CN111000783A - Whitening, relieving and anti-aging essence and preparation method thereof - Google Patents

Whitening, relieving and anti-aging essence and preparation method thereof Download PDF

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CN111000783A
CN111000783A CN202010008978.8A CN202010008978A CN111000783A CN 111000783 A CN111000783 A CN 111000783A CN 202010008978 A CN202010008978 A CN 202010008978A CN 111000783 A CN111000783 A CN 111000783A
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parts
whitening
extract
essence
mixture
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CN111000783B (en
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彭燕辉
贺秋平
许晓煌
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Peng Shi (huizhou) Industrial Development Co Ltd
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Peng Shi (huizhou) Industrial Development Co Ltd
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/673Vitamin B group
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    • A61K8/89Polysiloxanes
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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Abstract

The invention discloses whitening, relieving and anti-aging essence and a preparation method thereof, and relates to the field of skin care products. The whitening, relieving and anti-aging essence comprises the following components in parts by weight: 1.25-1.95 parts of emulsifier, 4.8-7.1 parts of emollient, 3.18-5.32 parts of thickener, 8.05-11.11 parts of humectant, 1.2-1.8 parts of skin conditioner, 1.13-1.67 parts of preservative, 2.74-5.08 parts of whitening anti-aging agent, 0.15-0.25 part of essence, 0.078-0.136 part of pH regulator and the balance of water, wherein the total weight part is 100; the emollient comprises refreshing oil and solid ester, and the skin conditioner comprises hydrolyzed sclerotium rolfsii gum, herba Dendrobii extract and stigma croci Sativi extract. The whitening, soothing and anti-aging essence disclosed by the invention is good in use texture and good in whitening, soothing and anti-allergy and anti-aging effects.

Description

Whitening, relieving and anti-aging essence and preparation method thereof
Technical Field
The invention relates to the field of skin care products, and in particular relates to whitening, soothing and anti-aging essence and a preparation method thereof.
Background
"A white covering clown", countless oriental women all dreams to have healthy, snow white and flawless skin. The skin pigmentation is regulated by more than 120 genes, and is mainly dependent on the mutual influence of melanocytes in an epidermal basal layer and cell tissues adjacent to the melanocytes, so that the synthesis, the transportation and the metabolism of the melanin are jointly regulated, wherein the regulation of various cytokines and signals is involved.
Chinese patent 201711110753.8 discloses a facial mask essence which is characterized by comprising the following components in parts by weight: phase A: purifying water: 10% -15%, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.12% -0.15%, phase B: purifying water: 2% -3%, fermented rice emulsifier: 0.50% -0.80%, phase C: purifying water: 2% -3%, hydrogenated lecithin: 0.20% -0.30%, phase D: purifying water: and the balance, glycerol: 5.0% -8.0%, butanediol: 5.0% -8.0%, EDTA-2 NA: 0.02% -0.10%, carboxymethyl chitosan: 0.02% -0.05%, sodium polyglutamate: 0.02% -0.05%, 1, 2-pentanediol: 0.5% -0.8%, 1, 2-hexanediol: 0.5% -0.8%, polyglycerol-6: 0.5% -1.0%, allantoin: 0.1% -0.2%, p-hydroxyacetophenone: 0.2% -0.3%; phase E: c14-22 alcohol and C12-20 alkyl glucoside complexes: 0.2% -0.3%, cyclopentadimethylsiloxane and cyclohexasiloxane complex: 1.0% -2.0%, phytosterol/octyldodecanol lauroyl glutamate and tocopherol (vitamin E) complex: 0.15% -0.3%, glyceryl caprylate: 0.15% -0.2%, caprylic/capric triglyceride: 0.5% -1.0%, DIAMOLEACTIF 0.5% -1.0%, phase F: purifying water: 0.30% -0.50%, arginine: 0.12% -0.15%, phase G: PEG/PPG/polytetramethylene glycol-8/5/3 glycerol: 0.5% -1.0%, trehalose: 0.5% -1.0%, hydrolyzed rice extract: 0.5% -1.0%, dipotassium glycyrrhizinate: 0.15% -0.3%, water-locking magnet: 0.3% -0.5%, aluminum starch octenyl succinate: 0.5-0.8%, tocopherol acetate 0.05-0.1%, rosemary essential oil: 0.005% -0.01%, rose essential oil: 0.005% -0.01%; the sum of the weight percentages of the raw materials is 100 percent. The silk mask is used together with a silk mask, and when the silk mask is directly applied, the effects of whitening, relieving and resisting aging are reduced.
Chinese patent 201410763128.3 discloses a 36-hour moisturizing cream containing nectar and avocado oil, which comprises the following components in percentage by mass: 2.3-23% of humectant, 3.7-65% of emollient, 0.3-15% of emulsifier, 0.5-13% of skin conditioner, 0.1-1% of thickener, 0.1-5% of neutralizer, 0.1-1% of preservative, 0.1-0.5% of aromatic, 0.002-0.2% of modifier and the balance of solvent; wherein the emollient contains avocado oil 0.1-5 wt%; the skin conditioner contains 0.1-5% of nectar by mass percent. The invention can deeply moisturize for a long time, restore the water balance activity of the skin ecosystem and make the skin more moist and tender, but has relatively poor soothing and anti-aging effects.
The invention mainly achieves the whitening purpose through two main ways: the pigment generation is prevented by inhibiting the activity of related enzymes in the process of melanin synthesis or inhibiting the activation of the activity of melanocyte differentiation and tyrosinase by endothelin; secondly, the synthesized pigment is diluted, the transfer of melanin, purpurine and the like to the horny layer is accelerated by promoting the renewal of epidermis and the pigment is discharged out of the body along with the shedding of aged horny cells, or the pigment is discharged out of the body through a blood circulation system in vivo after being decomposed, dissolved and absorbed in the skin, and simultaneously, the effects of smearing texture, aging resistance and anti-allergy relief are achieved.
Disclosure of Invention
The whitening, soothing and anti-aging essence provided by the invention has good use texture and good whitening, soothing and anti-allergy and anti-aging effects.
The invention provides whitening, relieving and anti-aging essence which comprises the following components in parts by weight:
1.25-1.95 parts of emulsifier, 4.8-7.1 parts of emollient, 3.18-5.32 parts of thickener, 8.05-11.11 parts of humectant, 1.2-1.8 parts of skin conditioner, 1.13-1.67 parts of preservative, 2.74-5.08 parts of whitening anti-aging agent, 0.15-0.25 part of essence, 0.078-0.136 part of pH regulator and the balance of water, wherein the total weight part is 100; the emollient comprises refreshing oil and solid ester, and the skin conditioner comprises herba Dendrobii extract and stigma croci Sativi extract.
Wherein the content of the first and second substances,
the refreshing grease comprises neopentyl glycol diheptanoate, polydimethylsiloxane, coco-caprylate/caprate, isononyl isononanoate, glycerol tri (ethyl acetate) ester, batyl alcohol, shea butter, PCA polydimethylsiloxane, phytosterol oleate and β -sitosterol, the solid esters comprise cetylstearyl alcohol, the emulsifying agents comprise polyglycerol-6 distearate, polyglycerol-10 stearate and sucrose stearate, the thickening agents comprise acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacryloyldimethyl taurate, carboxymethyl β -dextran sodium and cyclopentyldimethylsiloxane, the moisturizing agents comprise polyglutamic acid, β -dextran, methyl propylene glycol, methyl gluceth-20, polyglycerol-10, trehalose, erythritol and saccharide isomerate, the preservatives comprise propyl hydroxybenzoate, methylparaben, 1, 2-hexanediol and p-hydroxy acetophenone, the whitening anti-aging agents comprise pentaerythritol tetra (tert-butyl-hydroxy acetate), yeast acetate, yeast extract, sodium hydrogen acetate, sodium nicotinate, nicotinamide adenine dinucleotide acetate and nicotinamide adenine dinucleotide acetate, and a nicotinamide adenine dinucleotide acetate fermentation product comprising a fermentation product of arbutinate, sodium ursolate, sodium arbutinate and a nicotinamide adenine dinucleotide.
The water may be deionized water, purified water or distilled water.
The saccharide isomer is a Pentavidin product of Tesmann, Switzerland.
In the formula, the glycyrrhiza glabra is derived from roots of the glycyrrhiza glabra and mainly inhibits melanogenesis in three directions, namely active oxygen generation inhibition, oxidation resistance, tyrosinase activity inhibition and inflammation inhibition, nicotinamide can influence intercellular communication between melanocytes and keratinocytes in vitro and inhibit the transport of melanosomes from the melanocytes to the keratinocytes so as to reduce melanin synthesis, the nicotinamide has various effects on the skin by local application, has the effects of resisting inflammation, oxidation resistance, saccharification resistance, repair of DNA damage induced by ultraviolet rays and other physicochemical factors, promotes the anti-tumor activity of the keratinocytes and inhibits the photocarcinogenicity of UVB radiation, the transfer of hyaluronic acid in the keratinocytes is interfered, pigmentation caused by ultraviolet rays is prevented by inhibiting the structure of plasminogen and preventing the combination of plasminogen and lysine sites of the keratinocytes, meanwhile, the transport of melanin granules to the keratinocytes is reduced so as to achieve the effect of fading of spots, the α glycoside inhibits the tyrosinase activity so as to inhibit the production and deposition of melanin, the skin whitening effect is finally achieved, the properties are more stable than β, the safety is high, the extract of yeast extract is a stress yeast cell extract, the extract, promotes the activity of a yeast cell, the skin lightening, the skin allergy resistance, the skin synthesis of a stress cell, the skin activating of a skin activating a proinflammatory cell, the skin activating a skin activating cell, the skin moistening skin activating a skin activating cell, the skin activating a skin activating cell, the skin activating a skin.
Further, the whitening, soothing and anti-aging essence comprises the following components in parts by weight:
0.8-1.2 parts of neopentyl glycol diheptanoate, 0.8-1.2 parts of polydimethylsiloxane, 0.4-0.6 part of coco-caprylate/caprate, 0.8-1.2 parts of isononyl isononanoate, 0.4-0.6 part of glycerol tri (ethyl acetate), 0.15-0.25 part of batyl alcohol, 0.6-0.7 part of shea butter, 0.4-0.6 part of PCA polydimethylsiloxane, 0.3-0.5 part of phytosterol oleate and β -sitosterol, 0.15-0.25 part of cetylstearyl alcohol, 0.15-0.25 part of polyglycerol-6 distearate, 0.8-1.2 part of polyglycerol-10 stearate, 0.3-0.5 part of sucrose stearate, 0.42-30 parts of acrylic ester cross-linked polymer, 0.1-0.2 part of polyacrylic ester/C10-30 parts of propylene glycol cross-linked polymer, 0.2 part of polyacrylamide dimethyl propylene glycol ether, 0.8-1.2 part of polyoxyethylene sorbitan fatty acid, 0.7-0.7 part of polyoxyethylene lauryl ether, 0.7-0.7 parts of sorbitol, 0.6 part of sorbitol polyoxyethylene sorbitan fatty acid, 0.7-0.7 part of sorbitol, 0.7-0.7 part of sorbitol methyl ether, 0.6-0.7 part of sorbitol, 0.6 part of sorbitol methyl ether, 0.7-0.6 part of sorbitol, 0.7-0.2 part of sorbitol, 0.7-0.7 part of sorbitol methyl alcohol, 0.6 part of sorbitol, 0.7-0.7 part of sorbitol methyl alcohol, 0.6 part of sorbitol, 0.7-0.2 part of sorbitol, 0.7 part of sodium lactate, 0.7 part of sorbitol, 0.7-0.7 part of sorbitol, 0.6 part of sorbitol, 0.2 part of sodium lactate, 0-0.7-0-0.7 part of sorbitol, 0.7 part of sorbitol methyl alcohol, 0-0.7 part of sorbitol methyl alcohol, 0-0.7 part of sorbitol, 0.2 part of sorbitol, 0.7 part of sorbitol, 0-0.7 part of sorbitol, 0.7 part of sorbitol.
The weight ratio of the dendrobium officinale extract to the saffron extract is 1:1.5-2.5, preferably 1: 2.
Furthermore, the whitening, soothing and anti-aging essence preferably comprises the following components in parts by weight:
neopentyl glycol diheptanoate 1 part, polydimethyl siloxane 1 part, coco-caprylate/caprate 0.5 part, isononyl isononanoate 1 part, glycerol tri (ethyl acetate) 0.5 part, batyl alcohol 0.2 part, shea butter 0.7 part, PCA polydimethyl siloxane 0.5 part, phytosterol oleate and β -sitosterol 0.4 part, cetyl stearyl alcohol 0.2 part, polyglyceryl-6 distearate 0.2 part, polyglyceryl-10 stearate 1 part, sucrose stearate 0.4 part, acrylic acid (ester) 0.15 part/C10-30 alkanol acrylate cross-linked polymer, sodium acryloyldimethyl taurate 0.1 part, carboxymethyl 32-dextran sodium 2 part, cyclopenta dimethyl siloxane 2 part, polyglutamic acid 0.05 part, β -dextran 0.03 part, methyl propylene glycol 7 part, methyl glucitol polyether-200.5 part, polyglyceryl-100.149 part, sucrose dimethyl siloxane 2 part, sucrose stearate 0.05 part, sorbitol 0.05 part, sorbitol 12 part, sucrose stearate 0.05 part, sorbitol acetate 0.5 part, sorbitol ester 0.6 part, sorbitol acetate 0.5 part, 0.6 part, sorbitol acetate 0.5 part, 3.
The skin conditioner also comprises hydrolyzed sclerotium rolfsii gum, wherein the weight ratio of the hydrolyzed sclerotium rolfsii gum to the dendrobium officinale extract is 1:8-12, and preferably 1: 10.
In addition, the invention also provides a preparation method of the whitening, soothing and anti-aging essence, which comprises the following steps:
s1, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into water, pre-foaming and homogenizing to obtain a mixture 1;
s2, mixing neopentyl glycol diheptanoate, polydimethylsiloxane, coco-caprylate/caprate, isononyl isononanoate, glycerol tri (ethyl acetate) ester, batyl alcohol, shea butter, PCA polydimethylsiloxane, phytosterol oleate and β -sitosterol, cetearyl alcohol, polyglycerol-6 distearate, polyglycerol-10 stearate, polyphenyl propyl ester, pentaerythritol tetra (bis-tert-butyl hydroxy hydrocinnamic acid) ester and tocopherol acetate, and heating while stirring until complete dissolution to obtain a mixture 2;
s3, mixing hydrolyzed sclerotium rolfsii gum, polyglutamic acid, β -glucan, methyl propylene glycol, methyl glucitol polyether-20, polyglycerol-10, trehalose, erythritol, sucrose stearate, a dendrobium officinale extract, methylparaben and water, stirring, heating, adding the mixture 1 in the heating process until the mixture is completely dissolved to obtain a mixture 3;
s4, extracting all the water phases of the mixture 3, stirring, homogenizing, adding the mixture 2, stirring, homogenizing, adding cyclopentadimethylsiloxane and sodium polyacryloyldimethyltaurate, continuing homogenizing, cooling after homogenizing, cooling, and adding EDTA disodium, nicotinamide, aminomethyl propanol and water to obtain a mixture 4.
S5, cooling the mixture 4, stirring, adding carboxymethyl β -dextran sodium, saccharide isomer, crocus sativus extract, yeast lysate extract, methyl propylene glycol, glycyrrhiza glabra root extract, yeast fermentation product extract, α -arbutin, tranexamic acid, essence, methyl propylene glycol, 1, 2-hexanediol, p-hydroxyacetophenone and water to obtain a mixture 5.
And S6, cooling the mixture 5, discharging after the product control initial inspection is qualified, and obtaining the whitening, soothing and anti-aging essence.
Wherein the content of the first and second substances,
the pre-foaming time in step S1 is 12-48 h.
In the step S1, the mass ratio of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer to water is 1: 80-120.
The homogenizing time in step S1 is not less than 20 min.
The heating temperature in step S2 does not exceed 85 ℃.
In the step S3, the mass ratio of the total mass of the hydrolyzed sclerotium rolfsii gum, the polyglutamic acid, the β -glucan, the methyl propylene glycol, the methyl glucitol polyether-20, the polyglycerol-10, the trehalose, the erythritol, the sucrose stearate, the dendrobium officinale extract and the methylparaben to the water is 1: 5.98-11.57.
The temperature raised in step S3 is 78-82 ℃.
Step S4 specifically includes: pumping all the water phase of the mixture 3 into an emulsifying pot, stirring at the rotating speed of 35 r/min, homogenizing for 3 minutes, adding the mixture 2, stirring at the rotating speed of 45 r/min, homogenizing for 2-3 minutes, adding cyclopentadimethylsiloxane and sodium polyacryloyldimethyltaurate, continuing to homogenize for 3 minutes, cooling after homogenizing, and adding EDTA disodium, nicotinamide, aminomethyl propanol and water when the temperature is reduced to 70 ℃ to obtain a mixture 4.
In the step S4, the mass ratio of the total mass of the EDTA disodium, the nicotinamide and the aminomethyl propanol to the water is 1: 0.60-1.20.
In step S5, the stirring speed is set to 35-45 rpm.
The temperature of the temperature reduction in the step S5 is 40-45 ℃.
In the step S5, the mass ratio of the total mass of the methyl propylene glycol, the glycyrrhiza glabra root extract, the yeast fermentation product extract, α -arbutin and tranexamic acid to water is 1: 0.62-1.01.
The temperature of the cooled material in step S6 is 38 + -2 deg.C.
In the step S6, the material is discharged by a 100-mesh filter screen.
The heating manner in steps S1-S1 includes induction cooker heating and steam heating.
The stirring manner in steps S1-S1 includes gate stirring, rotary disk stirring and planetary stirring.
The invention has the following beneficial effects:
(1) the dendrobium officinale extract and the saffron can activate macrophages, resist oxidation, enhance immunity, activate expression of filaggrin, protect lipid from oxidation, enhance skin barrier function and synthesis of natural moisturizing factors, reduce activation of NF-KB, help to reduce proinflammatory reaction, relieve skin symptoms (red blood filaments, stabbing pain and burning heat), antagonize TRPV1 pain receptors, reduce discomfort of skin sense organs, relieve and resist allergy.
(2) The emollient comprises refreshing grease and solid ester, can increase texture, improve skin feeling and reduce skin burden;
(3) the invention achieves the whitening effect and has the functions of anti-allergy, comfort and anti-aging.
Detailed Description
The present invention will be further explained with reference to specific embodiments in order to make the technical means, the original characteristics, the achieved objects and the effects of the present invention easy to understand, but the following embodiments are only preferred embodiments of the present invention, and not all embodiments are possible. Based on the embodiments in the implementation, other embodiments obtained by those skilled in the art without any creative efforts belong to the protection scope of the present invention.
In the following examples, unless otherwise specified, the experimental procedures used were conventional and the reagents used were commercially available.
Examples 1 to 9
The whitening, soothing and anti-aging essence of examples 1 to 9 comprises the components shown in the following tables 1 to 2 in parts by weight:
TABLE 1 EXAMPLES 1-4 component tables
Figure BDA0002356419580000071
Figure BDA0002356419580000081
TABLE 2 EXAMPLES 6-9 composition tables
Figure BDA0002356419580000082
Figure BDA0002356419580000091
Figure BDA0002356419580000101
Comparative examples 1 to 8
The whitening, soothing and anti-aging essence of comparative examples 1 to 5 comprises the following components in parts by weight as shown in Table 3:
TABLE 3 comparative examples 1-5 composition tables
Figure BDA0002356419580000102
Figure BDA0002356419580000111
Figure BDA0002356419580000121
Wherein, in Table 1-Table 3, the mass percentages of the phytosterol oleate 86% and β -sitosterol 14% in 10A, the polyglycerol-10 content 79% in 22B2, the aminopropyl alcohol content 95% in 35E, the extract content of the yeast lysate in 40F is 24%, 22%, 27%, and 25% in examples 1,2, 3, and 4, respectively, and the rest is 24%, the yeast fermentation product extract 7% in 43G2, α -arbutin 59%, tranexamic acid 34%, and "-" indicates that the components are not present.
Preparation example
The formulations in tables 1-3 were prepared according to the following procedure:
1. pre-soaking B3 a day in advance, and then homogenizing for more than 20 minutes at 50HZ by using a mobile homogenizer;
2. weighing all the phase A by using a proper stainless steel barrel, and heating the phase A to be completely dissolved while stirring by using an induction cooker, wherein the temperature is not more than 85 ℃;
3. adding B, B1 and B2 into a water phase pot, stirring and heating, adding homogenized B3 during heating, heating to 78-82 deg.C, and dissolving completely;
4. pumping the water phase into an emulsifying pot, stirring for 35 r/min, homogenizing for 3 min at 50HZ, adding dissolved A, homogenizing for 2-3 min at 45 r/min under stirring, adding C, homogenizing for 3 min at 50HZ, and cooling after homogenizing; cooling to 70 deg.C, adding D, E;
5. cooling under vacuum, stirring at 35-45 rpm, cooling to 40-45 deg.C, and sequentially adding the rest components;
6. when the temperature is reduced to 38 +/-2 ℃, the materials are discharged by a 100-mesh filter screen after passing the product control initial inspection, and the whitening, soothing and anti-aging essence is obtained.
Effect detection
In each of the examples and comparative examples, 20 female volunteers aged 20 to 50 were located, 5 fixed regions of 2 cm square were drawn on the face in an indoor environment at 20 ℃ and 50% relative humidity, and after the above whitening, soothing and antiaging essence and commercially available general essence were applied to the fixed regions, the feeling of use was evaluated, and the results are shown in table 4. Meanwhile, spots, wrinkles, and red blood streaks were measured with a visia skin test apparatus after 15 days and 30 days of continuous use (the increase in percentage indicates that the skin becomes better), and the results of the measurements are shown in tables 5 and 6, respectively.
Table 4.
Feeling of use Absorbency of Lightness and thinness
Example 1 Has tactile sensation Quickly absorbed Light and thin
Example 2 Has tactile sensation Quickly absorbed Light and thin
Example 3 Has tactile sensation Quickly absorbed Light and thin
Example 4 Has tactile sensation Quickly absorbed Light and thin
Example 5 Has tactile sensation Quickly absorbed Light and thin
Example 6 Has tactile sensation Quickly absorbed Light and thin
Example 7 Has tactile sensation Quickly absorbed Light and thin
Example 8 Has tactile sensation Quickly absorbed Light and thin
Example 9 Has tactile sensation Quickly absorbed Light and thin
Comparative example 1 Sticky and non-textured Quickly absorbed Light and thin
Comparative example 2 Has slippery feel Quickly absorbed Light and thin
Comparative example 3 Has slippery feel Quickly absorbed Light and thin
Comparative example 4 Sticky and non-textured Quickly absorbed Light and thin
Comparative example 5 Sticky and coarse Slow absorption Thickness and weight
General essence on the market Sticky and non-textured Slow absorption Thickness and weight
TABLE 5 test results using 15 days
Figure BDA0002356419580000131
Figure BDA0002356419580000141
TABLE 6 test results using 30 days
Figure BDA0002356419580000142
The result shows that the essence has good hand feeling, is light and thin and is easy to absorb, and after the essence is used for one skin period, the skin of a test person is greatly improved in spots, wrinkles and subcutaneous red blood streaks, so that the essence achieves the whitening effect and also has the anti-allergy, relaxing and anti-aging effects. In addition, the whitening, anti-aging and relieving effects are improved by adding the saffron and the dendrobium officinale extracts, and as can be seen from example 1, particularly when the weight ratio of the saffron to the dendrobium officinale extracts is 1:2, the whitening, anti-aging and relieving effects are optimal, in addition, examples 6-9 show that the effects are further improved after adding the hydrolyzed sclerotium rolfsii gum, and example 6 shows that the effects are optimal when the weight ratio of the hydrolyzed sclerotium rolfsii gum to the dendrobium officinale extracts is 1: 10. As can be seen from comparative examples 2 and 3, the effect of saffron and dendrobium officinale can be influenced, and comparative example 1 shows that the lack of solid ester can cause the lack of texture and influence the use feeling. Comparative examples 4 and 5 show that too much or too little of all the active ingredients can reduce the effect.
The present invention has been further described with reference to specific embodiments, which are only exemplary and do not limit the scope of the present invention. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications may be made without departing from the spirit and scope of the invention.

Claims (10)

1. The whitening, soothing and anti-aging essence is characterized by comprising the following components in parts by weight:
1.25-1.95 parts of emulsifier, 4.8-7.1 parts of emollient, 3.18-5.32 parts of thickener, 8.05-11.11 parts of humectant, 1.2-1.8 parts of skin conditioner, 1.13-1.67 parts of preservative, 2.74-5.08 parts of whitening anti-aging agent, 0.15-0.25 part of essence, 0.078-0.136 part of pH regulator and the balance of water, wherein the total weight part is 100; the skin conditioner comprises dendrobium officinale extract and saffron extract.
2. The whitening, soothing and antiaging essence according to claim 1, wherein the refreshing oil comprises neopentyl glycol diheptanoate, dimethicone, coco-caprylate/caprate, isononyl isononanoate, glycerol tri (ethyl acetate) ester, batyl alcohol, shea butter, PCA dimethicone, phytosterol oleate and β -sitosterol, the solid esters comprise cetyl stearyl alcohol, the emulsifiers comprise polyglyceryl-6 distearate, polyglyceryl-10 stearate and sucrose stearate, the thickeners comprise acrylates/C10-30 alkanol acrylate crosspolymer, sodium polyacryloyldimethyltaurate, sodium carboxymethyl β -dextran and cyclopentyldimethylsiloxane, the moisturizers comprise polyglutamic acid, β -dextran, methyl propylene glycol, methyl gluceth-20, polyglyceryl-10, trehalose, erythritol and saccharide isomerate, the preservatives comprise hydroxypropyl hydroxybenzoate, methylparaben, 1, 2-hexanediol and yeast extract, the yeast extract comprises p-butyl hydroxy ethyl acetate, p-hydroxy ethyl acetate, sodium p-hydroxy propyl acetate, sodium benzoate, disodium p-butyl acetate, sodium p-hydroxy benzoate, sucrose acetate, sodium benzoate acetate, sucrose acetate, sodium benzoate acetate, sucrose acetate.
3. The whitening, soothing and anti-aging essence as claimed in claim 2, which is characterized by comprising the following components in parts by weight:
0.8-1.2 parts of neopentyl glycol diheptanoate, 0.8-1.2 parts of polydimethylsiloxane, 0.4-0.6 part of coco-caprylate/caprate, 0.8-1.2 parts of isononyl isononanoate, 0.4-0.6 part of glycerol tri (ethyl acetate), 0.15-0.25 part of batyl alcohol, 0.6-0.7 part of shea butter, 0.4-0.6 part of PCA polydimethylsiloxane, 0.3-0.5 part of phytosterol oleate and β -sitosterol, 0.15-0.25 part of cetylstearyl alcohol, 0.15-0.25 part of polyglycerol-6 distearate, 0.8-1.2 part of polyglycerol-10 stearate, 0.3-0.5 part of sucrose stearate, 0.42-30 parts of acrylic ester cross-linked polymer, 0.1-0.2 part of polyacrylamide, 0.7-0.7 part of hydroxypropyl methacrylate, 0.7-0.7 part of polyoxyethylene lauryl sulfate, 0.7-0.7 part of sorbitol, 0.7-0.7 part of polyoxyethylene lauryl sulfate, 0.7-0.7 part of polyoxyethylene lauryl sulfate, 0.6 part of polyoxyethylene lauryl sulfate, 0.7-0.7 part of sorbitol, 0.7-0.6 part of polyoxyethylene lauryl sulfate, 0.7-0.7 part of polyoxyethylene sorbitan, 0.6, 0.7-0.6 part of polyoxyethylene lauryl sulfate, 0.7-0.6, 0.7-0.7 part of polyoxyethylene sorbitan 15 parts of polyoxyethylene, 0.7 parts of polyoxyethylene sorbitan, 0.6, 0.7-0.6 part of polyoxyethylene lauryl ether, 0.7 parts of polyoxyethylene lauryl ether, 0.7-0.6 part of polyoxyethylene lauryl ether, 0.2 parts of polyoxyethylene lauryl ether, 0.7-0.7, 0.6, 0.7 parts of polyoxyethylene lauryl ether, 0.7 parts of polyoxyethylene sorbitan fatty acid, 0.7-0.7 parts of polyoxyethylene lauryl ether, 0.7-0.7 parts of polyoxyethylene ether, 0.7 parts of polyoxyethylene lauryl ether, 0.7 parts.
4. The whitening, soothing and anti-aging essence as claimed in claim 3, wherein the weight ratio of the dendrobium officinale extract to the saffron extract is 1: 1.5-2.5.
5. The essence of claim 1, wherein the skin conditioner further comprises hydrolyzed sclerotium rolfsii gum.
6. The whitening, soothing and anti-aging essence as claimed in claim 5, wherein the weight ratio of the hydrolyzed sclerotium rolfsii gum to the dendrobium officinale extract is 1: 8-12.
7. The preparation method of the whitening, soothing and anti-aging essence as claimed in any one of claims 1 to 6, comprising the steps of:
s1, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer into water, pre-foaming and homogenizing to obtain a mixture 1;
s2, mixing neopentyl glycol diheptanoate, polydimethylsiloxane, coco-caprylate/caprate, isononyl isononanoate, glycerol tri (ethyl acetate) ester, batyl alcohol, shea butter, PCA polydimethylsiloxane, phytosterol oleate and β -sitosterol, cetearyl alcohol, polyglycerol-6 distearate, polyglycerol-10 stearate, polyphenyl propyl ester, pentaerythritol tetra (bis-tert-butyl hydroxy hydrocinnamic acid) ester and tocopherol acetate, and heating while stirring until complete dissolution to obtain a mixture 2;
s3, mixing hydrolyzed sclerotium rolfsii gum, polyglutamic acid, β -glucan, methyl propylene glycol, methyl glucitol polyether-20, polyglycerol-10, trehalose, erythritol, sucrose stearate, a dendrobium officinale extract, methylparaben and water, stirring, heating, adding the mixture 1 in the heating process until the mixture is completely dissolved to obtain a mixture 3;
s4, extracting all water phases of the mixture 3, stirring, homogenizing, adding the mixture 2, stirring, homogenizing, adding cyclopentadimethylsiloxane and sodium polyacryloyldimethyltaurate, continuing homogenizing, cooling after homogenizing, and adding EDTA disodium, nicotinamide, aminomethyl propanol and water to obtain a mixture 4;
s5, cooling the mixture 4, stirring, adding carboxymethyl β -dextran sodium, saccharide isomer, crocus sativus extract, yeast lysate extract, methyl propylene glycol, glycyrrhiza glabra root extract, yeast fermentation product extract, α -arbutin, tranexamic acid, essence, methyl propylene glycol, 1, 2-hexanediol, p-hydroxyacetophenone and water to obtain a mixture 5;
and S6, cooling the mixture 5, discharging after the product control initial inspection is qualified, and obtaining the whitening, soothing and anti-aging essence.
8. The method according to claim 7, wherein the heating temperature in step S2 is not more than 85 ℃.
9. The production method according to claim 7, wherein the temperature at which the temperature is raised in step S3 is 78 to 82 ℃.
10. The method according to claim 7, wherein the temperature of the temperature decrease in the step S5 is 40-45 ℃.
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CN115429735A (en) * 2022-10-09 2022-12-06 伯德创研(广州)生物科技有限公司 Anti-aging skin moistening composition, skin moistening cream containing anti-aging skin moistening composition and preparation method of skin moistening cream
CN116725935A (en) * 2023-07-27 2023-09-12 广州市精锐生物研究有限公司 Essence composition with whitening, anti-allergy and anti-wrinkle functions, and preparation method and application thereof

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