CN111302715A - Method for preparing environment-friendly baking-free brick based on cementing material - Google Patents
Method for preparing environment-friendly baking-free brick based on cementing material Download PDFInfo
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- CN111302715A CN111302715A CN202010223481.8A CN202010223481A CN111302715A CN 111302715 A CN111302715 A CN 111302715A CN 202010223481 A CN202010223481 A CN 202010223481A CN 111302715 A CN111302715 A CN 111302715A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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Abstract
The method for preparing the environment-friendly baking-free brick based on the cementing material is characterized in that the environment-friendly baking-free brick is prepared by mixing 85-90 wt% of basic raw materials and 10-15 wt% of the cementing material, wherein the basic raw materials consist of the following raw materials: conglomerate, ceramic waste, magnetite tailings, quartz sand and boric sludge, and the basic raw material composition of the baking-free brick and the raw material composition of the cementing material are limited, so that the manufactured baking-free brick has high strength and strong practicability, and can be widely applied to curbs, roadside stones, square bricks, lawn bricks, auxiliary floor tiles, various types of hole-arranging bricks and the like; the basic raw materials take the conglomerate and the ceramic waste as main raw materials, and the magnetite tailings and the quartz sand as auxiliary raw materials, so that the conglomerate and the quartz sand have high strength, the ceramic waste has high content of silicon dioxide, and the strength of the prepared baking-free brick can be ensured by matching with other components.
Description
Technical Field
The invention belongs to the field of baking-free brick preparation, and particularly relates to a method for preparing an environment-friendly baking-free brick based on a cementing material.
Background
Because China has a large population and few cultivated lands, if bricks and tiles are made by using clay, a large amount of cultivated lands are wasted, and a sintered brick and tile factory destroys the ecological environment balance and wastes a large amount of land coal resources. Meanwhile, the clay baked brick can generate a large amount of carbon dioxide and other harmful flue gas in the baking process.
The baking-free brick is a new type wall material made up by using flyash, cinder, coal gangue, tail slag, chemical slag or natural sand and tidal marsh mud as main raw material and adopting no high-temp. calcination process, and is made up by using reasonable scientific formula and adding coagulator and trace chemical additive according to a certain proportion, and making the grain size, humidity and mixing degree be intensified by reasonable equipment process so as to obtain the optimum plastic state, then making high-pressure compression moulding so as to quickly harden the brick body, and its effect is good. The material has high strength, good durability, standard size, complete appearance and uniform color, has simple and natural appearance, and can be used as a dry wall or any external decoration. Therefore, the brick is a promising updated product for replacing clay bricks. At present, the baking-free brick has good development prospect in China, develops a novel building material taking industrial waste residues and other non-clay as main raw materials, and is an effective way for effectively protecting cultivated land resources and promoting the technical progress of wall material product structure adjustment, industrial optimization and upgrading and dismantling industry. The removal material production is an indispensable industry in the removal industry, meanwhile, the removal industry is related to the aspects of national life, the environment-friendly baking-free brick plays an irreplaceable role in promoting the national modernization construction process, and the huge removal market capacity of the environment-friendly baking-free brick also provides a very wide prospect for the production of the baking-free brick.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a method for preparing an environment-friendly baking-free brick based on a cementing material.
The invention adopts the following technical scheme:
the method for preparing the environment-friendly baking-free brick based on the cementing material is characterized in that the environment-friendly baking-free brick is prepared by mixing 85-90% of basic raw materials and 10-15% of the cementing material in percentage by weight, wherein the basic raw materials consist of the following raw materials in parts by weight: 50-60 parts of conglomerate, 25-30 parts of ceramic waste, 15-18 parts of magnetite tailings, 10-15 parts of quartz sand and 12-18 parts of boric sludge;
the cementing material is composed of the following raw materials in parts by weight: 30-40 parts of cement, 3-4 parts of tartaric acid, 2-3 parts of calcium lignosulfonate, 4-6 parts of silica powder, 2-3 parts of talcum powder and 1-2 parts of paraffin;
the preparation method comprises the following steps:
crushing boron mud, uniformly mixing the crushed boron mud with a cementing material, adding water with the mass twice that of the boron mud, and uniformly stirring to form bottom slurry for later use;
crushing, screening and mixing raw materials except boron mud in the basic raw materials, adding the raw materials into the bottom slurry prepared in the step one, and uniformly stirring to obtain a brick mixture;
step three, placing the brick mixture in an aging warehouse, and aging for 48-52 hours at 40-45 ℃;
conveying the aged brick mixture to a vibration machine for extrusion forming;
and step five, drying and curing for 20-30 days, then sending into a kiln with the kiln temperature of 210-230 ℃, and naturally cooling to room temperature along with the kiln to obtain the environment-friendly baking-free brick.
Further, the chemical composition of the ceramic waste is as follows: SiO 22:66.3-71.4%、Al2O3:8.2-9.8%、CaO:7.6-9.2%、K2O:3.2-4.6%、Na2O:2.3-3.4%、MgO:5.2-6.5%、MnO2:0.7-1.6%。
Further, the drying and maintaining temperature is 25-35 ℃, and water is sprayed once a day.
Further, in the first step, magnetic stirring is adopted for stirring, and the rotating speed of the magnetic stirring is 70-80 r/min.
Further, in the second step, magnetic stirring is adopted for stirring, and the rotating speed of the magnetic stirring is 100-.
Further, in the second step, after the base raw materials except the boric sludge are crushed, the crushed base raw materials are sieved by a 100-mesh and 150-mesh sieve, and then the crushed base raw materials are mixed.
Further, in the fourth step, the pressing pressure of the vibration machine is 35-40 Mpa.
As can be seen from the above description of the present invention, compared with the prior art, the beneficial effects of the present invention are: the invention limits the basic raw material composition of the baking-free brick and the raw material composition of the cementing material, so that the manufactured baking-free brick has high strength and strong practicability, and can be widely applied to curbs, roadside stones, square bricks, lawn bricks, auxiliary floor tiles, various types of row-hole bricks and the like;
the basic raw materials take conglomerate and ceramic waste as main raw materials, and magnetite tailings and quartz sand as auxiliary raw materials, so that the conglomerate and the quartz sand have high strength, the ceramic waste has high content of silicon dioxide, and the strength of the prepared baking-free brick can be ensured by matching with other components;
in the cementing material, cement is used as a curing agent, so that other raw materials can be firmly cemented together, and the strength of the baking-free brick is ensured; the tartaric acid and the calcium lignosulphonate are compounded to ensure that the brick mixture cannot be hardened in the aging process, so that the subsequent working procedures are prevented from being influenced; the silicon micropowder is matched with calcium lignosulphonate, so that the environment-friendly baking-free strength is improved on the premise of playing a role in reducing water; the talcum powder and the paraffin are matched to ensure that the press-formed baking-free brick is beneficial to falling off from a vibration machine;
after being pressed and molded, the baking-free bricks are dried and cured for 20-30 days, and then are sent into a kiln with residual temperature, and are naturally cooled to room temperature along with the kiln, so that the baking-free bricks are dried, the moisture in the centers of the baking-free bricks can be diffused outwards, the water content of the finally fired environment-friendly baking-free bricks is reduced, the strength of the environment-friendly baking-free bricks is ensured, the water content in the centers of the baking-free bricks is continuously reduced in the drying process, the temperature of the kiln is also continuously reduced, the situation that the baking-free bricks are broken due to the fact that the water content is reduced and the temperature is not changed is prevented, the strength of the environment.
Detailed Description
The invention is further described below by means of specific embodiments.
The environment-friendly baking-free brick prepared based on the cementing material is prepared by mixing 85-90% of basic raw materials and 10-15% of the cementing material in percentage by weight.
The base raw material comprises the following raw materials in parts by weight: 50-60 parts of conglomerate, 25-30 parts of ceramic waste, 15-18 parts of magnetite tailings, 10-15 parts of quartz sand and 12-18 parts of boric sludge.
The chemical composition of the ceramic waste is as follows: SiO 22:66.3-71.4%、Al2O3:8.2-9.8%、CaO:7.6-9.2%、K2O:3.2-4.6%、Na2O:2.3-3.4%、MgO:5.2-6.5%、MnO2:0.7-1.6%。
The cementing material is composed of the following raw materials in parts by weight: 30-40 parts of cement, 3-4 parts of tartaric acid, 2-3 parts of calcium lignosulphonate, 4-6 parts of silica powder, 2-3 parts of talcum powder and 1-2 parts of paraffin.
The preparation method comprises the following steps:
crushing boron mud, uniformly mixing the crushed boron mud with a cementing material, adding water with the mass twice that of the boron mud, and uniformly stirring to form bottom slurry for later use;
crushing, screening and mixing raw materials except boron mud in the basic raw materials, adding the raw materials into the bottom slurry prepared in the step one, and uniformly stirring to obtain a brick mixture;
step three, placing the brick mixture in an aging warehouse, and aging for 48-52 hours at 40-45 ℃;
conveying the aged brick mixture to a vibration machine for extrusion forming;
and step five, drying and curing for 20-30 days, then sending into a kiln with the kiln temperature of 210-230 ℃, and naturally cooling to room temperature along with the kiln to obtain the environment-friendly baking-free brick.
Specifically, in the first step, magnetic stirring is adopted, and the rotating speed of the magnetic stirring is 70-80 r/min.
In the second step, magnetic stirring is adopted, and the rotating speed of the magnetic stirring is 100-.
In the second step, the basic raw materials except the boron mud are crushed and then are mixed after being screened by a sieve with 100-150 meshes.
In the fourth step, the pressing pressure of the vibration machine is 35-40 Mpa.
In the fifth step, the temperature for drying and maintenance is 25-35 ℃, and water is sprayed once a day.
Example 1
The environment-friendly baking-free brick prepared based on the cementing material is prepared by mixing 85 weight percent of basic raw materials and 15 weight percent of the cementing material.
The base raw material comprises the following raw materials in parts by weight: 50 parts of conglomerate, 30 parts of ceramic waste, 15 parts of magnetite tailings, 15 parts of quartz sand and 12 parts of boric sludge.
The chemical composition of the ceramic waste is as follows: SiO 22:71.4%、Al2O3:8.2%、CaO:7.6%、K2O:4.6%、Na2O:2.3%、MgO:5.2%、MnO2:0.7%。
The cementing material is composed of the following raw materials in parts by weight: 30 parts of cement, 4 parts of tartaric acid, 2 parts of calcium lignosulphonate, 6 parts of silica powder, 2 parts of talcum powder and 2 parts of paraffin.
The preparation method comprises the following steps:
crushing boron mud, uniformly mixing the crushed boron mud with a cementing material, adding water with the mass twice that of the boron mud, and uniformly stirring to form bottom slurry for later use;
crushing, screening and mixing raw materials except boron mud in the basic raw materials, adding the raw materials into the bottom slurry prepared in the step one, and uniformly stirring to obtain a brick mixture;
step three, placing the brick mixture in an aging warehouse, and aging for 52 hours at 40 ℃;
conveying the aged brick mixture to a vibration machine for extrusion forming;
and step five, drying and curing for 20 days, then sending into a kiln with the kiln temperature of 230 ℃, and naturally cooling to room temperature along with the kiln to obtain the environment-friendly baking-free brick.
Specifically, in the first step, magnetic stirring is adopted, and the rotating speed of the magnetic stirring is 70 r/min.
And in the second step, magnetic stirring is adopted for stirring, and the rotating speed of the magnetic stirring is 120 r/min.
In the second step, the basic raw materials except the boron mud are crushed, sieved by a 100-mesh sieve and mixed.
In the fourth step, the pressing pressure of the vibration machine is 35 MPa.
And step five, drying and maintaining at the temperature of 35 ℃, and spraying water once a day.
Example 2
The environment-friendly baking-free brick prepared based on the cementing material is prepared by mixing 90 weight percent of basic raw materials and 10 weight percent of the cementing material.
The base raw material comprises the following raw materials in parts by weight: 60 parts of conglomerate, 25 parts of ceramic waste, 18 parts of magnetite tailings, 10 parts of quartz sand and 18 parts of boric sludge.
The chemical composition of the ceramic waste is as follows: SiO 22:66.3%、Al2O3:9.8%、CaO:9.2%、K2O:3.2%、Na2O:3.4%、MgO:6.5%、MnO2:1.6%。
The cementing material is composed of the following raw materials in parts by weight: 40 parts of cement, 3 parts of tartaric acid, 3 parts of calcium lignosulphonate, 4 parts of silica micropowder, 3 parts of talcum powder and 1 part of paraffin.
The preparation method comprises the following steps:
crushing boron mud, uniformly mixing the crushed boron mud with a cementing material, adding water with the mass twice that of the boron mud, and uniformly stirring to form bottom slurry for later use;
crushing, screening and mixing raw materials except boron mud in the basic raw materials, adding the raw materials into the bottom slurry prepared in the step one, and uniformly stirring to obtain a brick mixture;
step three, placing the brick mixture in an aging warehouse, and aging for 48 hours at 45 ℃;
conveying the aged brick mixture to a vibration machine for extrusion forming;
and step five, drying and curing for 30 days, then sending into a kiln with the kiln temperature of 210 ℃, and naturally cooling to room temperature along with the kiln to obtain the environment-friendly baking-free brick.
Specifically, in the first step, magnetic stirring is adopted, and the rotating speed of the magnetic stirring is 80 r/min.
And in the second step, magnetic stirring is adopted for stirring, and the rotating speed of the magnetic stirring is 100 r/min.
In the second step, the basic raw materials except the boron mud are crushed, sieved by a 150-mesh sieve and mixed.
In the fourth step, the pressing pressure of the vibration machine is 40 MPa.
And step five, drying and maintaining at 25 ℃, and spraying water once a day.
Example 3
The environment-friendly baking-free brick prepared based on the cementing material is prepared by mixing 88 weight percent of basic raw materials and 12 weight percent of the cementing material.
The base raw material comprises the following raw materials in parts by weight: 55 parts of conglomerate, 27 parts of ceramic waste, 16 parts of magnetite tailings, 12 parts of quartz sand and 15 parts of boric sludge.
The chemical composition of the ceramic waste is as follows: SiO 22:68.8%、Al2O3:9.1%、CaO:8.4%、K2O:3.9%、Na2O:2.7%、MgO:5.8%、MnO2:1.3%。
The cementing material is composed of the following raw materials in parts by weight: 35 parts of cement, 3.5 parts of tartaric acid, 2.5 parts of calcium lignosulphonate, 5 parts of silica micropowder, 2.5 parts of talcum powder and 1.5 parts of paraffin.
The preparation method comprises the following steps:
crushing boron mud, uniformly mixing the crushed boron mud with a cementing material, adding water with the mass twice that of the boron mud, and uniformly stirring to form bottom slurry for later use;
crushing, screening and mixing raw materials except boron mud in the basic raw materials, adding the raw materials into the bottom slurry prepared in the step one, and uniformly stirring to obtain a brick mixture;
step three, placing the brick mixture in an aging warehouse, and aging for 50h at 42 ℃;
conveying the aged brick mixture to a vibration machine for extrusion forming;
and step five, drying and curing for 25 days, then sending into a kiln with the kiln temperature of 220 ℃, and naturally cooling to room temperature along with the kiln to obtain the environment-friendly baking-free brick.
Specifically, in the first step, magnetic stirring is adopted, and the rotating speed of the magnetic stirring is 75 r/min.
And in the second step, magnetic stirring is adopted for stirring, and the rotating speed of the magnetic stirring is 110 r/min.
In the second step, the basic raw materials except the boron mud are crushed, sieved by a 150-mesh sieve and mixed.
In the fourth step, the pressing pressure of the vibration machine is 35 MPa.
And step five, drying and maintaining at the temperature of 30 ℃, and spraying water once a day.
The three examples and the prior baking-free brick are tested to obtain the following performance parameters:
TABLE 1 table of Performance parameters for the examples
The prepared baking-free brick has high strength and strong practicability and can be widely applied to curbs, roadside stones, square bricks, lawn bricks, auxiliary floor tiles, hole-discharging bricks of various models and the like by limiting the basic raw material composition of the baking-free brick and the raw material composition of a cementing material, wherein the basic raw material takes gravels and ceramic waste as main raw materials, takes magnetite tailings and quartz sand as auxiliary raw materials, the gravels and the quartz sand have high strength, the content of silicon dioxide in the ceramic waste is high, and the strength of the prepared baking-free brick can be ensured by matching with other components; in the cementing material, cement is used as a curing agent, so that other raw materials can be firmly cemented together, and the strength of the baking-free brick is ensured; the tartaric acid and the calcium lignosulphonate are compounded to ensure that the brick mixture cannot be hardened in the aging process, so that the subsequent working procedures are prevented from being influenced; the silicon micropowder is matched with calcium lignosulphonate, so that the environment-friendly baking-free strength is improved on the premise of playing a role in reducing water; the talcum powder and the paraffin are matched to ensure that the press-formed baking-free brick is beneficial to falling off from a vibration machine.
After being pressed and molded, the baking-free bricks are dried and cured for 20-30 days, and then are sent into a kiln with residual temperature, and are naturally cooled to room temperature along with the kiln, so that the baking-free bricks are dried, the moisture in the centers of the baking-free bricks can be diffused outwards, the water content of the finally fired environment-friendly baking-free bricks is reduced, the strength of the environment-friendly baking-free bricks is ensured, the water content in the centers of the baking-free bricks is continuously reduced in the drying process, the temperature of the kiln is also continuously reduced, the situation that the baking-free bricks are broken due to the fact that the water content is reduced and the temperature is not changed is prevented, the strength of the environment.
The above description is only a preferred embodiment of the present invention, and therefore should not be taken as limiting the scope of the invention, which is defined by the appended claims and their equivalents and modifications within the scope of the description.
Claims (7)
1. The method for preparing the environment-friendly baking-free brick based on the cementing material is characterized by comprising the following steps of: the environment-friendly baking-free brick is prepared by mixing 85-90% of basic raw materials and 10-15% of cementing materials in percentage by weight, wherein the basic raw materials comprise the following raw materials in parts by weight: 50-60 parts of conglomerate, 25-30 parts of ceramic waste, 15-18 parts of magnetite tailings, 10-15 parts of quartz sand and 12-18 parts of boric sludge;
the cementing material is composed of the following raw materials in parts by weight: 30-40 parts of cement, 3-4 parts of tartaric acid, 2-3 parts of calcium lignosulfonate, 4-6 parts of silica powder, 2-3 parts of talcum powder and 1-2 parts of paraffin;
the preparation method comprises the following steps:
crushing boron mud, uniformly mixing the crushed boron mud with a cementing material, adding water with the mass twice that of the boron mud, and uniformly stirring to form bottom slurry for later use;
crushing, screening and mixing raw materials except boron mud in the basic raw materials, adding the raw materials into the bottom slurry prepared in the step one, and uniformly stirring to obtain a brick mixture;
step three, placing the brick mixture in an aging warehouse, and aging for 48-52 hours at 40-45 ℃;
conveying the aged brick mixture to a vibration machine for extrusion forming;
and step five, drying and curing for 20-30 days, then sending into a kiln with the kiln temperature of 210-230 ℃, and naturally cooling to room temperature along with the kiln to obtain the environment-friendly baking-free brick.
2. The method for preparing environment-friendly baking-free bricks based on the cementing material according to claim 1, which is characterized in that: the chemical composition of the ceramic waste is as follows: SiO 22:66.3-71.4%、Al2O3:8.2-9.8%、CaO:7.6-9.2%、K2O:3.2-4.6%、Na2O:2.3-3.4%、MgO:5.2-6.5%、MnO2:0.7-1.6%。
3. The method for preparing environment-friendly baking-free bricks based on the cementing material according to claim 1, which is characterized in that: the drying and maintaining temperature is 25-35 ℃, and water is sprayed once a day.
4. The method for preparing environment-friendly baking-free bricks based on the cementing material according to claim 1, which is characterized in that: in the first step, magnetic stirring is adopted, and the rotating speed of the magnetic stirring is 70-80 r/min.
5. The method for preparing environment-friendly baking-free bricks based on the cementing material according to claim 1, which is characterized in that: in the second step, magnetic stirring is adopted for stirring, and the rotating speed of the magnetic stirring is 100-.
6. The method for preparing environment-friendly baking-free bricks based on gel materials according to claim 1, characterized in that: in the second step, the basic raw materials except the boric sludge are crushed, and then are mixed after being screened by a sieve with 100-150 meshes.
7. The method for preparing environment-friendly baking-free bricks based on gel materials according to claim 1, characterized in that: in the fourth step, the pressing pressure of the vibration machine is 35-40 Mpa.
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CN117209252A (en) * | 2023-01-10 | 2023-12-12 | 福建省德化县冠鸿陶瓷有限公司 | High-whiteness ceramic blank and firing method thereof |
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