CN110354062A - A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative - Google Patents

A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative Download PDF

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Publication number
CN110354062A
CN110354062A CN201910761241.0A CN201910761241A CN110354062A CN 110354062 A CN110354062 A CN 110354062A CN 201910761241 A CN201910761241 A CN 201910761241A CN 110354062 A CN110354062 A CN 110354062A
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parts
extract
powder
tremella
ultramicro
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王振宇
赵梦雅
王玮琛
王佳慧
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Harbin Institute of Technology
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Harbin Institute of Technology
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9771Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
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    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82Preparation or application process involves sonication or ultrasonication

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Abstract

The invention discloses the bitter buckwheat moisturizing sleep masks and preparation method thereof that one kind does not add preservative.The facial mask is prepared by following supplementary material: 10 ~ 30 parts of tartary buckwheat extract, 4 ~ 15 parts of ginkgo biloba p.e, 4 ~ 6 parts of dendrobium candidum extract, purslane extract 3 ~ 5, Leonurus extract 2 ~ 5, tremella Ultramicro-powder are homogenized 20 ~ 27 parts, 2 ~ 6 parts of collagen, 3 ~ 5 parts of pearl powder, 0.05 ~ 0.15 part of soluble perfume, 18 ~ 50 parts of deionized water.It is characteristic of the invention that utilizing the antibacterial, anti-oxidant, anti-inflammatory of natural plant active component, promotion capillary blood circulation, reduction melanin accumulation and other effects preparation moisturizing sleep mask, this facial mask does not add chemical preservative, Skin Cell will not be damaged, and has good moistening effect.

Description

A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative
Technical field
The present invention relates to dermocosmesis field, more particularly to a kind of bitter buckwheat moisturizing sleep mask for not adding preservative and its Preparation method.
Background technique
For Mrs man to like to be beautiful, facial mask increasingly becomes the necessity of life, in order to meet this consumer market demand, There is all kinds of whitenings, moisturizing, crease-resistant, freckle-removing mask.In order to facilitate preservation, most of facial masks can add chemical preservative, and The long-time service of these preservatives can stimulate skin, and skin disease is also resulted in when serious.Therefore, it is extracted from natural plants antibacterial The production that ingredient is applied to facial mask can mitigate the injury of chemical preservative, and natural plant essence facial mask will become following development Trend.
Summary of the invention
Present invention aim to address addition damage problems caused by skin of preservative in the sold facial mask in market, provide A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative.
The purpose of the present invention is what is be achieved through the following technical solutions:
A kind of bitter buckwheat moisturizing sleep mask for not adding preservative, is made of the raw material of following mass fraction:
A kind of bitter buckwheat moisturizing sleep mask for not adding preservative, according to mass percent by 10 ~ 30 parts of tartary buckwheat extract, ginkgo 4 ~ 15 parts of leaf extract, 4 ~ 6 parts of dendrobium candidum extract, purslane extract 3 ~ 5, Leonurus extract 2 ~ 5, tremella Ultramicro-powder 20 ~ 27 parts of homogenate, 2 ~ 6 parts of collagen, 3 ~ 5 parts of pearl powder, 0.05 ~ 0.15 part of soluble perfume, 18 ~ 50 parts of deionized water Ratio weighs pretreated supplementary material, obtains inventory.
A kind of bitter buckwheat moisturizing sleep mask for not adding preservative, its step are as follows:
One, weigh a certain amount of raw material, proceed as follows respectively: raw material → pretreatment → extraction → concentration, specific requirement is such as Under:
(1) raw material is chosen: picking out full grains bitter buckwheat seed, the ginkgo leaf of fresh no insect pest, high-quality dendrobium candidum, dent Amaranth, motherwort and tremella are spare;
(2) pre-process: 40 DEG C of thermostatic drying chamber drying pulverize, cross 80 meshes;
(3) tartary buckwheat extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating are low to moisture content Until 10%, whole process is aseptically operated;
(4) ginkgo biloba p.e: ginko leaves flavone class compound is extracted using ultrasonic wave counter-current extraction techniques, 70% ethyl alcohol is expected Liquor ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content are lower than 10% Only, whole process aseptically operates;
(5) dendrobium candidum extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture contain Until amount is lower than 10%, whole process is aseptically operated;
(6) purslane extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
(7) Leonurus extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
(8) tremella Ultramicro-powder is homogenized:
1) tremella Ultramicro-powder is placed in stirring-type saucepan, and setting temperature is 40 ~ 50 DEG C, impregnates 3 ~ 4h, heats the 20min that precooks later;
2) by spiral propeller by tremella material be delivered to three-dimensional ultrasonography assist high speed beating equipment, ultrasonic power 500 ~ 1000W, 15 ~ 30min of time, 10000 ~ 25000r/min of revolving speed obtain the homogenate of tremella Ultramicro-powder;
Two, homogeneous: tartary buckwheat extract, ginkgo biloba p.e, dendrobium candidum extract, purslane extract, motherwort are extracted Object, the homogenate of tremella Ultramicro-powder and other auxiliary material stirring at normal temperature it is uniform after, be put into high pressure homogenizer homogenate and obtain facial mask lotion.
The present invention selects bitter buckwheat to be subject to ginkgo biloba p.e, dendrobium candidum extract, purslane extract, benefit again for raw material A moisturizing sleep surface for not adding preservative obtained after Brittle Falsepimpernel Herb extract, the homogenate of tremella Ultramicro-powder and other auxiliary material homogeneous Film, the invention has the benefit that
1, bitter buckwheat: bitter buckwheat is a kind of crops of dual-purpose of drug and food, nutritional ingredient rich in, such as resistant starch, vitamin, class Carrotene and minerals, 8 kinds of required amino of the good protein and needed by human body that biological value is high, amino acid composition is balanced Acid.There are also polyphenol, flavonoids, phytosterol, sugar alcohol and d-chiro-inositol isoreactivity ingredients.Bitter buckwheat flavone have it is good it is antibacterial, Anti-oxidation efficacy, melanin deposition can be effectively reduced by adding bitter buckwheat flavone in cosmetics, play the effect of whitening.
2, ginkgo leaf: the flavone compound in ginkgo biloba p.e can promote the blood circulation of capillary, also Superoxide dismutase activity, removes the peroxide and free radical of skin surface, keeps skin moisturizing glossy, reduce melanin It is formed, delay skin aging.Ginkgo leaf alcohol extracting has stronger bacteriostasis, to Escherichia coli, staphylococcus aureus, verdigris Pseudomonad, saccharomyces cerevisiae, aspergillus oryzae etc. show strong bacteriostasis, are the natural bacteriostatic agent and preservative of cosmetics.
3, dendrobium candidum: polysaccharide, flavonoids, phenolic substances, amino acid and vitamin C in dendrobium candidum have good Skin care effect.Dendrobium officinale polysaccharide has very high free radical scavenging ability and metal chelating activity;Flavones and phenolic substances, dimension life Plain C is even more natural recognised by people, removes free radical, reduces the generation of wrinkle, enhances skin elasticity, is able to suppress Tyrosinase activity prevents melanin production and desalinates generated melanin, while can reduce the cell damage of ultraviolet induction Evil, has good maintenance and repair ability to skin.Aspartic acid, glutamic acid, glycine, valine and leucine are iron sheet stone The primary amino acid of dry measure used in former times accounts for about the 53% of total amino acid, there is good moisture-keeping function.
4, purslane: for Portulacaceae annual herb plant, main component has alkaloids, flavonoids, polysaccharide, three There is clearing heat and detoxicating, scattered blood to disappear for terpene alcohols, organic acid, catecholamines, vitamins, microelement and inorganic salts etc. It is swollen, antibacterial anti-inflammatory, the multiple efficacies such as anti-oxidant.In addition, a large amount of whitening compositions such as vitamin E abundant, vitamin C in purslane The activity of tyrosinase can be inhibited to prevent the generation of melanin, be a kind of preferable antibacterial, whitening and anti-aging, anti-inflammatory, anti- Quick cosmetic material.
5, motherwort: original name motherwort has the function such as radiation protection, anti-oxidant, whitening, antibacterial first recorded in Shennong's Herbal Effect, in recent years in cosmetic field using more.It is primarily due in motherwort containing there are many amino acid, protein, lipid and dimensions The ingredients such as raw element, can moisten skin nutrition, improve skin microcirculation, can also inhibit tyrosinase activity thin with B-16 melanoma The proliferation of born of the same parents, eliminates that face is black, face spot;Leonurine contained by motherwort, stachydrine, lauric acid and oleic acid etc. can promote skin Metabolism;Alkaloid in motherwort has bacteriostasis well;Rutin in motherwort, has ultraviolet light and X-ray Extremely strong absorption.
6, tremella: tremella is dual-purpose of drug and food fungi, is strengthening by means of tonics, the good medicine strengthened the body resistance to consolidate the constitution.Main active is silver Fungus polysaccharides are divided into acid heteroglycan, acid oligosaccharides and neutral heteropolysaccharide., have anti-oxidant, antitumor, anti-aging, reducing blood lipid, The effects of hypoglycemic, immunological regulation.Tremella polysaccharides have excellent moisture-keeping efficacy, can improve dermatoglyph degree, and it is thick to reduce skin Rugosity increases skin elasticity, can be used as functional component additive application in cosmetics.
The features of the present invention:
(1) supplementary material of product of the present invention derives from natural plants, and obtained facial mask is edible, to the non-stimulated work of skin With.
(2) present invention is to be subject to ginkgo leaf, iron sheet again as raw material using the bitter buckwheat flavone extract with antibacterial anti-corrosion effect Dendrobium nobile, purslane, motherwort neutraceutical active ingredients, tremella Ultramicro-powder homogenate and other auxiliary materials, by high-pressure homogeneous manufactured A bitter buckwheat moisturizing sleep mask for not adding preservative.
(3) tremella Ultramicro-powder precook by immersion-stirring-type-three-dimensional ultrasonography auxiliary high speed pulping process obtain it is smooth Fine and smooth tremella Ultramicro-powder homogenate.
(4) supplementary material passes through high pressure homogenizer, and slurries further refine, and nutrient substance more easily absorbs.
Specific embodiment
Further description of the technical solution of the present invention below, and however, it is not limited to this, all to the technology of the present invention Scheme is modified or is replaced on an equal basis, without departing from the spirit and scope of the technology of the present invention, should all cover in guarantor of the invention It protects in range.
Embodiment 1
A kind of processing method of bitter buckwheat moisturizing sleep mask that not adding preservative, its step are as follows:
1, raw material is chosen: pick out full grains bitter buckwheat seed, the ginkgo leaf of fresh no insect pest, high-quality dendrobium candidum, purslane, Motherwort and tremella are spare;
2, pre-process: 40 DEG C of thermostatic drying chamber drying pulverize, cross 80 meshes;
3, tartary buckwheat extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating are low to moisture content Until 10%, whole process is aseptically operated;
4, ginkgo biloba p.e: ginko leaves flavone class compound is extracted using ultrasonic wave counter-current extraction techniques, 70% ethyl alcohol is expected Liquor ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content are lower than 10% Only, whole process aseptically operates;
5, tremella Ultramicro-powder is homogenized:
(1) 50g tremella Ultramicro-powder is taken to be placed in stirring-type saucepan, setting temperature is 40 ~ 50 DEG C, impregnates 3 ~ 4h, heating is precooked later 20min;
(2) tremella material is delivered to by three-dimensional ultrasonography by spiral propeller and assists high speed beating equipment, ultrasonic power 500 ~ 1000W, 15 ~ 30min of time, 10000 ~ 25000r/min of revolving speed obtain tremella Ultramicro-powder homogenate 500mL;
6, ingredient: by 15 parts of tartary buckwheat extract, 15 parts of ginkgo biloba p.e, tremella Ultramicro-powder be homogenized 20 parts, 6 parts of collagen, 4 parts of pearl powder, 0.05 part of soluble perfume, 40 parts of deionized water, stirring at normal temperature is uniform.
7, homogeneous: above-mentioned resulting material is put into homogenate in high pressure homogenizer and obtains facial mask lotion.
Embodiment 2
A kind of processing method of bitter buckwheat moisturizing sleep mask that not adding preservative, its step are as follows:
1, raw material is chosen: pick out full grains bitter buckwheat seed, the ginkgo leaf of fresh no insect pest, high-quality dendrobium candidum, purslane, Motherwort and tremella are spare;
2, pre-process: 40 DEG C of thermostatic drying chamber drying pulverize, cross 80 meshes;
3, tartary buckwheat extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating are low to moisture content Until 10%, whole process is aseptically operated;
4, purslane extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
5, Leonurus extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
6, tremella Ultramicro-powder is homogenized:
(1) 50g tremella Ultramicro-powder is taken to be placed in stirring-type saucepan, setting temperature is 40 ~ 50 DEG C, impregnates 3 ~ 4h, heating is precooked later 20min;
(2) tremella material is delivered to by three-dimensional ultrasonography by spiral propeller and assists high speed beating equipment, ultrasonic power 500 ~ 1000W, 15 ~ 30min of time, 10000 ~ 25000r/min of revolving speed obtain tremella Ultramicro-powder homogenate 500mL;
7, ingredient: by 20 parts of tartary buckwheat extract, 4 parts of purslane extract, 5 parts of Leonurus extract, tremella Ultramicro-powder homogenate 15 Part, 6 parts of collagen, 4 parts of pearl powder, 0.10 part of soluble perfume, 46 parts of deionized water mixings;
8, homogeneous: above-mentioned resulting material is put into homogenate in high pressure homogenizer and obtains facial mask lotion.
Embodiment 3
A kind of processing method of bitter buckwheat moisturizing sleep mask that not adding preservative, its step are as follows:
1, raw material is chosen: pick out full grains bitter buckwheat seed, the ginkgo leaf of fresh no insect pest, high-quality dendrobium candidum, purslane, Motherwort and tremella are spare;
2, pre-process: 40 DEG C of thermostatic drying chamber drying pulverize, cross 80 meshes;
3, tartary buckwheat extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating are low to moisture content Until 10%, whole process is aseptically operated;
4, ginkgo biloba p.e: ginko leaves flavone class compound is extracted using ultrasonic wave counter-current extraction techniques, 70% ethyl alcohol is expected Liquor ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content are lower than 10% Only, whole process aseptically operates;
5, dendrobium candidum extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture contain Until amount is lower than 10%, whole process is aseptically operated;
6, purslane extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
7, Leonurus extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
8, tremella Ultramicro-powder is homogenized:
(1) 50g tremella Ultramicro-powder is taken to be placed in stirring-type saucepan, setting temperature is 40 ~ 50 DEG C, impregnates 3 ~ 4h, heating is precooked later 20min;
(2) tremella material is delivered to by three-dimensional ultrasonography by spiral propeller and assists high speed beating equipment, ultrasonic power 500 ~ 1000W, 15 ~ 30min of time, 10000 ~ 25000r/min of revolving speed obtain tremella Ultramicro-powder homogenate 500mL;
9, ingredient: by 10 parts of tartary buckwheat extract, 5 parts of ginkgo biloba p.e, 5 parts of dendrobium candidum extract, purslane extract 5 Part, 2 parts of Leonurus extract, tremella Ultramicro-powder be homogenized 25 parts, 5 parts of collagen, 5 parts of pearl powder, 0.05 part of soluble perfume, 38 parts of deionized water mixings;
10, homogeneous: above-mentioned resulting material is put into homogenate in high pressure homogenizer and obtains facial mask lotion.
Embodiment 4
A kind of processing method of bitter buckwheat moisturizing sleep mask that not adding preservative, its step are as follows:
1, raw material is chosen: pick out full grains bitter buckwheat seed, the ginkgo leaf of fresh no insect pest, high-quality dendrobium candidum, purslane, Motherwort and tremella are spare;
2, pre-process: 40 DEG C of thermostatic drying chamber drying pulverize, cross 80 meshes;
3, tartary buckwheat extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating are low to moisture content Until 10%, whole process is aseptically operated;
4, ginkgo biloba p.e: ginko leaves flavone class compound is extracted using ultrasonic wave counter-current extraction techniques, 70% ethyl alcohol is expected Liquor ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content are lower than 10% Only, whole process aseptically operates;
5, dendrobium candidum extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture contain Until amount is lower than 10%, whole process is aseptically operated;
6, purslane extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
7, Leonurus extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
8, tremella Ultramicro-powder is homogenized:
(1) 50g tremella Ultramicro-powder is taken to be placed in stirring-type saucepan, setting temperature is 40 ~ 50 DEG C, impregnates 3 ~ 4h, heating is precooked later 20min;
(2) tremella material is delivered to by three-dimensional ultrasonography by spiral propeller and assists high speed beating equipment, ultrasonic power 500 ~ 1000W, 15 ~ 30min of time, 10000 ~ 25000r/min of revolving speed obtain tremella Ultramicro-powder homogenate 500mL;
9, ingredient: 15 parts of tartary buckwheat extract, 4 parts of ginkgo biloba p.e, 4 parts of dendrobium candidum extract, 3 parts of purslane extract, 3 parts of Leonurus extract, tremella Ultramicro-powder are homogenized 20 parts, 4 parts of collagen, 4 parts of pearl powder, 0.08 part of soluble perfume, go 43 parts of ionized water mixings;
10, homogeneous: above-mentioned resulting material is put into homogenate in high pressure homogenizer and obtains facial mask lotion.
Embodiment 5
A kind of processing method of bitter buckwheat moisturizing sleep mask that not adding preservative, its step are as follows:
1, raw material is chosen: pick out full grains bitter buckwheat seed, the ginkgo leaf of fresh no insect pest, high-quality dendrobium candidum, purslane, Motherwort and tremella are spare;
2, pre-process: 40 DEG C of thermostatic drying chamber drying pulverize, cross 80 meshes;
3, tartary buckwheat extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating are low to moisture content Until 10%, whole process is aseptically operated;
4, ginkgo biloba p.e: ginko leaves flavone class compound is extracted using ultrasonic wave counter-current extraction techniques, 70% ethyl alcohol is expected Liquor ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content are lower than 10% Only, whole process aseptically operates;
5, dendrobium candidum extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture contain Until amount is lower than 10%, whole process is aseptically operated;
6, purslane extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
7, Leonurus extract: dendrobium candidum active constituent is extracted using ultrasonic wave counter-current extraction techniques.Extraction conditions are as follows: 70% Ethyl alcohol, solid-liquid ratio 1:30 (g/m L), 65 DEG C, 60 min of ultrasonic extraction under 500W, extracting solution filtering and concentrating to moisture content Until 10%, whole process is aseptically operated;
8, tremella Ultramicro-powder is homogenized:
(1) 50g tremella Ultramicro-powder is taken to be placed in stirring-type saucepan, setting temperature is 40 ~ 50 DEG C, impregnates 3 ~ 4h, heating is precooked later 20min;
(2) tremella material is delivered to by three-dimensional ultrasonography by spiral propeller and assists high speed beating equipment, ultrasonic power 500 ~ 1000W, 15 ~ 30min of time, 10000 ~ 25000r/min of revolving speed obtain tremella Ultramicro-powder homogenate 500mL;
9, ingredient: by 30 parts of tartary buckwheat extract, 6 parts of ginkgo biloba p.e, 6 parts of dendrobium candidum extract, purslane extract 3 Part, 4 parts of Leonurus extract, tremella Ultramicro-powder be homogenized 27 parts, 3 parts of collagen, 3 parts of pearl powder, 0.15 part of soluble perfume, 18 parts of deionized water mixings;
10, homogeneous: above-mentioned resulting material is put into homogenate in high pressure homogenizer and obtains facial mask lotion.

Claims (7)

1. the bitter buckwheat moisturizing sleep mask that one kind does not add preservative, it is characterised in that the facial mask is according to following mass percent Supplementary material be prepared: 10 ~ 30 parts of tartary buckwheat extract, 4 ~ 15 parts of ginkgo biloba p.e, 4 ~ 6 parts of dendrobium candidum extract, horse Sativa extract 3 ~ 5, Leonurus extract 2 ~ 5, tremella Ultramicro-powder are homogenized 20 ~ 27 parts, 2 ~ 6 parts of collagen, pearl powder 3 ~ 5 Part, 0.05 ~ 0.15 part of soluble perfume, 18 ~ 50 parts of deionized water.
2. the bitter buckwheat moisturizing sleep mask according to claim 1 for not adding preservative, it is characterised in that the facial mask by Following supplementary material is prepared: 15 parts of tartary buckwheat extract, 15 parts of ginkgo biloba p.e, tremella Ultramicro-powder are homogenized 20 parts, collagen egg White 6 parts, 4 parts of pearl powder, 0.05 part of soluble perfume, 40 parts of deionized water.
3. the bitter buckwheat moisturizing sleep mask according to claim 1 for not adding preservative, it is characterised in that the facial mask by Following supplementary material is prepared: 20 parts of tartary buckwheat extract, 4 parts of purslane extract, 5 parts of Leonurus extract, tremella Ultramicro-powder It is homogenized 15 parts, 6 parts of collagen, 4 parts of pearl powder, 0.10 part of soluble perfume, 46 parts of deionized water.
4. the bitter buckwheat moisturizing sleep mask according to claim 1 for not adding preservative, it is characterised in that the facial mask by Following supplementary material is prepared: 10 parts of tartary buckwheat extract, 5 parts of ginkgo biloba p.e, 5 parts of dendrobium candidum extract, purslane mention 5 parts of object, 2 parts of Leonurus extract, tremella Ultramicro-powder is taken to be homogenized 25 parts, 5 parts of collagen, 5 parts of pearl powder, soluble perfume 0.05 part, 38 parts of deionized water.
5. the bitter buckwheat moisturizing sleep mask according to claim 1 for not adding preservative, it is characterised in that the facial mask by Following supplementary material is prepared: 15 parts of tartary buckwheat extract, 4 parts of ginkgo biloba p.e, 4 parts of dendrobium candidum extract, purslane mention 3 parts of object, 3 parts of Leonurus extract, tremella Ultramicro-powder is taken to be homogenized 20 parts, 4 parts of collagen, 4 parts of pearl powder, soluble perfume 0.08 part, 43 parts of deionized water.
6. the bitter buckwheat moisturizing sleep mask according to claim 1 for not adding preservative, it is characterised in that the facial mask by Following supplementary material is prepared: 30 parts of tartary buckwheat extract, 6 parts of ginkgo biloba p.e, 6 parts of dendrobium candidum extract, purslane mention 3 parts of object, 4 parts of Leonurus extract, tremella Ultramicro-powder is taken to be homogenized 27 parts, 3 parts of collagen, 3 parts of pearl powder, soluble perfume 0.15 part, 18 parts of deionized water.
7. the bitter buckwheat moisturizing sleep mask according to claim 1 for not adding preservative, it is characterised in that in the facial mask The homogenate of tremella Ultramicro-powder high speed beating equipment is assisted using three-dimensional ultrasonography, 10000 ~ 25000r/min of revolving speed, gained is even Smooth exquisiteness is starched, thickener, stabilizer, moisturizer and bacteriostatic agent are used as in facial mask.
CN201910761241.0A 2019-08-17 2019-08-17 A kind of bitter buckwheat moisturizing sleep mask and preparation method thereof for not adding preservative Pending CN110354062A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111249201A (en) * 2020-03-25 2020-06-09 配方化妆品科技(广州)有限公司 Vitamin water powder skin care composition and preparation method thereof
CN113940910A (en) * 2021-11-17 2022-01-18 湖南科技学院 Gingko extract toning lotion
CN114129621A (en) * 2021-11-11 2022-03-04 泸州品创科技有限公司 Application of tartary buckwheat flavone in preparation of antibacterial or gastritis preventing and treating medicine or health-care product

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CN101829196A (en) * 2010-05-26 2010-09-15 南京泽朗农业发展有限公司 Preparation method of high-content buckwheat total flavone
CN103405380A (en) * 2013-09-06 2013-11-27 重庆市中药研究院 White fungus skin-care composition and application thereof
CN107669604A (en) * 2017-09-30 2018-02-09 佘延英 A kind of almond leaf duck wheat facial mask liquid
CN109157443A (en) * 2018-10-26 2019-01-08 重庆菩璞生物科技有限公司 A kind of tremella face mask

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Publication number Priority date Publication date Assignee Title
CN101829196A (en) * 2010-05-26 2010-09-15 南京泽朗农业发展有限公司 Preparation method of high-content buckwheat total flavone
CN103405380A (en) * 2013-09-06 2013-11-27 重庆市中药研究院 White fungus skin-care composition and application thereof
CN107669604A (en) * 2017-09-30 2018-02-09 佘延英 A kind of almond leaf duck wheat facial mask liquid
CN109157443A (en) * 2018-10-26 2019-01-08 重庆菩璞生物科技有限公司 A kind of tremella face mask

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111249201A (en) * 2020-03-25 2020-06-09 配方化妆品科技(广州)有限公司 Vitamin water powder skin care composition and preparation method thereof
CN114129621A (en) * 2021-11-11 2022-03-04 泸州品创科技有限公司 Application of tartary buckwheat flavone in preparation of antibacterial or gastritis preventing and treating medicine or health-care product
CN113940910A (en) * 2021-11-17 2022-01-18 湖南科技学院 Gingko extract toning lotion

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Application publication date: 20191022