CN110840770A - After-depilation repair emulsion and preparation method thereof - Google Patents
After-depilation repair emulsion and preparation method thereof Download PDFInfo
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- CN110840770A CN110840770A CN201911283611.0A CN201911283611A CN110840770A CN 110840770 A CN110840770 A CN 110840770A CN 201911283611 A CN201911283611 A CN 201911283611A CN 110840770 A CN110840770 A CN 110840770A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/002—Aftershave preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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Abstract
The invention relates to a repairing emulsion, in particular discloses a repairing emulsion after depilation and a preparation method thereof, and aims to solve the technical problem that the skin of the existing depilatory cream has itching, redness and burning irritation reaction in the using process. The repair milk after depilation mainly comprises the following raw materials: 3-10% of mineral oil, 0.5-3% of polydimethylsiloxane, 0.5-2% of cetostearyl alcohol, 0.5-2% of stearic acid, 0.5-3% of glyceryl stearate/PEG-100 stearate, 0.01-0.1% of disodium EDTA, 2-8% of betaine/proline, 0.1-0.4% of allantoin, 0.1-0.4% of carbomer, 0.05-0.3% of xanthan gum, 0.1-0.2% of methyl hydroxybenzoate, 0.05-0.15% of propyl hydroxybenzoate, 70.1-0.5% of polyacrylamide/C13-14 isoparaffin/laureth-laurate, 1-5% of propylene glycol, 0.1-0.4% of menthol, 0.05-0.2% of dipotassium glycyrrhizinate, 0.1-0.5% of triethanolamine and 0.3-0.6% of phenoxyethanol/ethylhexylglycerol. The raw materials are stirred and heated in batches, dissolved to be transparent and then mixed uniformly, so that the restoration cream after depilation is obtained. The invention can quickly relieve the symptoms of redness, itching, burning and the like after depilation.
Description
Technical Field
The invention relates to a repair emulsion, in particular to a repair emulsion after depilation and a preparation method thereof.
Background
The depilatory cream is prepared by using chemical depilatory under alkaline condition to break the disulfide bond of hair and break hair to achieve depilatory effect. The chemical depilatories commonly used today are thioglycolic acids. The pH of depilatory cream prepared from the depilatory is 11.5-12.5, and has great irritation to skin, damage to skin, and itching, redness, and burning irritation reaction during application. Currently, no repair product specially aiming at unhairing exists in the market, or the effect is not obvious.
Disclosure of Invention
The invention aims to provide the repair cream which is safe, effective, mild and non-irritating, can effectively supplement skin moisture and reduce irritation reaction after depilation.
In order to realize the purpose of the invention, the following technical scheme is provided:
the repair emulsion after depilation comprises the following raw materials in percentage by weight: 3% of mineral oil, 0.5% of polydimethylsiloxane, 1% of cetearyl alcohol, 1% of stearic acid, 1% of glyceryl stearate/PEG-100 stearate, 0.005% of disodium EDTA, 2% of betaine/proline, 0.1% of allantoin, 0.4% of carbomer, 0.1% of xanthan gum, 0.1% of methylparaben, 0.05% of propylparaben, 70.3% of polyacrylamide/C13-14 isoparaffin/laureth-yl ether, 3% of propylene glycol, 0.2% of menthol, 0.1% of dipotassium glycyrrhizinate, 0.5% of triethanolamine, 0.5% of phenoxyethanol/ethylhexylglycerin and the balance of deionized water.
The repair milk after depilation comprises the following raw materials in percentage by weight: mineral oil 4%, polydimethylsiloxane 0.5%, cetearyl alcohol 1%, stearic acid 1%, glyceryl stearate/PEG-100 stearate 1%, disodium EDTA 0.05%, betaine/proline 2%, allantoin 0.1%, carbomer 0.4%, xanthan gum 0.1%, methylparaben 0.1%, propylparaben 0.05%, polyacrylamide/C13-14 isoparaffin/laureth-70.3%, propylene glycol 3%, menthol 0.1%, dipotassium glycyrrhizinate 0.05%, triethanolamine 0.5%, phenoxyethanol/ethylhexylglycerin 0.5%, and the balance deionized water.
The repair milk after depilation comprises the following raw materials in percentage by weight: 5.5% mineral oil, 2% polydimethylsiloxane, 0.8% cetostearyl alcohol, 1.2% stearic acid, 2% glyceryl stearate/PEG-100 stearate, 0.05% disodium EDTA, 5% betaine/proline, 0.2% allantoin, 0.3% carbomer, 0.15% xanthan gum, 0.2% methylparaben, 0.1% propylparaben, polyacrylamide/C13-14 isoparaffin/laureth-70.2%, propylene glycol 3%, menthol 0.2%, dipotassium glycyrrhizinate 0.1%, triethanolamine 0.5%, phenoxyethanol/ethylhexylglycerin 0.5%, and the balance deionized water.
The invention also provides a preparation method of the post-depilation repair emulsion, which comprises the following steps:
(1) mixing mineral oil, polydimethylsiloxane, cetostearyl alcohol, stearic acid, glyceryl stearate/PEG-100 stearate, propyl hydroxybenzoate and methyl hydroxybenzoate, stirring and heating, and dissolving to transparent state to obtain a first mixture;
(2) pre-dispersing triethanolamine with deionized water accounting for 1 percent of the total weight of the repair emulsion to obtain a second mixture;
(3) stirring and dissolving the menthol and the propylene glycol to be transparent to obtain a third mixture;
(4) pre-dispersing dipotassium glycyrrhizinate with deionized water accounting for 1 percent of the total weight of the repair emulsion to obtain a fourth mixture;
(5) mixing disodium EDTA, betaine/proline, allantoin, xanthan gum, carbomer and the rest deionized water, stirring and heating to 80-85 ℃, homogenizing, keeping the temperature and stirring until the xanthan gum and the carbomer are completely dissolved to obtain a fifth mixture, adding the first mixture into the fifth mixture, homogenizing for 3-5 minutes, adding polyacrylamide/C13-14 isoparaffin/laureth-7, homogenizing and stirring for 3-5 minutes, keeping the temperature and stirring uniformly in vacuum, and then cooling;
(6) cooling to 55-60 deg.C, adding the second mixture, stirring, adjusting pH to 6-7, and cooling;
(7) cooling to 40-45 deg.C, adding the third and fourth mixtures, stirring, cooling to 40 deg.C, adding phenoxyethanol/ethylhexyl glycerol, and stirring to obtain depilatory repair emulsion.
Further, heating to 75-80 ℃ in the step (1).
Further, in the step (5), the vacuum heat preservation time is 10-15 minutes.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention relates to a post-depilation repair emulsion which is developed specially aiming at the properties and characteristics of a depilatory cream prepared from a chemical depilatory. The menthol crystal in the invention has the effects of cooling and relieving itching, and can relieve the burning and itching feeling of the skin. The dipotassium glycyrrhizinate has multiple effects of bacteriostasis, inflammation diminishing, detoxification, anti-allergy and the like, can relieve allergic symptoms caused by using the depilatory cream, and can quickly relieve irritation reaction caused by using the depilatory cream.
2. The preparation method is simple and suitable for quantitative production, and the prepared restoration lotion after depilation can quickly relieve symptoms such as redness, itching, burning and the like after depilation.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to the following embodiments, but the present invention is not limited thereto.
Example 1
A first mixture:
3% of mineral oil, 0.5% of polydimethylsiloxane, 1% of cetearyl alcohol, 1% of stearic acid, 1% of glyceryl stearate/PEG-100 stearate, 0.1% of propyl hydroxybenzoate and 0.05% of methyl hydroxybenzoate.
A second mixture:
0.5 percent of triethanolamine and 1 percent of deionized water.
A third mixture:
0.2 percent of menthol and 3 percent of propylene glycol.
A fourth mixture:
0.1 percent of dipotassium glycyrrhizinate and 1 percent of deionized water.
A fifth mixture:
disodium EDTA 0.05%, betaine/proline 2%, allantoin 0.1%, xanthan gum 0.1%, carbomer 0.4%, and the remainder deionized water 84%.
In addition, the composition also comprises polyacrylamide/C13-14 isoparaffin/laureth-70.3%, and phenoxyethanol/ethylhexyl glycerin 0.5%.
Example 2
A first mixture:
4% of mineral oil, 0.5% of polydimethylsiloxane, 1% of cetearyl alcohol, 1% of stearic acid, 1% of glyceryl stearate/PEG-100 stearate, 0.05% of propyl hydroxybenzoate and 0.1% of methyl hydroxybenzoate.
A second mixture:
0.5 percent of triethanolamine and 1 percent of deionized water.
A third mixture:
0.1 percent of menthol and 3 percent of propylene glycol.
A fourth mixture:
0.05 percent of dipotassium glycyrrhizinate and 1 percent of deionized water.
A fifth mixture:
disodium EDTA 0.05%, betaine/proline 2%, allantoin 0.1%, xanthan gum 0.1%, carbomer 0.4%, and the balance deionized water 85%.
In addition, the composition also comprises polyacrylamide/C13-14 isoparaffin/laureth-70.3%, and phenoxyethanol/ethylhexyl glycerin 0.5%.
Example 3
A first mixture:
5.5% of mineral oil, 2% of polydimethylsiloxane, 0.8% of cetostearyl alcohol, 1.2% of stearic acid, 2% of glyceryl stearate/PEG-100 stearate, 0.1% of propyl hydroxybenzoate and 0.2% of methyl hydroxybenzoate.
A second mixture:
0.5 percent of triethanolamine and 1 percent of deionized water.
A third mixture:
0.2 percent of menthol and 3 percent of propylene glycol.
A fourth mixture:
0.1 percent of dipotassium glycyrrhizinate and 1 percent of deionized water.
A fifth mixture:
disodium EDTA 0.05%, betaine/proline 5%, allantoin 0.2%, xanthan gum 0.15%, carbomer 0.3%, and the remainder deionized water 76%.
In addition, the composition also comprises polyacrylamide/C13-14 isoparaffin/laureth-70.2%, and phenoxyethanol/ethylhexyl glycerin 0.5%.
The preparation method of the repair milk comprises the following steps:
(1) mixing mineral oil, polydimethylsiloxane, cetostearyl alcohol, stearic acid, glyceryl stearate/PEG-100 stearate, propyl hydroxybenzoate and methyl hydroxybenzoate, stirring, heating to 75-80 deg.C, and dissolving to transparent state to obtain a first mixture;
(2) pre-dispersing triethanolamine with deionized water accounting for 1 percent of the total weight of the repair emulsion to obtain a second mixture;
(3) stirring and dissolving the menthol and the propylene glycol to be transparent to obtain a third mixture;
(4) pre-dispersing dipotassium glycyrrhizinate with deionized water accounting for 1 percent of the total weight of the repair emulsion to obtain a fourth mixture;
(5) mixing disodium EDTA, betaine/proline, allantoin, xanthan gum, carbomer and the rest deionized water, stirring and heating to 80-85 ℃, homogenizing, keeping the temperature and stirring until the xanthan gum and the carbomer are completely dissolved to obtain a fifth mixture, adding the first mixture into the fifth mixture, homogenizing for 3-5 minutes, adding polyacrylamide/C13-14 isoparaffin/laureth-7, homogenizing and stirring for 3-5 minutes, keeping the temperature in vacuum for 10-15 minutes, uniformly stirring, and then cooling;
(6) cooling to 55-60 deg.C, adding the second mixture, stirring, adjusting pH to 6-7, and cooling;
(7) cooling to 40-45 deg.C, adding the third and fourth mixtures, stirring, cooling to 40 deg.C, adding phenoxyethanol/ethylhexyl glycerol, and stirring to obtain depilatory repair emulsion.
To verify the effect of the repair milk of the present invention, it was tested as follows:
first, repair milk repair anti-allergy effect test
In the experiment, referring to the evaluation guideline for cosmetic moisturizing efficacy (QB/T4256-2011), the depilatory cream is applied to a depilatory cream in a single time for 10min in a constant-temperature and constant-humidity environment. During the test, the test and blank controls were randomly distributed on the inner side of the left and right forearm of the subject. The product is used for one time, the depilatory time is 10 minutes, and after depilation, the depilatory cream is rinsed and the depilatory repair emulsion is smeared. Product use and blank control areas were observed 5, 15, 20, 30 minutes after depilatory and after use of the repair milk, respectively. Each sample had 24 ginseng samples and the test was completed.
The short-term skin condition after use was significantly different. Four samples (commercial post-epilation repair milk, post-epilation repair milk of examples 1-3) were tested and observed to have a stimulating response in the skin starting 5 minutes after use. However, the difference in skin condition between the four samples was significant. Group a is a commercially available post-epilation repair milk, group B is the post-epilation repair milk of example 1, group C is the post-epilation repair milk of example 2, and group D is the post-epilation repair milk of example 3. The detailed results are shown in table 1.
TABLE 1 results of the test of the repairing anti-sensitization effect of the commercial mask and the after-depilation repairing creams of examples 1 to 3
From the above results, it can be seen that the skin condition gradually returned to normal with time after the use of the commercial repair milk, whereas the skin allergy level was rapidly reduced with B, C, D samples tested 5 minutes after the use of the repair milk in examples 1-3; the B, C, D samples had almost decreased levels of allergy 15 minutes after use; after 30 minutes, the skin of the B, C, D samples all returned to normal.
II, test of pH value and test of Heat and Cold resistance for 48 hours of the repair milks of examples 1 to 3 with reference to QB/T2872-2017
As can be seen from table 2, the stability of the repair milk of the present invention is good and the pH of the repair milk of example 3 is closer to the skin (about 5.8), the best pH of the repair milk of example 3.
TABLE 2
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (6)
1. The post-depilation repair emulsion is characterized by comprising the following raw materials in percentage by weight: 3-10% of mineral oil, 0.5-3% of polydimethylsiloxane, 0.5-2% of cetostearyl alcohol, 0.5-2% of stearic acid, 0.5-3% of glyceryl stearate/PEG-100 stearate, 0.01-0.1% of disodium EDTA, 2-8% of betaine/proline, 0.1-0.4% of allantoin, 0.1-0.4% of carbomer, 0.05-0.3% of xanthan gum, 0.1-0.2% of methyl hydroxybenzoate, 0.05-0.15% of propyl hydroxybenzoate, 70.1-0.5% of polyacrylamide/C13-14 isoparaffin/laureth-laurate, 1-5% of propylene glycol, 0.1-0.4% of menthol, 0.05-0.2% of dipotassium glycyrrhizinate, 0.1-0.5% of triethanolamine, 0.3-0.6% of phenoxyethanol/ethylhexylglycerol and the balance of deionized water.
2. The post-epilation repair emulsion according to claim 1, comprising the following raw materials in percentage by weight: 3-8% of mineral oil, 0.5-2% of polydimethylsiloxane, 0.5-1% of cetostearyl alcohol, 0.5-1.5% of stearic acid, 0.5-2% of glyceryl stearate/PEG-100 stearate, 0.01-0.05% of disodium EDTA, 2-5% of betaine/proline, 0.1-0.3% of allantoin, 0.2-0.4% of carbomer, 0.05-0.15% of xanthan gum, 0.1-0.2% of methyl hydroxybenzoate, 0.05-0.1% of propyl hydroxybenzoate, 1-3% of polyacrylamide/C13-14 isoparaffin/laureth-70.1-0.3% of polyacrylamide/C, 0.1-0.3% of menthol, 0.05-0.1% of dipotassium glycyrrhizinate, 0.1-0.5% of triethanolamine, 0.3-0.5% of phenoxyethanol/ethylhexylglycerol and the balance of deionized water.
3. The post-epilation repair cream according to claim 1 or 2, comprising the following raw materials in percentage by weight: 5.5% mineral oil, 2% polydimethylsiloxane, 0.8% cetostearyl alcohol, 1.2% stearic acid, 2% glyceryl stearate/PEG-100 stearate, 0.05% disodium EDTA, 5% betaine/proline, 0.2% allantoin, 0.3% carbomer, 0.15% xanthan gum, 0.2% methylparaben, 0.1% propylparaben, polyacrylamide/C13-14 isoparaffin/laureth-70.2%, propylene glycol 3%, menthol 0.2%, dipotassium glycyrrhizinate 0.1%, triethanolamine 0.5%, phenoxyethanol/ethylhexylglycerin 0.5%, and the balance deionized water.
4. A method of preparing a post-epilation repair cream as claimed in any of claims 1 to 3, comprising the steps of:
(1) mixing mineral oil, polydimethylsiloxane, cetostearyl alcohol, stearic acid, glyceryl stearate/PEG-100 stearate, propyl hydroxybenzoate and methyl hydroxybenzoate, stirring and heating, and dissolving to transparent state to obtain a first mixture;
(2) pre-dispersing triethanolamine with deionized water accounting for 1 percent of the total weight of the repair emulsion to obtain a second mixture;
(3) stirring and dissolving the menthol and the propylene glycol to be transparent to obtain a third mixture;
(4) pre-dispersing dipotassium glycyrrhizinate with deionized water accounting for 1 percent of the total weight of the repair emulsion to obtain a fourth mixture;
(5) mixing disodium EDTA, betaine/proline, allantoin, xanthan gum, carbomer and the rest deionized water, stirring and heating to 80-85 ℃, homogenizing, keeping the temperature and stirring until the xanthan gum and the carbomer are completely dissolved to obtain a fifth mixture, adding the first mixture into the fifth mixture, homogenizing for 3-5 minutes, adding polyacrylamide/C13-14 isoparaffin/laureth-7, homogenizing and stirring for 3-5 minutes, keeping the temperature and stirring uniformly in vacuum, and then cooling;
(6) cooling to 55-60 deg.C, adding the second mixture, stirring, adjusting pH to 6-7, and cooling;
(7) cooling to 40-45 deg.C, adding the third and fourth mixtures, stirring, cooling to 40 deg.C, adding phenoxyethanol/ethylhexyl glycerol, and stirring to obtain depilatory repair emulsion.
5. The method of preparing a post-depilation restoration milk according to claim 4, wherein the heating in step (1) is to 75 to 80 ℃.
6. The method for preparing a post-depilation restoration milk according to claim 4, wherein in the step (5), the vacuum insulation time is 10 to 15 minutes.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112716818A (en) * | 2021-02-05 | 2021-04-30 | 广州市德馨蜡制品有限公司 | Dewaxing and relieving liquid for human body depilation wax and preparation method thereof |
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Patent Citations (5)
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CN107519049A (en) * | 2017-09-07 | 2017-12-29 | 蝶柔化妆品(浙江)有限公司 | A kind of body frost of healthy skin |
CN107714562A (en) * | 2017-11-29 | 2018-02-23 | 诺斯贝尔化妆品股份有限公司 | A kind of night maintenance elite breast |
CN107929105A (en) * | 2017-12-27 | 2018-04-20 | 广州潮徽生物科技有限公司 | Removing miliaria and relieving itching balm that a kind of infant is applicable in and preparation method and application |
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CN112716818A (en) * | 2021-02-05 | 2021-04-30 | 广州市德馨蜡制品有限公司 | Dewaxing and relieving liquid for human body depilation wax and preparation method thereof |
CN112716818B (en) * | 2021-02-05 | 2022-08-30 | 广州市德馨蜡制品有限公司 | Dewaxing and relieving liquid for human body depilation wax and preparation method thereof |
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Application publication date: 20200228 |