CN110882190A - Soapberry plant extract face-cleaning mousse and preparation method thereof - Google Patents
Soapberry plant extract face-cleaning mousse and preparation method thereof Download PDFInfo
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Abstract
The invention provides a soapberry extract-containing face-cleaning mousse and a preparation method thereof, wherein the soapberry extract-containing face-cleaning mousse is prepared from the following raw materials, including 0.05-0.5 part by weight of EDTA disodium; 1-10 parts by weight of glycerol; 0.03 to 0.5 part by weight of hydroxyethyl cellulose; 2-10 parts by weight of sodium lauroyl sarcosinate; 0.05-1 weight part of capryloyl glycine; 0.5 to 5 parts by weight of sodium cocoyl isethionate; 0.05-3 parts by weight of polyquaternium-52; 0.5 to 5 parts by weight of sodium pyrrolidone carboxylate; 1-10 parts by weight of disodium cocoyl amphodiacetate; 4-20 parts by weight of cocamidopropyl betaine; 0.05-1 parts by weight of allantoin; 0.01-0.5 weight parts of zymosan; 0.01-0.5 parts by weight of carboxymethyl chitosan; 1-10 parts by weight of soapberry extract; 0.1-2 parts by weight of immature bitter orange extract; 0.1 to 2 parts by weight of hexanediol; 0.1-1 weight portion of p-hydroxyacetophenone. In the technical field of cosmetics, the problems that chemical cleaning agents are irritant to human skin and easily pollute the environment exist, and a natural soapberry plant extract facial mousse is provided.
Description
Technical Field
The invention relates to the technical field of separation and extraction of active ingredients of natural products, and particularly relates to a soapberry plant extract facial cleansing mousse and a preparation method thereof.
Background
With the improvement of the consumption level of people, the requirements of people on cosmetic products are more and more strict, and people have not only satisfied the aspect of efficacy, but also put forward higher requirements on the safety of cosmetics. Under the trend that people are more and more dislike synthetic chemical reagents and more interested natural raw materials, active ingredients are extracted from natural animals and plants to prepare high-added-value fine chemicals, and the active ingredients are fully synthesized, chemically modified and deeply processed, the soapberry plant extract cleansing mousse adopts the soapberry extract as a main cleaning agent component, and is mild in performance, strong in cleaning capacity, free of stimulation to human skin and free of pollution to the environment compared with the traditional chemical cleaning agent, and is an ideal cleaning agent. Meanwhile, the formula has multiple effects of strong foaming capacity, mild performance, oil control and the like due to the matching of multiple components in the formula.
Disclosure of Invention
In order to overcome the problems that a chemical cleaning agent in the prior art has irritation to human skin and easily causes pollution to the environment, a soapberry extract-containing face-cleaning mousse and a preparation method thereof are provided, wherein the soapberry extract-containing face-cleaning mousse comprises the following raw materials, including 0.05-0.5 part by weight of EDTA disodium; 1-10 parts by weight of glycerol; 0.03 to 0.5 part by weight of hydroxyethyl cellulose; 2-10 parts by weight of sodium lauroyl sarcosinate; 0.05-1 weight part of capryloyl glycine; 0.5 to 5 parts by weight of sodium cocoyl isethionate; 0.05-3 parts by weight of polyquaternium-52; 0.5 to 5 parts by weight of sodium pyrrolidone carboxylate; 1-10 parts by weight of disodium cocoyl amphodiacetate; 4-20 parts by weight of cocamidopropyl betaine; 0.05-1 parts by weight of allantoin; 0.01-0.5 weight parts of zymosan; 0.01-0.5 parts by weight of carboxymethyl chitosan; 1-10 parts by weight of soapberry extract; 0.1-2 parts by weight of immature bitter orange extract; 0.1 to 2 parts by weight of hexanediol; 0.1-1 weight parts of p-hydroxyacetophenone; 0.01-0.5 parts by weight of ethylhexyl glycerol; TO 100 parts by weight of yeast fermentation product filtrate.
The preparation method comprises the following steps: the method comprises the following steps: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
Preferably, the hexanediol is 1, 2-hexanediol.
By adopting the technical scheme, the 1, 2-hexanediol can be mixed and dissolved with water, ethanol and various organic solvents, can be matched with glycerin to be used as a wetting agent in cosmetics, toothpaste and perfumed soap, and is often used as a high-grade organic solvent.
Preferably, the soapberry fruits are washed by deionized water for 3 times before being crushed, drained, stripped of soapberry peels, dried in an electric heating constant-temperature air-blast drying box at 60 ℃, crushed by a miniature plant crusher and sieved by a 40-mesh standard sieve.
By adopting the technical scheme, the soapberry fruit is initially cleaned and dried, and is subjected to peeling treatment, crushing and standard screening to realize standard treatment of raw materials.
Preferably, the purity of the ethanol in the step is 95%.
By adopting the technical scheme, the raw materials are treated by adopting the high-purity alcohol, so that the sterilization can be effectively carried out, and meanwhile, the moisture in the raw materials can be absorbed.
Preferably, in the process of concentrating the filtrate in the sixth step and the ninth step, the ethanol solution is distilled by using a rotary evaporator, the inside of the rotary evaporator is vacuumized and heated, and in the process of stopping evaporation, the heating is stopped firstly, then the vacuumization is stopped, and finally the power supply of the rotary evaporator is cut off.
By adopting the technical scheme, the ethanol is removed through the rotary evaporator, the heating is carried out in a vacuum environment, the heating is stopped at last, then the vacuumizing is stopped, and finally the power supply is cut off, so that the ethanol is prevented from being remained.
Preferably, in the step eight, shaking vibration with a fixed frequency is carried out on the residue solution and the separating funnel by using a shaking table, wherein the rotation speed of the shaking table is 150 r/min.
By adopting the technical scheme, the residue solution and the dichloromethane are completely mixed at the fixed rotating speed of the shaking table, and the mixture is easy to stratify after standing.
Preferably, the temperature in the color removal process of the activated carbon in the fourth step is set between 45 and 55 ℃, and the powdered activated carbon in the 200-300-mesh interval is selected.
By adopting the technical scheme, the color removal effect of the activated carbon is better at about 50 ℃, and the powdered activated carbon is easy to filter after color removal.
Drawings
Fig. 1 is a flow chart of a preparation method of a soapberry plant extract facial mousse.
Detailed Description
The present invention will be described in further detail with reference to the following drawings and examples. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1
As shown in fig. 1: a soapberry plant extract face-cleaning mousse comprises the following formula components: 0.05 part by weight of disodium EDTA; 2 parts by weight of glycerol; 0.1 part by weight of hydroxyethyl cellulose; 4 parts by weight of sodium lauroyl sarcosinate; 0.05 part by weight of capryloyl glycine; 0.5 part by weight of sodium cocoyl isethionate; 0.1 part by weight of polyquaternium-52; 1 part by weight of sodium pyrrolidone carboxylate; 2 parts by weight of disodium cocoyl amphodiacetate; 5 parts by weight of cocamidopropyl betaine; 0.1 part by weight of allantoin; 0.1 part by weight of zymosan; 0.05 part by weight of carboxymethyl chitosan; 5 parts by weight of soapberry extract; 1 part by weight of immature bitter orange extract; 0.3 parts by weight of hexanediol; 0.4 part by weight of p-hydroxyacetophenone; 0.05 part by weight of ethylhexylglycerin; TO 100 parts by weight of yeast fermentation product filtrate.
As shown in fig. 1: the preparation method comprises the following steps: the method comprises the following steps: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
Example 2
As shown in fig. 1: a soapberry plant extract face-cleaning mousse comprises the following formula components: 0.1 part by weight of disodium EDTA; 4 parts by weight of glycerol; 0.2 part by weight of hydroxyethyl cellulose; 6 parts by weight of sodium lauroyl sarcosinate; 0.1 part by weight of capryloyl glycine; 1 part by weight of sodium cocoyl isethionate; 0.4 part by weight of polyquaternium-52; 2 parts by weight of sodium pyrrolidone carboxylate; 3 parts by weight of disodium cocoyl amphodiacetate; 8 parts by weight of cocamidopropyl betaine; 0.1 part by weight of allantoin; 0.1 part by weight of zymosan; 0.1 part by weight of carboxymethyl chitosan; 6 parts by weight of soapberry extract; 1 part by weight of immature bitter orange extract; 0.5 parts by weight of hexanediol; 0.3 part by weight of p-hydroxyacetophenone; 0.06 parts by weight of ethylhexyl glycerin; TO 100 parts by weight of yeast fermentation product filtrate.
As shown in fig. 1: the preparation method comprises the following steps: the method comprises the following steps: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
Example 3
As shown in fig. 1: a soapberry plant extract face-cleaning mousse comprises the following formula components: 0.2 part by weight of disodium EDTA; 6 parts by weight of glycerol; 0.2 part by weight of hydroxyethyl cellulose; 6 parts by weight of sodium lauroyl sarcosinate; 0.2 part by weight of capryloyl glycine; 4 parts by weight of sodium cocoyl isethionate; 0.8 part by weight of polyquaternium-52; 3 parts by weight of sodium pyrrolidone carboxylate; 5 parts by weight of disodium cocoyl amphodiacetate; 10 parts by weight of cocamidopropyl betaine; 0.2 parts by weight of allantoin; 0.2 part by weight of zymosan; 0.1 part by weight of carboxymethyl chitosan; 6 parts by weight of soapberry extract; 1 part by weight of immature bitter orange extract; 0.8 parts by weight of hexanediol; 0.3 part by weight of p-hydroxyacetophenone; 0.03 parts by weight of ethylhexyl glycerol; TO 100 parts by weight of yeast fermentation product filtrate.
As shown in fig. 1: the preparation method comprises the following steps: the method comprises the following steps: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
Example 4
As shown in fig. 1: a soapberry plant extract face-cleaning mousse comprises the following formula components: 0.3 part by weight of disodium EDTA; 8 parts by weight of glycerol; 0.1 part by weight of hydroxyethyl cellulose; 5 parts by weight of sodium lauroyl sarcosinate; 0.6 part by weight of capryloyl glycine; 2 parts by weight of sodium cocoyl isethionate; 0.1 part by weight of polyquaternium-52; 3 parts by weight of sodium pyrrolidone carboxylate; 6 parts by weight of disodium cocoyl amphodiacetate; 15 parts by weight of cocamidopropyl betaine; 0.3 part by weight of allantoin; 0.2 part by weight of zymosan; 0.3 part by weight of carboxymethyl chitosan; 10 parts by weight of soapberry extract; 1 part by weight of immature bitter orange extract; 1 part by weight of hexanediol; 0.2 part by weight of p-hydroxyacetophenone; 0.06 parts by weight of ethylhexyl glycerin; TO 100 parts by weight of yeast fermentation product filtrate.
As shown in fig. 1: the preparation method comprises the following steps: the method comprises the following steps: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
Example 5
As shown in fig. 1: a soapberry plant extract face-cleaning mousse comprises the following formula components: 0.5 part by weight of disodium EDTA; 10 parts by weight of glycerol; 0.5 part by weight of hydroxyethyl cellulose; 10 parts by weight of sodium lauroyl sarcosinate; 1 part by weight of capryloyl glycine; 2 parts by weight of sodium cocoyl isethionate; 1 part by weight of polyquaternium-52; 2 parts by weight of sodium pyrrolidone carboxylate; 8 parts by weight of disodium cocoyl amphodiacetate; 20 parts by weight of cocamidopropyl betaine; 0.4 parts by weight of allantoin; 0.5 part by weight of zymosan; 0.5 parts by weight of carboxymethyl chitosan; 10 parts by weight of soapberry extract; 0.5 part by weight of immature bitter orange extract; 1.5 parts by weight of hexanediol; 0.5 part by weight of p-hydroxyacetophenone; 0.1 part by weight of ethylhexylglycerin; TO 100 parts by weight of yeast fermentation product filtrate.
As shown in fig. 1: the preparation method comprises the following steps: the method comprises the following steps: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
While the foregoing description shows and describes the preferred embodiments of the present invention, it is to be understood that the invention is not limited to the forms disclosed herein, but is not to be construed as excluding other embodiments and is capable of use in various other combinations, modifications, and environments and is capable of changes within the scope of the inventive concept as described herein, commensurate with the above teachings, or the skill or knowledge of the relevant art. And that modifications and variations may be effected by those skilled in the art without departing from the spirit and scope of the invention as defined by the appended claims.
Attached 1: test of foaming function
From the above 5 examples, 3 soapberry plant extract facial mousses prepared in the examples were randomly selected, and each of the sapindus extract facial mousses was prepared as a 10% aqueous solution by adding water, and the samples were numbered as sample No. 1,2 and 3. In addition, the commonly used detergent sodium laureth sulfate in the market is also added with water to prepare 10% aqueous solution, which is sample No. 4. The method comprises the following steps of loading and taking 4 solutions in equal amount into 4 foaming bottles, simultaneously extruding 5 lower pump heads, extruding foam on a flat and clean desktop, taking an initial photo, then taking the photo once every half hour, recording an experimental result, and analyzing and comparing to obtain a conclusion.
| Number 1 | Number 2 | No. 3 | Number 4 | |
| 0 minute | Initial foam | Initial foam | Initial foam | Initial foam |
| 30 minutes | Without change | Without change | Without conversion | Without change |
| 60 minutes | Without change | Without change | Without change | Foam thickness reduction |
| 90 minutes | Without change | Without change | Without change | Continued elimination of foam |
| 120 minutes | Foam thickness reduction | Foam thickness reduction | Foam thickness reduction | Depletion of foam |
And (2) attached: oil removal capability test
From the above 5 examples, 3 soapberry plant extract facial mousses prepared in the examples were randomly selected, and each of the sapindus extract facial mousses was prepared as a 10% aqueous solution by adding water, and the samples were numbered as sample No. 1,2 and 3. In addition, the commonly used detergent sodium laureth sulfate in the market is also added with water to prepare 10% aqueous solution, which is sample No. 4. Taking TPE thermoplastic elastomer plates with the same size, uniformly opening small holes with the diameter of 1 mm on the TPE plates, uniformly coating 5 g of solid lard on the surfaces of the TPE plates, washing the TPE plates by adopting the prepared solution, wherein the required gram weight is as shown in the following table
| Sample No. 1 | Sample No. 2 | Sample No. 3 | Sample No. 4 | |
| Gram weight | 7.5 g | 6.8 g | 8.2 g | 15.3 g |
From the comparison of the data in the table above, it can be seen that the gram weight required for washing 5 g of the solid lard oil by the soapberry plant extract facial cleansing mousse is significantly less than the gram weight required for washing 5 g of the solid lard oil by the sodium laureth sulfate, and the oil removal capability of the soapberry plant extract facial cleansing mousse is better than that of the sodium laureth sulfate.
And (3) in addition: safety capability test
The subjects (average age 25 years, 24-27 years) were subjected to skin patch test (patch test) on the forearm using Finn Chamber. However, patients with psoriasis (psoriasis), eczema (rash) or other skin lesions who are pregnant, lactating or taking contraceptives, antihistamines etc. cannot participate in this study. After the test site was wiped with 70% ethanol and dried, 25-30. mu.L of the above random sample of the example was added to the Finnish chamber, which was fixed to the arm area without being wetted. Removing the patch after 24 h; the test site was marked with a marking pen and after 30 minutes, the test site was again observed 24 hours later and the tester information was recorded in detail. The degree of irritation was classified according to the criteria (ICDRG), and was determined 30 minutes after removal of the patch, again after 24 hours, and after determination according to the criteria (Table 1) of the International Contact Dermatitis research Association for skin reactions, the average score was estimated according to the formula of the average score of skin reactions [ Table 2], and whether irritation was observed or not was determined according to the score results in the skin patch test (patch test).
And (4) judging the standard:
TABLE 1 International research group of Contact Dermatitis ((International Contact Dermatitis research: ICDRG)
The standard for judging skin reaction
1) Negative (-): has no irritation
2) Double or slice interaction and erythrema (+ -); micro-stimulation
Faint barely visible mild erythema
Erythema + Industration (+); mild stimulation
Has obvious erythema and skin sclerosis
Erythema + Industration + Vesicle (++); middle stimulation
Erythema, sclerosis, blisters
5) Erythema + Industration + Bullae (++); strong stimulation
Erythema, sclerosis, and blisters
Equation for calculating average skin reaction score Mean score
i-results of respective scores obtained by removing the patch and measuring the site after 30 minutes and 24 hours according to the ICDRG standard. The two reactions labeled erythena and edema, all apply.
j-removal of the patch, 30 minutes later, 24 hours later, the respective skin responded to the number of testers, marking both the erythema and edema responses, and all were applicable.
| Determination (Grade) | Mean Score |
| Without irritation (1) | 0.00～0.75 |
| Micro-stimulation (2) | 0.76～1.50 |
| Light stimulus (3) | 1.51～2.50 |
| Middle stimulus (4) | 2.51～4.00 |
| Strong stimulation (5) | 4.01 |
TABLE 2 skin Patch test results
2. Results (ICDRG Score Total)
| Sample/time (hr) | Soapberry plant extract face-cleaning mousse |
| 30min | 0.00 |
Mean Score：
Soapberry plant extract facial cleansing mousse is 0.00; without irritation (1)
Personnel information
| Serial number | Name (I) | Age (age) | Sex |
| 1 | ZZ | 25 | Woman |
| 2 | WXB | 26 | Woman |
| 3 | LDM | 24 | For male |
| 4 | YR | 25 | |
| 5 | HB | 24 | For male |
| 6 | HGY | 26 | For male |
[ Table 3] test-participated person information
Removing the patch for 30min to obtain skin state
As a result: the experiment result of skin allergy test of the soapberry plant extract facial cleansing mousse sample shows that no irritation can be observed after 6 people remove the patch for 30 minutes.
Soapberry plant extract facial cleansing mousse is 0.00; has no irritation (1).
Claims (8)
1. A soapberry plant extract face-cleaning mousse is characterized in that: comprises the following raw materials of 0.05-0.5 weight portion of EDTA disodium; 1-10 parts by weight of glycerol; 0.03 to 0.5 part by weight of hydroxyethyl cellulose; 2-10 parts by weight of sodium lauroyl sarcosinate; 0.05-1 weight part of capryloyl glycine; 0.5 to 5 parts by weight of sodium cocoyl isethionate; 0.05-3 parts by weight of polyquaternium-52; 0.5 to 5 parts by weight of sodium pyrrolidone carboxylate; 1-10 parts by weight of disodium cocoyl amphodiacetate; 4-20 parts by weight of cocamidopropyl betaine; 0.05-1 parts by weight of allantoin; 0.01-0.5 weight parts of zymosan; 0.01-0.5 parts by weight of carboxymethyl chitosan; 1-10 parts by weight of soapberry extract; 0.1-2 parts by weight of immature bitter orange extract; 0.1 to 2 parts by weight of hexanediol; 0.1-1 weight parts of p-hydroxyacetophenone; 0.01-0.5 parts by weight of ethylhexyl glycerol; TO 100 parts by weight of yeast fermentation product filtrate.
2. The soapberry plant extract facial mousse according to claim 1, wherein: the hexanediol is 1, 2-hexanediol.
3. A method of preparing a soapberry plant extract facial mousse according to claim 1, comprising the steps of: the method comprises the following steps: selecting a soapberry raw material, and crushing the soapberry raw material by using a crusher; step two: according to the material ratio of 1: 1-5 proportion of ethanol, refluxing and extracting for 4-8 hours at 50-75 ℃; step three: cooling to room temperature, and filtering with 0.5-1 μm filter paper plate; step four: removing color of the filtrate with 0.5-3% active carbon for 0.5-2 hr; step five: filtering with 1 μm filter paper plate; step six: concentrating the filtrate at 60-70 deg.C until no ethanol remains; step seven: adding pure water 1-2 times of the weight of the concentrated residue to dissolve the concentrated residue; step eight: pouring the residual solution into a separating funnel, adding 1/3-1 volume of dichloromethane of the residual solution into the separating funnel, shaking and vibrating for 30-60 seconds, standing for completely layering, discharging the lower layer of dichloromethane solution, and repeating the process for 2-3 times; step nine: concentrating the filtrate at 60-70 deg.C until no dichloromethane remains; step ten: detecting the solid content, adding pure water and glycerol until the solid content is more than 20% and the glycerol content is 30-35%.
4. The method for preparing the soapberry plant extract facial mousse according to claim 3, wherein the method comprises the following steps: the soapberry fruit is washed by deionized water for 3 times before being crushed, water is drained, soapberry peel is stripped, the soapberry fruit peel is placed in an electric heating constant-temperature air blast drying box at 60 ℃ for drying, then the soapberry fruit is crushed by a miniature plant crusher, and the soapberry fruit is sieved by a standard sieve of 40 meshes.
5. The method for preparing the soapberry plant extract facial mousse according to claim 3, wherein the method comprises the following steps: the purity of the ethanol in the above steps is 95%.
6. The method for preparing the soapberry plant extract facial mousse according to claim 3, wherein the method comprises the following steps: and sixthly, distilling the ethanol solution in the filtrate concentration process in the step nine by using a rotary evaporator, vacuumizing the interior of the rotary evaporator, heating, stopping heating in the evaporation stopping process, stopping vacuumizing, and finally cutting off the power supply of the rotary evaporator.
7. The method for preparing the soapberry plant extract facial mousse according to claim 3, wherein the method comprises the following steps: and in the step eight, shaking at a fixed frequency is carried out on the residue solution and the separating funnel by adopting a shaking table, wherein the rotation speed of the shaking table is 150 r/min.
8. The method for preparing the soapberry plant extract facial mousse according to claim 3, wherein the method comprises the following steps: in the fourth step, the temperature in the color removing process of the activated carbon is set between 45 ℃ and 55 ℃, and the powdery activated carbon in the range of 200 meshes and 300 meshes is selected.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516050A (en) * | 2020-12-23 | 2021-03-19 | 现代百朗德生物科技(江苏)有限公司 | Facial cleanser containing soapberry fruit extract product and preparation method thereof |
| CN112656718A (en) * | 2021-02-03 | 2021-04-16 | 现代百朗德生物科技(江苏)有限公司 | Whitening mask containing cordyceps sinensis extract |
| CN114533603A (en) * | 2022-03-30 | 2022-05-27 | 威莱(广州)日用品有限公司 | Nourishing and moisturizing body wash |
| CN115721592A (en) * | 2022-12-12 | 2023-03-03 | 深圳市理然化妆品有限公司 | Soapberry face-cleaning mousse and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104840387A (en) * | 2015-04-28 | 2015-08-19 | 百朗德生物化学海门有限公司 | Low-irritation-smell soapberry fruit extract production method |
| CN108210399A (en) * | 2018-03-31 | 2018-06-29 | 佛山娇芙生物科技有限公司 | A kind of soapberry cleans gel |
| CN109528523A (en) * | 2018-12-28 | 2019-03-29 | 广州蔻赛生物科技有限公司 | A kind of amino acid cleansing cream |
| CN110339109A (en) * | 2019-07-05 | 2019-10-18 | 广州品爵生物科技有限公司 | A kind of mild multiple-effect facial cleaner and preparation method thereof |
-
2019
- 2019-11-05 CN CN201911073101.0A patent/CN110882190A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104840387A (en) * | 2015-04-28 | 2015-08-19 | 百朗德生物化学海门有限公司 | Low-irritation-smell soapberry fruit extract production method |
| CN108210399A (en) * | 2018-03-31 | 2018-06-29 | 佛山娇芙生物科技有限公司 | A kind of soapberry cleans gel |
| CN109528523A (en) * | 2018-12-28 | 2019-03-29 | 广州蔻赛生物科技有限公司 | A kind of amino acid cleansing cream |
| CN110339109A (en) * | 2019-07-05 | 2019-10-18 | 广州品爵生物科技有限公司 | A kind of mild multiple-effect facial cleaner and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 曾虹燕等: "《生物化学实验》", 31 October 2014, 湘潭大学出版社 * |
| 王昌涛等: "《化妆品植物添加剂的开发与应用》", 30 April 2013, 中国轻工业出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112516050A (en) * | 2020-12-23 | 2021-03-19 | 现代百朗德生物科技(江苏)有限公司 | Facial cleanser containing soapberry fruit extract product and preparation method thereof |
| CN112656718A (en) * | 2021-02-03 | 2021-04-16 | 现代百朗德生物科技(江苏)有限公司 | Whitening mask containing cordyceps sinensis extract |
| CN114533603A (en) * | 2022-03-30 | 2022-05-27 | 威莱(广州)日用品有限公司 | Nourishing and moisturizing body wash |
| CN115721592A (en) * | 2022-12-12 | 2023-03-03 | 深圳市理然化妆品有限公司 | Soapberry face-cleaning mousse and preparation method thereof |
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