98.2%, natural glycerin 1%～3%, Vitamin A 0.1%～0.5%, vitamin e 0.1%～0.5%, aminoacids complex 0.5%～2%, allantoin 0.1%～0.5%; When rose water is heated to 50～55 ℃; Add allantoin and aminoacids complex, stir, add Vitamin A, vitamin e, natural glycerin when reducing to 25～30 ℃; Stir, promptly get the astringent that contains rose water;
(4) will contain the astringent of rose water, and be positioned over 4 ℃, and be taken out to room temperature after static 48 hours, and filter, packing promptly gets the astringent finished product.
3. the method for preparing that contains the astringent of rose water according to claim 1 is characterized in that: Flos Rosae Rugosae is Damascus Flos Rosae Rugosae, rich colored Flos Rosae Rugosae, Corolla Flos Rosae Rugosae.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110410864.7A CN102415974B (en) | 2011-12-12 | 2011-12-12 | Rose-water-containing astringent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110410864.7A CN102415974B (en) | 2011-12-12 | 2011-12-12 | Rose-water-containing astringent and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102415974A true CN102415974A (en) | 2012-04-18 |
| CN102415974B CN102415974B (en) | 2013-07-31 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110410864.7A Expired - Fee Related CN102415974B (en) | 2011-12-12 | 2011-12-12 | Rose-water-containing astringent and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN102415974B (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102940700A (en) * | 2012-12-08 | 2013-02-27 | 昆明戈尔登纯净水有限公司 | Method for preparing rose extracting solution, rose water taking rose extracting solution as active ingredient, and preparation method of rose water |
| CN104069033A (en) * | 2014-06-27 | 2014-10-01 | 宁波御坊堂生物科技有限公司 | High-concentration allantoin homogeneity premix body series product and preparation method thereof |
| CN106726963A (en) * | 2016-12-23 | 2017-05-31 | 云南健牛生物科技有限公司 | A kind of rose moisturizing antibacterial toner and preparation method thereof |
| CN107625691A (en) * | 2017-10-23 | 2018-01-26 | 合肥卡迪尔化妆品有限公司 | Rose wate |
| CN109248132A (en) * | 2018-10-31 | 2019-01-22 | 无锡悦禧玫瑰科技有限公司 | A kind of formula and preparation method thereof of rose essence water |
| CN109602662A (en) * | 2019-01-25 | 2019-04-12 | 无锡悦禧玫瑰科技有限公司 | A kind of preparation method of rose lotion |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1339296A (en) * | 2000-08-17 | 2002-03-13 | 张著浩 | Skin-care rose water |
| DE102005033009A1 (en) * | 2005-02-15 | 2006-09-07 | Szaidel Cosmetic Gmbh | Pharmaceutical, dermatological or cosmetic preparation, useful e.g. sun protective cream and cleansing milk, comprises a part of aqueous phase or water of freshly prepared aqueous plant content |
| JP2008007526A (en) * | 2007-09-28 | 2008-01-17 | Rohto Pharmaceut Co Ltd | External composition |
| CN101518507A (en) * | 2009-03-31 | 2009-09-02 | 四川央金藏药科技有限公司 | Tibetan incense cosmetic daily chemical article and preparation method thereof |
-
2011
- 2011-12-12 CN CN201110410864.7A patent/CN102415974B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1339296A (en) * | 2000-08-17 | 2002-03-13 | 张著浩 | Skin-care rose water |
| DE102005033009A1 (en) * | 2005-02-15 | 2006-09-07 | Szaidel Cosmetic Gmbh | Pharmaceutical, dermatological or cosmetic preparation, useful e.g. sun protective cream and cleansing milk, comprises a part of aqueous phase or water of freshly prepared aqueous plant content |
| JP2008007526A (en) * | 2007-09-28 | 2008-01-17 | Rohto Pharmaceut Co Ltd | External composition |
| CN101518507A (en) * | 2009-03-31 | 2009-09-02 | 四川央金藏药科技有限公司 | Tibetan incense cosmetic daily chemical article and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 方燕玉: "天然活性成分在化妆品中的应用研究", 《中国优秀硕士学位论文全文数据库工程科技I辑》 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102940700A (en) * | 2012-12-08 | 2013-02-27 | 昆明戈尔登纯净水有限公司 | Method for preparing rose extracting solution, rose water taking rose extracting solution as active ingredient, and preparation method of rose water |
| CN104069033A (en) * | 2014-06-27 | 2014-10-01 | 宁波御坊堂生物科技有限公司 | High-concentration allantoin homogeneity premix body series product and preparation method thereof |
| CN106726963A (en) * | 2016-12-23 | 2017-05-31 | 云南健牛生物科技有限公司 | A kind of rose moisturizing antibacterial toner and preparation method thereof |
| CN107625691A (en) * | 2017-10-23 | 2018-01-26 | 合肥卡迪尔化妆品有限公司 | Rose wate |
| CN109248132A (en) * | 2018-10-31 | 2019-01-22 | 无锡悦禧玫瑰科技有限公司 | A kind of formula and preparation method thereof of rose essence water |
| CN109602662A (en) * | 2019-01-25 | 2019-04-12 | 无锡悦禧玫瑰科技有限公司 | A kind of preparation method of rose lotion |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102415974B (en) | 2013-07-31 |
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