KR20090074877A - Water in oil make-up cosmetic compositions containing silicone/silica powder - Google Patents
Water in oil make-up cosmetic compositions containing silicone/silica powder Download PDFInfo
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- KR20090074877A KR20090074877A KR1020080000561A KR20080000561A KR20090074877A KR 20090074877 A KR20090074877 A KR 20090074877A KR 1020080000561 A KR1020080000561 A KR 1020080000561A KR 20080000561 A KR20080000561 A KR 20080000561A KR 20090074877 A KR20090074877 A KR 20090074877A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/064—Water-in-oil emulsions, e.g. Water-in-silicone emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/60—Particulates further characterized by their structure or composition
- A61K2800/61—Surface treated
- A61K2800/62—Coated
- A61K2800/621—Coated by inorganic compounds
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Abstract
Description
본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물에 관한 것으로, 더욱 상세하게는 유상에 실리콘/실리카 복합 파우더를 함유하고 수상에 수용성 점증제를 함유함으로써 외상과 내상에 점성을 부여하여 탄성을 가지며 발림성이 우수하고 오일감이 없는 유중수 메이크업 화장료 조성물에 관한 것이다.The present invention relates to a water-in-oil makeup cosmetic composition having elasticity, and more particularly, by containing silicone / silica composite powder in an oil phase and a water-soluble thickener in an aqueous phase to impart viscosity to the trauma and the inner phase to have elasticity, and The present invention relates to an oil-in-water makeup cosmetic composition that is excellent in oil-free.
일반적으로 탄성을 갖는 파운데이션 메이크업 화장료 조성물은 유분산 제형과 수분산 제형이 있다. 유분산 제형의 파운데이션은 과량의 실리콘 젤과 실리콘 파우더로 구성되어 탄성을 지니며 지속성과 색상 표현이 우수하다. 수분산 제형의 파운데이션은 수용성의 가교 폴리머로 구성되어 탄성을 나타내며 사용감이 산뜻한 장점이 있다. In general, the foundation makeup cosmetic composition having elasticity is an oil dispersion formulation and a water dispersion formulation. The foundation of the oil-dispersed formulation is made up of excess silicone gel and silicone powder, which is elastic and has excellent persistence and color expression. The foundation of the water-dispersible formulation is composed of a water-soluble crosslinked polymer to exhibit elasticity and a fresh feel.
그러나, 유분산 제형의 경우 과량의 실리콘 젤과 실리콘 파우더에 의해서 탄성을 가지므로 실리콘 파우더 자체의 엉김과 실리콘 파우더와 실리콘 젤의 엉김에 의해서 도포시 뭉침 문제가 발생하며 분산을 위한 용매로 오일을 과량 사용하여 오일감이 높게 나타나고, 수분산 제형의 경우 지속성과 색상 표현력이 떨어지는 문제점이 있다. However, in the case of oil-dispersion formulations, elasticity is caused by excess silicone gel and silicone powder, so agglomeration problems occur during application due to the entanglement of the silicone powder itself and the entanglement of the silicone powder and the silicone gel. When used, the oil appears high, and in the case of the water-dispersible formulation, there is a problem in that the persistence and color expression are inferior.
이에, 도포감이 우수하고 오일감이 없으면서도 지속성과 커버력이 떨어지지 않는 탄성을 갖는 유중수 메이크업 화장료 조성물이 필요하다. Accordingly, there is a need for a water-in-oil makeup cosmetic composition having excellent elasticity and excellent elasticity that does not degrade the durability and coverage even without a feeling of oil.
이에, 본 발명자들은 상기한 문제점을 해결하기 위하여 연구한 결과, 유상에 실리콘/실리카 복합 파우더를 함유하고 수상에 수용성 점증제를 함유함으로써 메이크업 화장료에 탄성을 부여하고 밀림감 및 오일감이 없으며 발림성이 우수한 유중수 메이크업 화장료 조성물을 제공할 수 있음을 발견하고 본 발명을 완성하였다. Accordingly, the present inventors have studied to solve the above problems, and as a result, the silicone / silica composite powder in the oil phase and the water-soluble thickener in the water phase impart elasticity to the makeup cosmetics, have no feeling of denseness and oiliness, and have excellent applicability. The present invention has been found to be able to provide a water-in-oil makeup cosmetic composition.
따라서, 본 발명의 목적은 사용감이 우수하면서도 탄성을 갖는 유중수 메이크업 화장료 조성물을 제공하는 것이다. Accordingly, an object of the present invention is to provide a water-in-oil makeup cosmetic composition having excellent elasticity and elasticity.
상기한 목적을 달성하기 위하여 본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물로서, 유상 성분에 실리콘/실리카 복합파우더를 조성물 총 중량에 대하여 1.00~10.00중량%로 함유함을 특징으로 하는 유중수 메이크업 화장료 조성물을 제공한다.In order to achieve the above object, the present invention is a water-in-oil makeup cosmetic composition having elasticity, water-in-oil makeup cosmetics comprising a silicone / silica composite powder in the oil phase component of 1.00 ~ 10.00% by weight based on the total weight of the composition To provide a composition.
또한, 상기 실리콘/실리카 복합파우더는 실리콘 엘라스토머 구상 파우더의 표면을 미립자의 실리카 입자로 피복한 파우더임을 특징으로 한다.In addition, the silicon / silica composite powder is characterized in that the powder is coated with the silica particles of the surface of the silicone elastomer spherical powder.
본 발명에 의한 화장료 조성물은 유상에 실리콘/실리카 복합 파우더를 함유하여 탄성을 갖는 유중수 메이크업 화장료 조성물을 제조함으로써 기존의 유분산 제형 보다 뭉침이 없고 오일감이 없으며 퍼짐성이 우수하고 유분산 제형보다 제조가 용이하다. The cosmetic composition according to the present invention contains a silicone / silica composite powder in an oil phase, thereby preparing a water-in-oil makeup cosmetic composition having elasticity. It is easy.
본 발명은 탄성을 갖는 유중수 메이크업 화장료 조성물로서 기존의 분산 제형과는 달리 외상에 있는 유상에 실리콘/실리카 복합파우더를 함유하고 내상에 있는 수상에 수용성 점증제를 더 함유함을 특징으로 한다. 본 발명에서는 메이크업 화장료에 탄성을 부여하기 위하여 상기 실리콘/실리카 복합파우더를 사용하였으며 일정량 이상의 수상을 함유함으로써 사용시 수상이 휘발되며 오일감이 없고 밀림감이 없는 우수한 사용감을 나타낸다. The present invention is characterized in that the water-in-oil makeup cosmetic composition having elasticity, unlike conventional dispersion formulations, contains a silicone / silica composite powder in the oil phase in the external phase and further contains a water-soluble thickener in the aqueous phase in the internal phase. In the present invention, the silicone / silica composite powder is used to impart elasticity to the makeup cosmetics, and the aqueous phase is volatilized upon use by containing a predetermined amount or more of the water phase, and there is no oil feeling and no feeling of rolling.
본 발명에서 사용되는 실리콘/실리카 복합파우더는 실리콘 엘라스토머 구상 파우더의 표면을 미립자의 실리카 입자로 피복한 파우더로서 엘라스토머 파우더의 응집성이 없어 분산성이 높고 용이하다. 이와 같은 특성은 퍼짐성과 마무리 도포시 뭉침없이 매끄럽고 균일하게 도포되는 장점으로 작용하게 된다. The silicon / silica composite powder used in the present invention is a powder coated with silica particles of fine particles on the surface of the silicone elastomer spherical powder, and has a high dispersibility and easy dispersibility of the elastomer powder. Such properties act as an advantage of spreading smoothly and uniformly without agglomeration during finish application.
본 발명에서는 실리콘/실리카 복합파우더로서 디메치콘/비닐디메치콘 크로스 폴리머 실리카 (Dimethicone / Vinyldimethicone Crosspolymer Silica; 상품명 Dow Corning 9701 Cosmetic powder; 제조회사: Dow Corning사)가 사용되었다.In the present invention, dimethicone / vinyldimethicone crosspolymer silica (trade name: Dow Corning 9701 Cosmetic powder; manufacturer: Dow Corning) was used as the silicone / silica composite powder.
상기 실리콘/실리카 복합파우더는 조성물 총 중량에 대하여 1.00~10.00중량%, 바람직하게는 3.00~6.00중량%로 함유한다. 이는 실리콘/실리카 복합파우더 함량이 1중량% 미만인 경우 탄성이 떨어지고, 10중량%를 초과하는 경우 오일의 흡유로 유상의 점도가 상승하여 제조가 어렵기 때문이다. The silicone / silica composite powder is contained in an amount of 1.00 to 10.00% by weight, preferably 3.00 to 6.00% by weight, based on the total weight of the composition. This is because when the silicone / silica compound powder content is less than 1% by weight, the elasticity is lowered, and when the content of the silicon / silica compound powder is more than 10% by weight, the oil phase is increased due to oil absorption.
또한, 본 발명에서는 내상의 점도를 상승시키기 위해서 상기 조성물의 수상 성분에 수용성 점증제를 사용하였다. 수용성 점증제로는 잔탄검, 셀룰로오스, 벤토나이트, 마그네슘 알루미늄 실리케이트 등을 당업자가 용이하게 선택하여 사용할 수 있다. In addition, in this invention, in order to raise the viscosity of an internal phase, the water-soluble thickener was used for the water phase component of the said composition. As the water-soluble thickener, xanthan gum, cellulose, bentonite, magnesium aluminum silicate and the like can be easily selected and used by those skilled in the art.
상기 수용성 점증제는 조성물 총 중량에 대하여 0.01~0.20중량%, 바람직하게는 0.02~0.05중량%로 함유한다. 이는 수용성 점증제의 함량이 0.01중량% 미만에서는 내상의 점증이 되지 않으며, 0.20중량%를 초과하는 경우에는 유화시 유화 안정도가 떨어지기 때문이다. The water-soluble thickener is contained in 0.01 to 0.20% by weight, preferably 0.02 to 0.05% by weight relative to the total weight of the composition. This is because when the content of the water-soluble thickener is less than 0.01% by weight, the internal phase does not increase, and when it exceeds 0.20% by weight, the emulsion stability during emulsification is inferior.
본 발명에 의한 화장료 조성물은 내상의 수상과 외상의 유상(오일)의 중량비가 63.3:29.7 내지 50.7:39.3, 바람직하게는 20.7:69.3 내지 28.7:61.3으로 함유함으로써 오일감이 없고 밀림감이 없어 우수한 사용감을 나타낸다.The cosmetic composition according to the present invention contains a weight ratio of the aqueous phase of the inner phase and the oil phase (oil) of the outer phase in an amount of 63.3: 29.7 to 50.7: 39.3, preferably 20.7: 69.3 to 28.7: 61.3, thereby providing no feeling of oil and no feeling of denseness. Indicates.
본 발명의 유중수 메이크업 화장료 조성물은 유상성분, 수상성분, 및 안료성분으로 이루어져 있다. 유상성분에는 점도 조절제인 실리콘 왁스, 실리콘 젤, 트리에톡시카프릴릴실란 코팅 분체 안료, 분산용매인 실리콘 오일이 더 포함될 수 있다. 또한 수상성분으로는 에몰리언트제인 부틸렌글리콜 또는 글리세린이 더 포함될 수 있다.The water-in-oil makeup cosmetic composition of the present invention consists of an oil phase component, an aqueous phase component, and a pigment component. The oil phase component may further include a silicone wax as a viscosity modifier, a silicone gel, a triethoxycaprylylsilane coated powder pigment, and a silicone oil as a dispersion solvent. In addition, the aqueous phase may further include butylene glycol or glycerin which is an emollient.
본 발명에서 사용하는 실리콘 오일은 디메치콘, 사이클로메치콘, 알킬 트리메치콘 오일로 이루어진 군에서 선택하여 사용하는 것이 바람직하나, 이에만 한정되는 것은 아니다.Silicone oil used in the present invention is preferably selected from the group consisting of dimethicone, cyclomethicone, alkyl trimethicone oil, but is not limited thereto.
본 발명에서는 트리에톡시카프릴릴실란이 코팅된 고상의 분체 안료로서 티타늄옥사이드/알루미늄하이드록사이드/트리에톡시카프릴릴실란(TITANIUM OXIDE/ALUMINUM HYDROXIDE/TRIETHOXYCAPRYLYLSILANE)을 사용할 수 있으며, 분산을 원활하게 하여 유화 안정도를 높인 메이크업 화장료 조성물을 제조할 수 있다. 상기 고상 분체 안료의 함량은 조성물 총 중량에 대하여 5.0~30.0중량%, 바람직하게는 8.0~16.0 중량%이다.In the present invention, as a solid powder pigment coated with triethoxycaprylylsilane, titanium oxide / aluminum hydroxide / triethoxycaprylylsilane (TITANIUM OXIDE / ALUMINUM HYDROXIDE / TRIETHOXYCAPRYLYLSILANE) may be used, and the dispersion may be smooth. It is possible to produce a makeup cosmetic composition to increase the emulsion stability. The content of the solid powder pigment is 5.0 to 30.0% by weight, preferably 8.0 to 16.0% by weight based on the total weight of the composition.
또한 본 발명에서는 분산매인 실리콘 오일에 실리콘/실리카 파우더를 함유하고 고상의 트리에톡시카프릴릴실란 코팅 분체 안료를 균일하게 분산하여 유상을 제조하고 여기에 수상을 첨가하여 유중수 제형의 메이크업 화장료를 얻을 수 있다.In addition, in the present invention, a silicone oil containing silicone / silica powder in a dispersion medium and uniformly disperse the solid triethoxycaprylylsilane-coated powder pigment to prepare an oil phase and add an aqueous phase to make up a makeup cosmetic in a water-in-oil formulation. You can get it.
본 발명에 따른 화장료 조성물은 얼굴 또는 목에 적용되는 파운데이션, 컨실러(conealer), 또는 신체용 메이크업 화장료 조성물로 제형화될 수 있다.The cosmetic composition according to the present invention may be formulated with a foundation, concealer, or body makeup cosmetic composition applied to the face or neck.
이하, 실시예 및 비교예를 통하여 본 발명을 보다 구체적으로 설명하지만, 본 발명이 이들 예로만 한정되는 것은 아니다.Hereinafter, although an Example and a comparative example demonstrate this invention more concretely, this invention is not limited only to these examples.
[실시예 1~3 및 비교예 1][Examples 1-3 and Comparative Example 1]
하기의 실시예 1~3은 본 발명에 따른 유중수 파운데이션이며, 비교예 1은 기존의 유분산 파운데이션 제형이다. 이들 함량의 단위는 중량%이다. Examples 1 to 3 below are water-in-oil foundations according to the present invention, and Comparative Example 1 is a conventional oil-dispersion foundation formulation. The unit of these contents is weight percent.
실시예 1~3은 유중수 파운데이션을 제조하기 위하여, 점도 조절제로서 C30-45알킬메치콘/C30-45올레핀, 유상의 점성과 탄성을 부여하기 위한 실리콘/실리카 복합 파우더로서 디메치콘/비닐디메치콘 크로스 폴리머 실리카 (상품명 Dow Corning 9701 Cosmetic powder), 수상 점증제로서 실리콘 아크릴레이트의 잔탄검(Xanthan gum)을 사용하였다. Examples 1-3 are dimethicone / vinyl dimethicone as silicone / silica composite powder for imparting viscosity and elasticity of C30-45 alkyl methicones / C30-45 olefins as viscosity modifiers to prepare water-in-oil foundations. Cross polymer silica (trade name Dow Corning 9701 Cosmetic powder), Xanthan gum of silicone acrylate was used as an aqueous thickener.
<실시예 1~3의 제조방법> <Production Method of Examples 1-3>
1) 유상성분 1~5을 85~95℃에서 균일하게 혼합하였다.1) The oily components 1 to 5 were uniformly mixed at 85 to 95 ° C.
2) 상기 1)에 고상의 성분 6을 분산하였다.2) The solid component 6 was dispersed in 1).
3) 상기 성분 7~10을 가열한 후 상기 2)의 혼합물을 65~72℃를 유지하며 서서히 투입한 다음 균일하게 교반하고 성분 11의 향을 투입하여 크림상의 파운데이션을 얻었다.3) After heating the components 7 to 10, the mixture of 2) was slowly added while maintaining 65 to 72 ° C, then stirred uniformly, and the fragrance of the component 11 was added to obtain a creamy foundation.
[시험예 1][Test Example 1]
상기 실시예 1~3과 비교예 1에서 제조한 파운데이션의 물성을 SUN SCIENTIFIC RHEO METER CR-500DX 기기로 측정하여 비교하였다. The physical properties of the foundation prepared in Examples 1 to 3 and Comparative Example 1 were measured and compared with a SUN SCIENTIFIC RHEO METER CR-500DX instrument.
표 2에서 알 수 있는 바와 같이, 본 발명의 유중수 파운데이션의 실시예 1~3은 비교예 1과 비교하여 탄성이 높다는 것을 확인할 수 있었다. As can be seen from Table 2, Examples 1 to 3 of the water-in-oil foundation of the present invention was confirmed that the elasticity is high compared to Comparative Example 1.
[시험예 2][Test Example 2]
상기 실시예 1~3 및 비교예 1의 사용감 정도를 알아보기 위하여 메이크업 화장을 일주일에 3일 이상하는 20~40세 여성 50명을 대상으로 패널 테스트를 통하여 각각의 사용감(탄성감, 펴발림, 가벼움, 산뜻함, 오일감, 등등)을 평가하여 비교하였다. 그 결과를 하기 표 3에 나타내었다. 각 항목별로 1 내지 9점씩 점수를 부여하였으며, 점수가 높을수록 그 속성이 강하게 나타나는 것을 의미한다. 예를 들면, 펴발림성이 9점인 경우에는 가장 잘 펴발림을 의미하므로 사용감 면에서 좋으며, 오일감이 9점인 경우는 오일감이 제일 강하므로 사용감이 좋지 않게 된다.In order to determine the degree of feeling of Examples 1 to 3 and Comparative Example 1, each of the feeling (elasticity, spreading, Lightness, freshness, oiliness, etc.) were evaluated and compared. The results are shown in Table 3 below. Each item is given a score of 1 to 9 points, and the higher the score, the stronger the property. For example, when the spreadability is 9 points, it means the best spreading, so it is good in terms of feeling, and in the case of 9 points of oil feeling, the feeling of oil is the strongest, so the feeling is not good.
상기 결과에서 보여지는 바와 같이, 본 발명의 실시예 1~3은 탄성감을 가지며 퍼짐성이 비교예 1 보다 우수하고 수분이 함유되어 오일감이 낮으며, 시간 경과에 따른 피지에 대한 지속성이 우수함을 평가를 통하여 알 수 있었다.As can be seen from the above results, Examples 1 to 3 of the present invention have an elasticity and have an excellent spreading property than Comparative Example 1, contain moisture, have a low oily feeling, and have excellent sustainability for sebum over time. I could see through.
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WO2013039353A1 (en) * | 2011-09-16 | 2013-03-21 | (주)아모레퍼시픽 | Inner phase thickened water-in-oil cosmetic composition |
KR20140060927A (en) * | 2012-11-13 | 2014-05-21 | (주)아모레퍼시픽 | Make-up cosmetic composition of oil-dispersed liquid type |
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WO2005117813A1 (en) * | 2004-05-26 | 2005-12-15 | L'oreal | Cosmetic mousse formulations |
KR100654062B1 (en) * | 2005-01-06 | 2006-12-05 | 주식회사 코리아나화장품 | Partial Make-up Cosmetic Composition of Solid Type and Water-in-oil Type |
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US11040224B2 (en) | 2011-09-16 | 2021-06-22 | Amorepacific Corporation | Inner phase thickened water-in-oil cosmetic composition |
KR20140060927A (en) * | 2012-11-13 | 2014-05-21 | (주)아모레퍼시픽 | Make-up cosmetic composition of oil-dispersed liquid type |
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