KR101483974B1 - Water in oil make-up cosmetic compositions containing silicone/silica powder - Google Patents
Water in oil make-up cosmetic compositions containing silicone/silica powder Download PDFInfo
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- KR101483974B1 KR101483974B1 KR20080000561A KR20080000561A KR101483974B1 KR 101483974 B1 KR101483974 B1 KR 101483974B1 KR 20080000561 A KR20080000561 A KR 20080000561A KR 20080000561 A KR20080000561 A KR 20080000561A KR 101483974 B1 KR101483974 B1 KR 101483974B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/61—Surface treated
- A61K2800/62—Coated
- A61K2800/621—Coated by inorganic compounds
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Abstract
본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물에 관한 것으로, 더욱 상세하게는 유상에 실리콘/실리카 복합 파우더를 함유하고 수상에 수용성 점증제를 함유함으로써 외상과 내상에 점성을 부여하여 탄성을 가지며 발림성이 우수하고 오일감이 없는 유중수 메이크업 화장료 조성물에 관한 것이다. The present invention relates to a makeup cosmetic composition having elasticity, and more particularly, to a makeup cosmetic composition having an elasticity, and more particularly, to a makeup cosmetic composition having elasticity, which comprises silicone / silica composite powder in oil phase and water- And is excellent in oil-free feel.
유중수 파운데이션 * 실리콘/실리카 복합 파우더 * 탄성 * 발림성 * 오일감 Water-based water foundation * Silicone / silica composite powder * Elasticity * Wetting * Oiliness
Description
본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물에 관한 것으로, 더욱 상세하게는 유상에 실리콘/실리카 복합 파우더를 함유하고 수상에 수용성 점증제를 함유함으로써 외상과 내상에 점성을 부여하여 탄성을 가지며 발림성이 우수하고 오일감이 없는 유중수 메이크업 화장료 조성물에 관한 것이다.The present invention relates to a makeup cosmetic composition having elasticity, and more particularly, to a makeup cosmetic composition having an elasticity, and more particularly, to a makeup cosmetic composition having elasticity, which comprises silicone / silica composite powder in oil phase and water- And is excellent in oil-free feel.
일반적으로 탄성을 갖는 파운데이션 메이크업 화장료 조성물은 유분산 제형과 수분산 제형이 있다. 유분산 제형의 파운데이션은 과량의 실리콘 젤과 실리콘 파우더로 구성되어 탄성을 지니며 지속성과 색상 표현이 우수하다. 수분산 제형의 파운데이션은 수용성의 가교 폴리머로 구성되어 탄성을 나타내며 사용감이 산뜻한 장점이 있다. In general, a foundation makeup cosmetic composition having elasticity has an oil-dispersed formulation and an aqueous dispersion formulation. The foundation of oil dispersion type is composed of excessive amount of silicone gel and silicone powder, has elasticity, and has excellent durability and color expression. The foundation of the aqueous dispersion formulation is composed of a water-soluble crosslinked polymer and exhibits elasticity, and has a merit that the feeling of use is neat.
그러나, 유분산 제형의 경우 과량의 실리콘 젤과 실리콘 파우더에 의해서 탄성을 가지므로 실리콘 파우더 자체의 엉김과 실리콘 파우더와 실리콘 젤의 엉김에 의해서 도포시 뭉침 문제가 발생하며 분산을 위한 용매로 오일을 과량 사용하여 오일감이 높게 나타나고, 수분산 제형의 경우 지속성과 색상 표현력이 떨어지는 문제점이 있다. However, in the case of oil dispersion type, excessive silicone gel and silicone powder have an elasticity, so that the silicone powder itself and the silicon powder and silicone gel are entangled with each other to cause agglomeration problem, And the water dispersibility of the water-dispersed formulation is inferior in durability and color reproducibility.
이에, 도포감이 우수하고 오일감이 없으면서도 지속성과 커버력이 떨어지지 않는 탄성을 갖는 유중수 메이크업 화장료 조성물이 필요하다. Therefore, there is a need for a makeup cosmetic composition for a makeup product in a water-based and water-repellent state which has an excellent feeling of application and an elasticity that does not deteriorate persistence and coverage even when there is no oiliness.
이에, 본 발명자들은 상기한 문제점을 해결하기 위하여 연구한 결과, 유상에 실리콘/실리카 복합 파우더를 함유하고 수상에 수용성 점증제를 함유함으로써 메이크업 화장료에 탄성을 부여하고 밀림감 및 오일감이 없으며 발림성이 우수한 유중수 메이크업 화장료 조성물을 제공할 수 있음을 발견하고 본 발명을 완성하였다. The present inventors have conducted studies to solve the above-mentioned problems and found that a silicone / silica composite powder is contained in an oil phase and a water-soluble thickening agent is contained in the oil phase to impart elasticity to the makeup cosmetic, And can provide a water-in-oil make-up cosmetic composition. Thus, the present invention has been completed.
따라서, 본 발명의 목적은 사용감이 우수하면서도 탄성을 갖는 유중수 메이크업 화장료 조성물을 제공하는 것이다. Accordingly, it is an object of the present invention to provide a makeup cosmetic composition for a make-up in a water-based and water-based makeup that has excellent feeling and elasticity.
상기한 목적을 달성하기 위하여 본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물로서, 유상 성분에 실리콘/실리카 복합파우더를 조성물 총 중량에 대하여 1.00~10.00중량%로 함유함을 특징으로 하는 유중수 메이크업 화장료 조성물을 제공한다.In order to achieve the above object, the present invention provides a makeup cosmetic composition having elasticity, which comprises a silicone / silica composite powder in an oil phase component in an amount of 1.00 to 10.00 wt% based on the total weight of the composition, Lt; / RTI >
또한, 상기 실리콘/실리카 복합파우더는 실리콘 엘라스토머 구상 파우더의 표면을 미립자의 실리카 입자로 피복한 파우더임을 특징으로 한다.Also, the silicone / silica composite powder is characterized in that the surface of the silicone elastomer spherical powder is coated with fine silica particles.
본 발명에 의한 화장료 조성물은 유상에 실리콘/실리카 복합 파우더를 함유하여 탄성을 갖는 유중수 메이크업 화장료 조성물을 제조함으로써 기존의 유분산 제형 보다 뭉침이 없고 오일감이 없으며 퍼짐성이 우수하고 유분산 제형보다 제조가 용이하다. The cosmetic composition according to the present invention contains a silicone / silica composite powder in oil phase to produce a water-in-oil makeup cosmetic composition having elasticity, so that the oil-in-water cosmetic composition has no lumps, no oiliness and spreadability, It is easy.
본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물로서 기존의 분산 제형과는 달리 외상에 있는 유상에 실리콘/실리카 복합파우더를 함유하고 내상에 있는 수상에 수용성 점증제를 더 함유함을 특징으로 한다. 본 발명에서는 메이크업 화장료에 탄성을 부여하기 위하여 상기 실리콘/실리카 복합파우더를 사용하였으며 일정량 이상의 수상을 함유함으로써 사용시 수상이 휘발되며 오일감이 없고 밀림감이 없는 우수한 사용감을 나타낸다. The present invention is a water-based makeup cosmetic composition having elasticity and is characterized by containing a silicone / silica composite powder in an oil phase in an external phase and further containing a water-soluble thickening agent in an internal phase, unlike an existing dispersion formulation. In the present invention, the silicone / silica composite powder is used for imparting elasticity to makeup cosmetics, and the aqueous phase is volatilized by using a certain amount or more of water.
본 발명에서 사용되는 실리콘/실리카 복합파우더는 실리콘 엘라스토머 구상 파우더의 표면을 미립자의 실리카 입자로 피복한 파우더로서 엘라스토머 파우더의 응집성이 없어 분산성이 높고 용이하다. 이와 같은 특성은 퍼짐성과 마무리 도포시 뭉침없이 매끄럽고 균일하게 도포되는 장점으로 작용하게 된다. The silicone / silica composite powder used in the present invention is a powder in which the surface of the silicone elastomer spherical powder is coated with fine silica particles, and the dispersibility of the elastomer powder is high because of the lack of cohesiveness. Such properties are advantageous in spreadability and smoothness and uniform application without clumping during finishing.
본 발명에서는 실리콘/실리카 복합파우더로서 디메치콘/비닐디메치콘 크로스 폴리머 실리카 (Dimethicone / Vinyldimethicone Crosspolymer Silica; 상품명 Dow Corning 9701 Cosmetic powder; 제조회사: Dow Corning사)가 사용되었다.In the present invention, Dimethicone / Vinyldimethicone Crosspolymer Silica (trade name: Dow Corning 9701 Cosmetic powder; manufactured by Dow Corning) was used as a silicon / silica composite powder.
상기 실리콘/실리카 복합파우더는 조성물 총 중량에 대하여 1.00~10.00중량%, 바람직하게는 3.00~6.00중량%로 함유한다. 이는 실리콘/실리카 복합파우더 함량이 1중량% 미만인 경우 탄성이 떨어지고, 10중량%를 초과하는 경우 오일의 흡유로 유상의 점도가 상승하여 제조가 어렵기 때문이다. The silicone / silica composite powder is contained in an amount of 1.00 to 10.00 wt%, preferably 3.00 to 6.00 wt%, based on the total weight of the composition. This is because the elasticity is lowered when the silicone / silica composite powder content is less than 1 wt%, and when the silicone / silica composite powder content is more than 10 wt%, the viscosity of the oil-absorbing oil phase oil is increased and the production is difficult.
또한, 본 발명에서는 내상의 점도를 상승시키기 위해서 상기 조성물의 수상 성분에 수용성 점증제를 사용하였다. 수용성 점증제로는 잔탄검, 셀룰로오스, 벤토나이트, 마그네슘 알루미늄 실리케이트 등을 당업자가 용이하게 선택하여 사용할 수 있다. Further, in the present invention, a water-soluble thickener is used for the water component of the composition in order to increase the viscosity of the inner phase. As water-soluble thickener, xanthan gum, cellulose, bentonite, magnesium aluminum silicate and the like can be easily selected and used by those skilled in the art.
상기 수용성 점증제는 조성물 총 중량에 대하여 0.01~0.20중량%, 바람직하게는 0.02~0.05중량%로 함유한다. 이는 수용성 점증제의 함량이 0.01중량% 미만에서는 내상의 점증이 되지 않으며, 0.20중량%를 초과하는 경우에는 유화시 유화 안정도가 떨어지기 때문이다. The water-soluble thickener is contained in an amount of 0.01 to 0.20% by weight, preferably 0.02 to 0.05% by weight based on the total weight of the composition. This is because when the content of the water-soluble thickener is less than 0.01 wt%, the inner phase does not increase, and when it exceeds 0.20 wt%, the emulsion stability during emulsification is lowered.
본 발명에 의한 화장료 조성물은 내상의 수상과 외상의 유상(오일)의 중량비가 63.3:29.7 내지 50.7:39.3, 바람직하게는 20.7:69.3 내지 28.7:61.3으로 함유함으로써 오일감이 없고 밀림감이 없어 우수한 사용감을 나타낸다.The cosmetic composition according to the present invention contains an oil-in-water emulsion and oil-in-water emulsion (oil) at a weight ratio of 63.3: 29.7 to 50.7: 39.3, preferably 20.7: 69.3 to 28.7: 61.3, .
본 발명의 유중수 메이크업 화장료 조성물은 유상성분, 수상성분, 및 안료성분으로 이루어져 있다. 유상성분에는 점도 조절제인 실리콘 왁스, 실리콘 젤, 트리에톡시카프릴릴실란 코팅 분체 안료, 분산용매인 실리콘 오일이 더 포함될 수 있다. 또한 수상성분으로는 에몰리언트제인 부틸렌글리콜 또는 글리세린이 더 포함될 수 있다.The makeup cosmetic composition of the present invention comprises an oil component, an aqueous component, and a pigment component. The oil component may further include silicone wax, silicone gel, triethoxycaprylylsilane coated powder pigment, and silicone oil as a dispersion solvent, which are viscosity adjusting agents. The aqueous phase component may further include an emollient, butylene glycol or glycerin.
본 발명에서 사용하는 실리콘 오일은 디메치콘, 사이클로메치콘, 알킬 트리메치콘 오일로 이루어진 군에서 선택하여 사용하는 것이 바람직하나, 이에만 한정되는 것은 아니다.The silicone oil used in the present invention is preferably selected from the group consisting of dimethicone, cyclomethicone, and alkyltrimethicone oil, but is not limited thereto.
본 발명에서는 트리에톡시카프릴릴실란이 코팅된 고상의 분체 안료로서 티타늄옥사이드/알루미늄하이드록사이드/트리에톡시카프릴릴실란(TITANIUM OXIDE/ALUMINUM HYDROXIDE/TRIETHOXYCAPRYLYLSILANE)을 사용할 수 있으며, 분산을 원활하게 하여 유화 안정도를 높인 메이크업 화장료 조성물을 제조할 수 있다. 상기 고상 분체 안료의 함량은 조성물 총 중량에 대하여 5.0~30.0중량%, 바람직하게는 8.0~16.0 중량%이다.In the present invention, it is possible to use titanium oxide / aluminum hydroxide / triethoxycaprylylsilane (TITANIUM OXIDE / ALUMINUM HYDROXIDE / TRIETHOXYCAPRYLYLSILANE) as a solid phase powder pigment coated with triethoxycaprylylsilane, Thereby making it possible to produce a makeup cosmetic composition having enhanced emulsion stability. The content of the solid powdery pigment is 5.0 to 30.0% by weight, preferably 8.0 to 16.0% by weight based on the total weight of the composition.
또한 본 발명에서는 분산매인 실리콘 오일에 실리콘/실리카 파우더를 함유하고 고상의 트리에톡시카프릴릴실란 코팅 분체 안료를 균일하게 분산하여 유상을 제조하고 여기에 수상을 첨가하여 유중수 제형의 메이크업 화장료를 얻을 수 있다.In addition, in the present invention, the oil phase is prepared by uniformly dispersing the solid phase triethoxycaprylylsilane silane powder pigment in silicone oil, which is a dispersion medium, of silicone oil and silica, and water phase is added thereto to prepare a makeup cosmetic of a water- Can be obtained.
본 발명에 따른 화장료 조성물은 얼굴 또는 목에 적용되는 파운데이션, 컨실러(conealer), 또는 신체용 메이크업 화장료 조성물로 제형화될 수 있다.The cosmetic composition according to the present invention may be formulated into a makeup cosmetic composition for a foundation, a coneerer, or a body applied to the face or neck.
이하, 실시예 및 비교예를 통하여 본 발명을 보다 구체적으로 설명하지만, 본 발명이 이들 예로만 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail by way of examples and comparative examples, but the present invention is not limited to these examples.
[실시예 1~3 및 비교예 1][Examples 1 to 3 and Comparative Example 1]
하기의 실시예 1~3은 본 발명에 따른 유중수 파운데이션이며, 비교예 1은 기존의 유분산 파운데이션 제형이다. 이들 함량의 단위는 중량%이다. The following Examples 1 to 3 are water-based water-soluble bases according to the present invention, and Comparative Example 1 is a conventional oil-based foundation formulation. The units of these contents are% by weight.
실시예 1~3은 유중수 파운데이션을 제조하기 위하여, 점도 조절제로서 C30-45알킬메치콘/C30-45올레핀, 유상의 점성과 탄성을 부여하기 위한 실리콘/실리카 복합 파우더로서 디메치콘/비닐디메치콘 크로스 폴리머 실리카 (상품명 Dow Corning 9701 Cosmetic powder), 수상 점증제로서 실리콘 아크릴레이트의 잔탄검(Xanthan gum)을 사용하였다. Examples 1 to 3 were prepared by mixing C30-45 alkyl methicone / C30-45 olefin as a viscosity modifier, dimethicone / vinyl dimethicone as a silicon / silica composite powder for imparting oil viscosity and elasticity, Crosspolymer silica (trade name: Dow Corning 9701 Cosmetic powder) and Xanthan gum of silicone acrylate as an aqueous phase thickening agent were used.
<실시예 1~3의 제조방법> <Manufacturing Method of Examples 1 to 3>
1) 유상성분 1~5을 85~95℃에서 균일하게 혼합하였다.1) The oil components 1 to 5 were uniformly mixed at 85 to 95 ° C.
2) 상기 1)에 고상의 성분 6을 분산하였다.2) The solid phase component 6 was dispersed in 1) above.
3) 상기 성분 7~10을 가열한 후 상기 2)의 혼합물을 65~72℃를 유지하며 서서히 투입한 다음 균일하게 교반하고 성분 11의 향을 투입하여 크림상의 파운데이션을 얻었다.3) After heating the ingredients 7 to 10, the mixture of 2) was slowly added thereto while maintaining the temperature at 65 to 72 ° C, and the mixture was homogeneously stirred to give a creamy foundation.
[시험예 1][Test Example 1]
상기 실시예 1~3과 비교예 1에서 제조한 파운데이션의 물성을 SUN SCIENTIFIC RHEO METER CR-500DX 기기로 측정하여 비교하였다. The physical properties of the foundations prepared in Examples 1 to 3 and Comparative Example 1 were measured and compared with a SUN SCIENTIFIC RHEO METER CR-500DX instrument.
표 2에서 알 수 있는 바와 같이, 본 발명의 유중수 파운데이션의 실시예 1~3은 비교예 1과 비교하여 탄성이 높다는 것을 확인할 수 있었다. As can be seen from Table 2, it was confirmed that Examples 1 to 3 of the water-based water-based foundation of the present invention had higher elasticity than Comparative Example 1.
[시험예 2][Test Example 2]
상기 실시예 1~3 및 비교예 1의 사용감 정도를 알아보기 위하여 메이크업 화장을 일주일에 3일 이상하는 20~40세 여성 50명을 대상으로 패널 테스트를 통하여 각각의 사용감(탄성감, 펴발림, 가벼움, 산뜻함, 오일감, 등등)을 평가하여 비교하였다. 그 결과를 하기 표 3에 나타내었다. 각 항목별로 1 내지 9점씩 점수를 부여하였으며, 점수가 높을수록 그 속성이 강하게 나타나는 것을 의미한다. 예를 들면, 펴발림성이 9점인 경우에는 가장 잘 펴발림을 의미하므로 사용감 면에서 좋으며, 오일감이 9점인 경우는 오일감이 제일 강하므로 사용감이 좋지 않게 된다.In order to examine the feeling of use in Examples 1 to 3 and Comparative Example 1, 50 women aged 20 to 40 years who make up makeup more than three days a week were subjected to panel test to determine their feelings (elasticity, Lightness, freshness, oiliness, etc.) were evaluated and compared. The results are shown in Table 3 below. Each item is assigned a score of 1 to 9, and the higher the score, the stronger the attribute is. For example, when the spreadability is 9 points, it means the best spreading, so it is good for the feeling of use, and when the oiliness is 9 points, the feeling of feeling is the strongest because of the strong oiliness.
상기 결과에서 보여지는 바와 같이, 본 발명의 실시예 1~3은 탄성감을 가지며 퍼짐성이 비교예 1 보다 우수하고 수분이 함유되어 오일감이 낮으며, 시간 경과에 따른 피지에 대한 지속성이 우수함을 평가를 통하여 알 수 있었다.As shown in the above results, Examples 1 to 3 of the present invention were evaluated to have excellent elasticity, superior spreadability to Comparative Example 1, low moisture content and low oil resistance, and excellent durability against sebum over time .
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