CN110843275B - 一种高透气抗菌功能性复合面料的制备方法 - Google Patents
一种高透气抗菌功能性复合面料的制备方法 Download PDFInfo
- Publication number
- CN110843275B CN110843275B CN201911206018.6A CN201911206018A CN110843275B CN 110843275 B CN110843275 B CN 110843275B CN 201911206018 A CN201911206018 A CN 201911206018A CN 110843275 B CN110843275 B CN 110843275B
- Authority
- CN
- China
- Prior art keywords
- fabric
- layer
- antibacterial
- functional
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 251
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 137
- 239000002131 composite material Substances 0.000 title claims abstract description 78
- 238000002360 preparation method Methods 0.000 title claims abstract description 33
- 239000010410 layer Substances 0.000 claims abstract description 188
- 239000000835 fiber Substances 0.000 claims abstract description 59
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 37
- 150000001875 compounds Chemical class 0.000 claims abstract description 33
- 230000035699 permeability Effects 0.000 claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000003292 glue Substances 0.000 claims abstract description 18
- 239000010440 gypsum Substances 0.000 claims abstract description 18
- 229910052602 gypsum Inorganic materials 0.000 claims abstract description 18
- 239000002105 nanoparticle Substances 0.000 claims abstract description 18
- 239000000843 powder Substances 0.000 claims abstract description 18
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 18
- 239000003094 microcapsule Substances 0.000 claims abstract description 16
- 230000001954 sterilising effect Effects 0.000 claims description 31
- 238000004659 sterilization and disinfection Methods 0.000 claims description 31
- 239000000853 adhesive Substances 0.000 claims description 28
- 230000001070 adhesive effect Effects 0.000 claims description 28
- 239000000341 volatile oil Substances 0.000 claims description 27
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 22
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 22
- 241001330002 Bambuseae Species 0.000 claims description 22
- 235000009024 Ceanothus sanguineus Nutrition 0.000 claims description 22
- 240000003553 Leptospermum scoparium Species 0.000 claims description 22
- 235000015459 Lycium barbarum Nutrition 0.000 claims description 22
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 22
- 239000011425 bamboo Substances 0.000 claims description 22
- 239000011247 coating layer Substances 0.000 claims description 20
- 229920002635 polyurethane Polymers 0.000 claims description 20
- 239000004814 polyurethane Substances 0.000 claims description 20
- 125000003118 aryl group Chemical group 0.000 claims description 19
- 239000000679 carrageenan Substances 0.000 claims description 18
- 235000010418 carrageenan Nutrition 0.000 claims description 18
- 229920001525 carrageenan Polymers 0.000 claims description 18
- 229940113118 carrageenan Drugs 0.000 claims description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 18
- 239000011248 coating agent Substances 0.000 claims description 18
- 238000000576 coating method Methods 0.000 claims description 18
- 238000010438 heat treatment Methods 0.000 claims description 18
- 229920000728 polyester Polymers 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- 229920001285 xanthan gum Polymers 0.000 claims description 18
- 235000010493 xanthan gum Nutrition 0.000 claims description 18
- 239000000230 xanthan gum Substances 0.000 claims description 18
- 229940082509 xanthan gum Drugs 0.000 claims description 18
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 18
- 235000012239 silicon dioxide Nutrition 0.000 claims description 17
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 16
- 239000012964 benzotriazole Substances 0.000 claims description 16
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 16
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 16
- -1 polydimethylsiloxane Polymers 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 15
- 239000011858 nanopowder Substances 0.000 claims description 15
- 239000003921 oil Substances 0.000 claims description 15
- 244000068697 Vitis rotundifolia Species 0.000 claims description 13
- 235000006359 Vitis rotundifolia var rotundifolia Nutrition 0.000 claims description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 239000003610 charcoal Substances 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 11
- 241000721153 Chloranthus japonicus Species 0.000 claims description 9
- 229920000433 Lyocell Polymers 0.000 claims description 9
- 241000951473 Schizonepeta Species 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 238000009958 sewing Methods 0.000 claims description 9
- 239000004902 Softening Agent Substances 0.000 claims description 8
- 230000008569 process Effects 0.000 claims description 8
- 240000004160 Capsicum annuum Species 0.000 claims description 6
- 235000008534 Capsicum annuum var annuum Nutrition 0.000 claims description 6
- 241000255581 Drosophila <fruit fly, genus> Species 0.000 claims description 6
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 6
- 239000010692 aromatic oil Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000013329 compounding Methods 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 235000008397 ginger Nutrition 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 238000006116 polymerization reaction Methods 0.000 claims description 6
- 238000004080 punching Methods 0.000 claims description 6
- 238000005507 spraying Methods 0.000 claims description 6
- 238000009941 weaving Methods 0.000 claims description 6
- 229920002101 Chitin Polymers 0.000 claims description 5
- 230000003014 reinforcing effect Effects 0.000 claims description 4
- 244000273928 Zingiber officinale Species 0.000 claims 1
- 229920002521 macromolecule Polymers 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 7
- 230000001681 protective effect Effects 0.000 abstract description 5
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 abstract description 4
- 229910001424 calcium ion Inorganic materials 0.000 abstract description 4
- 230000003075 superhydrophobic effect Effects 0.000 abstract description 4
- 239000002344 surface layer Substances 0.000 abstract description 4
- 239000004753 textile Substances 0.000 abstract description 4
- 230000003385 bacteriostatic effect Effects 0.000 abstract description 2
- 239000002939 oilproofing Substances 0.000 abstract 1
- 230000002401 inhibitory effect Effects 0.000 description 25
- 229920001661 Chitosan Polymers 0.000 description 12
- 235000010679 Nepeta cataria Nutrition 0.000 description 10
- 244000063299 Bacillus subtilis Species 0.000 description 9
- 235000014469 Bacillus subtilis Nutrition 0.000 description 9
- 241000588724 Escherichia coli Species 0.000 description 9
- 241000191967 Staphylococcus aureus Species 0.000 description 9
- 230000003115 biocidal effect Effects 0.000 description 9
- 241001529733 Nepeta Species 0.000 description 8
- ZDKZHVNKFOXMND-UHFFFAOYSA-N epinepetalactone Chemical compound O=C1OC=C(C)C2C1C(C)CC2 ZDKZHVNKFOXMND-UHFFFAOYSA-N 0.000 description 8
- 241000894006 Bacteria Species 0.000 description 7
- 241000878007 Miscanthus Species 0.000 description 5
- 230000006750 UV protection Effects 0.000 description 5
- 241000234314 Zingiber Species 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- 230000036541 health Effects 0.000 description 5
- 239000007789 gas Substances 0.000 description 4
- 230000002209 hydrophobic effect Effects 0.000 description 4
- 230000004224 protection Effects 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 241000255925 Diptera Species 0.000 description 2
- 240000009215 Nepeta cataria Species 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 239000003242 anti bacterial agent Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000010292 electrical insulation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 210000004209 hair Anatomy 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 241000238876 Acari Species 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000002781 deodorant agent Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 239000010436 fluorite Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
- B32B5/08—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer the fibres or filaments of a layer being of different substances, e.g. conjugate fibres, mixture of different fibres
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B3/00—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form
- B32B3/26—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer
- B32B3/266—Layered products comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar shape; Layered products comprising a layer having particular features of form characterised by a particular shape of the outline of the cross-section of a continuous layer; characterised by a layer with cavities or internal voids ; characterised by an apertured layer characterised by an apertured layer, the apertures going through the whole thickness of the layer, e.g. expanded metal, perforated layer, slit layer regular cells B32B3/12
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B33/00—Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/02—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
- B32B5/06—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer characterised by a fibrous or filamentary layer mechanically connected, e.g. by needling to another layer, e.g. of fibres, of paper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B5/00—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
- B32B5/22—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
- B32B5/24—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
- B32B5/26—Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer another layer next to it also being fibrous or filamentary
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B7/00—Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
- B32B7/04—Interconnection of layers
- B32B7/12—Interconnection of layers using interposed adhesives or interposed materials with bonding properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
- D06N3/0006—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using woven fabrics
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
- D06N3/0015—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using fibres of specified chemical or physical nature, e.g. natural silk
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
- D06N3/0059—Organic ingredients with special effects, e.g. oil- or water-repellent, antimicrobial, flame-resistant, magnetic, bactericidal, odour-influencing agents; perfumes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
- D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2255/00—Coating on the layer surface
- B32B2255/02—Coating on the layer surface on fibrous or filamentary layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2255/00—Coating on the layer surface
- B32B2255/26—Polymeric coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
- B32B2262/02—Synthetic macromolecular fibres
- B32B2262/0276—Polyester fibres
- B32B2262/0284—Polyethylene terephthalate [PET] or polybutylene terephthalate [PBT]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
- B32B2262/10—Inorganic fibres
- B32B2262/106—Carbon fibres, e.g. graphite fibres
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2262/00—Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
- B32B2262/14—Mixture of at least two fibres made of different materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/20—Properties of the layers or laminate having particular electrical or magnetic properties, e.g. piezoelectric
- B32B2307/206—Insulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/20—Properties of the layers or laminate having particular electrical or magnetic properties, e.g. piezoelectric
- B32B2307/21—Anti-static
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/30—Properties of the layers or laminate having particular thermal properties
- B32B2307/304—Insulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/714—Inert, i.e. inert to chemical degradation, corrosion
- B32B2307/7145—Rot proof, resistant to bacteria, mildew, mould, fungi
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/724—Permeability to gases, adsorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/70—Other properties
- B32B2307/73—Hydrophobic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
本发明公开了一种高透气抗菌功能性复合面料的制备方法,包括面料本体,所述面料本体由面料基层、透气层和功能性抗菌层组成,所述面料本体两侧均设有功能性抗菌层。本发明通过采用舒适耐用的纤维纺品复合结构,配合透气孔内部的短毛绒,使面料保暖,提高透气散湿能力,能够使面料快速干燥,功能性抗菌层抗菌、抑菌、除螨、防臭,亲肤不刺激,面料柔软舒适,二氧化硅纳米微粒超疏水超疏油,使面料表层形成保护膜,避免水滴大分子通过,防水防油效果好,使面料便于清理,复合增强胶与石膏粉中的钙离子反应生成柔软、富有弹性的凝胶,包裹天然抗菌因子复合物形成微胶囊,缓释天然抗菌因子,使面料能够长久有效的抗菌灭菌。
Description
技术领域
本发明涉及面料领域,具体涉及一种高透气抗菌功能性复合面料的制备方法。
背景技术
衣服泛指身上穿的各种衣裳服装,衣服的本意是防寒保暖,护身的介质;而在现代社会衣服已经逐渐演化为人体的装饰物品,更多的时候象征了一个人的生活水准和社会地位;同时在衣服基本功能不变的基础上,人们越来越多的注重衣物对身体的保健作用,随着科技的发展和人民生活水平的提高,对于面料的安全性的需求也不断扩大,人们对服装面料的功能性、舒适性、健康性、环保性及保健性都有更高的要求。不断的研发衣服的新材料,利用适当的工艺将不同材料的各种功效添加到衣料中,增加了衣服的功能性。
近年来,人们对服装面料的舒适性、健康性、安全性和环保性等要求越来越高,对安全高效抗菌服饰的功能需求越来越多;在生活中,人们不可避免的接触到各种各样的细菌、真菌等微生物,这些微生物在合适的外界条件下,会迅速繁殖,并通过接触等方式传播疾病,影响人们的身体健康和正常的工作、学习和生活。纤维属于多孔性材料,叠加编织后又会形成无数空隙的多层体,因此织物较容易吸附菌类。同时,生态环境和微生物环境污染也日益严重,使得纤维很容易发生霉变、黄变和异味,且纤维纺织品在使用过程中与人体皮肤直接接触,人体的分泌物和污垢会粘附在纤维上滋生螨虫和细菌,对人体造成不可预知的安全隐患。
在现有的抗菌技术中,利用银、铜、锌等金属的抗菌能力,通过物理吸附离子交换等方法,将银、铜、锌等金属(或其离子)固定在氟石、硅胶等多孔材料的表面制成抗菌剂,然后将其加入到相应的织物中即获得具有抗菌能力的面料,虽然这些金属抗菌剂虽具有良好的抗菌性能,但可能并不适用于肌肤敏感人群,穿戴不舒适,容易造成肌肤过敏。
因此,发明一种高透气抗菌功能性复合面料的制备方法来解决上述问题很有必要。
发明内容
本发明的目的是提供一种高透气抗菌功能性复合面料的制备方法,通过采用舒适耐用的纤维纺品复合结构,配合透气孔内部的短毛绒,使面料保暖,提高透气散湿能力,能够使面料快速干燥,功能性抗菌层采用竹炭纤维与涤纶纤维经纬编织制成,配合功能涂料层,抗菌、抑菌、除螨、防臭,亲肤不刺激,面料柔软舒适,二氧化硅纳米微粒超疏水超疏油,使面料表层形成保护膜,避免水滴大分子通过,防水防油效果好,使面料便于清理,复合增强胶与石膏粉中的钙离子反应生成柔软、富有弹性的凝胶,包裹天然抗菌因子复合物形成微胶囊,缓释天然抗菌因子,使面料能够长久有效的抗菌灭菌,以解决技术中的上述不足之处。
为了实现上述目的,本发明提供如下技术方案:一种高透气抗菌功能性复合面料的制备方法,包括面料本体,所述面料本体由面料基层、透气层和功能性抗菌层组成,所述面料本体两侧均设有功能性抗菌层,所述面料基层和透气层设置在两层功能性抗菌层之间,且面料基层设置在透气层底部,靠近面料基层一侧的所述功能性抗菌层表面开设有若干均匀分布的透气孔,所述面料基层与透气层缝合连接,两个所述功能性抗菌层分别与面料基层和透气层通过胶黏剂胶接;
所述面料基层由莱赛尔纤维与莫代尔纤维混纺制成,所述透气层由戈尔特斯面料制成,所述功能性抗菌层由竹炭纤维与涤纶纤维经纬编织制成,所述功能性抗菌层表面设有功能涂料层,所述功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯60-70份、竹原纤维纳米粉末20-30份、二氧化硅纳米微粒10-15份、茶树精油8-12份、石膏粉8-12份、复合增强胶8-12份、天然抗菌因子复合物3-6份、油溶性苯并三唑1-3份、柔软剂ES 2-5份、聚二甲基硅氧烷2-5份和芳香剂1-3份,该复合面料的制备方法如下:
S1:使用莱赛尔纤维与莫代尔纤维混纺制成面料基层,使用竹炭纤维与涤纶纤维经纬编织成抗菌织物,并裁剪戈尔特斯面料,备用;
S2:制备功能涂料层,具体如下:
S2.1:将油溶性苯并三唑溶解在茶树精油中,并使用复合增强胶将天然抗菌因子复合物包成微胶囊;
S2.2:按比例将原纤维纳米粉末、二氧化硅纳米微粒和石膏粉加入双组分水性聚氨酯中,充分搅拌均匀后,加入S2.1中制备的微胶囊和茶树精油,并加入柔软剂ES、聚二甲基硅氧烷和芳香剂,搅拌均匀后获得功能增强复合物;
S2.3:将功能增强复合物移至反应釜中,抽真空至釜内真空度为6-12MPa,随后通入氮气至釜内压力为0.03-0.05MPa,加热至60-70℃,聚合反应1-2h后冷却,获得功能增强涂料;
S3:将生姜水和柠檬酸与水以3-4:1-2:16的比例混合,搅拌均匀后加热至沸腾,将面料基层、抗菌织物和戈尔特斯面料依次投入沸腾的混合液体中杀菌,5-8min后捞出晾干,备用;
S4:将功能增强涂料均匀喷洒在两个抗菌织物两侧表面,使其均匀浸透,将该结构层在50-80℃下预烘10-15min,缓慢升温至80-100℃下烘烤8min使功能增强涂料固化成型,得功能性抗菌层;
S5:将一个功能性抗菌层均匀打孔,使透气孔均匀分布在功能性抗菌层表面,将带有透气孔的功能性抗菌层与面料基层使用胶黏剂胶接,将另一功能性抗菌层与戈尔特斯面料使用胶黏剂胶接,制成第一面料层,使用涤纶纤维通过针孔扎绒工艺在透气孔内的面料基层表面添加短毛绒,制成第二面料层;
S6:将第一面料层与第二面料层压平除皱,随后将第一面料层与第二面料层对齐后再次压平,将两者缝合连接后完成功能性复合面料的制备。
优选的,所述功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯65-68份、竹原纤维纳米粉末23-26份、二氧化硅纳米微粒12-15份、茶树精油9-11份、石膏粉8-11份、复合增强胶8-11份、天然抗菌因子复合物3-5份、油溶性苯并三唑1-3份、柔软剂ES 2-4份、聚二甲基硅氧烷3-5份和芳香剂1-3份。
优选的,所述天然抗菌因子复合物包括脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油,所述脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油的添加比例设置为脱乙酰甲壳质:荆芥叶片提取物:逐蝇梅提取物:银线草芳香油=3:1:1:1。
优选的,所述复合增强胶由卡拉胶和黄原胶复合制成,所述卡拉胶和黄原胶的添加比例设置为卡拉胶:黄原胶=1:1。
优选的,所述胶黏剂设置为聚氨酯胶粘剂。
优选的,所述芳香剂设置为众香子油。
在上述技术方案中,本发明提供的技术效果和优点:
1、通过采用舒适耐用的纤维纺品复合结构,配合透气孔内部的短毛绒,使面料保暖,提高透气散湿能力,能够使面料快速干燥,功能性抗菌层采用竹炭纤维与涤纶纤维经纬编织制成,配合功能涂料层,抗菌、抑菌、除螨、防臭,亲肤不刺激,面料柔软舒适,二氧化硅纳米微粒超疏水超疏油,使面料表层形成保护膜,避免水滴大分子通过,防水防油效果好,使面料便于清理,复合增强胶与石膏粉中的钙离子反应生成柔软、富有弹性的凝胶,包裹天然抗菌因子复合物形成微胶囊,缓释天然抗菌因子,使面料能够长久有效的抗菌灭菌;
2、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油与茶树精油能够驱赶蚊虫,呵护肌肤,油溶性苯并三唑均匀的分布在功能性抗菌层内部,能够提高面料的抗紫外线能力,聚二甲基硅氧烷的加入使功能性抗菌层对热和化学试剂稳定,保证功能性抗菌层不被水润湿,拥有良好的耐老化性能、优异的疏水性与电绝缘性,能够增强纤维强度且使面料抗静电,避免灰尘吸附。
附图说明
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
图1为本发明的整体结构示意图;
图2为本发明的剖视图。
附图标记说明:
1面料本体、2面料基层、3透气层、4功能性抗菌层、5透气孔。
具体实施方式
为了使本领域的技术人员更好地理解本发明的技术方案,下面将结合附图对本发明作进一步的详细介绍。
本发明提供了如图1-2所示的一种高透气抗菌功能性复合面料的制备方法,包括面料本体1,所述面料本体1由面料基层2、透气层3和功能性抗菌层4组成,所述面料本体1两侧均设有功能性抗菌层4,所述面料基层2和透气层3设置在两层功能性抗菌层4之间,且面料基层2设置在透气层3底部,靠近面料基层2一侧的所述功能性抗菌层4表面开设有若干均匀分布的透气孔5,所述面料基层2与透气层3缝合连接,两个所述功能性抗菌层4分别与面料基层2和透气层3通过胶黏剂胶接;
所述面料基层2由莱赛尔纤维与莫代尔纤维混纺制成,所述透气层3由戈尔特斯面料制成,所述功能性抗菌层4由竹炭纤维与涤纶纤维经纬编织制成,所述功能性抗菌层4表面设有功能涂料层,
实施例1:
功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯65份、竹原纤维纳米粉末23份、二氧化硅纳米微粒12份、茶树精油9份、石膏粉8份、复合增强胶8份、天然抗菌因子复合物3份、油溶性苯并三唑1份、柔软剂ES 2份、聚二甲基硅氧烷3份和芳香剂1份,该复合面料的制备方法如下:
S1:使用莱赛尔纤维与莫代尔纤维混纺制成面料基层2,使用竹炭纤维与涤纶纤维经纬编织成抗菌织物,并裁剪戈尔特斯面料,备用;
S2:制备功能涂料层,具体如下:
S2.1:将油溶性苯并三唑溶解在茶树精油中,并使用复合增强胶将天然抗菌因子复合物包成微胶囊;
S2.2:按比例将原纤维纳米粉末、二氧化硅纳米微粒和石膏粉加入双组分水性聚氨酯中,充分搅拌均匀后,加入S2.1中制备的微胶囊和茶树精油,并加入柔软剂ES、聚二甲基硅氧烷和芳香剂,搅拌均匀后获得功能增强复合物;
S2.3:将功能增强复合物移至反应釜中,抽真空至釜内真空度为6MPa,随后通入氮气至釜内压力为0.03MPa,加热至60℃,聚合反应1h后冷却,获得功能增强涂料;
S3:将生姜水和柠檬酸与水以3:1:16的比例混合,搅拌均匀后加热至沸腾,将面料基层2、抗菌织物和戈尔特斯面料依次投入沸腾的混合液体中杀菌,5min后捞出晾干,备用;
S4:将功能增强涂料均匀喷洒在两个抗菌织物两侧表面,使其均匀浸透,将该结构层在50℃下预烘10min,缓慢升温至80℃下烘烤8min使功能增强涂料固化成型,得功能性抗菌层4;
S5:将一个功能性抗菌层4均匀打孔,使透气孔5均匀分布在功能性抗菌层4表面,将带有透气孔5的功能性抗菌层4与面料基层2使用胶黏剂胶接,将另一功能性抗菌层4与戈尔特斯面料使用胶黏剂胶接,制成第一面料层,使用涤纶纤维通过针孔扎绒工艺在透气孔5内的面料基层2表面添加短毛绒,制成第二面料层;
S6:将第一面料层与第二面料层压平除皱,随后将第一面料层与第二面料层对齐后再次压平,将两者缝合连接后完成功能性复合面料的制备。
进一步的,在上述技术方案中,所述天然抗菌因子复合物包括脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油,所述脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油的添加比例设置为脱乙酰甲壳质:荆芥叶片提取物:逐蝇梅提取物:银线草芳香油=3:1:1:1;
进一步的,在上述技术方案中,所述复合增强胶由卡拉胶和黄原胶复合制成,所述卡拉胶和黄原胶的添加比例设置为卡拉胶:黄原胶=1:1;
进一步的,在上述技术方案中,所述胶黏剂设置为聚氨酯胶粘剂,所述芳香剂设置为众香子油。
本实施例中制备的高透气抗菌功能性复合面料抗拉伸能力强,透气性好,透湿率好,且能够快速干燥,有效隔绝水滴大分子,疏水疏油、防潮耐磨,抗紫外线,面料柔软舒适,另外本实施例中对制备的高透气抗菌功能性复合面料进行了性能测试,结果显示:该复合面料透湿率为287g/m2·24h,透气率为66m2/s,制备的复合面料对金黄色葡萄球菌的抑制杀菌率为95.8%,对大肠杆菌的抑制杀菌率为96.8%,对枯草杆菌的抑制杀菌率为97.9%,将本复合面料洗涤10次后,该复合面料对金黄色葡萄球菌的抑制杀菌率为93.2%,对大肠杆菌的抑制杀菌率为94.6%,对枯草杆菌的抑制杀菌率为96.0%,能够满足衣物面料安全使用要求,而且相较于现有的面料,舒适性和透气性更好。
实施例2:
功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯66份、竹原纤维纳米粉末24份、二氧化硅纳米微粒13份、茶树精油10份、石膏粉9份、复合增强胶9份、天然抗菌因子复合物4份、油溶性苯并三唑2份、柔软剂ES 3份、聚二甲基硅氧烷4份和芳香剂2份,该复合面料的制备方法如下:
S1:使用莱赛尔纤维与莫代尔纤维混纺制成面料基层2,使用竹炭纤维与涤纶纤维经纬编织成抗菌织物,并裁剪戈尔特斯面料,备用;
S2:制备功能涂料层,具体如下:
S2.1:将油溶性苯并三唑溶解在茶树精油中,并使用复合增强胶将天然抗菌因子复合物包成微胶囊;
S2.2:按比例将原纤维纳米粉末、二氧化硅纳米微粒和石膏粉加入双组分水性聚氨酯中,充分搅拌均匀后,加入S2.1中制备的微胶囊和茶树精油,并加入柔软剂ES、聚二甲基硅氧烷和芳香剂,搅拌均匀后获得功能增强复合物;
S2.3:将功能增强复合物移至反应釜中,抽真空至釜内真空度为8MPa,随后通入氮气至釜内压力为0.04MPa,加热至65℃,聚合反应1.5h后冷却,获得功能增强涂料;
S3:将生姜水和柠檬酸与水以3:1:16的比例混合,搅拌均匀后加热至沸腾,将面料基层2、抗菌织物和戈尔特斯面料依次投入沸腾的混合液体中杀菌,6min后捞出晾干,备用;
S4:将功能增强涂料均匀喷洒在两个抗菌织物两侧表面,使其均匀浸透,将该结构层在60℃下预烘12min,缓慢升温至90℃下烘烤8min使功能增强涂料固化成型,得功能性抗菌层4;
S5:将一个功能性抗菌层4均匀打孔,使透气孔5均匀分布在功能性抗菌层4表面,将带有透气孔5的功能性抗菌层4与面料基层2使用胶黏剂胶接,将另一功能性抗菌层4与戈尔特斯面料使用胶黏剂胶接,制成第一面料层,使用涤纶纤维通过针孔扎绒工艺在透气孔5内的面料基层2表面添加短毛绒,制成第二面料层;
S6:将第一面料层与第二面料层压平除皱,随后将第一面料层与第二面料层对齐后再次压平,将两者缝合连接后完成功能性复合面料的制备。
进一步的,在上述技术方案中,所述天然抗菌因子复合物包括脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油,所述脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油的添加比例设置为脱乙酰甲壳质:荆芥叶片提取物:逐蝇梅提取物:银线草芳香油=3:1:1:1;
进一步的,在上述技术方案中,所述复合增强胶由卡拉胶和黄原胶复合制成,所述卡拉胶和黄原胶的添加比例设置为卡拉胶:黄原胶=1:1;
进一步的,在上述技术方案中,所述胶黏剂设置为聚氨酯胶粘剂,所述芳香剂设置为众香子油。
对比实施例1,本实施例中制备的高透气抗菌功能性复合面料抗拉伸能力强,透气性好,透湿率好,且能够快速干燥,有效隔绝水滴大分子,疏水疏油、防潮耐磨,抗紫外线,面料柔软舒适,另外本实施例中对制备的高透气抗菌功能性复合面料进行了性能测试,结果显示:该复合面料透湿率为288g/m2·24h,透气率为67m2/s,制备的复合面料对金黄色葡萄球菌的抑制杀菌率为96.0%,对大肠杆菌的抑制杀菌率为97.4%,对枯草杆菌的抑制杀菌率为98.5%,将本复合面料洗涤10次后,该复合面料对金黄色葡萄球菌的抑制杀菌率为93.8%,对大肠杆菌的抑制杀菌率为95.0%,对枯草杆菌的抑制杀菌率为96.3%,能够满足衣物面料安全使用要求,而且相较于现有的面料,舒适性和透气性更好。
实施例3:
功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯67份、竹原纤维纳米粉末25份、二氧化硅纳米微粒14份、茶树精油10份、石膏粉10份、复合增强胶10份、天然抗菌因子复合物4份、油溶性苯并三唑2份、柔软剂ES 3份、聚二甲基硅氧烷4份和芳香剂2份,该复合面料的制备方法如下:
S1:使用莱赛尔纤维与莫代尔纤维混纺制成面料基层2,使用竹炭纤维与涤纶纤维经纬编织成抗菌织物,并裁剪戈尔特斯面料,备用;
S2:制备功能涂料层,具体如下:
S2.1:将油溶性苯并三唑溶解在茶树精油中,并使用复合增强胶将天然抗菌因子复合物包成微胶囊;
S2.2:按比例将原纤维纳米粉末、二氧化硅纳米微粒和石膏粉加入双组分水性聚氨酯中,充分搅拌均匀后,加入S2.1中制备的微胶囊和茶树精油,并加入柔软剂ES、聚二甲基硅氧烷和芳香剂,搅拌均匀后获得功能增强复合物;
S2.3:将功能增强复合物移至反应釜中,抽真空至釜内真空度为10MPa,随后通入氮气至釜内压力为0.04MPa,加热至68℃,聚合反应1.5h后冷却,获得功能增强涂料;
S3:将生姜水和柠檬酸与水以4:2:16的比例混合,搅拌均匀后加热至沸腾,将面料基层2、抗菌织物和戈尔特斯面料依次投入沸腾的混合液体中杀菌,7min后捞出晾干,备用;
S4:将功能增强涂料均匀喷洒在两个抗菌织物两侧表面,使其均匀浸透,将该结构层在70℃下预烘13min,缓慢升温至90℃下烘烤8min使功能增强涂料固化成型,得功能性抗菌层4;
S5:将一个功能性抗菌层4均匀打孔,使透气孔5均匀分布在功能性抗菌层4表面,将带有透气孔5的功能性抗菌层4与面料基层2使用胶黏剂胶接,将另一功能性抗菌层4与戈尔特斯面料使用胶黏剂胶接,制成第一面料层,使用涤纶纤维通过针孔扎绒工艺在透气孔5内的面料基层2表面添加短毛绒,制成第二面料层;
S6:将第一面料层与第二面料层压平除皱,随后将第一面料层与第二面料层对齐后再次压平,将两者缝合连接后完成功能性复合面料的制备。
进一步的,在上述技术方案中,所述天然抗菌因子复合物包括脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油,所述脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油的添加比例设置为脱乙酰甲壳质:荆芥叶片提取物:逐蝇梅提取物:银线草芳香油=3:1:1:1;
进一步的,在上述技术方案中,所述复合增强胶由卡拉胶和黄原胶复合制成,所述卡拉胶和黄原胶的添加比例设置为卡拉胶:黄原胶=1:1;
进一步的,在上述技术方案中,所述胶黏剂设置为聚氨酯胶粘剂,所述芳香剂设置为众香子油。
对比实施例1和2,本实施例中制备的高透气抗菌功能性复合面料抗拉伸能力强,透气性好,透湿率好,且能够快速干燥,有效隔绝水滴大分子,疏水疏油、防潮耐磨,抗紫外线,面料柔软舒适,另外本实施例中对制备的高透气抗菌功能性复合面料进行了性能测试,结果显示:该复合面料透湿率为288g/m2·24h,透气率为66m2/s,制备的复合面料对金黄色葡萄球菌的抑制杀菌率为97.5%,对大肠杆菌的抑制杀菌率为98.5%,对枯草杆菌的抑制杀菌率为99.4%,将本复合面料洗涤10次后,该复合面料对金黄色葡萄球菌的抑制杀菌率为94.6%,对大肠杆菌的抑制杀菌率为95.1%,对枯草杆菌的抑制杀菌率为96.5%,能够满足衣物面料安全使用要求,而且相较于现有的面料,舒适性和透气性更好。
实施例4:
功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯68份、竹原纤维纳米粉末26份、二氧化硅纳米微粒15份、茶树精油11份、石膏粉11份、复合增强胶11份、天然抗菌因子复合物5份、油溶性苯并三唑3份、柔软剂ES 4份、聚二甲基硅氧烷5份和芳香剂3份,该复合面料的制备方法如下:
S1:使用莱赛尔纤维与莫代尔纤维混纺制成面料基层2,使用竹炭纤维与涤纶纤维经纬编织成抗菌织物,并裁剪戈尔特斯面料,备用;
S2:制备功能涂料层,具体如下:
S2.1:将油溶性苯并三唑溶解在茶树精油中,并使用复合增强胶将天然抗菌因子复合物包成微胶囊;
S2.2:按比例将原纤维纳米粉末、二氧化硅纳米微粒和石膏粉加入双组分水性聚氨酯中,充分搅拌均匀后,加入S2.1中制备的微胶囊和茶树精油,并加入柔软剂ES、聚二甲基硅氧烷和芳香剂,搅拌均匀后获得功能增强复合物;
S2.3:将功能增强复合物移至反应釜中,抽真空至釜内真空度为12MPa,随后通入氮气至釜内压力为0.05MPa,加热至70℃,聚合反应2h后冷却,获得功能增强涂料;
S3:将生姜水和柠檬酸与水以4:2:16的比例混合,搅拌均匀后加热至沸腾,将面料基层2、抗菌织物和戈尔特斯面料依次投入沸腾的混合液体中杀菌,8min后捞出晾干,备用;
S4:将功能增强涂料均匀喷洒在两个抗菌织物两侧表面,使其均匀浸透,将该结构层在80℃下预烘15min,缓慢升温至100℃下烘烤8min使功能增强涂料固化成型,得功能性抗菌层4;
S5:将一个功能性抗菌层4均匀打孔,使透气孔5均匀分布在功能性抗菌层4表面,将带有透气孔5的功能性抗菌层4与面料基层2使用胶黏剂胶接,将另一功能性抗菌层4与戈尔特斯面料使用胶黏剂胶接,制成第一面料层,使用涤纶纤维通过针孔扎绒工艺在透气孔5内的面料基层2表面添加短毛绒,制成第二面料层;
S6:将第一面料层与第二面料层压平除皱,随后将第一面料层与第二面料层对齐后再次压平,将两者缝合连接后完成功能性复合面料的制备。
进一步的,在上述技术方案中,所述天然抗菌因子复合物包括脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油,所述脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油的添加比例设置为脱乙酰甲壳质:荆芥叶片提取物:逐蝇梅提取物:银线草芳香油=3:1:1:1;
进一步的,在上述技术方案中,所述复合增强胶由卡拉胶和黄原胶复合制成,所述卡拉胶和黄原胶的添加比例设置为卡拉胶:黄原胶=1:1;
进一步的,在上述技术方案中,所述胶黏剂设置为聚氨酯胶粘剂,所述芳香剂设置为众香子油。
对比实施例1-3,本实施例中制备的高透气抗菌功能性复合面料抗拉伸能力强,透气性好,透湿率好,且能够快速干燥,有效隔绝水滴大分子,疏水疏油、防潮耐磨,抗紫外线,面料柔软舒适,另外本实施例中对制备的高透气抗菌功能性复合面料进行了性能测试,结果显示:该复合面料透湿率为286g/m2·24h,透气率为65m2/s,制备的复合面料对金黄色葡萄球菌的抑制杀菌率为97.3%,对大肠杆菌的抑制杀菌率为98.5%,对枯草杆菌的抑制杀菌率为99.3%,将本复合面料洗涤10次后,该复合面料对金黄色葡萄球菌的抑制杀菌率为94.1%,对大肠杆菌的抑制杀菌率为95.2%,对枯草杆菌的抑制杀菌率为96.4%,能够满足衣物面料安全使用要求,而且相较于现有的面料,舒适性和透气性更好。
根据实施例1-4得出下表:
由上表可知,实施例3中原材料比例适中,加工温度适中,该工艺制备的高透气抗菌功能性复合面料透气性和透湿性好,且对金黄色葡萄球菌、大肠杆菌和枯草杆菌的抑制杀菌率高,能够有效抑制细菌滋生,抗菌效果好,而且清洗多次后抗菌效果持久有效,并且设置面料基层2、透气层3、功能性抗菌层4和透气孔5,采用舒适耐用的纤维纺品复合结构,配合透气孔5内部的短毛绒,使面料温暖舒适,提高透气散湿能力,能够使面料快速干燥,功能性抗菌层4采用竹炭纤维与涤纶纤维经纬编织制成,耐磨耐用,且能够有效抗菌,配合功能涂料层,竹原纤维纳米粉末具有天然抗菌、抑菌、除螨、防臭和抗紫外线功能,二氧化硅纳米微粒超疏水超疏油,使面料表层形成保护膜,避免水滴大分子通过,防水防油效果好,使面料便于清理,复合增强胶与石膏粉中的钙离子反应生成柔软、富有弹性的凝胶,包裹天然抗菌因子复合物形成微胶囊,缓释天然抗菌因子,使面料能够长久有效的抗菌灭菌,且其中荆芥叶片提取物、逐蝇梅提取物和银线草芳香油与茶树精油能够驱赶蚊虫,呵护肌肤,油溶性苯并三唑均匀的分布在功能性抗菌层4内部,能够提高面料的抗紫外线能力,聚二甲基硅氧烷的加入使功能性抗菌层4对热和化学试剂稳定,保证功能性抗菌层4不被水润湿,拥有良好的耐老化性能、优异的疏水性与电绝缘性,能够增强纤维强度且使面料抗静电。
以上只通过说明的方式描述了本发明的某些示范性实施例,毋庸置疑,对于本领域的普通技术人员,在不偏离本发明的精神和范围的情况下,可以用各种不同的方式对所描述的实施例进行修正。因此,上述附图和描述在本质上是说明性的,不应理解为对本发明权利要求保护范围的限制,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (5)
1.一种高透气抗菌功能性复合面料的制备方法,包括面料本体(1),所述面料本体(1)由面料基层(2)、透气层(3)和功能性抗菌层(4)组成,其特征在于:所述面料本体(1)两侧均设有功能性抗菌层(4),所述面料基层(2)和透气层(3)设置在两层功能性抗菌层(4)之间,且面料基层(2)设置在透气层(3)底部,靠近面料基层(2)一侧的所述功能性抗菌层(4)表面开设有若干均匀分布的透气孔(5),所述面料基层(2)与透气层(3)缝合连接,两个所述功能性抗菌层(4)分别与面料基层(2)和透气层(3)通过胶黏剂胶接;
所述面料基层(2)由莱赛尔纤维与莫代尔纤维混纺制成,所述透气层(3)由戈尔特斯面料制成,所述功能性抗菌层(4)由竹炭纤维与涤纶纤维经纬编织制成,所述功能性抗菌层(4)表面设有功能涂料层,所述功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯60-70份、竹原纤维纳米粉末20-30份、二氧化硅纳米微粒10-15份、茶树精油8-12份、石膏粉8-12份、复合增强胶8-12份、天然抗菌因子复合物3-6份、油溶性苯并三唑1-3份、柔软剂ES2-5份、聚二甲基硅氧烷2-5份和芳香剂1-3份;
所述天然抗菌因子复合物包括脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油,所述脱乙酰甲壳质、荆芥叶片提取物、逐蝇梅提取物和银线草芳香油的添加比例设置为脱乙酰甲壳质:荆芥叶片提取物:逐蝇梅提取物:银线草芳香油=3:1:1:1;
该复合面料的制备方法如下:
S1:使用莱赛尔纤维与莫代尔纤维混纺制成面料基层(2),使用竹炭纤维与涤纶纤维经纬编织成抗菌织物,并裁剪戈尔特斯面料,备用;
S2:制备功能涂料层,具体如下:
S2.1:将油溶性苯并三唑溶解在茶树精油中,并使用复合增强胶将天然抗菌因子复合物包成微胶囊;
S2.2:按比例将竹原纤维纳米粉末、二氧化硅纳米微粒和石膏粉加入双组分水性聚氨酯中,充分搅拌均匀后,加入S2.1中制备的微胶囊和茶树精油,并加入柔软剂ES、聚二甲基硅氧烷和芳香剂,搅拌均匀后获得功能增强复合物;
S2.3:将功能增强复合物移至反应釜中,抽真空至釜内真空度为6-12 MPa,随后通入氮气至釜内压力为0.03-0.05 MPa,加热至60- 70℃,聚合反应1- 2h后冷却,获得功能增强涂料;
S3:将生姜水和柠檬酸与水以3-4:1-2:16的比例混合,搅拌均匀后加热至沸腾,将面料基层(2)、抗菌织物和戈尔特斯面料依次投入沸腾的混合液体中杀菌,5-8min后捞出晾干,备用;
S4:将功能增强涂料均匀喷洒在两个抗菌织物两侧表面,使其均匀浸透,得到功能增强结构层,将该结构层在50-80℃下预烘10-15min,缓慢升温至80-100℃下烘烤8min使功能增强涂料固化成型,得功能性抗菌层(4);
S5:将一个功能性抗菌层(4)均匀打孔,使透气孔(5)均匀分布在功能性抗菌层(4)表面,将带有透气孔(5)的功能性抗菌层(4)与面料基层(2)使用胶黏剂胶接,将另一功能性抗菌层(4)与戈尔特斯面料使用胶黏剂胶接,制成第一面料层,使用涤纶纤维通过针孔扎绒工艺在透气孔(5)内的面料基层(2)表面添加短毛绒,制成第二面料层;
S6:将第一面料层与第二面料层压平除皱,随后将第一面料层与第二面料层对齐后再次压平,将两者缝合连接后完成功能性复合面料的制备。
2.根据权利要求1所述的一种高透气抗菌功能性复合面料的制备方法,其特征在于:所述功能涂料层所使用的主料按重量计包括:双组分水性聚氨酯65-68份、竹原纤维纳米粉末23-26份、二氧化硅纳米微粒12-15份、茶树精油9-11份、石膏粉8-11份、复合增强胶8-11份、天然抗菌因子复合物3-5份、油溶性苯并三唑1-3份、柔软剂ES 2-4份、聚二甲基硅氧烷3-5份和芳香剂1-3份。
3.根据权利要求1所述的一种高透气抗菌功能性复合面料的制备方法,其特征在于:所述复合增强胶由卡拉胶和黄原胶复合制成,所述卡拉胶和黄原胶的添加比例设置为卡拉胶:黄原胶=1:1。
4.根据权利要求1所述的一种高透气抗菌功能性复合面料的制备方法,其特征在于:所述胶黏剂设置为聚氨酯胶粘剂。
5.根据权利要求1所述的一种高透气抗菌功能性复合面料的制备方法,其特征在于:所述芳香剂设置为众香子油。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911206018.6A CN110843275B (zh) | 2019-11-29 | 2019-11-29 | 一种高透气抗菌功能性复合面料的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911206018.6A CN110843275B (zh) | 2019-11-29 | 2019-11-29 | 一种高透气抗菌功能性复合面料的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN110843275A CN110843275A (zh) | 2020-02-28 |
CN110843275B true CN110843275B (zh) | 2021-12-10 |
Family
ID=69606711
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201911206018.6A Active CN110843275B (zh) | 2019-11-29 | 2019-11-29 | 一种高透气抗菌功能性复合面料的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN110843275B (zh) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112026302A (zh) * | 2020-09-03 | 2020-12-04 | 浙江鸿一箱包皮件有限公司 | 一种制作旅行箱包的复合面料及其加工工艺 |
CN112680975A (zh) * | 2020-12-11 | 2021-04-20 | 嘉兴市科富喷绘材料有限公司 | 一种复合型抗菌消臭鞋用材料及其制备方法 |
CN113089338B (zh) * | 2021-03-27 | 2023-04-18 | 浙江国富纺织科技有限公司 | 一种抗菌窗帘及其制备方法 |
DE102021109087A1 (de) * | 2021-04-12 | 2022-10-13 | Nuvi Releaf Gmbh | Neuartiger Schichtverbund zur Verwendung als Lederimitat |
CN113119540B (zh) * | 2021-04-15 | 2022-06-28 | 福建凤竹纺织科技股份有限公司 | 一种多层复合防水透气面料及其制备方法 |
CN113858736B (zh) * | 2021-09-29 | 2023-05-23 | 大连海关技术中心 | 一种防护面料和一种医用防护服 |
CN114103297A (zh) * | 2021-11-16 | 2022-03-01 | 浙江金鑫皮革有限公司 | 一种保暖透气卡丽羊软皮 |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1986952A (zh) * | 2005-12-22 | 2007-06-27 | 青岛通力达科技开发有限公司 | 一种多元改性壳聚糖抗菌保湿整理剂的制备方法 |
CN101588924A (zh) * | 2007-01-24 | 2009-11-25 | 小松精练株式会社 | 透湿性防水片材及其制造方法 |
WO2013137881A1 (en) * | 2012-03-13 | 2013-09-19 | Transhield Technology As | Vapor permeable fabric constructs with static or dynamic antimicrobial compositions |
CN103981588A (zh) * | 2014-06-09 | 2014-08-13 | 青岛嘉胜隆贸易有限公司 | 一种抗菌除臭纤维素纤维及其制备方法 |
CN106515152A (zh) * | 2016-10-11 | 2017-03-22 | 常州市鼎升环保科技有限公司 | 一种高透气抗菌功能性复合面料的制备方法 |
CN107383432A (zh) * | 2017-07-28 | 2017-11-24 | 广西师范学院 | 剑麻环保耐用装物袋及其制备方法 |
CN209409500U (zh) * | 2018-09-13 | 2019-09-20 | 杭州超峰布艺有限公司 | 一种多功能复合面料 |
CN209479124U (zh) * | 2018-12-11 | 2019-10-11 | 嘉兴市文新织造厂 | 一种防水透湿透气四面弹力春亚纺复合面料 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB0505618D0 (en) * | 2005-03-18 | 2005-04-27 | Unilever Plc | Fabric care compositions |
US20080289090A1 (en) * | 2007-05-25 | 2008-11-27 | Michael Brier | Performance wear formed of hydrophobic moisture management fabric |
-
2019
- 2019-11-29 CN CN201911206018.6A patent/CN110843275B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1986952A (zh) * | 2005-12-22 | 2007-06-27 | 青岛通力达科技开发有限公司 | 一种多元改性壳聚糖抗菌保湿整理剂的制备方法 |
CN101588924A (zh) * | 2007-01-24 | 2009-11-25 | 小松精练株式会社 | 透湿性防水片材及其制造方法 |
WO2013137881A1 (en) * | 2012-03-13 | 2013-09-19 | Transhield Technology As | Vapor permeable fabric constructs with static or dynamic antimicrobial compositions |
CN103981588A (zh) * | 2014-06-09 | 2014-08-13 | 青岛嘉胜隆贸易有限公司 | 一种抗菌除臭纤维素纤维及其制备方法 |
CN106515152A (zh) * | 2016-10-11 | 2017-03-22 | 常州市鼎升环保科技有限公司 | 一种高透气抗菌功能性复合面料的制备方法 |
CN107383432A (zh) * | 2017-07-28 | 2017-11-24 | 广西师范学院 | 剑麻环保耐用装物袋及其制备方法 |
CN209409500U (zh) * | 2018-09-13 | 2019-09-20 | 杭州超峰布艺有限公司 | 一种多功能复合面料 |
CN209479124U (zh) * | 2018-12-11 | 2019-10-11 | 嘉兴市文新织造厂 | 一种防水透湿透气四面弹力春亚纺复合面料 |
Also Published As
Publication number | Publication date |
---|---|
CN110843275A (zh) | 2020-02-28 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN110843275B (zh) | 一种高透气抗菌功能性复合面料的制备方法 | |
CN101716359B (zh) | 一种杀菌消毒材料及其应用 | |
CN103741486B (zh) | 一种金属基聚季铵盐硅胶涂层抗菌整理工艺 | |
CN102786709B (zh) | 一种具有抗菌功能的防水透气材料及其制备方法 | |
CN201399931Y (zh) | 一种鞋靴面料 | |
CN101760963B (zh) | 一种抗菌防霉纺织品及其制备方法 | |
CN110791962A (zh) | 抗菌水刺无纺布及其制备方法 | |
WO2011008204A1 (en) | Ionized performance fabric with antimicrobial/antibacterial/antifungal properties | |
CN103556476B (zh) | 一种多功能真丝及其制备方法 | |
CN106902382A (zh) | 一种抗菌医用敷料及其制备方法 | |
CN106924803A (zh) | 一种高性能医用液体创可贴及其制备方法 | |
CN101822430A (zh) | 纳米银抗菌除臭袜 | |
CN210062300U (zh) | 一种防菌除臭窗帘布 | |
CN103622210A (zh) | 一种模压鞋垫制作方法 | |
US20100136074A1 (en) | Biocidic textiles and fabrics | |
CN107627689B (zh) | 一种生物质超细纤维合成革 | |
CN103013138B (zh) | 一种明胶基纳米复合材料及其制备方法 | |
Massella et al. | Manufacture techniques of chitosan-based microcapsules to enhance functional properties of textiles | |
RO128032B1 (ro) | Ţesătură cu proprietăţi antialergice tip barieră bioactivă/fizică şi procedeu de realizare a acesteia | |
KR20120112968A (ko) | 아파타이트를 복합한 항균성 폴리우레탄 필름의 제조방법 | |
CN114073921A (zh) | 一种复合微球及其制备方法和应用 | |
KR102125578B1 (ko) | 항균 팬티형 기저귀 | |
CN115958854A (zh) | 一种抗菌耐霉变棉 | |
Montazer et al. | Antibacterial nanocoatings | |
WO2014117286A1 (es) | Matriz impregnable de origen vegetal, animal o sintética o mezclas de las mismas que contiene un compuesto antimicrobiano distribuido homogéneamente; procedimiento para impregnar un compuesto en dicha matriz; y su uso en la preparación de elementos antimicrobianos |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant |