CN111117750A - Trace lubricating oil, preparation method and supply device thereof - Google Patents
Trace lubricating oil, preparation method and supply device thereof Download PDFInfo
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- CN111117750A CN111117750A CN201911345124.2A CN201911345124A CN111117750A CN 111117750 A CN111117750 A CN 111117750A CN 201911345124 A CN201911345124 A CN 201911345124A CN 111117750 A CN111117750 A CN 111117750A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23Q—DETAILS, COMPONENTS, OR ACCESSORIES FOR MACHINE TOOLS, e.g. ARRANGEMENTS FOR COPYING OR CONTROLLING; MACHINE TOOLS IN GENERAL CHARACTERISED BY THE CONSTRUCTION OF PARTICULAR DETAILS OR COMPONENTS; COMBINATIONS OR ASSOCIATIONS OF METAL-WORKING MACHINES, NOT DIRECTED TO A PARTICULAR RESULT
- B23Q11/00—Accessories fitted to machine tools for keeping tools or parts of the machine in good working condition or for cooling work; Safety devices specially combined with or arranged in, or specially adapted for use in connection with, machine tools
- B23Q11/10—Arrangements for cooling or lubricating tools or work
- B23Q11/1038—Arrangements for cooling or lubricating tools or work using cutting liquids with special characteristics, e.g. flow rate, quality
- B23Q11/1046—Arrangements for cooling or lubricating tools or work using cutting liquids with special characteristics, e.g. flow rate, quality using a minimal quantity of lubricant
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/287—Partial esters
- C10M2207/289—Partial esters containing free hydroxy groups
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/04—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having a silicon-to-carbon bond, e.g. organo-silanes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Lubricants (AREA)
Abstract
The invention belongs to the technical field of micro-lubrication, and particularly relates to micro-lubricating oil, a preparation method and a supply device thereof; the trace lubricating oil is prepared by adding the antirust agent into water to obtain a water-based part, then uniformly mixing and stirring the refined soybean oil, the trihydroxy ester, the antioxidant and the water-based part, and then adding the defoaming agent to uniformly mix and stir; the feeding device comprises a base, a mixing barrel, a supporting seat, a low-temperature gas generator, a cooling box, a gas guide pipe, a feeding pipe, a movable ball block, a groove, a telescopic hose and an injector head. The trace lubricating oil can effectively reduce the friction between the cutter and the workpiece and between the cutter and the cutting chips, and prevent the adhesion; after the supply device replaces a cooling liquid lubricating system, a cutting liquid recovery device can be omitted, the feeding amount is increased, and the machining production efficiency of workpieces is improved.
Description
Technical Field
The invention belongs to the technical field of micro-lubrication, and particularly relates to micro-lubricating oil, a preparation method and a supply device thereof.
Background
On one hand, MQL reduces the consumption of the cutting fluid to a trace degree, not only obviously reduces the use cost of the cutting fluid, but also reduces the harm of the cutting fluid to the environment and human bodies to the utmost extent by using synthetic esters with high natural degradability as the lubricating agent; on the other hand, compared with dry cutting, the MQL introduces a cooling and lubricating medium, so that the cooling and lubricating conditions in the cutting process are greatly improved, the abrasion among the cutter, the workpiece and the chips is remarkably reduced, and the reduction of cutting force, cutting temperature and the abrasion of the cutter is facilitated.
The conventional trace amount of lubricating oil has a poor lubricating effect and is liable to cause wear of the cutting tool, and the conventional trace amount of lubricating oil supply device is insufficient, and the trace amount of lubricating oil supplied to the bearing is extremely small, so that if the trace amount of lubricating oil is small in consistency and relatively hard, it is extremely difficult to stably supply a predetermined amount of the trace amount of lubricating oil due to the piping resistance in cases where the piping path is long, or where there are many places where the piping path is bent or bent at right angles in the middle.
Disclosure of Invention
The present invention is directed to overcoming the above problems in the prior art and providing a minimal amount of lubricant, a method for preparing the same and a supply device for the same.
In order to achieve the technical purpose and achieve the technical effect, the invention is realized by the following technical scheme:
the trace lubricating oil consists of refined soybean oil in 40-50 wt%, trihydroxyester in 10-20 wt%, antioxidant in 5-10 wt%, antirust in 10-18 wt%, defoaming agent in 0.01-0.05 wt% and water for the rest.
Further, in the trace amount of lubricating oil, the refined soybean oil is prepared by mixing one or two of deodorized soybean oil and refined soybean oil.
Further, in the above trace amount of lubricating oil, the characteristic indexes of the trihydroxy ester are: the acid value was 1.8mgKOH/g, the hydroxyl value was 15mgKOH/g, and the saponification value was 175-195 mg/g.
Further, in the above trace amount of lubricating oil, the antioxidant is tea polyphenol extracted from unfermented green tea.
Further, in the trace amount of lubricating oil, the antirust agent is neutral synthetic calcium sulfonate, the content of calcium in the antirust agent is 10-13%, and the content of sulfur in the antirust agent is 1-3%.
Further, in the above minimal quantity of lubricating oil, the defoaming agent is a DF-18 type defoaming agent which is a three-dimensional siloxane compound.
Further, in the above-mentioned trace amount of lubricating oil, the total base number of the trace amount of lubricating oil is 290-310.
A preparation method of trace lubricating oil comprises the following steps: weighing refined soybean oil, trihydroxy ester, an antioxidant, an antirust agent, a defoaming agent and water according to the mass percentage, and adding the antirust agent into the water to obtain a water-based part; and then mixing and stirring the refined soybean oil, the trihydroxy ester, the antioxidant and the water-based part uniformly at 40-60 ℃, and then adding the defoaming agent and mixing and stirring uniformly.
The utility model provides a feeding device of trace lubricating oil to trace lubricating oil is for supplying with the material, this feeding device of trace lubricating oil includes base, mixing cylinder, supporting seat, low temperature gas generator, cooling box, air duct, feed pipe, activity ball piece, fluting, expansion hose and injector head, the upper end of base is fixed with mixing cylinder, supporting seat, low temperature gas generator and cooling box, the inner chamber one end of cooling box is equipped with the air inlet with the butt joint of low temperature gas generator output, and the other end passes through the feed pipe intercommunication that air duct and mixing cylinder draw forth, it has the activity ball piece of taking the injector head to rotate the restriction in the supporting seat, the supporting seat is located the rear side of activity ball piece and is equipped with the fluting, after the feed pipe passed the cooling box, through the expansion hose that is located the fluting and injector head intercommunication.
Furthermore, in the supply device for the trace lubricating oil, a one-way valve is arranged at the connection position of the air guide pipe and the supply pipe.
The invention has the beneficial effects that:
1. the consumption of the trace lubricating oil is only 0.03-0.2L/h, and compared with the consumption of 20-100L/min in the traditional wet cutting, the trace lubricating oil has the advantage of low consumption, effectively reduces the friction between a cutter and a workpiece and between the cutter and chips, prevents adhesion, prolongs the service life of the cutter, and improves the quality of a processed surface.
2. The lubricating oil supply device can stably supply a trace amount of lubricating oil in a preset amount, and a cutting fluid recovery device can be omitted after the supply device replaces a cooling fluid lubricating system; using a very small amount of lubricating oil, the amount of oil consumed is about the size of a disposable cup, calculated in 8 hours per shift; the feeding amount is increased, the workpiece processing production efficiency is improved, and the processing time is shortened by about 20-70%; the service life of the cutter is prolonged by 2-3 times, and the surface precision of the machined workpiece is improved.
Of course, it is not necessary for any one product that embodies the invention to achieve all of the above advantages simultaneously.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to the drawings without creative efforts.
FIG. 1 is a schematic view showing a structure of a minimal quantity lubrication oil supply apparatus according to the present invention;
FIG. 2 is a schematic structural view of a support base and a movable ball block according to the present invention;
FIG. 3 is a schematic view of the structure of the ejection head of the present invention.
In the drawings, the components represented by the respective reference numerals are listed below:
1-base, 2-mixing barrel, 3-support base, 4-low temperature gas generator, 5-cooling box, 6-gas inlet, 7-gas guide tube, 8-feed tube, 9-movable ball block, 10-slot, 11-flexible hose, 12-spray head, 13-fastening screw.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example one
The trace lubricating oil consists of refined soybean oil 45 wt%, trihydroxy ester 15 wt%, antioxidant 8 wt%, antirust 14 wt%, defoaming agent 0.03 wt% and water for the rest.
The refined soybean oil is prepared by mixing one or two of deodorized soybean oil and refined soybean oil.
The characteristic indexes of the trihydroxy ester are as follows: the acid value was 1.8mgKOH/g, the hydroxyl value was 15mgKOH/g, and the saponification value was 175-195 mg/g.
The antioxidant is tea polyphenols extracted from unfermented green tea.
The antirust agent is neutral synthetic calcium sulfonate, and the content of calcium in the antirust agent is 12 percent, and the content of sulfur in the antirust agent is 2 percent.
The defoaming agent is DF-18 type defoaming agent, which is a three-dimensional siloxane compound.
The total base number of the trace lubricating oil is 290-310.
The embodiment also provides a preparation method of the trace lubricating oil, which comprises the following steps: weighing refined soybean oil, trihydroxy ester, an antioxidant, an antirust agent, a defoaming agent and water according to the mass percentage, and adding the antirust agent into the water to obtain a water-based part; and then mixing and stirring the refined soybean oil, the trihydroxy ester, the antioxidant and the water-based part uniformly at 50 ℃, and then adding the defoaming agent to mix and stir uniformly.
Example two
The trace lubricating oil consists of refined soybean oil in 40 wt%, trihydroxy ester in 10 wt%, antioxidant in 5 wt%, antirust in 10 wt%, defoaming agent in 0.01 wt% and water for the rest.
The refined soybean oil is prepared by mixing one or two of deodorized soybean oil and refined soybean oil.
The characteristic indexes of the trihydroxy ester are as follows: the acid value was 1.8mgKOH/g, the hydroxyl value was 15mgKOH/g, and the saponification value was 175-195 mg/g.
The antioxidant is tea polyphenols extracted from unfermented green tea.
The antirust agent is neutral synthetic calcium sulfonate, and the content of calcium in the antirust agent is 10 percent, and the content of sulfur in the antirust agent is 1 percent.
The defoaming agent is DF-18 type defoaming agent, which is a three-dimensional siloxane compound.
The total base number of the trace lubricating oil is 290-310.
The embodiment also provides a preparation method of the trace lubricating oil, which comprises the following steps: weighing refined soybean oil, trihydroxy ester, an antioxidant, an antirust agent, a defoaming agent and water according to the mass percentage, and adding the antirust agent into the water to obtain a water-based part; and then mixing and stirring the refined soybean oil, the trihydroxy ester, the antioxidant and the water-based part uniformly at 40 ℃, and then adding the defoaming agent to mix and stir uniformly.
EXAMPLE III
The trace lubricating oil consists of refined soybean oil in 50 wt%, trihydroxy ester in 20 wt%, antioxidant in 10 wt%, antirust in 18 wt%, defoaming agent in 0.05 wt% and water for the rest.
The refined soybean oil is prepared by mixing one or two of deodorized soybean oil and refined soybean oil.
The characteristic indexes of the trihydroxy ester are as follows: the acid value was 1.8mgKOH/g, the hydroxyl value was 15mgKOH/g, and the saponification value was 175-195 mg/g.
The antioxidant is tea polyphenols extracted from unfermented green tea.
The antirust agent is neutral synthetic calcium sulfonate, and the content of calcium in the antirust agent is 13 percent, and the content of sulfur in the antirust agent is 3 percent.
The defoaming agent is DF-18 type defoaming agent, which is a three-dimensional siloxane compound.
The total base number of the trace lubricating oil is 290-310.
The embodiment also provides a preparation method of the trace lubricating oil, which comprises the following steps: weighing refined soybean oil, trihydroxy ester, an antioxidant, an antirust agent, a defoaming agent and water according to the mass percentage, and adding the antirust agent into the water to obtain a water-based part; and then mixing and stirring the refined soybean oil, the trihydroxy ester, the antioxidant and the water-based part uniformly at 60 ℃, and then adding the defoaming agent to mix and stir uniformly.
Example four
As shown in fig. 1-3, the present embodiment provides a supply device for a small amount of lubricating oil, which uses a small amount of lubricating oil as a supply material, and includes a base 1, a mixing cylinder 2, a support base 3, a low-temperature gas generator 4, a cooling box 5, a gas-guide tube 7, a supply tube 8, a movable ball 9, a slot 10, a flexible hose 11 and a spray head 12, wherein the mixing cylinder 2, the support base 3, the low-temperature gas generator 4 and the cooling box 5 are fixed at the upper end of the base 1. One end of the inner cavity of the cooling box 5 is provided with an air inlet 6 which is butted with the output end of the low-temperature gas generator 4, and the other end of the inner cavity is communicated with a feeding pipe 8 led out from the mixing barrel 2 through an air duct 7. The support seat 3 is internally provided with a movable ball block 9 with an injection head 12 in a rotation limiting way, the support seat 3 is provided with a slot 10 at the rear side of the movable ball block 9, and the feeding pipe 8 is communicated with the injection head 12 through a flexible hose 11 positioned in the slot 10 after passing through the cooling box 5.
In this embodiment, the gas-guide tube 7 is provided with a one-way valve at the connection with the feeding tube 8.
In this embodiment, the support base 3 is screwed with a fastening screw 13, and the movable ball 9 can be tightly fixed by screwing the fastening screw 13 inward.
In this embodiment, the cross section of the spray head 12 is waist-shaped, and 3-5 spray ports are arranged inside the spray head.
In the embodiment, after the supply device of the trace lubricating oil replaces a cooling liquid lubricating system, a cutting liquid recovery device can be omitted; using a very small amount of lubricating oil, the amount of oil consumed is about the size of a disposable cup, calculated in 8 hours per shift; the feeding amount is increased, the workpiece processing production efficiency is improved, and the processing time is shortened by about 20-70%; the service life of the cutter is prolonged by 2-3 times, and the surface precision of the machined workpiece is improved.
The preferred embodiments of the invention disclosed above are intended to be illustrative only. The preferred embodiments are not intended to be exhaustive or to limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best utilize the invention. The invention is limited only by the claims and their full scope and equivalents.
Claims (10)
1. A trace amount of lubricating oil, characterized in that: the trace lubricating oil consists of refined soybean oil 40-50 wt%, trihydroxyester 10-20 wt%, antioxidant 5-10 wt%, antirust 10-18 wt%, defoaming 0.01-0.05 wt% and water for the rest.
2. The minimal amount of lubricating oil according to claim 1, wherein: the refined soybean oil is prepared by mixing one or two of deodorized soybean oil and refined soybean oil.
3. The minimal amount of lubricating oil according to claim 1, wherein: the characteristic indexes of the trihydroxy ester are as follows: the acid value was 1.8mgKOH/g, the hydroxyl value was 15mgKOH/g, and the saponification value was 175-195 mg/g.
4. The minimal amount of lubricating oil according to claim 1, wherein: the antioxidant is tea polyphenol extracted from unfermented green tea.
5. The minimal amount of lubricating oil according to claim 1, wherein: the antirust agent is neutral synthetic calcium sulfonate, and the content of calcium in the antirust agent is 10-13%, and the content of sulfur in the antirust agent is 1-3%.
6. The minimal amount of lubricating oil according to claim 1, wherein: the defoaming agent is DF-18 type defoaming agent which is a three-dimensional siloxane compound.
7. The minimal amount of lubricating oil according to claim 1, wherein: the total base number of the trace lubricating oil is 290-310.
8. A method for preparing the minimal quantity of lubricating oil according to any one of claims 1 to 7, characterized by comprising the steps of: weighing refined soybean oil, trihydroxy ester, an antioxidant, an antirust agent, a defoaming agent and water according to the mass percentage, and adding the antirust agent into the water to obtain a water-based part; and then mixing and stirring the refined soybean oil, the trihydroxy ester, the antioxidant and the water-based part uniformly at 40-60 ℃, and then adding the defoaming agent and mixing and stirring uniformly.
9. A trace amount lubrication oil supply apparatus fed with the trace amount lubrication oil according to any one of claims 1 to 7, characterized in that: this feeding device of trace lubricating oil includes base, mixing cylinder, supporting seat, low temperature gas generator, cooling box, air duct, feed cylinder, activity ball piece, fluting, bellows and injector head, the upper end of base is fixed with mixing cylinder, supporting seat, low temperature gas generator and cooling box, the inner chamber one end of cooling box is equipped with the air inlet with the butt joint of low temperature gas generator output, and the other end passes through the feed cylinder intercommunication that air duct and mixing cylinder draw forth, it has the activity ball piece of taking the injector head to rotate the restriction in the supporting seat, the rear side that the supporting seat is located activity ball piece is equipped with the fluting, after the feed cylinder passed the cooling box, through the bellows and the injector head intercommunication that are located in the fluting.
10. The apparatus for supplying a trace amount of lubricating oil according to claim 9, wherein: the air duct is provided with a one-way valve at the joint with the feeding pipe.
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CN112171617A (en) * | 2020-09-26 | 2021-01-05 | 李万生 | Material case for machining |
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