CN111281831B - A full-plant dry facial mask with passion fruit peel as main material and its preparation method - Google Patents
A full-plant dry facial mask with passion fruit peel as main material and its preparation method Download PDFInfo
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- CN111281831B CN111281831B CN202010218118.7A CN202010218118A CN111281831B CN 111281831 B CN111281831 B CN 111281831B CN 202010218118 A CN202010218118 A CN 202010218118A CN 111281831 B CN111281831 B CN 111281831B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention belongs to the field of cosmetics, and discloses a full-vegetable dry facial mask taking passion fruit peel as a main raw material and a preparation method thereof. The preparation method comprises the following steps: taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small pieces with a chopper, and cooking in a cooking pot at 80-100 deg.C for 1-4 h; adding deionized water into the obtained peel residues according to the mass weight ratio of 1g (1-3) mL of the residue liquid, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit pulp, uniformly mixing, filtering the obtained mixed pulp to obtain a membrane casting solution, and standing in a refrigerator to remove bubbles; pouring the defoamed membrane casting solution on a polymer basement membrane or a glass plate for membrane scraping, controlling the membrane scraping thickness to be 50-500 mu m, drying at 50-80 ℃ for 1-10h, and stripping the dry membrane after drying to obtain the all-plant dry facial mask. The obtained facial mask has natural raw materials, good safety and fruit fragrance of passion fruit.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a full-vegetable dry facial mask taking passion fruit peel as a main raw material and a preparation method thereof.
Background
Passion fruit, the scientific name passion flower, is known as passion fruit because it has the fragrance of fruits such as guava, mango, banana and the like. The passion fruit juice has excellent color, fragrance, taste and nutrition, is rich in various beneficial components such as organic acid, nicotinic acid, amino acid, linoleic acid, mineral substances, beta-carotene, lycopene, soluble dietary fiber, alkaloid, flavonoid and the like, has higher health care effect and medicinal value, and is suitable for producing products such as fruit juice, jelly, fruit juice, jam and the like. The passion fruit peel, which is a waste in passion fruit processing, also has a certain nutritive value, and the passion fruit peel contains an active substance SOD, so that oxygen free radicals can be removed, deposition of harmful substances is avoided, and the effects of improving skin and maintaining beauty are achieved; meanwhile, the passion fruit peel contains antioxidant substances, such as carotene, vitamin C and the like, and has the effect of delaying human aging.
The mask is a popular skin care mode at present, is beneficial to the skin to remove products of epidermal cell metabolism and accumulated grease substances, promotes water in the mask to permeate into the horny layer of the skin epidermis, enables the skin to become soft and elastic, and is popular with women. The function, form and material of the face pack are all five-flower eight-door. The common facial mask is usually manufactured in a wet mode, non-woven fabric or elastic facial mask paper is soaked in essence with beauty components, a small package which can be carried about is formed after the package is sealed, the sealed package of the facial mask is torn off when the facial mask is used, and the facial mask which is full of the essence is directly taken out and applied to the face, so that the effects of beauty and maintenance are achieved. However, the wet facial mask is not easy to store, and as the components of the essence are mostly high-nutrient substances, the essence is easy to become a hotbed for breeding bacteria or mold after contacting with facial mask paper, and quality deterioration is easy to occur in each production and transportation link, so that the efficacy of the wet facial mask is affected. Meanwhile, the mask in which the mask paper and the essence are sealed in the same sealing bag has a short shelf life, and is often stored by adding preservatives, and the use of the preservatives is easy to cause safety problems such as allergy, contact dermatitis and the like.
At present, researches on passion fruit peels mainly focus on the extraction of some functional active ingredients, and the passion fruit peels are used for making preserved fruits, preserves, fruit wine and the like, such as: the gazania haichoensis et al extracts essential oil components of the peel of the passion fruit by a steam distillation method in the 'extraction of essential oil from the peel of the passion fruit and analysis of aroma components' (Fujian agricultural science, 2019), collects a sample by a solid phase micro-extraction technology, separates and analyzes the components of the sample by a gas chromatography-mass spectrometry (GCMS) method and a computer library, and identifies the essential oil components of the peel of the passion fruit by combining manual spectrogram analysis. The essential oil is found to contain 263 chemical components; the method comprises the steps of determining the changes of the sugar content, the pH value, the alcoholic strength and the total acid content of passion fruit wine in the fermentation process in the research of the fermentation influence of different dry yeasts on the passion fruit wine (food industry, 2019) by the Xiaochun et al, analyzing the influence of different yeasts on the brewing of the passion fruit wine by combining sensory evaluation, and screening out the optimal active saccharomyces cerevisiae. The above researches mainly focus on the extraction of effective components, and reports on the preparation of the all-plant facial mask by taking passion fruit peel waste as a raw material are few. Chinese patent CN201510974533.4 discloses a method for preparing a passion fruit facial mask, which is prepared by mixing a plurality of components such as passion fruit juice, emblic leafflower fruit juice, spiraea japonica root extract, dried rehmannia root extract, water chestnut starch, distilled water and the like, and has certain effects of nutrition, whitening, tenderization and moisture preservation. Although the above patent relates to the preparation of the passion fruit mask, the added components are more, but the preparation process is too simple and extensive, and the effect is general. Chinese patent CN201910481997.X discloses a preparation method of a peel composite acne-removing facial mask liquid and a facial mask processing method thereof, and a nano fibrous membrane is prepared from various raw materials such as passion fruit according to a traditional Chinese medicine theoretical formula and by combining an electrostatic spinning technology. The nanofiber facial mask has a plurality of components, and whether the function of the passion fruit in the formula is the main function or not is difficult to explain. At present, the dry mask prepared by taking passion fruit as a main raw material is not available.
Disclosure of Invention
In order to overcome the defects that the existing wet mask is easy to decay and deteriorate, added with a preservative, safe and not beneficial to storage and transportation, the invention mainly aims to provide a preparation method of a full-plant dry mask taking passion fruit peel as a main raw material.
The invention also aims to provide a full-plant dry facial mask which is prepared by the preparation method and takes passion fruit peel as a main raw material; the facial mask has no chemical additive, and has no irritation and side effect to skin after long-term use. The passion fruit mask prepared by the invention is fine and smooth in feeling after being smeared, good in absorption effect, rich in active ingredients such as pectin, vitamin C and plant polyphenol, remarkable in whitening and skin tendering effect, and has the effects of nutrition, whitening, tenderization and moisture preservation.
The purpose of the invention is realized by the following technical scheme:
a preparation method of a full-vegetable dry facial mask taking passion fruit peel as a main raw material comprises the following steps: taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with length and width of 5-10 mm and 2-4 mm respectively with a chopper, and steaming in a boiling pan at 80-100 deg.C for 1-4 hr to obtain peel residue; then, adding deionized water into the peel residues according to the mass ratio of 1g (1-3) mL of the residues to the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, and filtering the obtained mixed pulp by using a 60-mesh sieve to obtain a membrane casting solution; standing the casting solution in a refrigerator for 12-24h to remove bubbles; pouring the defoamed membrane casting solution on a high-molecular basement membrane or a glass plate for membrane scraping, controlling the membrane scraping thickness to be 50-500 mu m, drying at 50-80 ℃ for 1-10h, and stripping a dry membrane after drying to obtain the all-plant dry facial mask.
A full plant dry facial mask prepared by the above preparation method is provided.
Compared with the prior art, the invention has the following advantages and effects:
(1) the method takes the passion fruit peel as the raw material to prepare the all-plant dry facial mask, reduces waste, simultaneously utilizes the passion fruit peel to the maximum extent, takes the peel as the main material, takes primary pulp (passion fruit juice, original) as the auxiliary material, and adopts a mild and easily industrialized mode to process so as to prepare the all-plant dry facial mask; the technology about the passion fruit peel searched at present is less, most of the passion fruit peel powder is added, and then the passion fruit peel powder is mixed with a plurality of traditional Chinese medicinal materials or other materials and is only used as one component of the passion fruit powder, the passion fruit powder is not completely prepared by taking the passion fruit as a main material, and the inventor thinks that whether the formula meets the requirement or the theory of traditional Chinese medicine compatibility or not is difficult to explain whether the passion fruit plays a main role or not; the whole passion fruit is taken as a raw material, is natural, does not contain essence or preservative, and has high safety; and at present, related dry facial masks are not related to, and most of the dry facial masks are wet facial masks or facial mask powder.
(2) The invention takes the pure natural passion fruit peel as the main raw material and adds part of passion fruit pulp to prepare the full-vegetable dry facial mask, the raw material is natural, the safety is good, and the full-vegetable dry facial mask has the fruit fragrance of passion fruit;
(3) the raw materials of the dry mask prepared by the invention are all from passion fruits, can be completely degraded, and are environment-friendly and pollution-free;
(4) the all-plant dry facial mask prepared by the invention is free from chemical preservatives, easy to store, light in weight and convenient to carry;
(5) the all-plant dry mask prepared by the invention contains plant polyphenol substances and has an oxidation resistance function;
(6) the all-plant dry facial mask prepared by the invention has good solubility, can be uniformly adhered to the face after being slightly wetted by water, has good fitting property, is convenient to use and has good experience feeling;
(7) the preparation process is simple, and industrial production can be realized through continuous blade coating and drying equipment.
Drawings
FIG. 1 is a photograph of the mask obtained in examples 1, 5, 6 and 7 under a camera, wherein a is a photograph of the mask obtained in example 1 and has a thickness of 50 μm; b is a photograph of the mask obtained in example 5, the mask having a thickness of 200 μm; c is a photograph of the mask obtained in example 6, having a thickness of 300 μm; d is a photograph of the mask obtained in example 7, having a thickness of 400 μm.
Fig. 2 is a microscope photograph of the facial masks obtained in examples 1, 5, 6 and 7, wherein a is a 40-fold magnified image of the facial mask obtained in example 1, b is a 100-fold magnified image of the facial mask obtained in example 1, c is a 40-fold magnified image of the facial mask obtained in example 5, d is a 100-fold magnified image of the facial mask obtained in example 5, e is a 40-fold magnified image of the facial mask obtained in example 6, f is a 100-fold magnified image of the facial mask obtained in example 6, g is a 40-fold magnified image of the facial mask obtained in example 7, and h is a 100-fold magnified image of the facial mask obtained in example 7.
Fig. 3 is a graph showing the results of the hydrophilicity experiments (contact angle after 60 s) of the masks obtained in examples 1, 5, 6 and 7, in which a is the result of the hydrophilicity experiments of the mask obtained in example 1, b is the result of the hydrophilicity experiments of the mask obtained in example 5, c is the result of the hydrophilicity experiments of the mask obtained in example 6, and d is the result of the hydrophilicity experiments of the mask obtained in example 7.
Detailed description of the invention
The invention is further described in the following description with reference to the figures and specific examples, which should not be construed as limiting the invention. Unless otherwise specified, the technical means used in the examples are conventional means well known to those skilled in the art. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Example 1:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 5mm and 2mm respectively by using a chopper, cooking for 2 hours in a cooking pot at 80 ℃, adding deionized water into the obtained peel residues according to the weight ratio of 1g to 1mL of residue liquid after cooking is finished, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain a membrane casting solution, standing the membrane casting solution in a refrigerator for 15h to remove bubbles, pouring the defoamed membrane casting solution on a PE (polyethylene) base membrane for membrane scraping, controlling the thickness of the scraped membrane to be 50 microns, then placing the PE base membrane coated with the membrane casting solution in an electrothermal blowing drying oven for drying at 60 ℃ for 3h, peeling the PE base membrane with a knife after drying to obtain a full-vegetable dry membrane, wherein the thickness of the full-vegetable dry membrane is 50 microns, a picture under a camera is shown as a (40 times magnification) and b (100 times magnification) in fig. 2.
Example 2:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 6 mm and 3 mm respectively by using a chopper, and cooking in a cooking pot at the temperature of 80 ℃ for 2 hours to obtain peel residues; then, adding deionized water into the peel residues according to the mass ratio of 1g to 1mL of the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain a membrane casting solution, standing the membrane casting solution in a refrigerator for 20 hours to remove bubbles, pouring the defoamed membrane casting solution on a glass plate to scrape a membrane, controlling the thickness of the scraped membrane to be 200 mu m, drying at 65 ℃ for 5 hours, and stripping the dry membrane after drying to obtain the all-plant dry facial mask.
Example 3:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 6 mm and 3 mm respectively by a chopper, and steaming in a boiling pan at 80 ℃ for 2h to obtain peel residues. Then, adding deionized water into the peel residues according to the mass ratio of 1g to 1mL of the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain a membrane casting solution, standing the membrane casting solution in a refrigerator for 20 hours to remove bubbles, pouring the defoamed membrane casting solution on a glass plate to scrape a membrane, controlling the thickness of the scraped membrane to be 300 mu m, drying at 65 ℃ for 5 hours, and stripping the dry membrane after drying to obtain the all-plant dry facial mask.
Example 4:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 6 mm and 3 mm respectively by a chopper, and steaming in a boiling pan at 80 ℃ for 2h to obtain peel residues. Then, adding deionized water into the peel residues according to the mass ratio of 1g to 1mL of the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain a membrane casting solution, standing the membrane casting solution in a refrigerator for 20 hours to remove bubbles, pouring the defoamed membrane casting solution on a glass plate to scrape a membrane, controlling the thickness of the scraped membrane to be 400 mu m, drying at 65 ℃ for 5 hours, and stripping the dry membrane after drying to obtain the all-plant dry facial mask.
Example 5:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 10 mm and 4 mm respectively by using a chopper, and steaming in a boiling pan at 75 ℃ for 2h to obtain peel residues. Then, adding deionized water into the peel residues according to the mass ratio of 1g to 2mL of the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain membrane casting solution, standing the membrane casting solution in a refrigerator for 20h to remove bubbles, pouring the defoamed membrane casting solution on a glass plate to scrape a membrane, controlling the thickness of the scraped membrane to be 200 mu m, drying at 60 ℃ for 6.5h, peeling off a dry membrane after drying to obtain a full-plant dry facial mask with the thickness of 200 mu m, wherein a photo under a camera is shown as b in figure 1, and pictures under a microscope are shown as c (40 times magnification) and d (100 times magnification) in figure 2.
Example 6:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 10 mm and 4 mm respectively by using a chopper, and steaming in a boiling pan at 75 ℃ for 2h to obtain peel residues. Then, adding deionized water into the peel residues according to the weight ratio of 1g to 2mL of the residue liquid, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain membrane casting solution, standing the membrane casting solution in a refrigerator for 20h to remove bubbles, pouring the defoamed membrane casting solution on a glass plate to scrape a membrane, controlling the thickness of the scraped membrane to be 300 mu m, drying at 60 ℃ for 6.5h, peeling off a dry membrane after drying to obtain a full-vegetal dry facial mask, wherein the thickness of the full-vegetal dry facial mask is 300 mu m, a photograph under a camera is shown as c in figure 1, and pictures under a microscope are shown as e (40 times magnification) and f (100 times magnification) in figure 2.
Example 7:
taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 10 mm and 4 mm respectively by using a chopper, and steaming in a boiling pan at 75 ℃ for 2h to obtain peel residues. Then, adding deionized water into the peel residues according to the mass ratio of 1g to 2mL of the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp accounting for 20% of the weight of the fruit peel pulp, uniformly mixing, filtering the obtained mixed pulp with a 60-mesh sieve to obtain membrane casting solution, standing the membrane casting solution in a refrigerator for 20h to remove bubbles, pouring the defoamed membrane casting solution on a glass plate to scrape a membrane, controlling the thickness of the scraped membrane to be 400 microns, drying at 60 ℃ for 6.5h, peeling off a dry membrane after drying to obtain a full-vegetal dry facial mask with the thickness of 400 microns, wherein a photo under a camera is shown as d in figure 1, and pictures under a microscope are shown as g (40 times magnification) and h (100 times magnification) in figure 2.
Example 8
The pH value of the casting solution prepared in the above examples 1 to 7 was directly measured by using a pH test paper with reference to the standard QB/T2872-2017. And (3) uniformly stirring the casting solution by using a glass rod, dripping a small amount of solution on pH test paper, immediately comparing the pH test paper with a standard colorimetric card after the pH test paper slightly changes color, and recording the corresponding pH value, wherein the result is shown in table 1.
TABLE 1 pH of the casting solutions
Examples 1 to 4 | Examples 5 to 7 | |
pH value | 5.0 | 5.5 |
Through tests, the method conforms to the relevant regulations in QB/T2872-2017: pH 4.0-8.5
Example 9
The viscosities of the casting solutions prepared in examples 1 to 7 were measured by using a rotational viscometer of type NDJ-1. The casting solution was stirred uniformly with a glass rod, the rotor was immersed in the casting solution at an appropriate speed until the rotor page mark leveled with the page, the switch was turned on, the gear shift button was turned to rotate the rotor in the casting solution, after the rotational viscometer pointer leveled off, the pointer lever was pressed down to read, and the corresponding viscosity number was calculated, with the results shown in table 2.
Calculating the formula: (the formula η ═ k × a, where k is a constant and a is the deflection angle)
TABLE 2 viscosity values of casting solutions
Examples 1 to 4 | Examples 5 to 7 | |
Viscosity number (mPa/s) | 500 | 2100 |
Example 10
The all-vegetable dry facial films prepared in examples 1, 5, 6, 7 were subjected to hydrophilicity test using direct measurement:
the prepared film was laid flat on the stage of the contact angle measuring instrument, flattened, and then 2. mu.l of deionized water was dropped on the surface of the film. The baseline was adjusted to be in line with the surface of the film. The wet spreading state of water on the membrane surface is obtained by the image shooting software of the instrument.
As shown in FIG. 3, it can be seen that the obtained all-plant dry facial mask of the present invention has good hydrophilicity, increased thickness and enhanced hydrophilicity.
Example 11
The solubility of the all-vegetable dry mask was tested by direct measurement:
the time required for the dissolution of the whole plant type dry facial mask (corresponding to examples 1, 5, 6 and 7, respectively) was recorded by adding an appropriate amount of distilled water to each of the whole plant type dry facial masks (50, 200, 300 and 400 μm thick) and gently stirring the mixture with a glass rod at room temperature, and the amount of water consumed for the dissolution of the facial mask was recorded, and the results are shown in table 3.
TABLE 3 time required for dissolution of the Whole plant dry facial film and the amount of water consumed
Thickness of | 50 micron | 200 micron | 300 micron | 400 micron |
Quality (g) | 0.0302 | 0.0395 | 0.0372 | 0.0371 |
Consumption of Water (ml) | 50 | 50 | 50 | 50 |
Time (min) | 21s | 27s | 37s | 42s |
Example 12
2.0ml of the casting solution (the casting solution obtained in example 1) was taken in, 2.0ml of a 0.2mmol/L DPPH solution was added, and the mixture was shaken well and allowed to stand for 30 min. Absorbance at 517nm was then measured by zeroing with absolute ethanol (sample A). Meanwhile, the absorbance at 517nm of a mixture of 2.0ml of the casting solution and 2.0ml of absolute ethanol was measured (control A), and the absorbance at 517nm of a mixture of 2.0ml of DPPH solution and 2.0ml of absolute ethanol was measured (blank A).
Clearance (%) [ 1- (sample a-control)/blank a ] } 100
With phenanthroline-metal iron-H2O2Taking 1.5ml of 5mmol/L phenanthroline solution, adding 2.0ml of phosphate buffer solution with pH of 7.4 and 0.05mol/L, mixing well, adding 1.0ml of 7.5mmol/L FeSO4 solution, mixing well immediately after adding one tube, adding 0.1% H2O21.0ml, and finally, distilled water was added to make up a total volume of 10.0 ml. The reaction solution was incubated at 37 ℃ for 1h, and the absorbance (A damage) was measured at 510 nm. The sample solution is added with 1.0ml of casting solution and then added with H according to the experiment of the method2O2Incubate at 37 ℃ for 1h, and measure absorbance at 510nm (sample A). Undamaged tube without H2O2And casting solution, absorbance at 510nm (A is not damaged).
Clearance (%) ═ 100 [ (a sample-a lesion)/(a non-a lesion) ]
TABLE 4 removal of DPPH and hydroxyl radicals by the casting solutions
DPPH radical scavenging ratio (%) | Clearance of hydroxyl radical (%) | |
Ethanol extract | 79.49 | 81.97 |
Aqueous extracts | 91.62 | 77.33 |
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (2)
1. A preparation method of a full-vegetable dry facial mask taking passion fruit peel as a main raw material is characterized by comprising the following steps: taking passion fruit peel, removing residual seeds and fruit bases, cleaning with deionized water, cutting into small blocks with the length and width of 5-10 mm and 2-4 mm respectively by using a chopper, and steaming for 2 hours in a boiling pan at the temperature of 75-80 ℃ to obtain peel residues; then, adding deionized water into the peel residues according to the mass ratio of 1g (1-3) mL of the residues to the residues, and pulping by using a pulping machine to obtain peel pulp; adding passion fruit raw pulp which accounts for 20 percent of the weight of the fruit peel pulp, uniformly mixing, and filtering the obtained pulp by using a 60-mesh sieve to obtain membrane casting liquid; standing the casting solution in a refrigerator for 12-24h to remove bubbles; pouring the defoamed membrane casting solution on a polymer basement membrane or a glass plate for membrane scraping, controlling the membrane scraping thickness to be 50-500 mu m, drying at 50-80 ℃ for 1-10h, and stripping the dry membrane after drying to obtain the all-plant dry facial mask.
2. A full vegetal dry mask prepared by the preparation method of claim 1.
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Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104592415A (en) * | 2015-01-04 | 2015-05-06 | 砀山海升果胶有限责任公司 | Novel pretreating process of raw materials for producing pectin |
CN105534770A (en) * | 2015-12-18 | 2016-05-04 | 宁波高新区夏远科技有限公司 | A passiflora edulis facial mask and a preparing method thereof |
CN106361633A (en) * | 2016-09-06 | 2017-02-01 | 中国科学院重庆绿色智能技术研究院 | Moisturizing mask prepared from citrus peel pomace and preparation method thereof |
KR20170095486A (en) * | 2016-02-15 | 2017-08-23 | 금오공과대학교 산학협력단 | Mask pack using fruit peels and manufacturing apparatus and method thereof |
CN108514532A (en) * | 2018-04-10 | 2018-09-11 | 广西职业技术学院 | A kind of compound grape skin active skull cap components face mask cream and preparation method thereof |
CN108794651A (en) * | 2018-06-07 | 2018-11-13 | 绍兴文理学院 | The method that pectin is extracted in passion fruit pericarp |
KR101995199B1 (en) * | 2018-08-13 | 2019-07-02 | 김대원 | Manufacturing method of non-aqueous soluble fiber by beechtree cellulose fiber and water-soluble mask pack using the same |
CN110123716A (en) * | 2019-06-04 | 2019-08-16 | 扬州罗素生物技术有限公司 | A kind of preparation method of the compound acne-expelling face pack liquid of pericarp and its method for processing facial mask |
CN110151669A (en) * | 2019-07-02 | 2019-08-23 | 任国旺 | A kind of facial mask and its preparation process |
US20200069565A1 (en) * | 2018-08-10 | 2020-03-05 | Societe De Recherche Cosmetique S.A.R.L. | Cosmetic composition comprising a passionflower extract and edelweiss cells, and uses |
-
2020
- 2020-03-25 CN CN202010218118.7A patent/CN111281831B/en active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104592415A (en) * | 2015-01-04 | 2015-05-06 | 砀山海升果胶有限责任公司 | Novel pretreating process of raw materials for producing pectin |
CN105534770A (en) * | 2015-12-18 | 2016-05-04 | 宁波高新区夏远科技有限公司 | A passiflora edulis facial mask and a preparing method thereof |
KR20170095486A (en) * | 2016-02-15 | 2017-08-23 | 금오공과대학교 산학협력단 | Mask pack using fruit peels and manufacturing apparatus and method thereof |
CN106361633A (en) * | 2016-09-06 | 2017-02-01 | 中国科学院重庆绿色智能技术研究院 | Moisturizing mask prepared from citrus peel pomace and preparation method thereof |
CN108514532A (en) * | 2018-04-10 | 2018-09-11 | 广西职业技术学院 | A kind of compound grape skin active skull cap components face mask cream and preparation method thereof |
CN108794651A (en) * | 2018-06-07 | 2018-11-13 | 绍兴文理学院 | The method that pectin is extracted in passion fruit pericarp |
US20200069565A1 (en) * | 2018-08-10 | 2020-03-05 | Societe De Recherche Cosmetique S.A.R.L. | Cosmetic composition comprising a passionflower extract and edelweiss cells, and uses |
KR101995199B1 (en) * | 2018-08-13 | 2019-07-02 | 김대원 | Manufacturing method of non-aqueous soluble fiber by beechtree cellulose fiber and water-soluble mask pack using the same |
CN110123716A (en) * | 2019-06-04 | 2019-08-16 | 扬州罗素生物技术有限公司 | A kind of preparation method of the compound acne-expelling face pack liquid of pericarp and its method for processing facial mask |
CN110151669A (en) * | 2019-07-02 | 2019-08-23 | 任国旺 | A kind of facial mask and its preparation process |
Non-Patent Citations (2)
Title |
---|
果胶对面膜性能的影响;谭乾开等;《云南化工》;20190531;第46卷(第5期);第79-81页 * |
纤维素基面膜材料的应用进展;胡婷婷等;《纤维素科学与技术》;20181231;第26卷(第4期);第60-67页 * |
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