CN111249200A - Powder for fixing makeup and preparation method and application thereof - Google Patents
Powder for fixing makeup and preparation method and application thereof Download PDFInfo
- Publication number
- CN111249200A CN111249200A CN202010213760.6A CN202010213760A CN111249200A CN 111249200 A CN111249200 A CN 111249200A CN 202010213760 A CN202010213760 A CN 202010213760A CN 111249200 A CN111249200 A CN 111249200A
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- China
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- powder
- makeup
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- content
- phase
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- 239000000843 powder Substances 0.000 title claims abstract description 184
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 71
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 52
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 33
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 24
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 24
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 24
- 239000003906 humectant Substances 0.000 claims abstract description 18
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims abstract description 13
- 229940101267 panthenol Drugs 0.000 claims abstract description 13
- 235000020957 pantothenol Nutrition 0.000 claims abstract description 13
- 239000011619 pantothenol Substances 0.000 claims abstract description 13
- 239000004480 active ingredient Substances 0.000 claims abstract description 12
- 244000146462 Centella asiatica Species 0.000 claims abstract description 8
- 235000004032 Centella asiatica Nutrition 0.000 claims abstract description 8
- 239000012071 phase Substances 0.000 claims description 63
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 25
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 24
- 229920002674 hyaluronan Polymers 0.000 claims description 24
- 229960003160 hyaluronic acid Drugs 0.000 claims description 24
- 229920003217 poly(methylsilsesquioxane) Polymers 0.000 claims description 23
- 238000003756 stirring Methods 0.000 claims description 23
- 229920006037 cross link polymer Polymers 0.000 claims description 21
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 21
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 21
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 21
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 21
- 229920002554 vinyl polymer Polymers 0.000 claims description 21
- -1 polydimethylsiloxane Polymers 0.000 claims description 19
- 239000002537 cosmetic Substances 0.000 claims description 16
- 239000008346 aqueous phase Substances 0.000 claims description 11
- 235000011187 glycerol Nutrition 0.000 claims description 11
- 239000003755 preservative agent Substances 0.000 claims description 11
- 230000002335 preservative effect Effects 0.000 claims description 11
- 239000002738 chelating agent Substances 0.000 claims description 10
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 10
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 10
- 239000002826 coolant Substances 0.000 claims description 8
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 7
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 7
- 229960005323 phenoxyethanol Drugs 0.000 claims description 7
- 239000004302 potassium sorbate Substances 0.000 claims description 7
- 235000010241 potassium sorbate Nutrition 0.000 claims description 7
- 229940069338 potassium sorbate Drugs 0.000 claims description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims description 6
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims description 6
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 claims description 6
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 claims description 6
- 150000005846 sugar alcohols Polymers 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 229920005862 polyol Polymers 0.000 claims description 5
- 150000003077 polyols Chemical class 0.000 claims description 5
- 239000008213 purified water Substances 0.000 claims description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 4
- 241000167550 Centella Species 0.000 claims description 4
- 239000004288 Sodium dehydroacetate Substances 0.000 claims description 4
- 229960003415 propylparaben Drugs 0.000 claims description 4
- 235000019259 sodium dehydroacetate Nutrition 0.000 claims description 4
- 229940079839 sodium dehydroacetate Drugs 0.000 claims description 4
- DSOWAKKSGYUMTF-GZOLSCHFSA-M sodium;(1e)-1-(6-methyl-2,4-dioxopyran-3-ylidene)ethanolate Chemical compound [Na+].C\C([O-])=C1/C(=O)OC(C)=CC1=O DSOWAKKSGYUMTF-GZOLSCHFSA-M 0.000 claims description 4
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims description 3
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims description 3
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 3
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical group [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 3
- JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 claims description 3
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 3
- 229940041616 menthol Drugs 0.000 claims description 3
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 3
- 239000004299 sodium benzoate Substances 0.000 claims description 3
- 235000010234 sodium benzoate Nutrition 0.000 claims description 3
- RWAXQWRDVUOOGG-UHFFFAOYSA-N N,2,3-Trimethyl-2-(1-methylethyl)butanamide Chemical compound CNC(=O)C(C)(C(C)C)C(C)C RWAXQWRDVUOOGG-UHFFFAOYSA-N 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- DUFKCOQISQKSAV-UHFFFAOYSA-N Polypropylene glycol (m w 1,200-3,000) Chemical compound CC(O)COC(C)CO DUFKCOQISQKSAV-UHFFFAOYSA-N 0.000 claims description 2
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 229940008099 dimethicone Drugs 0.000 claims description 2
- 238000000227 grinding Methods 0.000 claims description 2
- 230000005661 hydrophobic surface Effects 0.000 claims description 2
- 229940089508 methyl diisopropyl propionamide Drugs 0.000 claims description 2
- 229960002216 methylparaben Drugs 0.000 claims description 2
- 239000010445 mica Substances 0.000 claims description 2
- 229910052618 mica group Inorganic materials 0.000 claims description 2
- CFJYNSNXFXLKNS-UHFFFAOYSA-N p-menthane Chemical compound CC(C)C1CCC(C)CC1 CFJYNSNXFXLKNS-UHFFFAOYSA-N 0.000 claims description 2
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 229960003191 potassium methylparaben Drugs 0.000 claims description 2
- 235000013772 propylene glycol Nutrition 0.000 claims description 2
- 229960003885 sodium benzoate Drugs 0.000 claims description 2
- 238000004381 surface treatment Methods 0.000 claims description 2
- 239000000454 talc Substances 0.000 claims description 2
- 229910052623 talc Inorganic materials 0.000 claims description 2
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 235000013312 flour Nutrition 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 12
- 230000003020 moisturizing effect Effects 0.000 abstract description 6
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 11
- 238000000034 method Methods 0.000 description 7
- 239000003921 oil Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical compound CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 description 3
- 239000004909 Moisturizer Substances 0.000 description 3
- 229940059958 centella asiatica extract Drugs 0.000 description 3
- 230000001333 moisturizer Effects 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 230000001815 facial effect Effects 0.000 description 2
- 210000000245 forearm Anatomy 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229940058015 1,3-butylene glycol Drugs 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 238000000149 argon plasma sintering Methods 0.000 description 1
- 239000001201 calcium disodium ethylene diamine tetra-acetate Substances 0.000 description 1
- 235000011188 calcium disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- SHWNNYZBHZIQQV-UHFFFAOYSA-L calcium;disodium;2-[2-[bis(carboxylatomethyl)azaniumyl]ethyl-(carboxylatomethyl)azaniumyl]acetate Chemical compound [Na+].[Na+].[Ca+2].[O-]C(=O)C[NH+](CC([O-])=O)CC[NH+](CC([O-])=O)CC([O-])=O SHWNNYZBHZIQQV-UHFFFAOYSA-L 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000004005 microsphere Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 235000014483 powder concentrate Nutrition 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
Abstract
The invention discloses a fixing powder and a preparation method and application thereof. The fixing powder comprises a powder phase and a water phase; the content of the powder phase is 25-60%; the percentage is the mass percentage of the powder phase in the makeup powder; the content of the water phase is 40-75%; the percentage is the mass percentage of the water phase in the makeup powder; the powder phase comprises skin feeling regulating powder; the skin feeling adjusting powder comprises silica; the silica includes silica silylate; the water phase comprises humectant and water; the humectant comprises one or more of sodium hyaluronate, panthenol and centella asiatica active ingredients; the content of the humectant is 1-10%, and the humectant accounts for the mass percent of the foundation powder; the content of the water is 30-74%, and the percentage is the mass percentage of the water in the makeup powder. The makeup fixing powder disclosed by the invention is good in makeup fixing effect and moisturizing effect, better in skin feel, and better in stability when the moisture content is higher.
Description
Technical Field
The invention relates to a powder for fixing cosmetics, a preparation method and application thereof.
Background
The powder for fixing cosmetics is a common cosmetic. The makeup fixing loose powder in the prior art comprises powder raw materials, wherein the powder raw materials which do not contain or contain a small amount of oil generally do not contain moisture, and are usually used for facial modification and makeup fixing after makeup, so that the makeup fixing loose powder has the effects of absorbing redundant oil and reducing facial gloss, and the makeup is more durable. However, excessive oil absorption tends to dry the skin.
Therefore, it is desired to provide a makeup fixing powder having a makeup fixing effect and an excellent moisturizing effect.
Disclosure of Invention
The cosmetic powder aims at solving the defect that the cosmetic powder in the prior art cannot realize the cosmetic effect and the moisturizing effect at the same time. The invention provides a fixing powder and a preparation method and application thereof. The makeup fixing powder disclosed by the invention can be used for fixing makeup, has a moisturizing effect, is good in skin feel, and can ensure good stability when the moisture content is high.
In order to achieve the purpose, the invention provides the following technical scheme:
one of the technical schemes provided by the invention is as follows: a makeup powder comprising a powder phase and an aqueous phase;
the content of the powder phase is 25-60%; the percentage is the mass percentage of the powder phase in the makeup fixing loose powder; the content of the water phase is 40-75%; the percentage is the mass percentage of the water phase in the makeup fixing loose powder;
the powder phase comprises skin feel adjusting powder;
the skin feel adjusting powder comprises silica; the silica comprises a silylated silica;
the aqueous phase comprises a humectant and water;
the humectant comprises one or more of sodium hyaluronate, panthenol and centella asiatica active ingredients;
the content of the humectant is 1-10%, and the percentage is the mass percentage of the humectant in the makeup fixing loose powder; the content of the water is 30-74%, and the percentage is the mass percentage of the water in the makeup powder;
wherein the sum of the contents of the components in the makeup fixing powder is 100%.
In the invention, the content of the powder phase is preferably 25-40%; the percentage is the mass percentage of the powder phase in the makeup fixing loose powder. The content of the water phase is preferably 40-65%; more preferably 50-65%; the percentage is the mass percentage of the water phase in the makeup fixing loose powder.
In the present invention, the silica may be silica conventional in the art, such as surface-modified silica or silica that has not been surface-modified. The non-surface-modified silica may be a conventional non-surface-modified silica in the art, and those skilled in the art will understand that the non-surface-modified silica generally refers to amorphous silica, and is generally white powder, and has the characteristics of porosity, light weight, softness and strong adsorbability.
In the present invention, the silica silylate may be silica silylate which is conventional in the art and commercially available, and is preferably silica silylate which has been subjected to hydrophobic surface treatment.
The preparation process of the silica silylate can be a conventional process in the field, and is preferably a gas phase method process. The content of the silica silylate can be the content of silica silylate which is conventional in the field, and is preferably 4 to 10 percent; the percentage is the mass percentage of the silica silylate to the powder.
Wherein the specific surface area of the silica silylate can be that of silica silylate conventional in the field, and is preferably 110-260 m2(ii)/g; more preferably 195 to 245m2(ii) in terms of/g. It is preferable thatWhen the specific surface area of the silica is 110 to 260m2At/g, the components in the water phase can be stably wrapped. The density of the silylated silica can be that of silica conventional in the art, for example, from 50 to 60 g/L.
In the invention, the content of the skin feeling adjusting powder can be the content of the skin feeling adjusting powder which is conventional in the field, such as 24.7%, 45%, 59.67%, preferably 15-56%; the percentage is the mass percentage of the skin feeling adjusting powder in the makeup powder.
In the invention, the skin feeling adjusting powder can also comprise one or more of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, polymethylsilsesquioxane, talc and mica; preferably vinyl dimethicone/polymethylsilsesquioxane crosspolymer and/or polymethylsilsesquioxane.
The vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer may be a vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer that is conventional in the art, and those skilled in the art will be aware of composite powders that generally refer to silicone resin-coated silicone rubber powders. When the skin-feel adjusting powder comprises vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, the content of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer is preferably 1-46%, and the percentage is the mass percentage of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer in the makeup powder.
Wherein the polymethylsilsesquioxane may be a polymethylsilsesquioxane conventional in the art. When the skin feeling adjusting powder comprises polymethylsilsesquioxane, the content of the polymethylsilsesquioxane is preferably 1-46%, and the percentage is the mass percentage of the polymethylsilsesquioxane in the makeup powder.
The vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer and the polymethylsilsesquioxane are both of organic silicon microsphere structures and have good oil absorption, water resistance and light scattering performance, so that a better makeup fixing effect is realized. When the skin-feel adjusting powder comprises vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer and polymethylsilsesquioxane, the content of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer and the polymethylsilsesquioxane is preferably more than 5%, and the percentage is the mass percentage of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer and the polymethylsilsesquioxane in the makeup powder.
In the present invention, the powder phase may further include a cooling agent.
Wherein, the cooling agent can be one or more of cooling agents conventional in the art, such as menthol lactate, menthane formylethylamine and methyl diisopropyl propionamide. The content of the cooling agent can be the content of the cooling agent which is conventional in the field, and is preferably 0.01-0.5%; the percentage is the mass percentage of the cool feeling agent in the makeup fixing powder.
In the present invention, the water may be water conventional in the art, and is preferably purified water. The content of the water is preferably 30-70%, such as 31.1%, 46.8%, 69.1999%, and more preferably 40-60%, wherein the percentage is the mass percentage of the water in the foundation powder.
In the invention, the content of the humectant is preferably 5-10%, such as 5.1301%, 7% and 8%, and the percentage is the mass percentage of the humectant in the makeup powder.
In the present invention, the sodium hyaluronate may be sodium hyaluronate that is conventional in the art and generally commercially available, such as low molecular sodium hyaluronate and/or high molecular sodium hyaluronate. The content of the sodium hyaluronate is preferably 0.0001-2%; the percentage is the mass percentage of the hyaluronic acid in the makeup powder.
Wherein the low molecular sodium hyaluronate may have a molecular weight <10 kDa. The molecular weight of the high molecular sodium hyaluronate can be more than 1000 kDa.
In the present invention, the panthenol may be conventional in the art, and those skilled in the art will know that it generally means a colorless to yellowish transparent viscous liquid and is easily soluble in water. The content of panthenol is preferably 0.1-1%; the percentage is the mass percentage of the panthenol in the makeup fixing loose powder.
In the present invention, the active ingredient in centella asiatica may be the active ingredient in centella asiatica which is conventional in the art, and those skilled in the art will know that the active ingredient is generally extracted and separated from centella asiatica. The content of the centella active ingredient can be 0.0001-0.1%; the percentage is the mass percentage of the centella active ingredient in the makeup fixing loose powder.
In the present invention, the humectant may further include a polyhydric alcohol and/or hyaluronic acid.
Wherein the polyol may be a polyol conventional in the art, preferably one or more of glycerol, 1, 3-butylene glycol, propylene glycol, dipropylene glycol and polyethylene glycol. The content of the polyhydric alcohol is preferably 1-10% but not 10%; the percentage is the mass percentage of the polyhydric alcohol in the makeup fixing loose powder.
Preferably, when glycerin is included in the polyol, the content of the glycerin is 2-8%; the percentage is the mass percentage of the glycerin in the makeup fixing loose powder.
The hyaluronic acid can be conventional hyaluronic acid in the field, and is preferably one or more of high molecular hyaluronic acid, low molecular hyaluronic acid and oligomeric hyaluronic acid. The content of the hyaluronic acid is preferably 0.0001-2%; more preferably 0.005-1%; the percentage is the mass percentage of the hyaluronic acid in the makeup powder.
Wherein the molecular weight of the hyaluronic acid may be a molecular weight of hyaluronic acid conventional in the art. The molecular weight of the high molecular hyaluronic acid is preferably 1800-2200 kDa.
In the present invention, a chelating agent may be further included in the aqueous phase.
Wherein the chelating agent can be a chelating agent conventional in the art, and is preferably disodium EDTA and/or calcium disodium EDTA. The content of the chelating agent can be the content of the chelating agent which is conventional in the field, such as 0.01-0.1%, and the percentage is the mass percentage of the chelating agent in the makeup powder.
In the present invention, the fixing powder may further include a preservative, which may be present in the powder phase and/or the aqueous phase.
Wherein the preservative may be a preservative conventional in the art, such as one or more of sodium dehydroacetate, phenoxyethanol, sodium benzoate, potassium sorbate, methylparaben, propylparaben, and 1, 2-pentanediol, preferably one or more of sodium dehydroacetate, phenoxyethanol, potassium sorbate, methylparaben, and propylparaben. The content of the preservative can be the content of the preservative which is conventional in the field, such as 0.001-1.5%; the percentage is the mass percentage of the preservative in the makeup fixing loose powder.
In the present invention, the pH of the makeup powder can be appropriately set, for example, 6 to 9, depending on the kind and content of the powder phase and/or the water phase component.
In a preferred embodiment of the present invention, the makeup fixing powder preferably comprises the following components by mass: 25% of powder phase and 75% of water phase; wherein the powder phase comprises 7 percent of silica silylate, 10 percent of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 7.7 percent of polymethylsilsesquioxane, 0.2 percent of methyl p-hydroxybenzoate and 0.1 percent of propyl p-hydroxybenzoate; the water phase comprises 5% of glycerol, 0.01% of high-molecular sodium hyaluronate, 0.01% of low-molecular sodium hyaluronate, 0.01% of oligomeric hyaluronic acid, 0.1% of panthenol, 0.0001% of centella asiatica extract, 0.02% of EDTA disodium, 0.5% of phenoxyethanol, 0.15% of potassium sorbate and 69.1999% of purified water; the percentage is the mass percentage of each component in the total mass of the makeup removing powder.
In a preferred embodiment of the present invention, the makeup fixing powder preferably comprises the following components by mass: 45% of powder phase and 55% of water phase; wherein the powder phase comprises 5 percent of silica silylate, 25 percent of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer and 15 percent of polymethylsilsesquioxane; the water phase comprises 6.19% of glycerin, 0.1% of high-molecular sodium hyaluronate, 0.1% of low-molecular sodium hyaluronate, 0.1% of high-molecular hyaluronic acid, 0.5% of panthenol, 0.01% of centella asiatica extract, 0.1% of EDTA disodium, 0.5% of phenoxyethanol, 0.3% of potassium sorbate, 0.3% of sodium benzoate and 46.8% of purified water; the percentage is the mass percentage of each component in the total mass of the makeup removing powder.
In a preferred embodiment of the present invention, the makeup fixing powder preferably comprises the following components by mass: 60% of powder phase and 40% of water phase; wherein the powder phase comprises 10 percent of silica silylate, 25 percent of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 24.67 percent of polymethylsilsesquioxane, 0.2 percent of methyl p-hydroxybenzoate, 0.1 percent of propyl p-hydroxybenzoate and 0.03 percent of menthol lactate; the water phase comprises 7.45% of glycerin, 0.05% of high-molecular sodium hyaluronate, 0.05% of low-molecular sodium hyaluronate, 0.05% of high-molecular hyaluronic acid, 0.3% of panthenol, 0.1% of centella asiatica extract, 0.1% of EDTA disodium, 0.5% of phenoxyethanol, 0.3% of potassium sorbate and 31.1% of purified water; the percentage is the mass percentage of each component in the total mass of the makeup removing powder.
The second technical scheme provided by the invention is as follows: a preparation method of the makeup fixing powder specifically comprises the following steps: mixing the aqueous phase and the powder phase as described above to obtain the make-up fixing powder.
Wherein the mixing can be conventional mixing in the field, and preferably the water phase is added into the powder phase, and the stirring is carried out until the water phase is completely wrapped by the powder phase to obtain the fixing loose powder.
Wherein the stirring speed can be the conventional stirring speed in the field, and is preferably 1500-2500 rpm/min; more preferably 2000 rpm/min.
Wherein, preferably, the components in the powder phase are stirred uniformly. The temperature of the stirring may be room temperature. The room temperature may be 25 ℃ ± 5 ℃. The stirring device can be a powdering pot. The stirring speed can be the conventional stirring speed in the field, and is preferably 1500-2500 rpm/min; more preferably 2000 rpm/min.
Wherein, preferably, the components in the water phase are dissolved and stirred uniformly. The stirring device can be a stirrer or a disperser. The stirring speed can be the conventional stirring speed in the field, and is preferably 500-800 rpm/min; more preferably 600 rpm/min.
The third technical scheme provided by the invention is as follows: a powder for fixing cosmetic is prepared by the above method.
The fourth technical scheme provided by the invention is as follows: an application of a powder for fixing cosmetic is provided.
Wherein, the application can be used in the last step of makeup.
On the basis of the common knowledge in the field, the above preferred conditions can be combined randomly to obtain the preferred embodiments of the invention.
The reagents and starting materials used in the present invention are commercially available.
The positive progress effects of the invention are as follows: in the process of using the makeup fixing powder, the powder phase can realize oil control and makeup fixing effects, and can release moisture wrapped by the powder phase, so that a moisturizing effect is realized, the skin feel is good, and the stability of the makeup fixing powder can be guaranteed to be good when the moisture content is high.
Detailed Description
The invention is further illustrated by the following examples, which are not intended to limit the scope of the invention. The experimental methods without specifying specific conditions in the following examples were selected according to the conventional methods and conditions, or according to the commercial instructions.
In the following examples and comparative examples, the manufacturers and models of the respective components are shown in the following Table 1.
TABLE 1
Example 1 preparation of a powder for fixing cosmetics
The components and contents of the powder for fixing make-up in example 1 are shown in table 2.
In example 1, the preparation steps of the makeup remover powder are as follows:
(1) rapidly and uniformly stirring the components of the powder phase in the table 1 at room temperature by using a powder stirring pot to obtain a uniform powder phase; wherein the stirring speed is 2000 rpm/min;
(2) dissolving the components of the water phase in the table 1, and uniformly stirring by using a stirrer to obtain a uniform water phase; wherein the stirring speed is 600 rpm/min;
(3) and adding the uniform water phase into the uniform powder phase, and stirring at high speed (2000rpm/min) until the water phase is completely wrapped by the powder phase and is uniformly wrapped to obtain the make-up fixing loose powder.
TABLE 2
Examples 2-3 preparation of the powder for fixing cosmetic according to examples 2-3 the components and contents of the powder for fixing cosmetic according to examples 2-3 are shown in tables 3-4. The preparation steps of the make-up fixing powder in the embodiments 2 to 3 are the same as those in the embodiment 1.
TABLE 3
TABLE 4
Comparative examples 1-2 preparation of powder for fixing cosmetics
The preparation steps of the make-up fixing loose powder in the comparative examples 1-2 are the same as those in the example 1.
The components and contents of the makeup remover powder in comparative examples 1 to 2 are shown in tables 5 to 6.
Wherein the moisturizer of comparative example 1 does not include sodium hyaluronate, panthenol, or centella asiatica active ingredient; the moisturizer in comparative example 2 does not include sodium hyaluronate, panthenol, or centella asiatica active ingredients, and the content of the moisturizer is not within the range claimed in the present application.
TABLE 5
TABLE 6
Comparative example 3
A non-aqueous make-up powder is commercially available under the trade name megbaolian powder.
Effect example 1 stability test
The stability of the powder of the make-up remover of example 1 was tested according to the procedure of heat and cold resistance in Q31/0120000051C 030: the makeup fixing powder in the example 1 is filled in a colorless and transparent 30mL glass container and is stored at 25 ℃, 45 ℃, minus 10 ℃ and 5 ℃; after 24 hours, the behavior of the make-up fixing powder is observed, a small amount of the make-up fixing powder is smeared on the back of the hand after the room temperature is recovered, and the usability of the make-up fixing powder is evaluated.
The results show that the stability of the powder concentrates of examples 1 to 3 is better, as shown in the evaluation results in table 7.
TABLE 7
Note that good in Table 7 means that the powder was uniform and no abnormality was observed, △ means that the powder was slightly agglomerated and adhered, and X means that the powder was increased in particle size and significantly agglomerated and pasty.
Effect example 2 cosmetic effect test
Sensory evaluation was performed on the makeup fixing effect for 4h, 8h, and 12h after 9 women used the makeup fixing loose powder.
Wherein, when 9 women use the make-up fixing loose powder in the embodiments 1-3, the make-up surface is still relatively complete after 12 hours, and no mottle or make-up removal phenomenon exists.
Effect example 3 moisturizing effect test
The skin moisture content of 9 women after using the loose powder was measured at 0.5h, 2h and 6h, wherein the skin moisture content values were all higher than before using the make-up fixing loose powder of examples 1-3.
The method for testing the skin moisture content value comprises the following steps: after cleaning the inner sides of the forearms of 9 subjects, the forearms to be tested are exposed and sit still for 30min in a constant-temperature and constant-humidity laboratory. The area of 3cm multiplied by 3cm is marked on the double arms, the initial value of the moisture content of the skin of the marked part is measured by an instrument, then 0.0020g of the make-up fixing loose powder prepared in the embodiment 1-3 is evenly smeared on the marked part, the make-up fixing loose powder is wiped for 3 times by using cosmetic cotton with the same pressure, and the moisture content value of the skin is respectively tested after the make-up fixing loose powder is smeared for 0.5h, 2h and 6 h. The test instrument is a German CK skin moisture tester CM 825; and SPSS software is adopted to carry out relevant statistical analysis on the result data, and the significance difference level is p < 0.05.
Table 8 skin moisture content change value (%)
| 0.5h after use | 2h after use | 6h after use | |
| Example 1 | 1.48+ | 1.84 | 2.96+++ |
| Example 2 | 1.28+ | 1.02 | 2.33++ |
| Example 3 | 0.68 | 0.64 | 1.88+ |
| Comparative example 1 | 1.45+ | 1.08 | 0.80 |
| Comparative example 2 | -0.63 | 0.75 | 0.72 |
| Comparative example 3 | -0.72 | 0.89 | 2.14+ |
Tests show that the fixing powder in the example 1 is obviously superior to the initial value of the moisture content of the skin after 0.5h and 6h after the use, and is obviously superior to the comparative examples 1-3.
Claims (10)
1. A makeup powder, characterized in that the makeup powder comprises a powder phase and a water phase;
the content of the powder phase is 25-60%; the percentage is the mass percentage of the powder phase in the makeup fixing loose powder; the content of the water phase is 40-75%; the percentage is the mass percentage of the water phase in the makeup fixing loose powder;
the powder phase comprises skin feel adjusting powder;
the skin feel adjusting powder comprises silica; the silica comprises a silylated silica;
the aqueous phase comprises a humectant and water;
the humectant comprises one or more of sodium hyaluronate, panthenol and centella asiatica active ingredients;
the content of the humectant is 1-10%, and the percentage is the mass percentage of the humectant in the makeup fixing loose powder; the content of the water is 30-74%, and the percentage is the mass percentage of the water in the makeup powder;
wherein the sum of the contents of the components in the makeup fixing powder is 100%.
2. The makeup base powder according to claim 1, wherein the content of the powder phase is 25 to 40%; the percentage is the mass percentage of the powder phase in the makeup fixing loose powder;
and/or the content of the water phase is 40-65%, preferably 50-65%; the percentage is the mass percentage of the water phase in the makeup fixing loose powder.
3. The makeup powder according to claim 1 or 2, wherein the silica silylate is a silica silylate subjected to hydrophobic surface treatment;
and/or the content of the silica silylate is 4-10%; the percentage is the mass percentage of the silica silylate to the powder
And/or the silica silylate has a specific surface area of 110 to 260m2Preferably 195 to 245 m/g2/g；
And/or the silylated silica has a density of from 50 to 60 g/L.
4. The makeup fixing loose powder according to any one of claims 1 to 3, wherein the content of the skin feel adjusting powder is 15 to 56%; the percentage is the mass percentage of the skin feeling adjusting powder in the makeup powder;
and/or the skin feel adjusting powder comprises one or more of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, polymethylsilsesquioxane, talc and mica; preferably vinyl dimethicone/polymethylsilsesquioxane crosspolymer and/or polymethylsilsesquioxane;
preferably, the content of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer is 1-46%, and the percentage is the mass percentage of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer in the makeup fixing loose powder;
preferably, the content of the polymethylsilsesquioxane is 1-46%, and the percentage is the mass percentage of the polymethylsilsesquioxane in the makeup powder;
preferably, when the skin feel adjusting powder comprises the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer and the polymethylsilsesquioxane, the content of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer and the polymethylsilsesquioxane is preferably more than 5%, and the percentage is the mass percentage of the vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer and the polymethylsilsesquioxane in the makeup loose powder;
and/or the flour phase comprises a cooling agent;
preferably, the cooling agent is one or more of menthol lactate, menthane formylethylamine and methyl diisopropyl propionamide; the content of the cooling agent is 0.01-0.5%; the percentage is the mass percentage of the cool feeling agent in the makeup fixing powder.
5. The makeup powder according to claim 1, wherein the water is purified water;
and/or the content of the water is 30-70%, preferably 40-60%, and the percentage is the mass percentage of the water in the makeup fixing loose powder;
and/or the content of the humectant is 5-10%, wherein the humectant accounts for the mass percent of the makeup fixing loose powder;
and/or the sodium hyaluronate is low-molecular sodium hyaluronate and/or high-molecular sodium hyaluronate; the content of the sodium hyaluronate is preferably 0.0001-2%; the percentage is the mass percentage of the hyaluronic acid in the makeup powder;
preferably, the low molecular sodium hyaluronate has a molecular weight of <10 kDa;
preferably, the molecular weight of the high molecular sodium hyaluronate is more than 1000 kDa;
and/or the content of panthenol is 0.1-1%; the percentage is the mass percentage of the panthenol in the makeup fixing loose powder;
and/or the content of the centella active ingredient is 0.0001-0.1%; the percentage is the mass percentage of the centella active ingredient in the makeup fixing loose powder;
and/or, the humectant comprises a polyol and/or hyaluronic acid;
the polyalcohol is preferably one or more of glycerol, 1, 3-butanediol, propylene glycol, dipropylene glycol and polyethylene glycol; the content of the polyhydric alcohol is preferably 1-10% but not 10%; the percentage is the mass percentage of the polyhydric alcohol in the makeup setting loose powder;
preferably, when the glycerin is included in the polyol, the content of the glycerin is 2 to 8%; the percentage is the mass percentage of the glycerin in the makeup fixing loose powder;
the hyaluronic acid is preferably one or more of high molecular hyaluronic acid, low molecular hyaluronic acid and oligomeric hyaluronic acid; the content of the hyaluronic acid is preferably 0.0001-2%; more preferably 0.005-1%; the percentage is the mass percentage of the hyaluronic acid in the makeup powder;
preferably, the molecular weight of the high molecular hyaluronic acid is 1800-2200 kDa;
and/or, the aqueous phase comprises a chelating agent;
the chelating agent is preferably disodium EDTA and/or disodium EDTA calcium; the content of the chelating agent is preferably 0.01-0.1%, and the percentage is the mass percentage of the chelating agent in the makeup powder.
6. The makeup powder according to claim 1, comprising a preservative; the preservative is present in the powder phase and/or the aqueous phase;
the preservative is preferably one or more of sodium dehydroacetate, phenoxyethanol, sodium benzoate, potassium sorbate, methylparaben, propylparaben and 1, 2-pentanediol; more preferably one or more of sodium dehydroacetate, phenoxyethanol, potassium sorbate, methylparaben and propylparaben;
the content of the preservative is preferably 0.001-1.5%; the percentage is the mass percentage of the preservative in the makeup fixing loose powder;
and/or the pH value of the fixing loose powder is 6-9.
7. The preparation method of the makeup fixing loose powder is characterized by comprising the following steps: mixing the aqueous phase and the powder phase according to claims 1 to 6 to obtain the powder for fixing cosmetics.
8. The preparation method according to claim 7, wherein the mixing is adding the aqueous phase into the powder phase, and stirring until the aqueous phase is completely wrapped by the powder phase to obtain the fixing loose powder;
and/or the stirring speed is 1500-2500 rpm/min; preferably 2000 rpm/min;
preferably, the components in the powder phase are stirred uniformly; the stirring temperature is room temperature; the room temperature is 25 +/-5 ℃; the stirring device is a powdering pot; the stirring speed is 1500-2500 rpm/min, preferably 2000 rpm/min;
preferably, the components in the water phase are dissolved and stirred uniformly; the stirring equipment is a stirrer or a disperser; the stirring speed is 500-800 rpm/min, preferably 600 rpm/min.
9. A makeup base powder characterized by being produced by the production method according to claim 7 or 8.
10. Use of the powder of claim 1 or 9 in cosmetics.
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| CN113181067A (en) * | 2021-05-24 | 2021-07-30 | 上海大喂科技发展有限公司 | Long-lasting oil-control makeup-fixing powder and preparation method thereof |
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Address after: 201403 Shanghai City, Fengxian District Lifenglu No. 12 Patentee after: Shanghai Natural Hall Group Co.,Ltd. Country or region after: China Address before: 201403 Shanghai City, Fengxian District Lifenglu No. 12 Patentee before: JALA Group Co. Country or region before: China |