CN110903083A - 无线充电器用铁氧体磁片配方及其制备新方法 - Google Patents
无线充电器用铁氧体磁片配方及其制备新方法 Download PDFInfo
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- CN110903083A CN110903083A CN201811079475.9A CN201811079475A CN110903083A CN 110903083 A CN110903083 A CN 110903083A CN 201811079475 A CN201811079475 A CN 201811079475A CN 110903083 A CN110903083 A CN 110903083A
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- 229910000859 α-Fe Inorganic materials 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 22
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 22
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 22
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 22
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 claims abstract description 22
- JKQOBWVOAYFWKG-UHFFFAOYSA-N molybdenum trioxide Chemical compound O=[Mo](=O)=O JKQOBWVOAYFWKG-UHFFFAOYSA-N 0.000 claims abstract description 22
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000005751 Copper oxide Substances 0.000 claims abstract description 11
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 11
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(II) oxide Inorganic materials [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910000431 copper oxide Inorganic materials 0.000 claims abstract description 11
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims abstract description 11
- 229910052808 lithium carbonate Inorganic materials 0.000 claims abstract description 11
- 229910000480 nickel oxide Inorganic materials 0.000 claims abstract description 11
- ZKATWMILCYLAPD-UHFFFAOYSA-N niobium pentoxide Inorganic materials O=[Nb](=O)O[Nb](=O)=O ZKATWMILCYLAPD-UHFFFAOYSA-N 0.000 claims abstract description 11
- URLJKFSTXLNXLG-UHFFFAOYSA-N niobium(5+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Nb+5].[Nb+5] URLJKFSTXLNXLG-UHFFFAOYSA-N 0.000 claims abstract description 11
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims abstract description 11
- BPUBBGLMJRNUCC-UHFFFAOYSA-N oxygen(2-);tantalum(5+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Ta+5].[Ta+5] BPUBBGLMJRNUCC-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 11
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 11
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 11
- PBCFLUZVCVVTBY-UHFFFAOYSA-N tantalum pentoxide Inorganic materials O=[Ta](=O)O[Ta](=O)=O PBCFLUZVCVVTBY-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 11
- 239000011787 zinc oxide Substances 0.000 claims abstract description 11
- WMWLMWRWZQELOS-UHFFFAOYSA-N bismuth(III) oxide Inorganic materials O=[Bi]O[Bi]=O WMWLMWRWZQELOS-UHFFFAOYSA-N 0.000 claims abstract description 8
- IUYLTEAJCNAMJK-UHFFFAOYSA-N cobalt(2+);oxygen(2-) Chemical compound [O-2].[Co+2] IUYLTEAJCNAMJK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 239000003292 glue Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 238000003825 pressing Methods 0.000 claims description 8
- 230000002950 deficient Effects 0.000 claims description 4
- 238000005469 granulation Methods 0.000 claims description 4
- 230000003179 granulation Effects 0.000 claims description 4
- 238000007689 inspection Methods 0.000 claims description 4
- 239000011812 mixed powder Substances 0.000 claims description 4
- 238000004806 packaging method and process Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 238000005245 sintering Methods 0.000 claims description 4
- 239000002002 slurry Substances 0.000 claims description 4
- 239000007921 spray Substances 0.000 claims description 4
- 238000000227 grinding Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 6
- 241001391944 Commicarpus scandens Species 0.000 abstract description 4
- 238000009434 installation Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 description 10
- 229910000416 bismuth oxide Inorganic materials 0.000 description 3
- 229910000428 cobalt oxide Inorganic materials 0.000 description 3
- TYIXMATWDRGMPF-UHFFFAOYSA-N dibismuth;oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Bi+3].[Bi+3] TYIXMATWDRGMPF-UHFFFAOYSA-N 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 239000000696 magnetic material Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000005308 ferrimagnetism Effects 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 229910052755 nonmetal Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
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Abstract
本发明公开了一种无线充电器用铁氧体磁片配方及其制备新方法,其包括以下重量份数配比的成分原料制得:氧化铁:50‑52份、氧化锰:20‑22份、氧化锌:10‑12份、二氧化钛:0.1‑0.3份、碳酸钙:0.1‑0.3份、二氧化硅:0.4‑0.6份、三氧化二钴:0.05‑0.15份、三氧化二铋:1‑3份、三氧化钼:3‑5份、五氧化二铌:0.3‑0.5份、五氧化二钽:0.4‑0.6份、氧化铜:0.1‑0.3份、氧化镍:1‑3份、碳酸锂:1.5‑2.5份、碳酸钠:15‑17份、去离子水:100‑200份、胶:50‑60份;本发明能够替代传统的铁氧体磁块切割的方法,该磁片不易碎可以弯曲,而且可以做到0.5毫米以下,节省了安装空间,极大地提高了效率及产品合格率,降低了成本。
Description
技术领域
本发明涉及一种铁氧体磁片配方及其制备方法,特别是涉及一种无线充电器用铁氧体磁片配方及其制备新方法。
背景技术
铁氧体是一种具有亚铁磁性的金属氧化物,就电特性来说,铁氧体的电阻率比单质金属或合金磁性材料大得多,而且还有较高的介电性能。铁氧体的磁性能还表现在高频时具有较高的磁导率,因而,铁氧体已成为高频弱电领域用途广泛的非金属磁性材料,由于铁氧体单位体积中储存的磁能较低,饱合磁感应强度也较低,因而限制了它在要求较高磁能密度的低频强电和大功率领域的应用,目前的铁氧体制备成本高,效率低并且合格率差。
发明内容
本发明所要解决的技术问题是提供一种无线充电器用铁氧体磁片配方及其制备新方法,其能够替代传统的铁氧体磁块切割的方法,该磁片不易碎可以弯曲,而且可以做到0.5毫米以下,节省了安装空间,极大地提高了效率及产品合格率,降低了成本。
根据本发明的一个方面,提供一种无线充电器用铁氧体磁片配方,其包括以下重量份数配比的成分原料制得:氧化铁:50-52份、氧化锰:20-22份 、氧化锌:10-12份、二氧化钛:0.1-0.3份、碳酸钙:0.1-0.3份、二氧化硅:0.4-0.6份、三氧化二钴:0.05-0.15份、三氧化二铋:1-3份、三氧化钼:3-5份、五氧化二铌:0.3-0.5份、五氧化二钽:0.4-0.6份、氧化铜:0.1-0.3份、氧化镍:1-3份、碳酸锂:1.5-2.5份、碳酸钠:15-17份、去离子水:100-200份、胶:50-60份。
本发明还提供一种无线充电器用铁氧体磁片制备新方法,其包括如下步骤:
步骤一,首先将氧化铁、氧化锰、氧化锌、二氧化钛、碳酸钙、二氧化硅、三氧化二钴、三氧化二铋、三氧化钼、五氧化二铌、五氧化二钽、氧化铜、氧化镍、碳酸锂、碳酸钠分别碾碎成粉末,再把粉末全部混合在一起;
步骤二,将步骤一混合好的粉末压制成一定形状的毛坯,放入气氛保护窑,在1320摄氏度和气氛下进行烧结,使之生成铁氧体的密度在4.7-5.1克每立方厘米,晶粒尺寸在5-50微米;
步骤三,把生成的铁氧体先进行粗粉碎,粉碎后的粉末再进行细粉碎,使粉碎后的颗粒粒度在1-30微米;
步骤四,将步骤三中粉碎后的粉末与去离子水及胶混合制成料浆,然后进行喷雾造粒,接着把制成的粉料根据用途压制成不同尺寸及形状的磁片材料;
步骤五,把步骤四压制出来的磁片材料放入窑中在100-500摄氏度下进行烧结固化形成磁片;
步骤六,将固化后的磁片进行产品质检,去除瑕疵品,把良品进行包装并存储在仓库。
与现有技术相比,本发明具有如下的有益效果:本发明能够替代传统的铁氧体磁块切割的方法,该磁片不易碎可以弯曲,而且可以做到0.5毫米以下,节省了安装空间,极大地提高了效率及产品合格率,降低了成本。
附图说明
图1为本发明的流程图。
具体实施方式
下面结合具体实施例对本发明进行详细说明。以下实施例将有助于本领域的技术人员进一步理解本发明,但不以任何形式限制本发明。应当指出的是,对本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进。这些都属于本发明的保护范围。
本发明无线充电器用铁氧体磁片配方包括以下重量份数配比的成分原料制得:氧化铁:50-52份、氧化锰:20-22份 、氧化锌:10-12份、二氧化钛:0.1-0.3份、碳酸钙:0.1-0.3份、二氧化硅:0.4-0.6份、三氧化二钴:0.05-0.15份、三氧化二铋:1-3份、三氧化钼:3-5份、五氧化二铌:0.3-0.5份、五氧化二钽:0.4-0.6份、氧化铜:0.1-0.3份、氧化镍:1-3份、碳酸锂:1.5-2.5份、碳酸钠:15-17份、去离子水:100-200份、胶:50-60份。
本发明还包括一种无线充电器用铁氧体磁片制备新方法,其包括如下步骤:
步骤一,首先将氧化铁、氧化锰、氧化锌、二氧化钛、碳酸钙、二氧化硅、三氧化二钴、三氧化二铋、三氧化钼、五氧化二铌、五氧化二钽、氧化铜、氧化镍、碳酸锂、碳酸钠分别碾碎成粉末,再把粉末全部混合在一起;
步骤二,将步骤一混合好的粉末压制成一定形状的毛坯,放入气氛保护窑,在1320摄氏度和气氛下进行烧结,使之生成铁氧体的密度在4.7-5.1克每立方厘米,晶粒尺寸在5-50微米;
步骤三,把生成的铁氧体先进行粗粉碎,粉碎后的粉末再进行细粉碎,使粉碎后的颗粒粒度在1-30微米;
步骤四,将步骤三中粉碎后的粉末与去离子水及胶混合制成料浆,然后进行喷雾造粒,接着把制成的粉料根据用途压制成不同尺寸及形状的磁片材料;
步骤五,把步骤四压制出来的磁片材料放入窑中在100-500摄氏度下进行烧结固化形成磁片;
步骤六,将固化后的磁片进行产品质检,去除瑕疵品,把良品进行包装并存储在仓库。
与现有技术相比,本发明具有如下的有益效果:能够替代传统的铁氧体磁块切割的方法,该磁片不易碎可以弯曲,而且可以做到0.5毫米以下,节省了安装空间,极大地提高了效率及产品合格率,降低了成本。
以下实施例的原料均按重量份数配比制得:
实施例1
氧化铁:50份;
氧化锰:20份 ;
氧化锌:10份;
二氧化钛:0.1份;
碳酸钙:0.1份;
二氧化硅:0.4份;
三氧化二钴:0.05份;
三氧化二铋:1份;
三氧化钼:3份;
五氧化二铌:0.3份;
五氧化二钽:0.4份;
氧化铜:0.1份;
氧化镍:1份;
碳酸锂:1.5份;
碳酸钠:15份;
第一先将氧化铁:50份、氧化锰:20份 、氧化锌:10份、二氧化钛:0.1份、碳酸钙:0.1份、二氧化硅:0.4份、三氧化二钴:0.05份、三氧化二铋:1份、三氧化钼:3份、五氧化二铌:0.3份、五氧化二钽:0.4份、氧化铜:0.1份、氧化镍:1份、碳酸锂:1.5份、碳酸钠:15份分别碾碎成粉末,再把粉末全部混合在一起;第二将步骤一混合好的粉末压制成一定形状的毛坯,放入气氛保护窑,在1320摄氏度和气氛下进行烧结,使之生成铁氧体的密度在4.7-5.1克每立方厘米,晶粒尺寸在5-50微米;第三把生成的铁氧体先进行粗粉碎,粉碎后的粉末再进行细粉碎,使粉碎后的颗粒粒度在1-30微米;第四将步骤三中粉碎后的粉末与去离子水及胶混合制成料浆,然后进行喷雾造粒,接着把制成的粉料根据用途压制成不同尺寸及形状的磁片材料;第五把步骤四压制出来的磁片材料放入窑中在100-500摄氏度下进行烧结固化形成磁片;第六将固化后的磁片进行产品质检,去除瑕疵品,把良品进行包装并存储在仓库。
实施例2
氧化铁:51份;
氧化锰:21份 ;
氧化锌:11份;
二氧化钛:0.2份;
碳酸钙:0.2份;
二氧化硅:0.5份;
三氧化二钴:0.1份;
三氧化二铋:2份;
三氧化钼:4份;
五氧化二铌:0.4份;
五氧化二钽:0.5份;
氧化铜:0.2份;
氧化镍:2份;
碳酸锂:2份;
碳酸钠:16份;
本实施例的制配方法与实施例1完全相同。
实施例3
氧化铁:52份;
氧化锰:22份 ;
氧化锌:12份;
二氧化钛:0.3份;
碳酸钙:0.3份;
二氧化硅:0.6份;
三氧化二钴:0.15份;
三氧化二铋:3份;
三氧化钼:5份;
五氧化二铌:0.5份;
五氧化二钽:0.6份;
氧化铜:0.3份;
氧化镍:3份;
碳酸锂:2.5份;
碳酸钠:17份;
本实施例的制配方法与实施例1完全相同。
以上所述的具体实施例,对本发明的解决的技术问题、技术方案和有益效果进行了进一步详细说明,所应理解的是,以上所述仅为本发明的具体实施例而已,并不用于限制本发明,凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (2)
1.一种无线充电器用铁氧体磁片配方,其特征在于,其包括以下重量份数配比的成分原料制得:氧化铁:50-52份、氧化锰:20-22份 、氧化锌:10-12份、二氧化钛:0.1-0.3份、碳酸钙:0.1-0.3份、二氧化硅:0.4-0.6份、三氧化二钴:0.05-0.15份、三氧化二铋:1-3份、三氧化钼:3-5份、五氧化二铌:0.3-0.5份、五氧化二钽:0.4-0.6份、氧化铜:0.1-0.3份、氧化镍:1-3份、碳酸锂:1.5-2.5份、碳酸钠:15-17份、去离子水:100-200份、胶:50-60份。
2.一种制备无线充电器用铁氧体磁片制备新方法,其特征在于,其包括如下步骤:
步骤一,首先将氧化铁、氧化锰、氧化锌、二氧化钛、碳酸钙、二氧化硅、三氧化二钴、三氧化二铋、三氧化钼、五氧化二铌、五氧化二钽、氧化铜、氧化镍、碳酸锂、碳酸钠分别碾碎成粉末,再把粉末全部混合在一起;
步骤二,将步骤一混合好的粉末压制成一定形状的毛坯,放入气氛保护窑,在1320摄氏度和气氛下进行烧结,使之生成铁氧体的密度在4.7-5.1克每立方厘米,晶粒尺寸在5-50微米;
步骤三,把生成的铁氧体先进行粗粉碎,粉碎后的粉末再进行细粉碎,使粉碎后的颗粒粒度在1-30微米;
步骤四,将步骤三中粉碎后的粉末与去离子水及胶混合制成料浆,然后进行喷雾造粒,接着把制成的粉料根据用途压制成不同尺寸及形状的磁片材料;
步骤五,把步骤四压制出来的磁片材料放入窑中在100-500摄氏度下进行烧结固化形成磁片;
步骤六,将固化后的磁片进行产品质检,去除瑕疵品,把良品进行包装并存储在仓库。
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FR3121930A1 (fr) * | 2021-04-19 | 2022-10-21 | Thales | Materiau ferrite de lithium faibles pertes pour dispositif hyperfrequence commandable de puissance |
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FR3121930A1 (fr) * | 2021-04-19 | 2022-10-21 | Thales | Materiau ferrite de lithium faibles pertes pour dispositif hyperfrequence commandable de puissance |
EP4079701A1 (fr) * | 2021-04-19 | 2022-10-26 | Thales | Materiau ferrite de lithium faibles pertes pour dispositif hyperfrequence commandable de puissance |
CN115028444A (zh) * | 2022-05-30 | 2022-09-09 | 安徽继胜磁性材料有限公司 | 一种5g快充电源用小型化锰锌铁氧体磁芯及其制备工艺 |
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