CN111109302A - Antimicrobial aerosol and toxicant exposure spray suspended particle spray and preparation method thereof - Google Patents
Antimicrobial aerosol and toxicant exposure spray suspended particle spray and preparation method thereof Download PDFInfo
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- CN111109302A CN111109302A CN202010109748.0A CN202010109748A CN111109302A CN 111109302 A CN111109302 A CN 111109302A CN 202010109748 A CN202010109748 A CN 202010109748A CN 111109302 A CN111109302 A CN 111109302A
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- 239000002245 particle Substances 0.000 title claims abstract description 78
- 239000007921 spray Substances 0.000 title claims abstract description 54
- 239000000443 aerosol Substances 0.000 title claims abstract description 30
- 230000000845 anti-microbial effect Effects 0.000 title claims abstract description 22
- 231100000167 toxic agent Toxicity 0.000 title claims abstract description 14
- 239000003440 toxic substance Substances 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title abstract description 6
- 239000000725 suspension Substances 0.000 claims abstract description 27
- 239000002131 composite material Substances 0.000 claims abstract description 25
- 239000000654 additive Substances 0.000 claims abstract description 24
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 18
- 244000166124 Eucalyptus globulus Species 0.000 claims abstract description 12
- 235000004692 Eucalyptus globulus Nutrition 0.000 claims abstract description 12
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 11
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 11
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 11
- 239000000661 sodium alginate Substances 0.000 claims abstract description 11
- 239000004599 antimicrobial Substances 0.000 claims abstract description 9
- 239000000463 material Substances 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 238000011049 filling Methods 0.000 claims abstract description 4
- 239000007787 solid Substances 0.000 claims abstract description 4
- 230000000996 additive effect Effects 0.000 claims description 20
- 238000009924 canning Methods 0.000 claims description 6
- 238000009826 distribution Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 238000007873 sieving Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
- KFFCKOBAHMGTMW-LGQRSHAYSA-N Forsythin Chemical compound C1=C(OC)C(OC)=CC=C1[C@H]1[C@@H](CO[C@@H]2C=3C=C(OC)C(O[C@H]4[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O4)O)=CC=3)[C@@H]2CO1 KFFCKOBAHMGTMW-LGQRSHAYSA-N 0.000 claims description 4
- JJVGFDTWFVSBIM-UHFFFAOYSA-N Phillyrin Natural products COc1ccc(cc1OC)C2OCC3C2COC3c4ccc(OC)c(OC5OC(CO)C(O)C(O)C5O)c4 JJVGFDTWFVSBIM-UHFFFAOYSA-N 0.000 claims description 4
- 239000012620 biological material Substances 0.000 claims description 4
- 230000001954 sterilising effect Effects 0.000 claims description 4
- 238000009690 centrifugal atomisation Methods 0.000 claims description 3
- 238000000151 deposition Methods 0.000 claims description 3
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 229910010272 inorganic material Inorganic materials 0.000 claims description 3
- 239000011147 inorganic material Substances 0.000 claims description 3
- 239000010954 inorganic particle Substances 0.000 claims description 3
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 3
- 239000002086 nanomaterial Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 6
- 206010035664 Pneumonia Diseases 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 4
- 210000002345 respiratory system Anatomy 0.000 abstract description 3
- 208000020061 Hand, Foot and Mouth Disease Diseases 0.000 abstract description 2
- 208000025713 Hand-foot-and-mouth disease Diseases 0.000 abstract description 2
- 206010047482 Viral upper respiratory tract infection Diseases 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000000903 blocking effect Effects 0.000 abstract description 2
- 210000004072 lung Anatomy 0.000 abstract description 2
- 210000004400 mucous membrane Anatomy 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 238000005070 sampling Methods 0.000 description 18
- 241000894006 Bacteria Species 0.000 description 5
- 241000700605 Viruses Species 0.000 description 5
- 244000005700 microbiome Species 0.000 description 5
- 230000009471 action Effects 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 3
- 230000000840 anti-viral effect Effects 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
- 241000711573 Coronaviridae Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 241000195493 Cryptophyta Species 0.000 description 1
- 241000576429 Forsythia suspensa Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000219926 Myrtaceae Species 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 235000011869 dried fruits Nutrition 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 206010022000 influenza Diseases 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 208000030194 mouth disease Diseases 0.000 description 1
- 229920005615 natural polymer Polymers 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
- A01N25/06—Aerosols
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/08—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing solids as carriers or diluents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
Abstract
The invention provides an antimicrobial aerosol and toxicant exposure spray suspended particle, which utilizes supercritical CO2The solid suspension particle spray is obtained by introducing a composite nano-additive flow aid into the phillylphenol, eucalyptus globulus and sodium alginate disinfection main body suspension particles and rapidly expanding the mixture, and the invention has the beneficial effects that: the antimicrobial aerosol and toxicant-exposure spray suspension particle prepared by the preparation process and the method are applied to human bodiesThe product has no toxicity (the traditional Chinese medicine type disinfection material which is already produced in quantity is purchased and used as the main body of the disinfection suspension particles), has the effects of preventing viral upper respiratory tract infection, new crown pneumonia and hand-foot-and-mouth disease, and blocking harmful substances in the air from being absorbed through respiratory tract mucous membranes and lungs, adopts a manual pump spray bottle, and has the advantages of simple filling, low cost and convenient use.
Description
[ technical field ] A method for producing a semiconductor device
The invention relates to the technical field of antimicrobial compounds or compositions thereof, in particular to an antimicrobial aerosol and toxicant-exposure spray suspended particles and a preparation method thereof.
Air contains a large amount of nitrogen oxides, aerosols and respirable particles, and a large number of harmful particles spread in the air stream and human stream, which may lead to further proliferation of a large number of viruses, bacteria and fungi in the attached particles. New coronary pneumonia, influenza and hand-foot-mouth disease are mostly affected through respiratory tract. The spread of the aerosol and the contamination droplets of the microorganisms in the atmosphere is very harmful and difficult to control, and the disease of some severe patients develops quickly, even the virus can spread in a contact way. The existing mask cannot be used in the processes of eating and sleeping and has antiviral and bactericidal effects in the air.
[ summary of the invention ]
The invention aims to provide a novel antimicrobial aerosol and toxicant spray suspension particle spray and a preparation method thereof, wherein the existing disinfectant mainly disinfects the surface of a general object by a liquid method, and aims at the defects of insufficient technologies of microbial aerosol and toxicant spray due to the problem of liquid sedimentation.
The invention is realized by the following technical scheme:
an antimicrobial aerosol and toxicant-exposure spray suspension granule is prepared by introducing composite nanometer additive glidant into supercritical CO2 and phillyrin, eucalyptus globulus and sodium alginate to sterilize main suspension granules, and rapidly expanding to obtain solid suspension spray.
Further, the antimicrobial aerosol and the toxicant-exposure spray suspended particle are composed of the following components in percentage by weight:
and (3) forsythol: 6 percent of
Eucalyptus globulus Labill: 3 percent of
Sodium alginate: 0.3 percent of
The composite nano additive comprises: and (4) the balance.
Furthermore, the particle size of the suspended particles is 10-15 μm, the particle size distribution is uniform, and the geometric structure is uniform.
Further, the particle size of the composite nano additive is less than 1 μm.
Further, the composite nano additive is a montmorillonite inorganic material.
A method for preparing an antimicrobial aerosol and toxicant spray suspension particle spray, comprising the steps of:
s1, firstly, preparing the composite nano additive with the particle size less than 1 mu m for later use;
s2, mixing phillyrin, eucalyptus globulus and sodium alginate uniformly;
s3, mixing the materials in the step S2 uniformly, introducing the mixture into the composite nano additive by an air classification ACM grinding, cold crushing, numerical control feeding speed fine crushing, C-grade sieving, quick expansion, wind sieving separation and deposition method to prepare suspension particle spray;
s4, filtering the suspended particle spray prepared in the step S3 through a special bag;
s5, filtering the special bag in the step S4, and then quantitatively filling the special bag into a spray bottle through canning equipment to form suspended particle spray;
and S6, finally, canning the suspended particle spray in a spray bottle to obtain a finished product.
Further, the composite nano additive in step S1 is prepared by activating and slowly releasing a biological material system with supercritical CO2 and Bi particles, heating at a temperature, accelerating centrifugal atomization drying, and removing the nano material attached to the surface of the inorganic particles.
The invention has the beneficial effects that: the antimicrobial aerosol and the contamination spray suspension particle spray prepared by the preparation process and the method are nontoxic to human bodies (the purchased and used traditional Chinese medicine type disinfection materials in mass production are taken as main bodies of the disinfection suspension particles), have the effects of preventing viral upper respiratory tract infection, new crown pneumonia and hand-foot-and-mouth disease, and blocking harmful substances in the air from being absorbed through respiratory tract mucous membranes and lungs, and are simple to fill, low in cost and convenient to use by adopting a manual pump spray bottle.
[ detailed description ] embodiments
The invention is further described below with reference to specific embodiments:
example 1:
an antimicrobial aerosol and toxicant-exposure spray suspension, using supercritical CO2And introducing a composite nano-additive flow aid into the phillylphenol, eucalyptus globulus and sodium alginate mixed sterilization main body suspension particles, and rapidly expanding to obtain the solid suspension particle spray.
Further, the antimicrobial aerosol and the toxicant-exposure spray suspended particle are composed of the following components in percentage by weight:
and (3) forsythol: 6 percent of
Eucalyptus globulus Labill: 3 percent of
Sodium alginate: 0.3 percent of
The composite nano additive comprises: the balance;
further, the forsythia suspensa powder is obtained by extracting dried fruits of forsythiasusapona (Thunb.) Vakl, a plant of the family of trifoliaceae, (purchased from a Chinese medicine factory in Jiangxi);
eucalyptus globulus Labill, which is extracted from dried leaves of Eucalyptus globulus Labill, a plant of Myrtaceae (purchased from Chinese medicine factories in Jiangxi province);
sodium alginate is a natural polymer compound, and is extracted from algae organisms (purchased from Shenzhen Chinese medicinal institute);
raw materials for composite nano-additive manufacturing, (partially purchased from canada and chinese particle technology collaboration).
Furthermore, the suspended particles have the particle size of 10 microns, are uniform in particle size distribution and uniform in geometric structure, and are characterized in that the interaction force among the particles is far higher than the gravity of the particles, and the suspended particles are extremely easy to adhere to microbial aerosol and toxicant droplets in air to form agglomeration.
In a room, the sterilizing suspended particles with the particle size of 10 mu m are optimally distributed and concentrated within 60 seconds, trace sterilizing suspended particles can still be detected within 48 hours, and an FA-1 impact type air microorganism sampler is adopted; the sampling flow is 30L/min, a point is arranged at the center of the room and 1m away from the ground for sampling, the sampling is carried out when the disinfection action time is 0min and 60min, the sampling time of the control group sampler is 5s and 5s respectively, the sampling time of the experimental group sampler is 5s and 1min respectively, the number of viable bacteria stored at different time is measured after sampling, and the killing rate of 3 times of experiments is more than 98.3 percent.
Further, the particle size of the composite nano additive is less than 1 μm.
Further, the composite nano additive is a montmorillonite inorganic material.
A method for preparing an antimicrobial aerosol and toxicant spray suspension particle spray, comprising the steps of:
s1, firstly, preparing the composite nano additive with the particle size less than 1 mu m for later use;
s2, mixing phillyrin, eucalyptus globulus and sodium alginate uniformly;
s3, mixing the materials in the step S2 uniformly, introducing the mixture into the composite nano additive by an air classification ACM grinding, cold crushing, numerical control feeding speed fine crushing, C-grade sieving, quick expansion, wind sieving separation and deposition method to prepare suspension particle spray;
s4, filtering the suspended particle spray prepared in the step S3 through a special bag;
s5, filtering the special bag in the step S4, and then quantitatively filling the special bag into a spray bottle through canning equipment to form suspended particle spray;
and S6, finally, canning the suspended particle spray in a spray bottle to obtain a finished product.
Further, the composite nano additive in step S1 is prepared by activating and slowly releasing a biological material system with supercritical CO2 and Bi particles, heating at a temperature, accelerating centrifugal atomization drying, and removing the nano material attached to the surface of the inorganic particles.
Example 2
Preferably, when the particle size of the suspended particles is 13 microns, the particle size distribution is uniform, the geometric structure is uniform, and the suspended particle disinfection suspended particles are sprayed in the air, can float away from the original area of the suspended particle disinfection suspended particles due to wind direction and wind speed, and can be diffused to the position 1km downwind to keep the viscosity of the suspended particle disinfection suspended particles;
in a room, the distribution concentration of the disinfection suspended particles with the particle size of 15 mu m is optimal within 60 seconds, and trace disinfection suspended particles can still be detected within 48 hours, and an FA-1 impact type air microorganism sampler is adopted; the sampling flow is 30L/min, a point is arranged at the center of the room and 1.5m away from the ground for sampling, the sampling is carried out when the disinfection action time is 0min and 60min, the sampling time of the control group sampler is 5s and 5s respectively, the sampling time of the experimental group sampler is 5s and 1min respectively, the number of viable bacteria stored at different time is measured after sampling, and the killing rate of 3 times of experiments is more than 98.6 percent.
Example 3
In a room, when the distribution concentration of the disinfection suspended particles with the particle size of 15 mu m is optimal within 60 seconds, trace disinfection suspended particles can still be detected within 48 hours, and an FA-1 impact type air microorganism sampler is adopted; the sampling flow is 50L/min, a point is arranged at the center of the room and 4.5m away from the ground for sampling, the sampling is carried out when the disinfection action time is 0min and 60min, the sampling time of the control group sampler is 5s and 5s respectively, the sampling time of the experimental group sampler is 5s and 1min respectively, the number of viable bacteria stored at different time is measured after sampling, and the killing rate of 3 times of experiments is more than 98.8 percent.
In the above-mentioned examples, in order to verify whether the antimicrobial aerosol and the contamination spray suspension particle spray of the present invention achieve the expected invention effect, the antiviral and antibacterial test was performed on the harmful microorganism aerosol, virus and bacteria resistant spray powder of the present invention, and the results of the antiviral and antibacterial rates were as follows:
note that, the test of the disinfection and bacteriostasis rate is only performed on common viruses and germs, and the invention aims at the new coronavirus, and the pneumonia virus sample is not obtained. According to the data and the effect of the above embodiments, all can kill the new coronavirus in the air.
Appropriate changes and modifications to the embodiments described above will become apparent to those skilled in the art from the disclosure and teachings of the foregoing description. Therefore, the present invention is not limited to the specific embodiments disclosed and described above, and some modifications and variations of the present invention should fall within the scope of the claims of the present invention. Furthermore, although specific terms are employed herein, they are used in a generic and descriptive sense only and not for purposes of limitation.
Claims (7)
1. An antimicrobial aerosol and toxicant-exposure spray of suspended particles, characterized in that: by using supercritical CO2And introducing a composite nano-additive flow aid into the phillylphenol, eucalyptus globulus and sodium alginate mixed sterilization main body suspension particles, and rapidly expanding to obtain the solid suspension particle spray.
2. The antimicrobial aerosol and toxicant spray aerosol suspension of claim 1, wherein: the composite material comprises the following components in percentage by weight:
and (3) forsythol: 6 percent of
Eucalyptus globulus Labill: 3 percent of
Sodium alginate: 0.3 percent of
The composite nano additive comprises: and (4) the balance.
3. The antimicrobial aerosol and toxicant spray aerosol suspension of claim 1, wherein: the particle size of the suspended particles is 10-15 mu m, the particle size distribution is uniform, and the geometric structure is uniform.
4. The antimicrobial aerosol and toxicant spray aerosol suspension of claim 2, wherein: the particle size of the composite nano additive is less than 1 mu m.
5. The antimicrobial aerosol and toxicant spray aerosol suspension of claim 2, wherein: the composite nano additive is a montmorillonite inorganic material.
6. The method of making an antimicrobial aerosol and toxicant spray suspension of particles of claim 1, comprising the steps of:
s1, firstly, preparing the composite nano additive with the particle size less than 1 mu m for later use;
s2, mixing phillyrin, eucalyptus globulus and sodium alginate uniformly;
s3, mixing the materials in the step S2 uniformly, introducing the mixture into the composite nano additive by an air classification ACM grinding, cold crushing, numerical control feeding speed fine crushing, C-grade sieving, quick expansion, wind sieving separation and deposition method to prepare suspension particle spray;
s4, filtering the suspended particle spray prepared in the step S3 through a special bag;
s5, filtering the special bag in the step S4, and then quantitatively filling the special bag into a spray bottle through canning equipment to form suspended particle spray;
and S6, finally, canning the suspended particle spray in a spray bottle to obtain a finished product.
7. The method of making an antimicrobial aerosol and toxicant spray suspension of particles of claim 6, wherein: the composite nano additive in the step S1 is prepared by using supercritical CO2The Bi particles are utilized to activate and slowly release a biological material system, then the biological material system is heated at a temperature, and then the nano material with the formula attached to the surfaces of the inorganic particles is removed by accelerated centrifugal atomization drying, so that the composite nano additive is obtained.
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Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040116551A1 (en) * | 1999-12-15 | 2004-06-17 | Terry Richard N. | Antimicrobial compositions containing colloids of oligodynamic metals |
| CN1879705A (en) * | 2006-05-10 | 2006-12-20 | 上海玉森新药开发有限公司 | Medicine having anti-bacterial anti-viral functions and formulation thereof |
| CN101491243A (en) * | 2009-03-05 | 2009-07-29 | 黄安宏 | Preparation method of room air virus pathogenic-bacteria jinx |
| CN102895316A (en) * | 2012-10-23 | 2013-01-30 | 深圳市英杰汇生物科技有限公司 | Face cleanser for treating and preventing acne and preparation method thereof |
| CN103461394A (en) * | 2007-12-14 | 2013-12-25 | 永正顾问有限公司 | Air refreshing disinfectant |
| CN104225651A (en) * | 2014-08-26 | 2014-12-24 | 赵兰 | Air freshener for preventing influenza and preparation method thereof |
| CN105052917A (en) * | 2015-08-14 | 2015-11-18 | 湖南新南方养殖服务有限公司 | Dry powder modified disinfection agent |
| CN106234355A (en) * | 2016-07-28 | 2016-12-21 | 东莞市雄林新材料科技股份有限公司 | A kind of organic-inorganic nano antibacterial and preparation method thereof |
| CN106386876A (en) * | 2016-08-31 | 2017-02-15 | 苏州华泰空气过滤器有限公司 | Air disinfectant and preparation method thereof |
| KR20190058851A (en) * | 2017-11-22 | 2019-05-30 | 오순지 | Environment friendly Hygiene Composition effectively comprising natural plant extract |
-
2020
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Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040116551A1 (en) * | 1999-12-15 | 2004-06-17 | Terry Richard N. | Antimicrobial compositions containing colloids of oligodynamic metals |
| CN1879705A (en) * | 2006-05-10 | 2006-12-20 | 上海玉森新药开发有限公司 | Medicine having anti-bacterial anti-viral functions and formulation thereof |
| CN103461394A (en) * | 2007-12-14 | 2013-12-25 | 永正顾问有限公司 | Air refreshing disinfectant |
| CN101491243A (en) * | 2009-03-05 | 2009-07-29 | 黄安宏 | Preparation method of room air virus pathogenic-bacteria jinx |
| CN102895316A (en) * | 2012-10-23 | 2013-01-30 | 深圳市英杰汇生物科技有限公司 | Face cleanser for treating and preventing acne and preparation method thereof |
| CN104225651A (en) * | 2014-08-26 | 2014-12-24 | 赵兰 | Air freshener for preventing influenza and preparation method thereof |
| CN105052917A (en) * | 2015-08-14 | 2015-11-18 | 湖南新南方养殖服务有限公司 | Dry powder modified disinfection agent |
| CN106234355A (en) * | 2016-07-28 | 2016-12-21 | 东莞市雄林新材料科技股份有限公司 | A kind of organic-inorganic nano antibacterial and preparation method thereof |
| CN106386876A (en) * | 2016-08-31 | 2017-02-15 | 苏州华泰空气过滤器有限公司 | Air disinfectant and preparation method thereof |
| KR20190058851A (en) * | 2017-11-22 | 2019-05-30 | 오순지 | Environment friendly Hygiene Composition effectively comprising natural plant extract |
Non-Patent Citations (3)
| Title |
|---|
| 吴晓球 主编: "《实用内科医师处方手册》", 31 March 2005, 科学技术文献出版社 * |
| 牟涛 等著: "《绿色化学》", 30 June 2018, 天津科学技术出版社 * |
| 王慧琴 等主编: "《实用消毒剂生产技术与使用方法》", 31 October 2006, 江西科学技术出版社 * |
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| CN111109302B (en) | 2021-04-06 |
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