CN110833796A

CN110833796A - Novel material composite particle with sleep-promoting function and preparation method thereof

Info

Publication number: CN110833796A
Application number: CN201911102447.9A
Authority: CN
Inventors: 林永忠; 张永禄; 林琳; 张红梅; 张雪冰; 张瑜
Original assignee: Wall Tianjin Household Goods Co ltd
Current assignee: Wall Tianjin Household Goods Co ltd
Priority date: 2019-11-12
Filing date: 2019-11-12
Publication date: 2020-02-25

Abstract

The invention belongs to the technical field of new materials, and particularly relates to new material composite particles with a sleep-promoting function and a preparation method thereof. The formula comprises the following components: 550-650kg of concentrated hot spring jade powder (325-400 meshes); 80-100kg of modified diatomite raw material (325-400 meshes); 80-100kg of tourmaline powder (325-400 meshes); 60-80kg of Chinese medical stone (325-400 meshes); 40-60kg of zeolite powder (325-400 meshes); 40-60kg of attapulgite powder (325-400 meshes); 40-60kg of magnetite powder (325-400 meshes); 10-20kg of bentonite (325-400 meshes). According to the invention, the hot spring jade powder and other auxiliary materials are adsorbed and loaded through the nano-scale pores of the diatomite to form granules, and various components interact with each other to release infrared rays, negative oxygen ions and a biological magnetic field, so that the sleep is promoted by adjusting the local air quality through moisture absorption and release, and the ecological physiotherapy effect is achieved.

Description

Novel material composite particle with sleep-promoting function and preparation method thereof

Technical Field

The invention belongs to the technical field of new materials, and particularly relates to new material composite particles with a sleep-promoting function and a preparation method thereof.

Background

China is a big jade producing country, particularly Xiuyan jade in Liaoning province is more famous for a long time in the aspect of high storage amount and is four famous jade in China. The Xiuyan jade has the quality characteristics of mountain raw water storage, fineness, warmness, brightness, rich coating and the like; the chemical components are complicated due to many reasons of historical change of geology, but the hsiuyen jade can be comprehensively analyzed by modern detection means such as a microscope, a transmission electron microscope, X-ray diffraction analysis, differential thermal analysis and the like, so that good chemical analysis and physical characteristic big data of the hsiuyen jade are obtained, and the method is widely applied to data support for new invention creation. The medical health-care function of jade on human body has been discovered by human beings for a long time, the famous traditional Chinese medicine treatises in Shennong Ben Cao, Tang Ben Cao and Ben Cao gang mu are described in the book, the Ben Cao gang mu-the eighth volume of the golden stone department are recorded in the book, and the jade has: removing stomach heat, relieving asthma, relieving restlessness, nourishing hair, nourishing five internal organs, softening tendons, strengthening bone, quenching thirst, moistening heart and lung, nourishing sound, soothing soul, promoting blood circulation, improving eyesight, and improving eyesight.

The hot spring generally contains a plurality of active microelements, has a certain mineralization degree, and has certain help for improving the physique, enhancing the resistance and preventing diseases. The aged ice of Chinese medical mineral spring experts is considered in the book of mineral spring and recuperation that the hot spring generally contains a plurality of active microelements and has a certain mineralization degree, and the temperature of spring water is usually higher than 30 ℃. The warm mineral spring has medical effect on the following diseases: obesity, motor system diseases (such as trauma and chronic rheumatoid arthritis), nervous system diseases (nerve injury, neuritis and the like), early-stage mild cardiovascular system diseases, gout, skin diseases and the like.

According to the health care function of the hot spring and the jade on the human body, the composite particles which take the hot spring jade powder with the sleep promoting function as the main body are innovatively developed by combining the traditional Chinese medicine theory with the modern technological means, and are recorded in the prior art;

diatoms are unicellular algae, the individual of which is small, typically in the order of microns or millimeters, and the debris of dead diatoms is deposited in the ocean or lake to form diatomaceous earth. The main component of the diatomite is silicon dioxide, and also contains a small amount of aluminum, iron, calcium, magnesium, sodium, potassium, phosphorus and the like, and the diatomite has the advantages of porosity, small density, large specific surface area, good adsorbability, acid resistance, alkali resistance and insulation. The diatomite has abundant reserves and good physical and chemical properties, so the diatomite has wide application in various fields such as environment, petroleum, chemical engineering and the like. The patent develops a new method, and utilizes the super strong loading capacity of the diatomite to load various mineral substances such as hot springs, jade powder and the like. The world-wide trial and application in the sleep industry have achieved favorable results.

Because of the accelerated social rhythm, many people suffer from insomnia, which is the source of breeding diseases, and the sleep problem is a worldwide problem at present. Day 21 of this year 3 is the 19 th world sleep day. The subject of our country in this year is "regular work and rest healthy sleep" which aims to emphasize the importance of circadian rhythms in healthy sleep. Data show that people with more than three adults have problems in sleeping in China. Sleep is a spontaneous and reversible periodic state, about one third of the life of a human is spent in sleep, consciousness of the human body is temporarily interrupted in the sleep process, the response to external stimulation is reduced, the sleep is an important link for recovering the human body, integrating information and consolidating memory, the sleep is important for human health, and long-term insomnia or insufficient sleep can bring serious harm to the human body. Insufficient sleep is directly affecting human health. The invention relates to a novel method for promoting sleep health and preserving health by applying the physical principle of materials science and researching across the boundary.

Disclosure of Invention

The invention aims to solve the technical problem of providing a novel material composite particle with a sleep-promoting function and a preparation method thereof. The diatomite is adsorbed and loaded with the hot spring jade powder and other auxiliary materials through the nanometer pores of the diatomite to form particles, and various components interact with each other to promote sleep by releasing infrared rays, negative oxygen ions and a biological magnetic field and absorbing and releasing moisture to adjust the local air quality, so that the ecological physiotherapy effect is achieved.

In order to solve the technical problems, the technical scheme of the invention is as follows:

a new material composite particle with a sleep promoting function comprises the following formula: 550-650kg of concentrated hot spring jade powder (325-400 meshes); 80-100kg of modified diatomite raw material (325-400 meshes); 80-100kg of tourmaline powder (325-400 meshes); 60-80kg of Chinese medical stone (325-400 meshes); 40-60kg of zeolite powder (325-400 meshes); 40-60kg of attapulgite powder (325-400 meshes); 40-60kg of magnetite powder (325-400 meshes); 10-20kg of bentonite (325-400 meshes).

A preparation method of new material composite particles with sleep-promoting function is characterized by comprising the following processing flows: 1. concentrating hot spring water; 2. crushing the jade; 3. soaking the hot spring jade rice grains → heating → drying → crushing into powder; 4. modifying diatomite; 5. selecting and crushing tourmaline; 6. selecting and crushing Chinese medical stone; 7. selecting and crushing zeolite; 8. selecting and crushing attapulgite; 9. selecting and crushing the magnetite; 10. selecting and crushing bentonite; 11. compounding; 12. the dry powder is evenly stirred and compounded for granulation; 13. screening uniform particles; 14. calcining to obtain qualified product.

The preparation process comprises the following steps: (1) selecting jade rice grains of hsiuyen rock; (2) washing and removing impurities; (3) concentrating hot spring water, and soaking for 15-20 days; (4) continuously heating to 30-50 deg.C to further enhance absorption of therapeutic effects of hot spring and jade; (5) adsorption drying; (6) crushing to 325-400 meshes; (7) mixing with other adjuvants, and stirring; (8) compound granulation; (9) screening uniform particles, (10) calcining to obtain qualified products; (11) and packaging the finished product for delivery.

Further, the xiuyan jade rice grains are residual waste residues of carving and mining.

Further, the particle size of the particles in the step (9) is 0.1-0.15 mm.

Further, the modified diatomite has the specific surface area of 85m²G, SiO in diatomaceous earth²The content accounts for 50-68% of the total weight, and the fineness is as follows: 325- & ltwbr- & gt 400 meshes and the whiteness is 65-75.

The invention has the beneficial effects that:

the new material composite formula particle with the sleep-promoting function provided by the invention is innovated and invented on hot spring jade powder. The absorbed hot spring jade powder integrates the functions of hot springs and jade, has the optimal proportion and has physical effects mutually; the health-preserving, medical and health-care tea bag is used for human health preserving, medical treatment and health care together, and provides one or more forms of new ways and new methods for health preserving, medical treatment and health care for human health and longevity.

Drawings

FIG. 1 is a schematic view of the preparation process of the present invention.

Detailed Description

Example 1

A new material composite particle with the functions of promoting sleep and health care is specifically composed of the following formula:

550kg of concentrated hot spring jade powder (325-400 meshes)

100kg of modified diatomite raw material (325-400 meshes)

100kg of tourmaline powder (325-400 mesh)

100kg of Chinese medical stone (325-mesh and 400-mesh)

40kg of zeolite powder (325-400 meshes)

Attapulgite powder (325-400 mesh) 50kg

50kg of magnetite powder (325-400 meshes)

10kg of bentonite (325-400 meshes)

Example 2

600kg of concentrated hot spring jade powder (325-400 meshes)

90kg of modified diatomite raw material (325-400 meshes)

90kg of tourmaline powder (325-400 meshes)

90kg of Chinese medical stone (325 meshes)

35kg of zeolite powder (325-400 meshes)

Attapulgite powder (325-400 mesh) 50kg

40kg of magnetite powder (325-400 meshes)

5kg of bentonite (325-400 meshes)

Example 3

650kg of concentrated hot spring jade powder (325-400 meshes)

80kg of modified diatomite raw material (325-400 meshes)

80kg of tourmaline powder (325-400 meshes)

80kg of Chinese medical stone (325) with 400 meshes

30kg of zeolite powder (325-400 meshes)

Attapulgite powder (325-400 mesh) 40kg

35kg of magnetite powder (325-400 meshes)

5kg of bentonite (325-400 meshes)

Example 4

620kg of concentrated hot spring jade powder (325-400 meshes)

85kg of modified diatomite raw material (325-400 meshes)

85kg of tourmaline powder (325-400 meshes)

85kg of Chinese medical stone (325) and 400 meshes

35kg of zeolite powder (325-400 meshes)

45kg of attapulgite powder (325-400 mesh)

40kg of magnetite powder (325-400 meshes)

5kg of bentonite (325-400 meshes)

Example 5

A preparation method of novel material composite particles with sleep-promoting and health-care functions comprises the following steps: dividing into three blocks: main materials, auxiliary materials and auxiliary materials. The process of the invention mainly comprises the processing and manufacturing of the main materials, and the processing and manufacturing method of the main materials comprises the following steps: firstly, the jade rice grain selecting force is 0.2-0.25 mm. Most of the jade slag is waste jade slag, and the jade slag is manufactured after crushing and screening. And secondly, washing with water to remove impurities and soil. The third step: soaking in concentrated hot spring water for 15-20 days. And fourthly, simultaneously using electricity to heat to 30-50 ℃ at constant temperature. And fifthly, naturally drying. Sixthly, tourmaline powder (325 meshes) and Chinese medical stone powder (325) are added. Adding a very small amount of modified diatomite and auxiliary materials such as attapulgite powder, zeolite, bentonite and the like and ingredients into the modified diatomite simultaneously, stirring and compounding the mixture, granulating the mixture in a granulator until the granularity is 0.1-0.15mm, and feeding the granules into a rotary kiln to be calcined to increase the strength of the granules. The temperature is required to be gradually increased from 180 ℃ to 480 ℃ to prevent calcination carbonization and pore collapse. And eighthly, performing spot inspection on various technical indexes of the calcined pearly crystal ceramic bead particles, packaging the pearly crystal ceramic bead particles after the technical indexes are checked to be qualified, discharging the pearly crystal ceramic bead particles into a factory, and conveying the pearly crystal ceramic bead particles to a daily necessities processing workshop to manufacture a new product.

Example 6

Brief introduction of the materials used in the present invention:

tourmaline: tourmaline (Toumaline) is a generic name of various tourmaline group minerals, is a cyclic silicate mineral with complex composition components, and is characterized by containing boron. It is called "tourmaline" because it can adsorb fine paper pieces and charged stones. The tourmaline is a crystal which has both voltage effect and thermoelectric effect, and the research in recent years finds that the tourmaline not only can be used as an ore exploring indicator and has important effect on the formation of diagenesis and ores, but also can emit infrared rays, release negative ions, resist bacteria and deodorize, and has purification and improvement effects on water and air. Therefore, tourmaline is gradually becoming a popular natural mineral functional material, and is receiving general attention from all countries in the world, and the application range is expanding continuously. The patent innovations and creates the structure, performance, preparation method, application field and the like of the novel composite material, and provides a basis for the development of the technology and products.

The tourmaline has the functions of ⑴ balancing bioelectricity of human body, ⑵ releasing far infrared ray, far infrared ray released by tourmaline being able to produce resonance effect of human body cell and body fluid molecule, making capillary vessel dilate and blood flow speed increase, thus increasing oxygen content of human body, activating protein and other macromolecular substances, thus increasing tissue repair and regeneration ability, improving immunity of human body, ⑶ releasing negative ion, the negative ion released by tourmaline being able to improve air quality, promote cell metabolism, enhance cell activity, sooth nerves, recover fatigue, promote appetite, etc. furthermore, the negative ion is confirmed to have the functions of killing germ, purifying air in medical field, ⑷ activating cell in natural energy field, the tourmaline crystal is named as natural solar cell, it can absorb, store solar energy, convert it into electric energy (bioelectricity) and heat energy, and convert it into harmful energy, thus it can provide harmful elements to human body, resist harmful water, resist harmful elements, provide harmful water, resist harmful elements, and provide harmful water, and provide health-care effects.

China medical stone: the Chinese medical stone is one kind of medical stone, and the medical stone produced in Nemantha mountain of inner Mongolia is called Chinese medical stone, and is a special non-metal mineral resource, which is shaped like a spot or yellow or white and rather like wheat grains.

Zeolite: zeolite is a generic term for minerals of the zeolite family, an aqueous alkali or alkaline earth aluminosilicate mineral. Natural zeolites 40 have been found throughout the world, with clinoptilolite, mordenite, chabazite, erionite, phillipsite, heulandite, laumontite, stilbite, analcime, and the like being the most common. Clinoptilolite and mordenite have been used in large quantities. The zeolite minerals belong to different crystal systems, and the crystals are mostly in the form of fibers, hairs and columns, and the crystals are few in the form of plates or short columns. Zeolites have ion-exchange, adsorptive separation, catalytic, stable, chemical reactivity, reversible dehydration, electrical conductivity, and the like. The zeolite is mainly produced in cracks of volcanic rock or almond bodies and coexists with calcite, pith and quartz; also in volcaniclastic sedimentary rock and hot spring sedimentary rock, the zeolite used in the invention is Baokun zeolite in Fakuchi county of Liaoning province, and is domestic high-quality zeolite.

Attapulgite: attapulgite is an aqueous magnesium aluminum silicate, and is a kind of clay mineral. The attapulgite clay can replace the prior active carbon and active clay, and is used for decoloring and refining products with higher viscosity, such as vegetable oil, animal fat, gelatin, and the like. The attapulgite clay activated by hydrochloric acid can improve the decoloring capability of edible oil such as rape oil, soybean oil and the like by more than 2 times. The decolorized and purified salad oil has low acid value and can save the dehydration process. The filter cake (vegetable oil, animal fat, etc.) after filtration can be recycled, and does not pollute the environment. The attapulgite powder can also be used as filtering agent and clarifier for syrup, cane juice, beet juice, low-turbidity natural water, mineral water, beer, malt juice, fruit juice, wine, fruit wine, etc., and can decolorize and remove microorganisms and other impurities (such as pesticide in fruit juice and wine). It also has special and specific adsorption, can adsorb aflatoxin which is a strong carcinogen in vegetable oil, and is very simple and convenient to use without changing the original production process.

A magnet: the magnet is an ore of oxide mineral magnetite, and is divided into calcined magnet and vinegar magnet, the efficacy and the function of the magnet are to calm the liver and suppress yang, calm the nerves and relieve convulsion, improve hearing and eyesight, and receive qi and relieve asthma, the function of the magnet is to treat dizziness and blurred vision, deafness and tinnitus and the like, the medication contraindication of the magnet is caused by bupleurum, the magnet is peony and shikimic, the magnet is intolerant to xanthate, and iron toxicity is killed; it should be taken with magnet for a long time and more for deficiency of spleen and stomach.

In summary, the main material and the auxiliary material are functional mineral materials, in addition, a small amount of one or more auxiliary materials such as bentonite, montmorillonite and the like are compounded in an auxiliary mode, and the new material composite particle with the sleep-promoting function is obtained through hundred-percent suboptimal combination, repeated tests and blending.

Example 7

After the composite particles prepared by the embodiment of the invention are prepared into products, the clinical application population is preferably selected to be 45-80 years old. The female of the group is just after or in progress of the menopause, the menopause of the male is slow, and the chronic change of each part of the body can cause the change of dizziness, headache, fullness in the head and slow rise of blood pressure along with the increase of age. The symptoms of red face, red ears, tinnitus, amnesia, palpitation, insomnia and the like appear in different degrees, and a plurality of people can carry out drug treatment. Hypotensor, hypoglycemic, hypolipidemic, etc. are needed to be taken every day, and some effects are still not satisfactory or ideal. Under the background condition, the cross-border thinking is selected, the ancient medical treatment and modern medical treatment medicament principles are referred, the natural mineral substance principle and the physiological change principle are selected, the natural mineral substance is selected for deep processing, the special and specific functions of the natural mineral substance are exerted, the natural mineral substance is made into particles and filled in a pillow, so that people can carry out friction massage in sleep, a physical effect is generated when the natural mineral substance is in contact with the head, a patient with serious symptoms can be used as the auxiliary medical treatment of the medicament, a patient with light symptoms can be directly used as the main medical treatment, and a patient without obvious symptoms can be used for health preservation. Can be used for both general and general purpose. Has the advantages of no disadvantages. From the first batch to the second batch, 2000 deep sleep health pillows are produced in sequence, a large number of clinics are carried out, and complaints and feedback of one patient are not received so far. Next, we perform big data analysis on the tracking survey user;

case selection user 200

Case one, we selected an age group for feedback investigation, where;

the 10 capsules are 5% after 30-40 years old

30 capsules at 40-45 years old account for 15%

70 capsules at 50-60 years old account for 35%

70 capsules at the age of 60-70 years account for 35%

20 in 70-80 years old account for 10%

Investigating feedback effect

A comprehensive case; clinical response effects at different ages are as follows;

age group

Number of people

％

The effect is obvious

％

Has the effects of

％

The effect is not obvious

％

30-40 years old

10 persons

100％

3 persons

30％

4 persons

40％

3 persons

30％

40-50 years old

30 persons

100％

9 persons

30％

11 persons

43.33％

10 persons

33.33％

50-60 years old

70 persons

100％

25 persons

35.71％

26 persons

37.14％

19 persons

27.14％

60-70 years old

70 persons

100％

29 persons

41.43％

33 persons

47.14％

8 persons

11.43％

70-80 years old

20 persons

100％

7 persons

35％

10 persons

50％

3 persons

15％

Case two; 100 people who have poor sleep or are not good at times and are not ideal are selected to carry out clinical tests for 90-360 days, wherein;

case three; performing sleep feedback investigation on normal people (100 people);

1. has deep sleep promoting effect, 20% of 20 people

2. 45 people with certain sleep promoting effect

3. Non-responsive 35 people 35%

Case four; satisfaction survey 200 people

1. The granules in the pillow have effect of massaging cervical vertebra

Number of people

％

The effect is obvious

％

Has the effects of

％

The effect is not obvious

％

200 persons

100％

140 persons

70％

40 persons

20％

20 persons

10％

2. Comfort of particle-to-head contact in pillow

Number of people

％

Is very comfortable

％

In general

％

Has hardness

％

200 persons

100％

100 persons

50％

60 persons

30％

40 persons

20％

3. Biomagnetic field perceptibility in pillow granules

Number of people

％

Has a feeling of

％

In general

％

Has poor reaction

％

200 persons

100％

120 persons

60％

80 persons

40％

0 person

0％

4. Far infrared rays in particles in pillow

Number of people

％

Has a feeling of

％

Has no feeling of feeling

％

Has poor reaction

％

200 persons

100％

90 persons

45％

110 persons

55％

0 person

0％

5. Release negative oxygen ions in the counter pillow

Number of people

％

Has a feeling of

％

Has no feeling of feeling

％

Has poor reaction

％

200 persons

100％

130 persons

65％

70 persons

35％

0 person

0％

6. Clip design for pillow

Number of people

％

Satisfaction

％

In general

％

Is not satisfied with

％

200 persons

100％

140 persons

70％

60 persons

30％

0 person

0％

7. For arrangement and combination of particles in pillow

Number of people

％

Satisfaction

％

In general

％

It has been proposed

％

200 persons

100％

150 persons

75％

40 persons

20％

10 persons

5％

8. The use of the pillow is suspected to have psychological influence

9. Adsorption capacity of particles in pillow to peculiar smell in air

Number of people

％

Is very good

％

In general

％

Is not obvious

％

200 persons

100％

150 persons

75％

44 persons

22％

6 persons

3％

The questionnaire survey is combined to obtain a plurality of beneficial big data, and the good promotion effect is achieved on the positive sleep promotion effect and the improvement of the product quality. Besides the questionnaire survey, the invention also carries out 1. air negative ion concentration measurement and 2. detection of more than ten indexes such as free formaldehyde, volatile organic compounds toluene, ethylbenzene and the like in the national building decoration material quality safety supervision and detection center, Shenyang product quality supervision and inspection institute and Liaoning province product quality supervision and inspection institute. 3. And (4) carrying out radionuclide quantity limit detection. 4. And (5) detecting far infrared rays, and detecting a biological magnetic field. All reach the standard and are qualified. And conforms to the national standard.

The preferred embodiments of the invention disclosed above are intended to be illustrative only, and not to be exhaustive or to limit the invention to the precise embodiments and formulations disclosed, and obviously many modifications and variations are possible in light of the above teaching. The granulation can be carried out firstly or separately, and the function and the effect are not influenced by the granulation. The embodiments were chosen and described in order to best explain the principles of the invention and its practical applications. Thus, it will be appreciated that those skilled in the art will be able to make and use the invention, which is limited only by the following claims and their full scope and equivalents.

Claims

1. The new material composite particle with the sleep promoting function is characterized by comprising the following formula: 550-650kg of concentrated hot spring jade powder (325-400 meshes); 80-100kg of modified diatomite raw material (325-400 meshes); 80-100kg of tourmaline powder (325-400 meshes); 60-80kg of Chinese medical stone (325-400 meshes); 40-60kg of zeolite powder (325-400 meshes); 40-60kg of attapulgite powder (325-400 meshes); 40-60kg of magnetite powder (325-400 meshes); 10-20kg of bentonite (325-400 meshes).

2. The method for preparing the composite particle of the new material with the function of promoting sleep as claimed in claim 1, is characterized by comprising the following processing procedures: 1. concentrating hot spring water; 2. crushing the jade; 3. soaking the hot spring jade rice grains → heating → drying → crushing into powder; 4. modifying diatomite; 5. selecting and crushing tourmaline; 6. selecting and crushing Chinese medical stone; 7. selecting and crushing zeolite; 8. selecting and crushing attapulgite; 9. selecting and crushing the magnetite; 10. selecting and crushing bentonite; 11. compounding; 12. the dry powder is evenly stirred and compounded for granulation; 13. screening uniform particles; 14. calcining to obtain qualified product.

3. The method for preparing the novel material composite particle with the sleep-promoting function according to claim 1, is characterized by comprising the following specific preparation processes: (1) selecting jade rice grains of hsiuyen rock; (2) washing and removing impurities; (3) concentrating hot spring water, and soaking for 15-20 days; (4) continuously heating to 30-50 deg.C to further enhance absorption of therapeutic effects of hot spring and jade; (5) adsorption drying; (6) crushing to 325-400 meshes; (7) mixing with other adjuvants, and stirring; (8) compound granulation; (9) screening uniform particles, (10) calcining to obtain qualified products; (11) and packaging the finished product for delivery.

4. The method for preparing novel material composite particles with sleep-promoting function as claimed in claim 3, wherein the Xiuyan rock jade rice grains are residual waste residues of carving and mining.

5. A method for preparing a new material composite particle with sleep promoting function as claimed in claim 3, wherein the particle size of the particle in the step (9) is 0.1-0.15 mm.

6. The method for preparing composite particles of new material with sleep-promoting function as claimed in claim 2, wherein the modified diatomite has a specific surface area of 85m²G, SiO in diatomaceous earth₂The content accounts for 50-68% of the total weight, and the fineness is as follows: 325- & ltwbr- & gt 400 meshes and the whiteness is 65-75.