CN111249201A - Vitamin water powder skin care composition and preparation method thereof - Google Patents
Vitamin water powder skin care composition and preparation method thereof Download PDFInfo
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- CN111249201A CN111249201A CN202010219691.XA CN202010219691A CN111249201A CN 111249201 A CN111249201 A CN 111249201A CN 202010219691 A CN202010219691 A CN 202010219691A CN 111249201 A CN111249201 A CN 111249201A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- General Health & Medical Sciences (AREA)
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- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
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Abstract
The invention discloses a vitamin water powder skin care composition and a preparation method thereof. The vitamin water powder skin care composition comprises the following raw materials: humectant, chelating agent, glyceryl polyether-26, polyglycerol-6, bis-PEG-18 methyl ether dimethylsilane, carnosine, arginine, hydroxyethyl piperazine ethane sulfonic acid, preservative, pH regulator, herba Portulacae extract, Thymus vulgaris extract, vitamin C, and water. According to the invention, the pH value of the essence is maintained between 7.2 and 8.2 through arginine, hydroxyethyl piperazine ethane sulfonic acid and a pH regulator, when the essence is used, after vitamin C is mixed into the essence, the pH value is 3.5 to 4.2, the stability of the vitamin C can be effectively ensured in an acidic environment, and the effects of fading color spots and brightening skin color are achieved through the synergistic effect of the vitamin C, the thyme extract, the purslane extract and other components.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a vitamin water powder skin care composition and a preparation method thereof.
Background
Under the action of tyrosinase, melanin produced by melanocytes is converted into dopa by tyrosinase, and then is produced through a series of complex biochemical processes. Melanocytes are present in the basal layer of the epidermis, and ultraviolet light, pollution, and hormones can initiate melanogenesis, which is the transfer of melanin to the keratinocyte layer by melanosomes. Due to the fact that abnormal melanin in the body is exuberant in secretion and is deposited on the surface of the skin in a large amount, the skin cannot metabolize the abnormal melanin in time to form various color spots, such as color spots, chloasma, freckles, early age spots and the like; due to endocrine dysfunction, poor skin quality, oily skin, dark skin, and color marks and pigmentation left by whelk. With the development of the times, more and more women pursue healthy, uniform and fair skin color. At present, commercially available whitening essence is full of precious, vitamin C with a whitening effect is added into essence of the mask, and the vitamin C permeates into the skin epidermis through the essence to achieve the whitening effect, but the vitamin C in the product is easily oxidized, the pH value of the product also easily influences the stability of the vitamin C, and the activity of the vitamin C is reduced.
Disclosure of Invention
The invention aims to provide a vitamin water powder skin care composition and a preparation method thereof, and aims to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
according to the first aspect, the vitamin water powder skin care composition provided by the invention comprises the following raw materials in percentage by weight: 3.5-8% of a humectant, 0.01-0.02% of a chelating agent, 261.5-2.0% of glyceryl polyether, 60.6-1.0% of polyglycerol, 0.4-1.0% of bis-PEG-18 methyl ether dimethyl silane, 0.5-1.0% of carnosine, 0.2-1.0% of arginine, 0.5-1.0% of hydroxyethyl piperazine ethane sulfonic acid, 0.2-0.6% of a preservative, 0.1-1.0% of a pH regulator, 0.5-1.0% of a purslane extract, 0.5-3.0% of a thyme extract, 8.0-15.0% of vitamin C and the balance of water.
Preferably, the humectant is selected from one or more of glycerin, butylene glycol, propylene glycol, sodium lactate, trehalose, sodium hyaluronate, xanthan gum and 1, 2-hexanediol.
More preferably, the humectant comprises glycerin, butanediol, sodium hyaluronate, xanthan gum and 1, 2-hexanediol, and in the vitamin water powder skin care composition, the addition amount of the glycerin is 2.0-4.0%, the addition amount of the butanediol is 1.0-3.0%, the addition amount of the sodium hyaluronate is 0.01-0.04%, the addition amount of the xanthan gum is 0.08-0.2%, and the addition amount of the 1, 2-hexanediol is 0.5-1.0%.
Preferably, the chelating agent is disodium edetate.
Preferably, the pH adjusting agent is selected from any one or more of citric acid, sodium citrate and potassium citrate.
Preferably, the preservative is selected from one or two of phenoxyethanol and ethylhexyl glycerol.
In a second aspect, the present invention provides a method for preparing a vitamin water powder skin care composition according to the first aspect, comprising the following steps:
(1) adding the humectant, the chelating agent, the glyceryl polyether-26, the polyglycerol-6 and the bis-PEG-18 methyl ether dimethyl silane into a water phase pot, heating to 70-80 ℃, and stirring until the components are completely dissolved;
(2) cooling the mixed material to 40-50 ℃, transferring the cooled mixed material into an emulsifying pot, adding carnosine, arginine, hydroxyethyl piperazine ethanesulfonic acid, a preservative, a pH regulator, a purslane extract and a thyme extract into the emulsifying pot, and stirring and mixing uniformly;
(3) cooling to 30-35 ℃, checking, filtering, discharging, filling into bottles to obtain essence;
(4) filling the vitamin C into a powder bin to obtain powder.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, the pH value of the essence is maintained between 7.2 and 8.2 through arginine, hydroxyethyl piperazine ethane sulfonic acid and a pH regulator, when the essence is used, after vitamin C is mixed into the essence, the pH value is 3.5 to 4.2, and the stability of the vitamin C can be effectively ensured under an acidic environment.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Example 1
In this embodiment, the raw materials are weighed according to the raw material ratios shown in table 1, and the preparation method of the vitamin water powder skin care composition provided in this embodiment includes the following steps:
(1) adding glycerol, butanediol, sodium hyaluronate, xanthan gum, 1, 2-hexanediol, disodium ethylene diamine tetraacetate, glyceryl polyether-26, polyglycerol-6 and bis-PEG-18 methyl ether dimethyl silane into a water phase pot, heating to 70 ℃, and stirring until the materials are completely dissolved;
(2) cooling the mixture to 40 ℃, transferring the mixture into an emulsifying pot, adding carnosine, arginine, hydroxyethyl piperazine ethanesulfonic acid, phenoxyethanol, ethylhexyl glycerin, sodium citrate, a purslane extract and a thyme extract into the emulsifying pot, and stirring and mixing uniformly;
(3) cooling to 30 ℃, carrying out inspection, filtering, discharging, and filling into bottles (the volume is 7.0mL) to obtain essence;
(4) filling the vitamin C into a powder bin to obtain powder.
Example 2
In this embodiment, the raw materials are weighed according to the raw material ratios shown in table 1, and the preparation method of the vitamin water powder skin care composition provided in this embodiment includes the following steps:
(1) adding glycerol, butanediol, sodium hyaluronate, xanthan gum, 1, 2-hexanediol, disodium ethylene diamine tetraacetate, glyceryl polyether-26, polyglycerol-6 and bis-PEG-18 methyl ether dimethyl silane into a water phase pot, heating to 75 ℃, and stirring until the materials are completely dissolved;
(2) cooling the mixture to 45 ℃, transferring the mixture into an emulsifying pot, adding carnosine, arginine, hydroxyethyl piperazine ethanesulfonic acid, phenoxyethanol, ethylhexyl glycerin, sodium citrate, a purslane extract and a thyme extract into the emulsifying pot, and stirring and mixing uniformly;
(3) cooling to 32 ℃, carrying out inspection, filtering, discharging, and filling into bottles (the volume is 10.0mL) to obtain essence;
(4) filling the vitamin C into a powder bin to obtain powder.
Example 3
In this embodiment, the raw materials are weighed according to the raw material ratios shown in table 1, and the preparation method of the vitamin water powder skin care composition provided in this embodiment includes the following steps:
(1) adding glycerol, butanediol, sodium hyaluronate, xanthan gum, 1, 2-hexanediol, disodium ethylene diamine tetraacetate, glyceryl polyether-26, polyglycerol-6 and bis-PEG-18 methyl ether dimethyl silane into a water phase pot, heating to 80 ℃, and stirring until the materials are completely dissolved;
(2) cooling the mixture to 50 ℃, transferring the mixture into an emulsifying pot, adding carnosine, arginine, hydroxyethyl piperazine ethanesulfonic acid, phenoxyethanol, ethylhexyl glycerin, sodium citrate, a purslane extract and a thyme extract into the emulsifying pot, and stirring and mixing uniformly;
(3) cooling to 35 ℃, carrying out inspection, filtering, discharging, and filling into bottles (the volume is 11.0mL) to obtain essence;
(4) filling the vitamin C into a powder bin to obtain powder.
Examples 4 to 5
The raw materials were weighed according to the raw material ratios shown in table 1, and then the finished product was obtained according to the procedure of example 2.
TABLE 1 raw material ratio statistics
Comparative example 1
To further illustrate the beneficial effects of the present invention, this comparative example produced a finished product using a similar manufacturing process as example 2, and differs from example 2 in that: this comparative example did not add purslane extract, but replaced the purslane extract of example 2 with an equal amount of water.
Comparative example 2
To further illustrate the beneficial effects of the present invention, this comparative example produced a finished product using a similar manufacturing process as example 2, and differs from example 2 in that: this comparative example did not add thyme extract but replaced the thyme extract of example 2 with an equal amount of water.
In order to further illustrate the beneficial effects of the invention, the invention also detects the pH value of the essence in the product obtained in the above embodiment, the test result shows that the pH value is 7.2-8.2, the powder (i.e. vitamin C) of each embodiment is respectively mixed into the essence, the pH value test is carried out again, the test result shows that the pH value is 3.5-4.2, and the essence in the range can effectively ensure the stability and activity of the vitamin C. The volume of a packaging bottle of the essence disclosed by the embodiment of the invention is designed to be 7.0-11.0 mL, the essence can be supplied to consumers for 7-15 days, and the activity of vitamin C can be ensured in the short time.
In order to further illustrate the beneficial effects of the present invention, the powders in the products obtained in the examples and the comparative examples are respectively dissolved in the liquid, the sample solution to be tested with the concentration of 1mg/L is prepared by using dimethyl sulfoxide, and then the tyrosinase activity inhibition rate of each sample solution to be tested is tested, and the test results are shown in table 2 below.
Table 2 results of performance testing
To further illustrate the beneficial effects of the present invention, the following tests were also performed on the products obtained in the above examples and comparative examples:
140 female volunteers aged 22-45 years were selected and randomly divided into 7 groups of 20 persons each,
the using method comprises the following steps: vitamin C is mixed into the essence to obtain a skin care composition, the skin care composition is smeared after the face is washed in the morning and evening every day, the skin care composition is continuously used for two weeks, after the test is finished, the whitening improvement degree of each face of a volunteer is investigated and evaluated, the whitening improvement degree is divided into three grades of obvious improvement, effective improvement and ineffective improvement, and the evaluation result is shown in a table 3.
Table 3 results of performance testing
| Group of | Product source | Obviously improve the number of people | Effectively improve the number of people | Number of invalid persons |
| 1 | Example 1 | 15 | 4 | 1 |
| 2 | Example 2 | 19 | 1 | 0 |
| 3 | Example 3 | 18 | 2 | 0 |
| 4 | Example 4 | 16 | 4 | 0 |
| 5 | Example 5 | 16 | 4 | 0 |
| 6 | Comparative example 1 | 5 | 11 | 4 |
| 7 | Comparative example 2 | 8 | 9 | 3 |
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (6)
1. The vitamin water powder skin care composition is characterized by comprising the following raw materials in percentage by weight: 3.5-8% of a humectant, 0.01-0.02% of a chelating agent, 261.5-2.0% of glyceryl polyether, 60.6-1.0% of polyglycerol, 0.4-1.0% of bis-PEG-18 methyl ether dimethyl silane, 0.5-1.0% of carnosine, 0.2-1.0% of arginine, 0.5-1.0% of hydroxyethyl piperazine ethane sulfonic acid, 0.2-0.6% of a preservative, 0.1-1.0% of a pH regulator, 0.5-1.0% of a purslane extract, 0.5-3.0% of a thyme extract, 8.0-15.0% of vitamin C and the balance of water.
2. The vitamin water powder skin care composition as claimed in claim 1, wherein the humectant is one or more selected from glycerin, butylene glycol, propylene glycol, sodium lactate, trehalose, sodium hyaluronate, xanthan gum, and 1, 2-hexanediol.
3. The vitamin water powder skin care composition according to claim 2, wherein the moisturizer comprises glycerin, butanediol, sodium hyaluronate, xanthan gum and 1, 2-hexanediol, and in the vitamin water powder skin care composition, the addition amount of the glycerin is 2.0-4.0%, the addition amount of the butanediol is 1.0-3.0%, the addition amount of the sodium hyaluronate is 0.01-0.04%, the addition amount of the xanthan gum is 0.08-0.2%, and the addition amount of the 1, 2-hexanediol is 0.5-1.0%.
4. The vitamin water powder skin care composition as claimed in claim 1, wherein the pH regulator is selected from any one or more of citric acid, sodium citrate and potassium citrate.
5. The vitamin water powder skin care composition as claimed in claim 1, wherein the preservative is selected from one or two of phenoxyethanol and ethylhexyl glycerin.
6. The preparation method of the vitamin water powder skin care composition according to any one of claims 1 to 5, which is characterized by comprising the following steps:
(1) adding the humectant, the chelating agent, the glyceryl polyether-26, the polyglycerol-6 and the bis-PEG-18 methyl ether dimethyl silane into a water phase pot, heating to 70-80 ℃, and stirring until the components are completely dissolved;
(2) cooling the mixed material to 40-50 ℃, transferring the cooled mixed material into an emulsifying pot, adding carnosine, arginine, hydroxyethyl piperazine ethanesulfonic acid, a preservative, a pH regulator, a purslane extract and a thyme extract into the emulsifying pot, and stirring and mixing uniformly;
(3) cooling to 30-35 ℃, checking, filtering, discharging, filling into bottles to obtain essence;
(4) filling the vitamin C into a powder bin to obtain powder.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010219691.XA CN111249201A (en) | 2020-03-25 | 2020-03-25 | Vitamin water powder skin care composition and preparation method thereof |
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| CN202010219691.XA CN111249201A (en) | 2020-03-25 | 2020-03-25 | Vitamin water powder skin care composition and preparation method thereof |
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| CN109157429A (en) * | 2018-09-20 | 2019-01-08 | 深圳市维琪医药研发有限公司 | A kind of active peptides and tyrosinase inhibitor composition for whitening spot-removing |
| CN110354062A (en) * | 2019-08-17 | 2019-10-22 | 哈尔滨工业大学 | A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative |
| CN110559226A (en) * | 2019-09-12 | 2019-12-13 | 广州雨昕生物技术有限公司 | Whitening lotion and preparation method thereof |
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2020
- 2020-03-25 CN CN202010219691.XA patent/CN111249201A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106109296A (en) * | 2016-06-30 | 2016-11-16 | 彭燕辉 | A kind of moisturizing essence lotion and preparation method thereof |
| CN106580797A (en) * | 2016-12-30 | 2017-04-26 | 广州科盈化妆品有限公司 | Whitening and freckle-removing cream and preparation method thereof |
| CN107898699A (en) * | 2017-12-15 | 2018-04-13 | 广东盛美化妆品有限公司 | A kind of flesh bottom Essence of the Herba Dendrobii extract containing iron sheet and preparation method thereof |
| CN108186457A (en) * | 2018-03-08 | 2018-06-22 | 佛山市汇汾化妆品科技有限公司 | A kind of melanin composite inhibiting |
| CN108514519A (en) * | 2018-05-11 | 2018-09-11 | 珠海伊斯佳科技股份有限公司 | A kind of skin care compositions and methods and its application method of whitening and anti-aging |
| CN109157429A (en) * | 2018-09-20 | 2019-01-08 | 深圳市维琪医药研发有限公司 | A kind of active peptides and tyrosinase inhibitor composition for whitening spot-removing |
| CN110354062A (en) * | 2019-08-17 | 2019-10-22 | 哈尔滨工业大学 | A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative |
| CN110559226A (en) * | 2019-09-12 | 2019-12-13 | 广州雨昕生物技术有限公司 | Whitening lotion and preparation method thereof |
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