CN111281948A - Preparation method of Baicao antibacterial cream - Google Patents
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- CN111281948A CN111281948A CN202010322173.0A CN202010322173A CN111281948A CN 111281948 A CN111281948 A CN 111281948A CN 202010322173 A CN202010322173 A CN 202010322173A CN 111281948 A CN111281948 A CN 111281948A
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Abstract
The invention discloses a preparation method of Baicao bacteriostatic cream, which comprises the following steps: s1: preparing the following raw materials in parts by weight: 30-40 parts of golden larch bark, 15-30 parts of white stone flower, 20-30 parts of angelica sinensis, 10-20 parts of rhizome of wild ginger, 20-30 parts of black taro, 25-40 parts of glabrous sarcandra herb, 20-30 parts of fructus aurantii, 15-30 parts of herba lespedezae cuneatae, 20-35 parts of salvia miltiorrhiza, 10-25 parts of pink reineckea herb, 5-10 parts of plantain herb, 20-30 parts of astragalus membranaceus, 5-20 parts of tetragonal vine, 15-25 parts of scutellaria baicalensis, 8-12 parts of platycodon grandiflorum, 8-12 parts of philippine violet herb, 8-12 parts of rhizoma acori graminei, 8-12 parts of safflower, 5-15 parts of mint, 25-35 parts of reed rhizome and 20-. The antibacterial paste prepared by taking various traditional Chinese medicinal materials as main preparation raw materials can effectively inhibit and treat diseases of eczema patients, and can play a good inhibiting and treating effect on symptoms such as skin itch, fester, swelling and pain, swelling and stasis and the like, so that the current social demand is met.
Description
Technical Field
The invention relates to the technical field of medical treatment, in particular to a preparation method of Baicao bacteriostatic cream.
Background
Currently, with the continuous development of economic level, the income per capita is continuously improved, the attention degree of people to the health condition is also continuously improved, skin diseases are the most common diseases, wherein eczema is a common disease in skin diseases, the cause of eczema is complex, the eczema is often the result of interaction between internal and external factors, the internal factors are chronic digestive system diseases, mental stress, insomnia, excessive fatigue, emotional changes, endocrine dyscrasia, infection, metabolic disturbance and the like, the external factors are living environment, climate changes, food and the like, the occurrence of eczema can be influenced, the external stimulus is sunlight, cold, dryness, heat, hot water scalding and washing, and various animal skins, plants, cosmetics, soaps, artificial fibers and the like can be induced, and the skin diseases are delayed allergic reactions caused by the complex internal and external factors.
The traditional Chinese medicine is well inherited in China, the traditional Chinese medicine is prepared from medicinal herbs in nature, conditions of patients are conditioned, and then the effect of curing the conditions is achieved.
Disclosure of Invention
The invention aims to solve the problem that the symptoms of the eczema patient cannot be effectively inhibited and treated at present, and provides a preparation method of Baicao antibacterial cream.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of Baicao bacteriostatic paste comprises the following steps:
s1: preparing the following raw materials in parts by weight: 30-40 parts of golden larch bark, 15-30 parts of lithospermum, 20-30 parts of angelica sinensis, 10-20 parts of rhizome of wild ginger, 20-30 parts of taro, 25-40 parts of glabrous sarcandra herb, 20-30 parts of fructus aurantii, 15-30 parts of herba lespedezae cuneatae, 20-35 parts of salvia miltiorrhiza, 10-25 parts of reineckea carnea, 5-10 parts of plantain herb, 20-30 parts of astragalus membranaceus, 5-20 parts of tetragonal vine, 15-25 parts of scutellaria baicalensis, 8-12 parts of platycodon grandiflorum, 8-12 parts of philippine violet herb, 8-12 parts of rhizoma acori graminei, 8-12 parts of safflower, 5-15 parts of mint, 25-35 parts of reed rhizome, 20-30 parts of cinnamon, 8-12 parts of radix angelicae, 3-6 parts of crinis carbonisatus, 5-8 parts of talc, 4-7 parts of sulfur;
s2: washing the surface of golden larch bark, white stone flower, Chinese angelica, rhizome of wild yam, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root, pink reineckea herb, plantain herb, astragalus root, tetragonal vine, scutellaria root, platycodon root, Chinese violet, grassleaf sweelflag rhizome, safflower, mint, reed rhizome, cinnamon, angelica dahurica and talcum sequentially with clean water for 1-3min, after washing, sequentially sucking water drops on the surface of the materials through absorbent paper, placing the materials sucking the water drops at a ventilation opening for ventilation for 10-20 min;
s3: sequentially cutting cortex pseudolaricis, radix Angelicae sinensis, radix Steudnerae Dillenii, herba Pileae Scriptae, fructus Aurantii, herba Lespedezae Cuneatae, Saviae Miltiorrhizae radix, herba Reineckeae Carneae, radix astragali, caulis et folium Gaultheriae Yunnanensis, Scutellariae radix, radix Platycodi, rhizoma Acori Graminei, rhizoma Phragmitis, cortex Cinnamomi, and radix Angelicae Dahuricae to make their diameters all in 3-6 cm; sequentially grinding the lithospermum, the rhizome of wild verbena, the plantain, the Chinese violet, the mint, the crinis carbonisatus, the talc, the sulfur, the borneol and the pearl;
s4: argon gas replacement reaction work is carried out on the reaction kettle, then the chopped golden larch bark, Chinese angelica, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root and dahurian angelica root are sequentially put into the reaction kettle, and purified water is put into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 10: 1, heating the reaction kettle to a temperature of 10-20 ℃, keeping the heating time for 10-30min, heating the reaction kettle to a temperature of 80-120 ℃, keeping the heating time for 60-100min, and filtering liquid residues after heating to obtain a liquid medicine I and a residue I; sequentially putting pink reineckea herb, astragalus, tetragonal vine stem, scutellaria baicalensis, platycodon grandiflorum, rhizoma acori graminei, reed rhizome, cinnamon, crinis carbonisatus, talc, sulfur, borneol and pearl into a reaction kettle, adding purified water into the reaction kettle according to the mass ratio of 8:1, heating the reaction kettle to 10-20 ℃ for 10-20min, heating the reaction kettle to 80-100 ℃ for 50-80min, and filtering liquid residues after heating to obtain a second liquid medicine and a second residue medicine; putting the first medicine residue and the second medicine residue into a reaction kettle, and putting purified water into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 3: 1, heating the reaction kettle to 60-100 ℃, keeping the heating time for 60-80min, and filtering liquid residues after heating to obtain a liquid medicine III and a liquid residue III; mixing and stirring the first liquid medicine, the second liquid medicine and the third liquid medicine by a stirring rod, and filtering the first liquid medicine, the second liquid medicine and the third liquid medicine by filter cloth after the mixing and stirring are finished to obtain a first mixed liquid medicine; sequentially putting the ground lithospermum, the rhizome of wild mountain whip, the plantain, the Chinese violet and the mint into the mixed liquid medicine I, mixing and stirring the materials by a stirring rod, and standing for 10-15 hours; after standing, filtering the mixture through filter cloth to obtain a second mixed liquid medicine;
s5: concentrating the mixed liquid medicine II under reduced pressure, and freeze drying to obtain powdery extract; mixing and stirring the medical vaseline and the powdery extract, wherein the mass ratio of the medical vaseline to the powdery extract is 4:6, and thus obtaining the Baicao antibacterial paste.
Preferably, in S4, the number of times of performing the argon replacement reaction on the reaction kettle is 3-6.
Compared with the prior art, the invention has the beneficial effects that:
the golden larch bark has good insecticidal and antipruritic effects; baishihua is mainly used for treating sore and intractable tinea; radix Angelicae sinensis is used for treating superficial infection, pyocutaneous disease; the rhizome of Mount Shanzhu is mainly used for treating carbuncle and furuncle; the purple yam has the effects of promoting the growth and development of a human body and maintaining physiological functions; the glabrous sarcandra herb has the effects of resisting bacteria and diminishing inflammation, dispelling wind and dredging collaterals; the fructus aurantii has a good treatment effect on the edema; the closing door has the effects of bacteriostasis and blood circulation promotion; the red sage root has the effects of promoting blood circulation, removing blood stasis and relieving itching; the pink reineckea herbs have the effects of dissipating blood stasis and activating blood; the plantain herb has good effect of treating psoriasis; the astragalus has good effects of tonifying qi, strengthening exterior, reducing blood pressure, resisting bacteria, expelling pus and promoting tissue regeneration; the four-vine has good efficacy for treating bacteriostasis and relieving itching; scutellaria can treat carbuncle, swelling and sore; the platycodon root is beneficial to discharging pus; the herba Violae has effects of clearing away heat and toxic materials, cooling blood, and relieving swelling; the grass-leaved sweetflag has good bacteriostatic effect; safflower has the function of treating sore and ulcer swelling and pain; herba Menthae can be used for treating skin rubella pruritus and measles without adequate eruption; rhizoma Phragmitis has lung abscess and pus discharge effects; cinnamon has a good bacteriostatic effect; the angelica has the functions of dispelling diseases, removing dampness, expelling pus, promoting granulation, promoting blood circulation, relieving pain and the like; the crinis carbonisatus has good effect of removing blood stasis; the talcum has obvious effect on treating eczema and miliaria; the sulfur has the effects of sterilizing and relieving itching; borneolum Syntheticum can be used for treating conjunctival congestion, swelling and pain, sore throat, and aphtha; the pearl is suitable for throat rot, mouth and tongue sore, and ulcer for a long time;
in conclusion, the antibacterial cream is reasonable in design, can effectively inhibit and treat the symptoms of eczema patients, can well inhibit and treat symptoms such as skin itch, fester, swelling and pain, swelling and stasis and the like, and further meets the current social requirements.
Detailed Description
The following will clearly and completely describe the technical solutions in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments.
Example 1
A preparation method of Baicao bacteriostatic paste comprises the following steps:
s1: preparing the following raw materials in parts by weight: 30 parts of golden larch bark, 15 parts of white stone flower, 20 parts of Chinese angelica, 10 parts of wild ginger rhizome, 20 parts of combined spicebush root, 25 parts of glabrous sarcandra herb, 20 parts of bitter orange, 15 parts of herba lespedezae cuneatae, 20 parts of salvia miltiorrhiza, 10 parts of reineckea carnea, 5 parts of plantain herb, 20 parts of astragalus, 5 parts of tetragonal vine, 15 parts of baical skullcap root, 8 parts of platycodon root, 8 parts of philippine violet herb, 8 parts of grassleaf sweelflag rhizome, 8 parts of safflower, 5 parts of mint, 25 parts of reed rhizome, 20 parts of cinnamon, 8 parts of angelica root, 3 parts of crinis carbonisatus, 5 parts of talcum, 4 parts of sulfur;
s2: washing the surface of golden larch bark, white stone flower, Chinese angelica, rhizome of wild yam, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root, pink reineckea herb, plantain herb, astragalus root, tetragonal vine, scutellaria root, platycodon root, Chinese violet, grassleaf sweelflag rhizome, safflower, mint, reed rhizome, cinnamon, angelica dahurica and talcum sequentially with clean water for 1min, after washing, sequentially sucking water drops on the surface of the materials through absorbent paper, placing the materials with the sucked water drops at a ventilation opening for ventilation for 10 min;
s3: sequentially cutting cortex pseudolaricis, radix Angelicae sinensis, radix Steudnerae Dillenii, herba Pileae Scriptae, fructus Aurantii, herba Lespedezae Cuneatae, Saviae Miltiorrhizae radix, herba Reineckeae Carneae, radix astragali, caulis et folium Gaultheriae Yunnanensis, Scutellariae radix, radix Platycodi, rhizoma Acori Graminei, rhizoma Phragmitis, cortex Cinnamomi, and radix Angelicae Dahuricae to make their diameters all at 3 cm; sequentially grinding the lithospermum, the rhizome of wild verbena, the plantain, the Chinese violet, the mint, the crinis carbonisatus, the talc, the sulfur, the borneol and the pearl;
s4: argon gas replacement reaction work is carried out on the reaction kettle, then the chopped golden larch bark, Chinese angelica, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root and dahurian angelica root are sequentially put into the reaction kettle, and purified water is put into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 10: 1, heating the reaction kettle to a temperature of 10 ℃ for 10min, heating the reaction kettle to a temperature of 80 ℃ for 60min, and filtering liquid residues to obtain a first liquid medicine and a first residue medicine after heating; sequentially putting pink reineckea herb, astragalus, tetragonal vine stem, scutellaria baicalensis, platycodon grandiflorum, rhizoma acori graminei, reed rhizome, cinnamon, crinis carbonisatus, talc, sulfur, borneol and pearl into a reaction kettle, adding purified water into the reaction kettle, wherein the mass ratio of the purified water to the added materials is 8:1, heating the reaction kettle to enable the temperature to be 10 ℃, keeping the heating time for 10min, then heating the reaction kettle to 80 ℃, keeping the heating time for 50min, and filtering liquid residues after heating to obtain a second liquid medicine and a second residue medicine; putting the first medicine residue and the second medicine residue into a reaction kettle, and putting purified water into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 3: 1, heating the reaction kettle to 60 ℃ for 60min, and filtering liquid residues to obtain a liquid medicine III and a liquid medicine III after heating; mixing and stirring the first liquid medicine, the second liquid medicine and the third liquid medicine by a stirring rod, and filtering the first liquid medicine, the second liquid medicine and the third liquid medicine by filter cloth after the mixing and stirring are finished to obtain a first mixed liquid medicine; sequentially putting the ground lithospermum, the rhizome of wild mountain whip, the plantain, the Chinese violet and the mint into the mixed liquid medicine I, mixing and stirring the mixture by a stirring rod, and standing for 10 hours; after standing, filtering the mixture through filter cloth to obtain a second mixed liquid medicine;
s5: concentrating the mixed liquid medicine II under reduced pressure, and freeze drying to obtain powdery extract; mixing and stirring the medical vaseline and the powdery extract, wherein the mass ratio of the medical vaseline to the powdery extract is 4:6, and thus obtaining the Baicao antibacterial paste.
Example 2
A preparation method of Baicao bacteriostatic paste comprises the following steps:
s1: preparing the following raw materials in parts by weight: 33 parts of golden larch bark, 20 parts of white stone flower, 25 parts of Chinese angelica, 13 parts of wild ginger rhizome, 23 parts of combined spicebush root, 30 parts of glabrous sarcandra herb, 24 parts of bitter orange, 18 parts of lespedeza cuneata, 25 parts of salvia miltiorrhiza, 15 parts of reineckea carnea, 7 parts of plantain herb, 25 parts of astragalus, 10 parts of tetragonal vine, 18 parts of baical skullcap root, 10 parts of platycodon root, 10 parts of philippine violet herb, 10 parts of grassleaf sweelflag rhizome, 9 parts of safflower, 8 parts of mint, 28 parts of reed rhizome, 24 parts of cinnamon, 9 parts of angelica root, 4 parts of crinis carbonisatus, 6 parts of talc, 5 parts of sulfur;
s2: washing the surface of golden larch bark, white stone flower, Chinese angelica, rhizome of wild yam, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root, pink reineckea herb, plantain herb, astragalus root, tetragonal vine, scutellaria root, platycodon root, Chinese violet, grassleaf sweelflag rhizome, safflower, mint, reed rhizome, cinnamon, angelica dahurica and talcum sequentially with clean water for 1.5min, after washing, sequentially sucking water drops on the surface of the materials through absorbent paper, placing the materials sucking the water drops at a ventilation opening for ventilation for 13 min;
s3: sequentially cutting cortex pseudolaricis, radix Angelicae sinensis, radix Steudnerae Dillenii, herba Pileae Scriptae, fructus Aurantii, herba Lespedezae Cuneatae, Saviae Miltiorrhizae radix, herba Reineckeae Carneae, radix astragali, caulis et folium Gaultheriae Yunnanensis, Scutellariae radix, radix Platycodi, rhizoma Acori Graminei, rhizoma Phragmitis, cortex Cinnamomi, and radix Angelicae Dahuricae to make their diameters all at 4 cm; sequentially grinding the lithospermum, the rhizome of wild verbena, the plantain, the Chinese violet, the mint, the crinis carbonisatus, the talc, the sulfur, the borneol and the pearl;
s4: argon gas replacement reaction work is carried out on the reaction kettle, then the chopped golden larch bark, Chinese angelica, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root and dahurian angelica root are sequentially put into the reaction kettle, and purified water is put into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 10: 1, heating the reaction kettle to 12 ℃ for 15min, heating the reaction kettle to 90 ℃ for 70min, and filtering liquid residues to obtain a first liquid medicine and a first residue medicine after heating; sequentially putting pink reineckea herb, astragalus, tetragonal vine stem, scutellaria baicalensis, platycodon grandiflorum, rhizoma acori graminei, reed rhizome, cinnamon, crinis carbonisatus, talc, sulfur, borneol and pearl into a reaction kettle, adding purified water into the reaction kettle, wherein the mass ratio of the purified water to the added materials is 8:1, heating the reaction kettle to ensure that the temperature is 12 ℃, the heating time lasts for 12min, heating the reaction kettle to 85 ℃, the heating time lasts for 60min, and filtering liquid residues after heating to obtain a second liquid medicine and a second residue medicine; putting the first medicine residue and the second medicine residue into a reaction kettle, and putting purified water into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 3: 1, heating the reaction kettle to 70 ℃ for 65min, and filtering liquid residues to obtain a liquid medicine III and a liquid medicine III after heating; mixing and stirring the first liquid medicine, the second liquid medicine and the third liquid medicine by a stirring rod, and filtering the first liquid medicine, the second liquid medicine and the third liquid medicine by filter cloth after the mixing and stirring are finished to obtain a first mixed liquid medicine; sequentially putting the ground lithospermum, the rhizome of wild mountain whip, the plantain, the Chinese violet and the mint into the mixed liquid medicine I, mixing and stirring the mixture by a stirring rod, and standing for 12 hours; after standing, filtering the mixture through filter cloth to obtain a second mixed liquid medicine;
s5: concentrating the mixed liquid medicine II under reduced pressure, and freeze drying to obtain powdery extract; mixing and stirring the medical vaseline and the powdery extract, wherein the mass ratio of the medical vaseline to the powdery extract is 4:6, and thus obtaining the Baicao antibacterial paste.
Example 3
A preparation method of Baicao bacteriostatic paste comprises the following steps:
s1: preparing the following raw materials in parts by weight: 35 parts of golden larch bark, 25 parts of white stone flower, 27 parts of Chinese angelica, 15 parts of wild ginger rhizome, 25 parts of combined spicebush root, 35 parts of glabrous sarcandra herb, 28 parts of bitter orange, 25 parts of herba lespedezae cuneatae, 30 parts of salvia miltiorrhiza, 20 parts of reineckea carnea, 9 parts of plantain herb, 27 parts of astragalus, 15 parts of tetragonal vine, 27 parts of baical skullcap root, 11 parts of platycodon root, 11 parts of philippine violet herb, 11 parts of grassleaf sweelflag rhizome, 10 parts of safflower, 12 parts of mint, 30 parts of reed rhizome, 28 parts of cinnamon, 10 parts of angelica root, 5 parts of crinis carbonisatus, 7 parts of talc, 6 parts of sulfur;
s2: washing the surface of golden larch bark, white stone flower, Chinese angelica, rhizome of wild yam, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root, pink reineckea herb, plantain herb, astragalus root, tetragonal vine, scutellaria root, platycodon root, Chinese violet, grassleaf sweelflag rhizome, safflower, mint, reed rhizome, cinnamon, angelica dahurica and talcum sequentially with clean water for 2min, after washing, sequentially sucking water drops on the surface of the materials through absorbent paper, placing the materials with the sucked water drops at a ventilation opening for ventilation for 15 min;
s3: sequentially cutting cortex pseudolaricis, radix Angelicae sinensis, radix Steudnerae Dillenii, herba Pileae Scriptae, fructus Aurantii, herba Lespedezae Cuneatae, Saviae Miltiorrhizae radix, herba Reineckeae Carneae, radix astragali, caulis et folium Gaultheriae Yunnanensis, Scutellariae radix, radix Platycodi, rhizoma Acori Graminei, rhizoma Phragmitis, cortex Cinnamomi, and radix Angelicae Dahuricae to make their diameters all at 5 cm; sequentially grinding the lithospermum, the rhizome of wild verbena, the plantain, the Chinese violet, the mint, the crinis carbonisatus, the talc, the sulfur, the borneol and the pearl;
s4: argon gas replacement reaction work is carried out on the reaction kettle, then the chopped golden larch bark, Chinese angelica, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root and dahurian angelica root are sequentially put into the reaction kettle, and purified water is put into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 10: 1, heating the reaction kettle to 15 ℃ for 18min, heating the reaction kettle to 100 ℃ for 80min, and filtering liquid residues to obtain a first liquid medicine and a first residue medicine after heating; sequentially putting pink reineckea herb, astragalus, tetragonal vine stem, scutellaria baicalensis, platycodon grandiflorum, rhizoma acori graminei, reed rhizome, cinnamon, crinis carbonisatus, talc, sulfur, borneol and pearl into a reaction kettle, adding purified water into the reaction kettle, wherein the mass ratio of the purified water to the added materials is 8:1, heating the reaction kettle to 15 ℃ for 15min, heating the reaction kettle to 90 ℃ for 70min, and filtering liquid residues after heating to obtain a second liquid medicine and a second residue medicine; putting the first medicine residue and the second medicine residue into a reaction kettle, and putting purified water into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 3: 1, heating the reaction kettle to 80 ℃, keeping the heating time for 75min, and filtering liquid residues after heating to obtain a liquid medicine III and a liquid medicine III; mixing and stirring the first liquid medicine, the second liquid medicine and the third liquid medicine by a stirring rod, and filtering the first liquid medicine, the second liquid medicine and the third liquid medicine by filter cloth after the mixing and stirring are finished to obtain a first mixed liquid medicine; sequentially putting the ground lithospermum, the rhizome of wild mountain whip, the plantain, the Chinese violet and the mint into the mixed liquid medicine I, mixing and stirring the mixture by a stirring rod, and standing for 14 hours; after standing, filtering the mixture through filter cloth to obtain a second mixed liquid medicine;
s5: concentrating the mixed liquid medicine II under reduced pressure, and freeze drying to obtain powdery extract; mixing and stirring the medical vaseline and the powdery extract, wherein the mass ratio of the medical vaseline to the powdery extract is 4:6, and thus obtaining the Baicao antibacterial paste.
Example 4
A preparation method of Baicao bacteriostatic paste comprises the following steps:
s1: preparing the following raw materials in parts by weight: 40 parts of golden larch bark, 30 parts of white stone flower, 30 parts of Chinese angelica, 20 parts of wild ginger rhizome, 30 parts of combined spicebush root, 40 parts of glabrous sarcandra herb, 30 parts of bitter orange, 30 parts of lespedeza cuneata, 35 parts of salvia miltiorrhiza, 25 parts of reineckea carnea, 10 parts of plantain herb, 30 parts of astragalus, 20 parts of tetragonal vine, 25 parts of baical skullcap root, 12 parts of platycodon root, 12 parts of philippine violet herb, 12 parts of grassleaf sweelflag rhizome, 12 parts of safflower, 15 parts of mint, 35 parts of reed rhizome, 30 parts of cinnamon, 12 parts of angelica root, 6 parts of crinis carbonisatus, 8 parts of talc, 7 parts of sulfur;
s2: washing the surface of golden larch bark, white stone flower, Chinese angelica, rhizome of wild yam, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root, pink reineckea herb, plantain herb, astragalus root, tetragonal vine, scutellaria root, platycodon root, Chinese violet, grassleaf sweelflag rhizome, safflower, mint, reed rhizome, cinnamon, angelica dahurica and talcum sequentially with clean water for 3min, after washing, sequentially sucking water drops on the surface of the materials through absorbent paper, placing the materials with the sucked water drops at a ventilation opening for ventilation for 20 min;
s3: sequentially cutting cortex pseudolaricis, radix Angelicae sinensis, radix Steudnerae Dillenii, herba Pileae Scriptae, fructus Aurantii, herba Lespedezae Cuneatae, Saviae Miltiorrhizae radix, herba Reineckeae Carneae, radix astragali, caulis et folium Gaultheriae Yunnanensis, Scutellariae radix, radix Platycodi, rhizoma Acori Graminei, rhizoma Phragmitis, cortex Cinnamomi, and radix Angelicae Dahuricae to make their diameters all at 6 cm; sequentially grinding the lithospermum, the rhizome of wild verbena, the plantain, the Chinese violet, the mint, the crinis carbonisatus, the talc, the sulfur, the borneol and the pearl;
s4: argon gas replacement reaction work is carried out on the reaction kettle, then the chopped golden larch bark, Chinese angelica, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root and dahurian angelica root are sequentially put into the reaction kettle, and purified water is put into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 10: 1, heating the reaction kettle to 20 ℃ for 30min, heating the reaction kettle to 120 ℃ for 100min, and filtering liquid residues to obtain a first liquid medicine and a first residue medicine after heating; sequentially putting pink reineckea herb, astragalus, tetragonal vine stem, scutellaria baicalensis, platycodon grandiflorum, rhizoma acori graminei, reed rhizome, cinnamon, crinis carbonisatus, talc, sulfur, borneol and pearl into a reaction kettle, adding purified water into the reaction kettle, wherein the mass ratio of the purified water to the added materials is 8:1, heating the reaction kettle to enable the temperature to be 20 ℃, keeping the heating time for 20min, then heating the reaction kettle to 100 ℃, keeping the heating time for 80min, and filtering liquid residues after heating to obtain a second liquid medicine and a second residue medicine; putting the first medicine residue and the second medicine residue into a reaction kettle, and putting purified water into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 3: 1, heating the reaction kettle to 100 ℃, keeping the heating time for 80min, and filtering liquid residues after heating to obtain a liquid medicine III and a liquid medicine III; mixing and stirring the first liquid medicine, the second liquid medicine and the third liquid medicine by a stirring rod, and filtering the first liquid medicine, the second liquid medicine and the third liquid medicine by filter cloth after the mixing and stirring are finished to obtain a first mixed liquid medicine; sequentially putting the ground lithospermum, the rhizome of wild mountain whip, the plantain, the Chinese violet and the mint into the mixed liquid medicine I, mixing and stirring the mixture by a stirring rod, and standing for 15 hours; after standing, filtering the mixture through filter cloth to obtain a second mixed liquid medicine;
s5: concentrating the mixed liquid medicine II under reduced pressure, and freeze drying to obtain powdery extract; mixing and stirring the medical vaseline and the powdery extract, wherein the mass ratio of the medical vaseline to the powdery extract is 4:6, and thus obtaining the Baicao antibacterial paste.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (2)
1. A preparation method of Baicao bacteriostatic paste is characterized by comprising the following steps:
s1: preparing the following raw materials in parts by weight: 30-40 parts of golden larch bark, 15-30 parts of lithospermum, 20-30 parts of angelica sinensis, 10-20 parts of rhizome of wild ginger, 20-30 parts of taro, 25-40 parts of glabrous sarcandra herb, 20-30 parts of fructus aurantii, 15-30 parts of herba lespedezae cuneatae, 20-35 parts of salvia miltiorrhiza, 10-25 parts of reineckea carnea, 5-10 parts of plantain herb, 20-30 parts of astragalus membranaceus, 5-20 parts of tetragonal vine, 15-25 parts of scutellaria baicalensis, 8-12 parts of platycodon grandiflorum, 8-12 parts of philippine violet herb, 8-12 parts of rhizoma acori graminei, 8-12 parts of safflower, 5-15 parts of mint, 25-35 parts of reed rhizome, 20-30 parts of cinnamon, 8-12 parts of radix angelicae, 3-6 parts of crinis carbonisatus, 5-8 parts of talc, 4-7 parts of sulfur;
s2: washing the surface of golden larch bark, white stone flower, Chinese angelica, rhizome of wild yam, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root, pink reineckea herb, plantain herb, astragalus root, tetragonal vine, scutellaria root, platycodon root, Chinese violet, grassleaf sweelflag rhizome, safflower, mint, reed rhizome, cinnamon, angelica dahurica and talcum sequentially with clean water for 1-3min, after washing, sequentially sucking water drops on the surface of the materials through absorbent paper, placing the materials sucking the water drops at a ventilation opening for ventilation for 10-20 min;
s3: sequentially cutting cortex pseudolaricis, radix Angelicae sinensis, radix Steudnerae Dillenii, herba Pileae Scriptae, fructus Aurantii, herba Lespedezae Cuneatae, Saviae Miltiorrhizae radix, herba Reineckeae Carneae, radix astragali, caulis et folium Gaultheriae Yunnanensis, Scutellariae radix, radix Platycodi, rhizoma Acori Graminei, rhizoma Phragmitis, cortex Cinnamomi, and radix Angelicae Dahuricae to make their diameters all in 3-6 cm; sequentially grinding the lithospermum, the rhizome of wild verbena, the plantain, the Chinese violet, the mint, the crinis carbonisatus, the talc, the sulfur, the borneol and the pearl;
s4: argon gas replacement reaction work is carried out on the reaction kettle, then the chopped golden larch bark, Chinese angelica, black taro, glabrous sarcandra herb, bitter orange, lespedeza cuneata, red sage root and dahurian angelica root are sequentially put into the reaction kettle, and purified water is put into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 10: 1, heating the reaction kettle to a temperature of 10-20 ℃, keeping the heating time for 10-30min, heating the reaction kettle to a temperature of 80-120 ℃, keeping the heating time for 60-100min, and filtering liquid residues after heating to obtain a liquid medicine I and a residue I; sequentially putting pink reineckea herb, astragalus, tetragonal vine stem, scutellaria baicalensis, platycodon grandiflorum, rhizoma acori graminei, reed rhizome, cinnamon, crinis carbonisatus, talc, sulfur, borneol and pearl into a reaction kettle, adding purified water into the reaction kettle according to the mass ratio of 8:1, heating the reaction kettle to 10-20 ℃ for 10-20min, heating the reaction kettle to 80-100 ℃ for 50-80min, and filtering liquid residues after heating to obtain a second liquid medicine and a second residue medicine; putting the first medicine residue and the second medicine residue into a reaction kettle, and putting purified water into the reaction kettle, wherein the mass ratio of the purified water to the put materials is 3: 1, heating the reaction kettle to 60-100 ℃, keeping the heating time for 60-80min, and filtering liquid residues after heating to obtain a liquid medicine III and a liquid residue III; mixing and stirring the first liquid medicine, the second liquid medicine and the third liquid medicine by a stirring rod, and filtering the first liquid medicine, the second liquid medicine and the third liquid medicine by filter cloth after the mixing and stirring are finished to obtain a first mixed liquid medicine; sequentially putting the ground lithospermum, the rhizome of wild mountain whip, the plantain, the Chinese violet and the mint into the mixed liquid medicine I, mixing and stirring the materials by a stirring rod, and standing for 10-15 hours; after standing, filtering the mixture through filter cloth to obtain a second mixed liquid medicine;
s5: concentrating the mixed liquid medicine II under reduced pressure, and freeze drying to obtain powdery extract; mixing and stirring the medical vaseline and the powdery extract, wherein the mass ratio of the medical vaseline to the powdery extract is 4:6, and thus obtaining the Baicao antibacterial paste.
2. The preparation method of the herbal bacteriostatic paste according to claim 1, wherein in the step S4, the number of argon replacement reaction operations performed on the reaction kettle is 3-6.
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CN111700981A (en) * | 2020-08-06 | 2020-09-25 | 辽宁宝一堂科技发展有限公司 | Preparation method of Baicao antibacterial patch |
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CN111569043A (en) * | 2020-07-08 | 2020-08-25 | 魏峰 | Preparation method of traditional Chinese medicine ointment for removing nevus, wart and color spots |
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