CN111096943A - Shampoo composition with anti-dandruff effect and preparation method and application thereof - Google Patents
Shampoo composition with anti-dandruff effect and preparation method and application thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention belongs to the field of cosmetics, and particularly relates to a shampoo composition with an anti-dandruff effect and a preparation method thereof, wherein the shampoo composition comprises 1-3 parts by weight of sodium hyaluronate, 0.1-0.5 part by weight of guar gum, 0.3-1 part by weight of piroctone olamine, 0.1-0.5 part by weight of oat kernel extract and 0.5-1.5 parts by weight of calendula extract. This patent is mainly through piroctone olamine salt restraines malassezia's growth, reduces the production of dandruff, and sodium hyaluronate this kind is similar with human skin stratum corneum constitutional structure again, and the higher moisturizing factor of affinity brings abundant moist sense for the skin. And finally, oat kernel extract and calendula extract with antibacterial and anti-inflammatory effects are added to strengthen the anti-allergy of the sebum membrane and reduce the stimulation and invasion of the external environment to the skin.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a shampoo composition with an anti-dandruff effect and a preparation method thereof.
Background
Dandruff is a phenomenon of massive desquamation caused by excessive proliferation of scalp keratinocytes. According to the statistics of the Ministry of health, about 60 percent of adults in China suffer from the scurf problem in different degrees, and 15 percent of people have serious symptoms. At present, the anti-dandruff shampoo accounts for more than 35 percent of the total amount of the shampoo, however, 70 percent of people using the anti-dandruff product consider the effect not ideal. The dandruff removing agents such as salicylic acid and tar which are commonly used in the early stage rapidly achieve the purpose of reducing dandruff by removing cutin and inhibiting excessive keratinocyte proliferation, but the dandruff removing agents can not treat symptoms and root causes, and can also damage the epidermal structure, disturb the self-balance of the epidermis, generate symptoms such as allergic pruritus and the like after long-term use. An antidandruff agent such as selenium disulphide, which is a cytostatic agent, is mainly capable of reducing the rate of replacement of the cells of the stratum corneum, and the normal physiological processes of keratinization and desquamation improve as the length of the regeneration cycle of the cells is restored. However, many clinical experiments show that the medicine can not well control the clinical symptoms of the dandruff. Moreover, the main components of the shampoo have strong irritation, the hair feels coarse after use, if the shampoo is not thoroughly rinsed, the hair may be decolorized, and a small part of users have hair loss.
Disclosure of Invention
The invention aims to provide a shampoo composition with anti-dandruff effect and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
a shampoo composition with anti-dandruff effect comprises sodium hyaluronate, guar gum, piroctone olamine salt, oat kernel extract and calendula extract, and comprises 1-3 parts by weight of sodium hyaluronate and 0.1-0.5 part by weight of guar gum; 0.3-1 part of piroctone olamine salt, 0.1-0.5 part of oat kernel extract and 0.5-1.5 parts of calendula extract.
Preferably, the feed comprises 1 part of sodium hyaluronate, 0.2 part of guar gum, 0.5 part of piroctone olamine salt, 0.2 part of oat kernel extract and 0.5 part of calendula extract.
The mass content of the washing composition in the cosmetics is 6-15%. The cosmetic is prepared by the following method:
(1) weighing deionized water, a surfactant, a chelating agent and a rheological modifier, adding the deionized water, the surfactant, the chelating agent and the rheological modifier into a reaction kettle, starting stirring, adjusting the revolution of a scraper stirrer to 60 revolutions per minute, starting a heating switch, controlling the temperature to be 70-80 ℃, stirring until the raw materials are completely dissolved, and then cooling;
(2) cooling to 45-55 deg.C, adding washing composition, essence, antiseptic, and pH regulator, stirring, stopping stirring, breaking vacuum, sampling, testing, and discharging;
(3) standing for 24 hours, and filling when the temperature is lower than 38 ℃.
Wherein, the dosage of the washing composition is 3-5%; the surfactant is one or any combination of sodium laureth sulfate, sodium cocoyl methyl taurate, sodium cocoamidopropionate, sodium lauroyl sarcosinate, sodium lauroamphoacetate, cocamidopropyl betaine, lauryl hydroxy sulfobetaine and decyl glucoside, the dosage is 5-30%, and the chelating agent is disodium EDTA, the dosage is 0.1%; the rheology modifier is one or any combination of PEG-120 methyl glucose dioleate, distearyl polyether-5 lauroyl glutamate and cocamide MEA, and the dosage is 1-4%; the amount of the essence is 0.2-0.5%; the preservative is one or any combination of bronopol, phenoxyethanol, methyl paraben and sodium benzoate, and the dosage of the preservative is 0.6-1.0%.
The cosmetic is transparent shampoo.
The application also comprises a preparation method of the shampoo composition with the anti-dandruff effect, which is characterized in that: the preparation method comprises the following specific steps:
(1) weighing sodium hyaluronate, guar gum, piroctone olamine salt, oat kernel extract and calendula flower extract as raw materials according to formula amount;
(2) mixing sodium hyaluronate, guar gum, piroctone olamine salt, herba Avenae Fatuae kernel extract, and herba Sidae Rhombifoliae extract uniformly.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, sodium hyaluronate, guar gum and piroctone olamine are creatively combined, wherein the sodium hyaluronate and the guar gum can form a complex to cover the surface of scalp, the piroctone olamine uniformly fills the gap of the complex and is tightly adsorbed on the surface of the complex, so that the complex is fully contacted with scalp and can not be easily washed off even being washed by water, and the piroctone olamine can inhibit the growth of malassezia, thereby reducing the generation of dandruff.
Meanwhile, the mass ratio of the sodium hyaluronate to the guar gum is selected, so that the sodium hyaluronate is complexed with the guar gum, the water locking property of the sodium hyaluronate is kept, the water which is 500-fold of the self weight can be locked at most, the root cause of dandruff generation is that the scalp ecological balance is damaged, and when the environment of scalp flora is unbalanced, a large amount of harmful bacteria are bred, and the scalp itching phenomenon can occur; the stratum corneum of the scalp is metabolized too quickly and falls off to form dandruff. The purpose of the stratum corneum is to form a barrier consisting of keratinocytes and intercellular lipids, the keratinocytes containing horizontally aligned keratins, which can contain large amounts of water in the cells, enhancing the skin's moisturization and thus improving the desquamation of the scalp. Meanwhile, the complexation of the sodium hyaluronate and the guar gum enables the hyaluronic acid to have higher affinity and adsorbability. The shampoo is matched with some anti-dandruff components to be used in a shampoo product, the flocculation capacity of hair in a cleaning process can be further enhanced, when the shampoo is diluted in a using process, unstable polymers can appear and act on scalp and hair in a coagulation, precipitation and deposition method, after emulsion breaking, the anti-dandruff agent is wrapped in a coagulation body and deposited on the scalp when flocculation occurs, and the effect is achieved.
Oat kernel extract: the main effective component is oat alkaloid, which is a polyphenol alkaloid existing in oat kernel. Research proves that the oat alkaloid has quick anti-allergy, anti-stimulation and itching-relieving activities. Skin inflammation is a complex process of self-protective immune response of the human body against external antigens (cell damage, infection, pathogens). The immune response is controlled by the production of cytokines by inflammatory cells. The expression of cytokines is regulated by the nuclear transcription factor Kappa B (NF-. kappa.B). Many studies have shown that avenanthramides can effectively reduce the production of proinflammatory cytokines IL-6, IL-8 and MCP-1 to inhibit the activation of NF-kappa B, thereby inhibiting the activated expression of inflammatory response genes. The avenanthramides also have potent antihistamine activity and are effective in reducing itching and erythema.
Calendula extract: contains active ingredients such as saponin, brass (especially quercetin-3-O-glucoside), triterpenes and carotene, has antibacterial, antiinflammatory (especially good effect on staphylococci and streptococcus), irritation relieving, and wound healing promoting effects, and can be added into cosmetics for sensitive and/or irritant skin to enhance the anti-allergy of sebum membrane and protect skin from irritation and invasion of external environment.
This patent is mainly through piroctone olamine salt restraines malassezia's growth, reduces the production of dandruff, and sodium hyaluronate this kind is similar with human skin stratum corneum constitutional structure again, and the higher moisturizing factor of affinity brings abundant moist sense for the skin. And finally, oat kernel extract and calendula extract with antibacterial and anti-inflammatory effects are added to strengthen the anti-allergy of the sebum membrane and reduce the stimulation and invasion of the external environment to the skin. Therefore, the components of the washing composition have synergistic effect, the dandruff is reduced, the effect is more obvious and lasting, the washing composition has good storage stability, and the washing composition can also play roles in regulating water and oil balance and maintaining scalp.
Description of the drawings:
FIG. 1 is a graph showing typical effects of the sample group and the control groups 1 and 2;
FIG. 2 is a graph showing the inhibitory effect of a detergent composition on malassezia.
Detailed Description
In order to make the technical solutions of the present invention better understood by those skilled in the art, the present invention will be further described in detail with reference to the accompanying drawings and preferred embodiments.
Example 1
A washing composition with anti-dandruff effect comprises sodium hyaluronate, piroctone olamine salt, oat kernel extract and calendula officinalis flower extract, wherein the sodium hyaluronate is 1 part, the guar gum is 0.2 part, the piroctone olamine salt is 0.5 part, the oat kernel extract is 0.2 part and the calendula officinalis flower extract is 0.5 part.
The preparation method of the washing composition with the anti-dandruff effect comprises the following specific preparation steps:
(1) weighing sodium hyaluronate, guar gum, piroctone olamine salt, oat kernel extract and calendula flower extract as raw materials according to formula amount;
(2) mixing sodium hyaluronate, guar gum, piroctone olamine salt, herba Avenae Fatuae kernel extract, and herba Sidae Rhombifoliae extract uniformly.
Example 2
A lotion composition with anti-dandruff effect comprises sodium hyaluronate, piroctone olamine salt, oat kernel extract and calendula officinalis flower extract, wherein the sodium hyaluronate is 1 part, the guar gum is 0.5 part, the piroctone olamine salt is 0.5 part, the oat kernel extract is 0.3 part and the calendula officinalis flower extract is 0.5 part.
The preparation method is the same as example 1.
Example 3
A washing composition with anti-dandruff effect comprises sodium hyaluronate, piroctone olamine salt, oat kernel extract and calendula officinalis flower extract, wherein the sodium hyaluronate is 1.5 parts, guar gum is 0.1 part, the piroctone olamine salt is 1 part, the oat kernel extract is 0.3 part, and the calendula officinalis flower extract is 0.8 part.
The function of the composition described in example 1 was determined.
The principle of the washing composition in a malassezia bacteriostasis test is as follows: malassezia on the scalp breaks down triglycerides in sebum by releasing lipases, which initiate hydrolysis of triglycerides to produce unsaturated fatty acids, which disrupt the scalp barrier, the stratum corneum, causing the unsaturated fatty acids to infiltrate into the epidermis, stimulating the skin to produce an inflammatory response. Thereby causing problems such as excessive proliferation of scalp keratinocytes or incomplete keratinization. Whether the washing composition has the effect of reducing dandruff is reflected by an inhibition test of the washing composition on malassezia.
The method comprises the following steps:
(1) respectively placing 0, 1ml, 2ml, 3ml, 4ml and 5ml of the washing composition in a medicine bottle, supplementing 10ml with distilled water, shaking
(2) Olive oil medium: 10g of peptone, 40ml of glucose, 0.1g of yeast extract, 2.5g of glycerol monostearate, 802.0 ml of tween-40 g, 40g of olive oil, 18g of agar and 1L of water, and sterilizing at 121 ℃ for 40min
(3) Coating: a sample is provided with 3 parallel control groups, each culture medium is marked and numbered, diluted bacteria liquid is used for coating, the sterilization of the tool is noticed during coating, and the steps are repeated for 5 times
(4) Paster filter paper: pasting the patch on the corresponding culture medium corresponding to the serial number
(5) Culturing: culturing at 34 deg.C for 72 hr, observing thallus growth condition every day, and determining whether thallus growth control growth is good
(6) And (4) interpretation of results: the growth of the thalli is observed by naked eyes to be good compared with the growth of the thalli in the control hole, the growth of the thalli is not inhibited, the growth of the aseptic colony is inhibited, and the size of the inhibition zone is measured by a vernier caliper. The results are shown in FIG. 2.
According to the test results, the following results are obtained: 1-5% of the washing composition has an inhibiting effect on malassezia, and the inhibiting effect on the malassezia is more obvious along with the increase of the mass fraction of the washing composition.
(Chinese cosmetic hygiene Specification (2015 edition) maximum allowable addition amount of piroctone olamine salt in rinsing hair products is 1%, so 5% is selected as upper limit in efficacy test of rinsing composition)
Clinical trials of lotion compositions
(1) Sample group: shampoo prepared in Experimental example 1
(2) Control group 1: experimental example 1 shampoo prepared without addition of piroctone olamine salt
(2) Control group 2: adding shampoo prepared by removing guar gum.
The test method comprises the following steps: 30 volunteers were evenly divided into three groups-two control groups and test groups, and shampooed every two days for eight times for a total of eight times to compare the anti-dandruff effect of the control products and the test products. Wherein, figure 1 shows a typical usage effect chart of the sample group and the control groups 1 and 2.
According to the clinical application test results, a reduction in dandruff intensity was detectable in 100% of the volunteers. Wherein 83% of volunteers were able to perceive a significant reduction in the total amount of dandruff and 92% of volunteers agreed to the anti-dandruff effect of the product.
The preparation method is the same as example 1.
The technical purpose can be still achieved by increasing or reducing the dosage of each component in the above examples 1-3 in equal proportion, and the invention belongs to the protection scope of the invention.
Application example 1
A shampoo was prepared using the shampoo composition having anti-dandruff effect described in example 1, and the components of the shampoo are shown in table 1. The preparation steps are as follows:
adding the raw materials in the phase A into a reaction kettle, starting stirring, adjusting the revolution of a scraper stirrer to 60 revolutions per minute, starting a heating switch, controlling the temperature to be 70-80 ℃, stirring until the raw materials are completely dissolved, and then cooling. Cooling to 45-55 deg.C, adding B phase raw material, stirring for 30 min, stopping stirring, breaking vacuum, sampling, testing, and discharging. Standing for 24 hours, and filling when the temperature is lower than 38 ℃.
TABLE 1
Application example 2
Shampoos were prepared using the anti-dandruff shampoo compositions described in example 1, and the shampoo compositions are shown in table 2. The preparation steps are as follows:
adding the raw materials in the phase A into a reaction kettle, starting stirring, adjusting the revolution of a scraper stirrer to 60 revolutions per minute, starting a heating switch, controlling the temperature to be 70-80 ℃, stirring until the raw materials are completely dissolved, and then cooling. Cooling to 45-55 deg.C, adding B phase raw material, stirring, adding C phase raw material, stirring for 30 min, stopping stirring, breaking vacuum, sampling, testing, and discharging. Standing for 24 hours, and filling when the temperature is lower than 38 ℃.
TABLE 2
Application example 3
Shampoos were prepared using the antidandruff shampoo composition described in example 1, and the shampoo compositions are shown in table 3.
The preparation steps are as follows:
adding the raw materials in the phase A into a reaction kettle, starting stirring, adjusting the revolution of a scraper stirrer to 60 revolutions per minute, starting a heating switch, controlling the temperature to be 70-80 ℃, stirring until the raw materials are completely dissolved, and then cooling. Cooling to 45-55 deg.C, adding B phase raw material, stirring for 30 min, stopping stirring, breaking vacuum, sampling, testing, and discharging. Standing for 24 hours, and filling when the temperature is lower than 38 ℃.
TABLE 3
The above detailed description of the shampoo composition with anti-dandruff effect and the preparation method thereof with reference to the examples is illustrative and not restrictive, and several examples are listed according to the limited scope, so that variations and modifications without departing from the general concept of the present invention shall fall within the protection scope of the present invention.
The above description is only a preferred embodiment of the present invention, and for those skilled in the art, the present invention should not be limited by the description of the present invention, which should be interpreted as a limitation.
Claims (7)
1. A shampoo composition with an anti-dandruff effect is characterized by comprising 1-3 parts by weight of sodium hyaluronate, 0.1-0.5 part by weight of guar gum, 0.3-1 part by weight of piroctone olamine, 0.1-0.5 part by weight of oat kernel extract and 0.5-1.5 parts by weight of calendula extract.
2. Shampoo composition with anti-dandruff effect according to claim 1, characterized in that: the composition comprises 1 part of sodium hyaluronate, 0.2 part of guar gum, 0.5 part of piroctone olamine salt, 0.2 part of oat kernel extract and 0.5 part of calendula extract in parts by weight.
3. Shampoo composition with anti-dandruff effect according to claim 1, characterized in that: the mass content of the washing composition in the cosmetics is 6-15%.
4. Shampoo composition with anti-dandruff effect according to claim 3, characterized in that: the cosmetic is transparent shampoo.
5. A method for preparing a shampoo composition with anti-dandruff effect according to any one of claims 1 to 4, characterized in that: the preparation method comprises the following specific steps:
(1) weighing sodium hyaluronate, guar gum, piroctone olamine salt, oat kernel extract and calendula flower extract as raw materials according to formula amount;
(2) mixing sodium hyaluronate, guar gum, piroctone olamine salt, herba Avenae Fatuae kernel extract, and herba Sidae Rhombifoliae extract uniformly.
6. Use of a shampoo composition with anti-dandruff effect according to any one of claims 1 to 4, wherein the shampoo is prepared by the following process:
(1) weighing deionized water, a surfactant, a chelating agent and a rheological modifier, adding the deionized water, the surfactant, the chelating agent and the rheological modifier into a reaction kettle, starting stirring, adjusting the revolution of a scraper stirrer to 60 revolutions per minute, starting a heating switch, controlling the temperature to be 70-80 ℃, stirring until the raw materials are completely dissolved, and then cooling;
(2) cooling to 45-55 deg.C, adding the washing composition, essence, antiseptic, and pH regulator, stirring, breaking vacuum, sampling, testing, and discharging;
(3) standing for 24 hours, and filling when the temperature is lower than 38 ℃.
7. Use of a shampoo composition with anti-dandruff effect according to claim 6, characterized in that: the dosage of the washing composition is 3-5%; the surfactant is one or any combination of sodium laureth sulfate, sodium cocoyl methyl taurate, sodium cocoamidopropionate, sodium lauroyl sarcosinate, sodium lauroamphoacetate, cocamidopropyl betaine, lauryl hydroxy sulfobetaine and decyl glucoside, the dosage is 5-30%, and the chelating agent is disodium EDTA, the dosage is 0.1%; the rheology modifier is one or any combination of PEG-120 methyl glucose dioleate, distearyl polyether-5 lauroyl glutamate and cocamide MEA, and the dosage is 1-4%; the amount of the essence is 0.2-0.5%; the preservative is one or any combination of bronopol, phenoxyethanol, methyl paraben and sodium benzoate, and the dosage of the preservative is 0.6-1.0%.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112999138A (en) * | 2021-03-19 | 2021-06-22 | 河南董欣生物科技有限公司 | Plant dandruff-removing and itching-relieving composition, plant dandruff-removing and itching-relieving shampoo and preparation method thereof |
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