CN110809622A - 新型的龙涎香类和/或吲哚类的芳香剂组合物 - Google Patents
新型的龙涎香类和/或吲哚类的芳香剂组合物 Download PDFInfo
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- CN110809622A CN110809622A CN201780092323.XA CN201780092323A CN110809622A CN 110809622 A CN110809622 A CN 110809622A CN 201780092323 A CN201780092323 A CN 201780092323A CN 110809622 A CN110809622 A CN 110809622A
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- NPFVOOAXDOBMCE-UHFFFAOYSA-N trans-3-hexenyl acetate Natural products CCC=CCCOC(C)=O NPFVOOAXDOBMCE-UHFFFAOYSA-N 0.000 description 1
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 description 1
- XJPBRODHZKDRCB-UHFFFAOYSA-N trans-alpha-ocimene Natural products CC(=C)CCC=C(C)C=C XJPBRODHZKDRCB-UHFFFAOYSA-N 0.000 description 1
- BJIOGJUNALELMI-UHFFFAOYSA-N trans-isoeugenol Natural products COC1=CC(C=CC)=CC=C1O BJIOGJUNALELMI-UHFFFAOYSA-N 0.000 description 1
- HETFMJQWNWIBPN-UHFFFAOYSA-N undec-2-enenitrile Chemical compound CCCCCCCCC=CC#N HETFMJQWNWIBPN-UHFFFAOYSA-N 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- WCTNXGFHEZQHDR-UHFFFAOYSA-N valencene Natural products C1CC(C)(C)C2(C)CC(C(=C)C)CCC2=C1 WCTNXGFHEZQHDR-UHFFFAOYSA-N 0.000 description 1
- 235000016788 valerian Nutrition 0.000 description 1
- 239000010679 vetiver oil Substances 0.000 description 1
- KAKZBPTYRLMSJV-UHFFFAOYSA-N vinyl-ethylene Natural products C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 1
- 239000001846 viola odorata l. leaf absolute Substances 0.000 description 1
- 239000009637 wintergreen oil Substances 0.000 description 1
- QRPLZGZHJABGRS-UHFFFAOYSA-N xi-5-Dodecanolide Chemical compound CCCCCCCC1CCCC(=O)O1 QRPLZGZHJABGRS-UHFFFAOYSA-N 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 229930007850 β-damascenone Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- Fats And Perfumes (AREA)
Abstract
Description
技术领域
本发明主要涉及如本文所述的式(I)的一种或多种化合物作为芳香剂(Riechstoff)的用途。本发明还涉及包含如本文所述的新型的芳香剂组合物,其包括式(I)的一种或多种化合物,所述芳香剂组合物的用途,包含所述芳香剂组合物的加香制品,以及用于对所述制品进行加香或者用于赋予、改变和/或强化特定香调的多种方法。
本发明的其他方面和优选实施方案从接下来的实施方案、所附实施例以及特别地所附的权利要求中得出。
背景技术
在香水业中,已知用于赋予香味的大量各种各样的化合物。然而,始终存在对新型的有利化合物的需求,所述化合物除了具有其正面的和原始的嗅觉特性外,还具有附加的正面的次级特性。
在寻找适合的化合物时,本领域技术人员面临着如下艰巨的任务:要么从大量已知的化合物中辨别出合适的芳香剂,要么制备具有所期望的特性的新型的化合物。在此,无法预测新型的化合物到底有没有气味,以及该气味是具有所期望嗅觉特性还是具有所不期望的嗅觉特性。在发现具有正面的气味的化合物时,它是什么气味以及该化合物在多大程度上还具有正面的次级特性也是成问题的。
迄今为止已知的许多芳香剂一方面具有明显的缺点。例如,它们通常具有非常有限的稳定性和扩散性、低附着能力、低散发度、差的溶解性,并且经常必须以高剂量使用。
另外,对新型的芳香剂提出很高的要求。因此,它们例如应具有非常好的生物可降解性,并且在皮肤病学和毒理学上无害。
气味“龙涎香”或者“琥珀”是香水中高度优选的香调之一。它给予香水特有的排他性和奢华感。最初,琥珀是从抹香鲸的消化道中提取的;如今,优选来自其他来源的龙涎香香味。许多龙涎香芳香剂的缺点是,它们的嗅觉印象仅逐渐地被感知到,因此很难在香水的前调中表现出龙涎香气味。
吲哚类香调极其频繁地在香水中使用,并且属于非常流行的香调,以便赋予香水特有的花香散发度。此外也散发出吲哚气味的龙涎香调在此被感觉为是特别高品质的。
发明内容
本发明的目的在于,提供不具有或减轻现有技术的一开始提到的缺点的化合物。特别地,本发明的目的在于,提供如下芳香剂,所述芳香剂能够赋予、改变和/或强化龙涎香和/或吲哚类香调并且还具有正面的次级特性,例如良好的生物降解性和/或高的皮肤相容性。
根据本发明,所提出的目的通过使用式(I)的一种或多种化合物作为芳香剂来实现
其中R是甲基或乙基,并且R1是H、甲基或乙基。
根据本发明待使用的式(I)的化合物能够以任意立体异构形式存在。在本发明的范畴中,也能够使用式(I)的化合物的立体异构体的任意混合物,例如非对映异构体混合物、对映异构体混合物或外消旋物,也就是说,术语“式(I)的化合物”在本文的范畴中也包括式(I)的化合物的不同的立体异构体的所述任意混合物。
在本文中针对式(I)的化合物所述的内容,特别是本文所述的优点,也适用于式(I)的化合物的立体异构体的根据本发明待使用或应用的混合物。
只要在本文的范畴中无意间在化学名称与所示结构式之间存在差异,那么请以所示结构式为准。
已经令人惊讶地发现,根据本发明待应用的式(I)的化合物具有龙涎香类和/或吲哚类的香调。此外,它们具有高的稳定性和扩散性、良好的附着能力、非常高的散发度、低的气味阈值、非常好的溶解度和可混合性、与其他芳香剂发生反应的低的倾向、非常好的皮肤病学和毒理学相容性以及良好的生物可降解性。
根据本发明待应用的式(I)的化合物的另一个优点是其在相对较低的剂量下高的气味强度。出于环境污染的原因,这尤其引人关注,因为由此能够将释放到环境中的物质的量保持在最低水平。此外,龙涎香调特别快地被感觉到,以至于式(I)的化合物例如适合于作为香油中的前调。
式(I)的化合物本身是非常稳定的,并且在不利的条件下,例如在高的氧含量、高含量的氧化剂或还原剂含量以及高的pH值下同样具有高的稳定性。
优选的是根据本发明的用途,其中一种、多种或所有式(I)的化合物选自式(Ia)的化合物、式(Ib)的化合物和式(Ic)的化合物。
式(Ia)、(Ib)和(Ic)的化合物的特征在于,其即使在剂量低时也具有特别复杂、散发性和高强度的龙涎香气味。此外,它们具有吲哚类香味,以至于产生了由龙涎香与花香散发性构成的特别期望的组合。下文的概述描述了根据本发明优选待应用的式(Ia)、(Ib)和(Ic)的化合物的嗅觉特性:
因此,优选地,根据本发明的用途涉及式(I)的一种或多种化合物,优选选自式(Ia)的化合物、式(Ib)的化合物和式(Ic)的化合物的一种或多种式(I)的化合物的用途,用于赋予、改变和/或强化选自龙涎香、吲哚和木质调的一种或多种香调,优选地用于修饰、调和和/或改善一种或多种其他芳香剂的天然嗅觉印象和/或用于赋予、改变和/或强化龙涎香类和/或木质调和/或吲哚类嗅觉前调。
本发明的另一方面涉及芳香剂组合物,其包含式(I)的一种或多种化合物或由其组成
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选地包含式(Ia)和/或(Ib)和/或(Ic)的化合物中的一种或多种或由其组成,
和
一种或更多种溶剂,其中优选地,一种、多种或所有的溶剂选自乙醇、异丙醇、二乙二醇单乙醚、甘油、丙二醇、1,2-丁二醇、二丙二醇、邻苯二甲酸二乙酯、柠檬酸三乙酯和肉豆蔻酸异丙酯,
和/或一种或多种其他芳香剂,
其中,优选地,芳香剂混合物中的式(I)的化合物的总质量与芳香剂混合物中的一种或多种其他芳香剂(如果存在的话)的总质量的比为1:999至999:1,优选地1:99至1:1,尤其优选地1:99至1:2,更优选地1:90至1:5,并且特别优选地1:80至1:10。
使用上述溶剂在此是特别有利的,因为根据本发明待使用的式(I)的化合物能够特别好地溶解在这些溶剂中。
还有利的是,根据本发明待应用的式(I)的化合物尤其好并且以非常宽的浓度比溶于其他芳香剂中,并且与其他芳香剂具有低的反应性。式(I)的化合物,如上所限定的那样,在包含一种或多种其他芳香剂的芳香剂组合物中此外在嗅觉方面起修饰、圆滑过渡的作用并且总体上改进芳香剂组合物的天然的嗅觉印象。
能够有利地与根据本发明待应用的式(I)的化合物组合的其他芳香剂的实例例如能够在S.Arctander,Perfume and Flavor Materials,第I和II卷,Montclair、N.J.1969,Eigenverlag或K.Bauer等、Common Fragrance and Flavor Materials,第4版,Wiley-VCH,Weinheim 2006中找到。
需要详细说明:来自天然原材料的提取物,例如精油、凝脂、净油、树脂、类树脂、香脂、酊,例如如龙涎香酊(ambergris tincture);阿米香树油(amyris oil);当归籽油;当归根油;茴香油;缬草油;罗勒油(basil oil);树苔净油(tree moss absolute);月桂油(bayoil);艾蒿油;安息香树脂(benzoe resin);佛手柑油(bergamot oil);蜂蜡净油;桦树油;苦杏仁油;香薄荷油(savory oil);布枯叶油(bucco leaf oil);巴西檀木油(cabreuvaoil);杜松油(cade oil);菖蒲油(calmus oil);樟脑油;衣兰油(cananga oil);小豆蔻油(cardamom oil);卡黎油(cascarilla oil);肉桂油(cassia oil);合金欢净油(cassieabsolue);海狸香净油(castoreum absolue);雪松叶油;雪松木油;岩蔷薇油;香茅油;柠檬油;苦配巴香脂(copaiba balsam);配巴香脂油;芫荽油;闭鞘姜根油(costus root oil);孜然油;柏树油;印蒿油(davana oil);莳萝草油(dill herb oil);莳萝籽油;淡香水净油(eau de brouts absolue);橡苔净油(oak moss absolue);榄香油(elemi oil);龙蒿油;柠檬桉油(eucalyptus citriodora oil);桉树油;茴香油;云杉针油;白松香油(galbanumoil);白松香树脂(galbanum resin);香叶油;葡萄柚油;愈创木油;古芸香(gurjunbalsam);古芸香油;蜡菊净油(helichrysum absolue);蜡菊油(helichrysum oil);姜油;鸢尾根净油;鸢尾根油;茉莉净油;菖蒲油;蓝洋甘菊油(chamomile oil blue);罗马洋甘菊油(roman chamomile oil);胡萝卜籽油;卡黎油(cascarilla oil);松针油;留兰香油;香菜油(caraway oil);岩蔷薇油(labdanum oil);岩蔷薇净油(labdanum absolue);岩蔷薇树脂(labdanum resin);醒目薰衣草净油(lavandin absolue);醒目薰衣草油(lavandinoil);薰衣草净油;薰衣草油;柠檬草油;独活草油(lovage oil);蒸馏梨莓油(distilledlime oil);压榨梨莓油(pressed lime oil);里那油;山苍子油(litsea cubeba oil);月桂叶油;马西斯油(macis oil);马郁兰油;柑橘油;马尾松油(massoi bark oil);含羞草净油;麝香籽油;麝香酊;马斯喀特鼠尾草油(muscat sage oil);肉豆蔻油;没药净油;没药油;桃金娘油;丁香叶油;丁香花油;橙花油;乳香净油(olibanum absolue);乳香油(olibanum oil);合金欢油(opopanax oil);橙花净油;橙油;牛至油;玫瑰草油(palmarosaoil);广藿香油;紫苏油;秘鲁香脂油;欧芹叶油;欧芹籽油;橙叶油(petite grain oil);薄荷油;胡椒油;多香果油(pimento oil);松油;波莱油(poley oil);玫瑰净油;红木油;玫瑰油;迷迭香油;达尔马提亚鼠尾草油(dalmatian sage oil);西班牙鼠尾草油(spanishsage oil);檀香油;芹菜籽油;加标薰衣草油(spiked lavender oil);八角油;苏合香油(styrax oil);万寿菊;冷杉针油;茶树油;松节油;百里香油;吐鲁香脂(tolu balsam);香豆净油(tonka absolue);夜来香净油;香草提取物;紫罗兰叶净油;马鞭草油;香根草油;杜松子油;葡萄酒酵母油;艾草油;冬青油;依兰油;神香草油(ysop oil);麝猫净油(civetabsolue);肉桂叶油;肉桂皮油及其级分,或从中离析出的内含物;
来自烃类的单一芳香剂,例如3-蒈烯(3-carene);α-蒎烯;β-蒎烯;α-萜品烯;γ-萜品烯;对聚伞花素(p-cymol);红没药烯;莰烯;石竹烯;雪松烯(cedrene);金合欢烯;柠檬烯;长叶烯;月桂烯;罗勒烯;瓦伦烯(valencene);(E,Z)-1,3,5-十一碳三烯;苯乙烯;二苯基甲烷;
脂族醇,例如己醇;辛醇;3-辛醇;2,6-二甲基庚醇;2-甲基-2-庚醇;2-甲基-2-辛醇;(E)-2-己烯醇;(E)-和(Z)-3-己烯醇;1-辛烯-3-醇;3,4,5,6,6-五甲基-3,4-庚烯-2-醇和3,5,6,6-四甲基-4-亚甲基庚-2-醇的混合物;(E,Z)-2,6-壬二烯醇;3,7-二甲基-7-甲氧基辛烷-2-醇;9-癸烯醇;10-十一烯醇;4-甲基-3-癸烯-5-醇;
脂族醛及其缩醛,例如己醛;庚醛;辛醛;壬醛;癸醛;十一醛;十二醛;十三醛;2-甲基辛醛;2-甲基壬醛;(E)-2-己烯醛;(Z)-4-庚烯醛;2,6-二甲基-5-庚烯醛;10-十一碳烯醛;(E)-4-癸烯醛;2-十二碳烯醛;2,6,10-三甲基-9-十一碳烯醛;2,6,10-三甲基-5,9-十一碳二烯醛;庚醛二乙烯醛;1,1-二甲氧基-2,2,5-三甲基-4-己烯;香茅基氧基乙醛;1-(1-甲氧基-丙氧基)-(E/Z)-3-己烯;
脂族酮及其肟,例如2-庚酮;2-辛酮;3-辛酮;2-壬酮;5-甲基-3-庚酮;5-甲基-3-庚酮肟;2,4,4,7-四甲基-6-辛烯-3-酮;6-甲基-5-庚烯-2-酮;
脂族含硫化合物,例如3-甲基硫基己醇;3-甲基硫基己基乙酸酯;3-巯基己醇;3-巯基己基乙酸酯;3-巯基己基丁酸酯;3-乙酰基硫基己基乙酸酯;1-薄荷烯-8-硫醇;
脂族腈,例如2-壬烯酸腈;2-十一碳烯酸腈;2-十三碳烯酸腈;3,12-十三碳二烯酸腈;3,7-二甲基-2,6-辛二烯酸腈;3,7-二甲基-6-辛烯酸腈;
脂族羧酸的酯,例如(E)-和(Z)-3-己烯基甲酸酯;乙酰乙酸乙酯;乙酸异戊酯;乙酸己酯;3,5,5-三甲基己基乙酸酯;3-甲基-2-丁烯基乙酸酯;(E)-2-己烯基乙酸酯;(E)-和(Z)-3-己烯基乙酸酯;乙酸辛酯;3-辛基乙酸酯;1-辛烯-3-基乙酸酯;丁酸乙酯;丁酸丁酯;丁酸异戊酯;丁酸己酯;(E)-和(Z)-3-己烯基异丁酸酯;巴豆酸己酯;异戊酸乙酯;2-甲基戊酸乙酯;己酸乙酯;己酸烯丙酯;庚酸乙酯;庚酸烯丙酯;辛酸乙酯;乙基-(E,Z)-2,4-癸二烯酸酯;甲基-2-辛炔酸酯(methyl-2-octinate);甲基-2-壬炔酸酯(methyl-2-noninate);烯丙基-2-异戊氧基乙酸酯;甲基-3,7-二甲基-2,6-辛二酸酯;4-甲基-2-戊基巴豆酸酯;
非环状萜烯醇,例如香茅醇;香叶醇;橙花醇;芳樟醇;薰衣草醇(lavadulol);橙花叔醇;金合欢醇;四氢芳樟醇;四氢香叶醇;2,6-二甲基-7-辛烯-2-醇;2,6-二甲基辛-2-醇;2-甲基-6-亚甲基-7-辛烯-2-醇;2,6-二甲基-5,7-辛二烯-2-醇;2,6-二甲基-3,5-辛二烯-2-醇;3,7-二甲基-4,6-辛二烯-3-醇;3,7-二甲基-1,5,7-辛三烯-3-醇;2,6-二甲基-2,5,7-辛三烯-1-醇;及其甲酸酯、乙酸酯、丙酸酯、异丁酸酯、丁酸酯、异戊酸酯、戊酸酯、己酸酯、巴豆酸酯、惕各酸烯酯(tiglinate)和3-甲基-2-丁烯酸酯;
非环状萜烯醛和酮,例如香叶醛;橙花醛;香茅醛;7-羟基-3,7-二甲基辛醛;7-甲氧基-3,7-二甲基辛醛;2,6,10-三甲基-9-十一碳烯醛;香叶基丙酮;以及香叶醛、橙花醛、7-羟基-3,7-二甲基辛醛的二甲基和二乙基缩醛;
环状萜烯醇,例如薄荷醇;异胡薄荷醇;α-萜品醇;萜品醇-4;薄荷烷-8-醇;薄荷烷-1-醇;薄荷烷-7-醇;冰片;异冰片;芳樟醇氧化物;诺卜醇(nopol);雪松醇;龙涎醇(ambrinol);岩兰草醇(vetiverol);愈创木醇(guaiol);及其甲酸酯、乙酸酯、丙酸酯、异丁酸酯、丁酸酯、异戊酸酯、戊酸酯、己酸酯、巴豆酸酯、惕各酸烯酯(tiglinate)和3-甲基-2-丁烯酸酯;
环状萜烯醛和酮,例如薄荷酮;异薄荷酮;8-巯基薄荷烷-3-酮(8-mercaptomenthan-3-one);香芹酮;樟脑;葑酮;α-紫罗兰酮;β-紫罗兰酮;α-正甲基紫罗兰酮;β-正甲基紫罗兰酮;α-异甲基紫罗兰酮;β-异甲基-紫罗兰酮;α-鸢尾酮;α-二氢大马酮;β-二氢大马酮;β-大马酮;δ-二氢大马酮;γ-二氢大马酮;1-(2,4,4-三甲基-2-环己烯-1-基)-2-丁烯-1-酮;1,3,4,6,7,8a-六氢-1,1,5,5-四甲基-2H-2,4a-桥亚甲基-萘-8(5H)-酮;2-甲基-4-(2,6,6-三甲基-1-环己烯-1-基)-2-丁烯醛;诺卡酮;二氢诺卡酮;4,6,8-巨豆三烯-3-酮(4,6,8-megastigmatrien-3-one);α-甜橙醛;β-甜橙醛;乙酰化柏木油(甲基柏木酮);
环状醇,例如4-叔丁基环己醇;3,3,5-三甲基环己醇;3-异龙脑基环己醇;2,6,9-三甲基Z2,Z5,E9-环十二碳三烯-1-醇;2-异丁基-4-甲基四氢-2H-吡喃-4-醇;
脂环族醇,例如α,3,3-三甲基环己基甲醇;1-(4-异丙基环己基)乙醇;2-甲基-4-(2,2,3-三甲基-3-环戊-1-基)丁醇;2-甲基-4-(2,2,3-三甲基-3-环戊-1-基)-2-丁烯-1-醇;2-乙基-4-(2,2,3-三甲基-3-环戊烯-1-基)-2-丁烯-1-醇;3-甲基-5-(2,2,3-三甲基-3-环戊-1-基)-戊烷-2-醇;3-甲基-5-(2,2,3-三甲基-3-环戊-1-基)-4-戊烯-2-醇;3,3-二甲基-5-(2,2,3-三甲基-3-环戊-1-基)-4-戊烯-2-醇;1-(2,2,6-三甲基环己基)戊烷-3-醇;1-(2,2,6-三甲基环己基)己烷-3-醇;环状和脂环族醚,例如桉油酚(cineol);甲基柏木醚;环十二烷基甲醚;1,1-二甲氧基环十二烷;(乙氧基甲氧基)环-十二烷;α-雪松烯环氧化物;3a,6,6,9a-四甲基十二碳萘并[2,1-B]呋喃;3a-乙基6,6,9a-三甲基十二碳萘并[2,1-b]呋喃;1,5,9-三甲基-13-氧杂二环[10.1.0]十三碳-4,8-二烯;玫瑰氧化物(roseoxide);2-(2,4-二甲基-3-环己烯-1-基)-5-甲基-5-(1-甲基丙基)-1,3-二氧六环;
环状和大环酮,例如4-叔丁基环己酮;2,2,5-三甲基-5-戊基环戊酮;2-庚基环戊酮;2-戊基环戊酮;2-羟基-3-甲基-2-环戊烯-1-酮;3-甲基-顺式-2-戊烯-1-基-2-环戊烯-1-酮;3-甲基-2-戊基-2-环戊烯-1-酮;3-甲基-4-环十五烯酮(3-methyl-4-cyclopentadecenone);3-甲基-5-环十五烯酮;3-甲基环十五烷酮(3-methylcyclopentadecanon);4-(1-乙氧基乙烯基)-3,3,5,5-四甲基环己酮;4-叔戊基环己酮;5-环十六烯-1-酮;6,7-二氢-1,1,2,3,3-五甲基-4(5H)-茚酮;8-环十六烯-1-酮;9-环十七烯-1-酮;环十五烷酮;环十六烷酮;
脂环族醛,例如2,4-二甲基-3-环己烯甲醛;2-甲基-4-(2,2,6-三甲基-环己烯-1-基)-2-丁烯醛;4-(4-羟基-4-甲基戊基)-3-环己烯甲醛;4-(4-甲基-3-戊烯-1-基)-3-环己烯甲醛;
脂环族酮,例如1-(3,3-二甲基环己基)-4-戊烯-1-酮;2,2-二甲基-1-(2,4-二甲基-3-环己烯-1-基)-1-丙酮;1-(5,5-二甲基-1-环己烯-1-基)-4-戊烯-1-酮;2,3,8,8-四甲基-1,2,3,4,5,6,7,8-八氢-2-萘烯基甲基酮;甲基-2,6,10-三甲基-2,5,9-环十二碳三烯酮;叔丁基-(2,4-二甲基-3-环己烯-1-基)酮;
环状醇的酯,例如2-叔丁基环己基乙酸酯;4-叔丁基环己基乙酸酯;2-叔戊基环己基乙酸酯;4-叔戊基环己基乙酸酯;3,3,5-三甲基环己基乙酸酯;十氢-2-萘基乙酸酯;2-环戊基环戊基巴豆酸酯;3-戊基四氢-2H-吡喃-4-基乙酸酯;十氢-2,5,5,8a-四甲基-2-萘基乙酸酯;4,7-桥亚甲基-3a,4,5,6,7,7a-六氢-5-茚基乙酸酯或4,7-桥亚甲基-3a,4,5,6,7,7a-六氢-6-茚基乙酸酯;4,7-桥亚甲基-3a,4,5,6,7,7a-六氢-5-茚基丙酸酯或4,7-桥亚甲基-3a,4,5,6,7,7a-六氢-6-茚基丙酸酯;4,7-桥亚甲基-3a,4,5,6,7,7a-六氢-5-茚基异丁酸酯或4,7-桥亚甲基-3a,4,5,6,7,7a-六氢-6-茚基异丁酸酯;4,7-桥亚甲基八氢-5-茚基乙酸酯或4,7-桥亚甲基八氢-6-茚基乙酸酯;
脂环族醇的酯,例如1-环己基乙基巴豆酸酯;
脂环族羧酸的酯,例如烯丙基-3-环己基丙酸酯;烯丙基环己氧基乙酸酯;顺式和反式甲基二氢茉莉酮酸酯;顺式和反式甲基茉莉酮酸酯;甲基-2-己基-3-氧代环戊烷羧酸酯;乙基2-乙基-6,6-二甲基-2-环己烯羧酸酯;乙基-2,3,6,6-四甲基-2-环己烯羧酸酯;乙基-2-甲基-1,3-二氧戊环-2-乙酸酯;芳脂族醇,例如苯甲醇;1-苯基乙醇;2-苯基乙醇;3-苯基丙醇;2-苯基丙醇;2-苯氧基乙醇;2,2-二甲基-3-苯基丙醇;2,2-二甲基-3-(3-甲基苯基)丙醇;1,1-二甲基-2-苯基乙醇;1,1-二甲基-3-苯基丙醇;1-乙基-1-甲基-3-苯基丙醇;2-甲基-5-苯基戊醇;3-甲基-5-苯基戊醇;3-苯基-2-丙烯-1-醇;4-甲氧基苯甲醇;1-(4-异丙基苯基)乙醇;
芳脂族醇和脂族羧酸的酯,例如乙酸苄酯;丙酸苄酯;异丁酸苄酯;异戊酸苄酯;2-苯基乙基乙酸酯;2-苯基乙基丙酸酯;2-苯基乙基异丁酸酯;2-苯基乙基异戊酸酯;1-苯基乙基乙酸酯;α-三氯甲基苄基乙酸酯;α,α-二甲基苯基乙基乙酸酯;α,α-二甲基苯基乙基丁酸酯;乙酸肉桂酯;2-苯氧基乙基异丁酸酯;4-甲氧基苄基乙酸酯;
芳脂族醚,例如2-苯基乙基甲基醚;2-苯基乙基异戊基醚;2-苯基乙基-1-乙氧基乙基醚;苯乙醛二甲基缩醛;苯乙醛二乙基缩醛;氢化阿托醛二甲基缩醛(hydratropaaldehyde dimethylacetal);苯乙醛甘油缩醛;2,4,6-三甲基-4-苯基-1,3-二氧六环;4,4a,5,9b-四氢茚并[1,2-d]-间-二恶英;4,4a,5,9b-四氢-2,4-二甲基茚并[1,2-d]-间-二恶英;
芳族和芳脂族醛,例如苯甲醛;苯乙醛;3-苯基丙醛;氢化阿托醛;4-甲基苯甲醛;3-(4-乙基苯基)-2,2-二甲基丙醛;2-甲基-3-(4-异丙基苯基)丙醛;2-甲基-3-(4-叔丁基苯基)丙醛;3-(4-叔丁基苯基)丙醛;2-甲基-3-(4-异丙基苯基)丙醛;3-(4-叔丁基苯基)丙醛;肉桂醛;α-丁基肉桂醛;α-戊基肉桂醛;α-己基肉桂醛;3-甲基-5-苯基戊醛;4-甲氧基苯甲醛;4-羟基-3-甲氧基苯甲醛;4-羟基-3-乙氧基苯甲醛;3,4-亚甲基二氧基苯甲醛;3,4-二甲氧基苯甲醛;2-甲基-3-(4-甲氧基苯基)丙醛;2-甲基-3-(4-亚甲基二氧基苯基)丙醛;芳族和芳脂族酮,例如苯乙酮;4-甲基苯乙酮;4-甲氧基苯乙酮;4-叔丁基-2,6-二甲基苯乙酮;4-苯基-2-丁酮;4-(4-羟基苯基)-2-丁酮;1-(2-萘-烯基)乙酮;2-苯并呋喃基乙酮;(3-甲基-2-苯并呋喃基)乙酮;二苯甲酮;1,1,2,3,3,6-六甲基-5-茚基甲基酮;6-叔丁基-1,1-二甲基-4-茚基甲基酮;1-[2,3-二氢-1,1,2,6-四甲基-3-(1-甲基乙基)-1H-5-茚基]乙酮;5’,6’,7’,8’-四氢-3’,5’,5’,6’,8’,8’-六甲基-2-苯乙酮;
芳族和芳脂族羧酸及其酯,例如苯甲酸;苯乙酸;苯甲酸甲酯;苯甲酸乙酯;苯甲酸己酯;苯甲酸苄酯;苯乙酸甲酯;苯乙酸乙酯;苯乙酸香叶基酯;苯乙酸苯乙基酯;肉桂酸甲酯;肉桂酸乙酯;肉桂酸苄酯;肉桂酸苯乙酯;肉桂酸肉桂基酯;烯丙基苯氧基乙酸酯;水杨酸甲酯;水杨酸异戊酯;水杨酸己酯;水杨酸环己酯;顺式-3-己烯基水杨酸酯;水杨酸苄酯;水杨酸苯乙酯;2,4-二羟基-3,6-二甲基苯甲酸甲酯;乙基-3-苯基缩水甘油酸酯;乙基-3-甲基-3-苯基缩水甘油酸酯;
含氮芳族化合物,例如2,4,6-三硝基-1,3-二甲基-5-叔丁基苯;3,5-二硝基-2,6-二甲基-4-叔丁基苯乙酮;肉桂酸腈;3-甲基-5-苯基-2-戊烯酸腈;3-甲基-5-苯基戊酸腈;邻氨基苯甲酸甲酯;甲基-N-邻氨基苯甲酸甲酯;邻氨基苯甲酸甲酯与7-羟基-3,7-二甲基辛醛、2-甲基-3-(4-叔丁基-苯基)丙醛或2,4-二甲基-3-环己烯甲醛的席夫碱;6-异丙基喹啉;6异丁基喹啉;6-仲丁基喹啉;2-(3-苯丙基)吡啶;吲哚;粪臭素(skatol);2-甲氧基-3-异丙基吡嗪;2-异丁基-3-甲氧基吡嗪;
苯酚、苯醚和苯酯,例如草蒿脑;茴香脑;丁香油酚;丁香基甲基醚;异丁香酚;异丁香基甲基醚;百里酚;香芹酚;二苯基醚;β-萘基甲基醚;β-萘基乙基醚;β-萘基异丁基醚;1,4-二甲氧基苯;丁香基乙酸酯;2-甲氧基-4-甲基苯酚;2-乙氧基-5-(1-丙烯基)苯酚;对甲苯基苯乙酸酯;
杂环化合物,例如2,5-二甲基-4-羟基-2H-呋喃-3-酮;2-乙基-4-羟基-5-甲基-2H-呋喃-3-酮;3-羟基-2-甲基-4H-吡喃-4-酮;2-乙基-3-羟基-4H-吡喃-4-酮;
内酯,例如1,4-辛内脂;3-甲基-1,4-辛内脂;1,4-壬内脂;1,4-癸内脂;8-癸烯-1,4-内酯;1,4-十一内脂;1,4-十二内酯;1,5-癸内脂;1,5-十二内酯;4-甲基-1,4-癸内酯;1,15-十五内酯;顺式-11-十五碳烯-1,15-内酯和反式-11-十五碳烯-1,15-内酯;顺式-12-十五碳烯-1,15-内酯和反式-12-十五碳烯-1,15-内酯;1,16-十六内脂;9-十六碳烯-1,16-内酯;10-氧杂-1,16-十六内酯;11-氧杂-1,16-十六内脂;12-氧杂-1,16-十六内酯;乙烯-1,12-十二烷二酸酯;乙烯-1,13-十三烷二酸酯;香豆素;2,3-二氢香豆素;八氢香豆素。
此外优选的是如上所述的根据本发明的芳香剂组合物,其中按芳香剂组合物的总重量计,芳香剂组合物中的式(I)的化合物的总量的份额为0.1重量%至50重量%,更优选为0.5重量%至15重量%,特别优选为0.75重量%至2重量%。
特别优选的是如上所述的根据本发明的芳香剂组合物,其包含如上所述的和根据一个可行的设计方案的一种或多种溶剂——优选不包含任何其他芳香剂,其中按式(I)的化合物和一种/多种溶剂的总重量计,芳香剂组合物中的式(I)的化合物的总量的份额为0.1重量%至50重量%,更优选为0.5重量%至15重量%,尤其优选为0.75重量%至2重量%。
此外,优选的是根据本发明的芳香剂组合物,其中所述芳香剂组合物包含式(I)的一种或多种化合物或由其组成
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选式(Ia)和/或(Ib)和/或(Ic)的化合物中的一种或多种,
和
如上所述的一种或多种溶剂,
以及一种或多种另外的芳香剂,
其中优选地,按芳香剂组合物的总重量计,所述芳香剂组合物中的式(I)的化合物的总量与一种或多种另外的芳香剂的总量的份额为0.1重量%至50重量%,和/或其中优选地,芳香剂混合物中的式(I)的化合物的总质量与芳香剂混合物中的一种或多种另外的芳香剂的总质量的比例在1:90至1:5的范围中。
根据本发明的芳香剂组合物优选是香油;香水;香水提取物;浓香水;淡香水;剃须露;淡古龙水;须前产品;古龙敷拍水。在此,根据本发明待应用的式(I)的化合物优选形成香水或香精油的前调。香油的前调包括其气味能够被尤其快地感知到的调。
本发明的另一个方面涉及如上所述的芳香剂组合物的用途,用于赋予、改变和/或强化选自龙涎香、吲哚和木质的一种或多种香调,优选地用于修饰、调和和/或改善一种或多种另外的芳香剂的天然的嗅觉印象和/或用于赋予、改变和/或增强龙涎香类和/或木质和/或吲哚类的嗅觉香调。
本发明的另一个方面涉及一种方法,所述方法用于赋予、改变和/或强化选自龙涎香、吲哚和木质的一种或多种香调,优选地用于修饰、调和和/或改善一种或多种另外的芳香剂的天然的嗅觉印象和/或用于赋予、改变和/或增强龙涎香类和/或木质和/或吲哚类的嗅觉前调,所述方法包括以下步骤或由其组成:
(a)提供
(a.1)式(I)的一种或多种化合物
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选式(Ia)和/或(Ib)和/或(Ic)的化合物中的一种或多种,
和
(a.2)一种、两种、三种、四种、五种、六种、七种、八种、九种、十种或更多种另外的芳香剂,
(b)将式(I)的化合物(a.1)以感官有效量添加给所述一种或多种另外的芳香剂(a.2),优选以如下量添加,所述量足以赋予、强化和/或改变选自龙涎香、吲哚和木质的一种或多种香调,优选以如下量添加,所述量足以修饰、调和和/或改善所述一种或多种另外的芳香剂的天然的嗅觉印象和/或足以赋予、增强和/或改变龙涎香类和/或木质和/或吲哚类的嗅觉前调。
本发明的另一个方面涉及加香制品,其包含以下或由以下组成:
(i)根据本发明的芳香剂组合物(如本文中所述)
或
式(I)的一种或多种化合物
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选式(Ia)和/或(Ib)和/或(Ic)的化合物中的一种或多种,
和任选地一种或多种溶剂,优选如上所述,和/或一种或多种另外的芳香剂。
(ii)一种或多种另外的组分,优选至少一种或多种,优选一种、两种、三种、四种、五种或更多种添加剂、助剂和/或活性物质。
在根据本发明的加香制品中使用根据本发明待应用的式(I)的化合物在此由于其与其他化合物的反应性低是特别有利的,,使得既不会不利地改变根据本发明待应用的式(I)化合物也不会不利地改变根据本发明的加香制品的内含物。另外,根据本发明待应用的式(I)的化合物在对于实现所期望的香味效果所必需的浓度中不会不利地影响根据本发明的加香制品的物理或物理化学特性(例如其黏度或pH值)。
优选的是根据本发明的加香制品,其中所述制品选自:化妆品;洗涤剂和清洁剂;织物柔软剂;漂白剂;消毒剂;香味释放系统;皮肤防晒霜;头发护理产品;除臭剂;酸性、碱性和中性清洁剂,优选地板清洁剂、窗户玻璃清洁剂、餐具洗涤剂、浴室和卫生清洁剂、擦拭乳(scouring milk)、固体和液体WC清洁剂、粉末和泡沫地毯清洁剂、液体洗涤剂、粉末洗涤剂;洗衣预处理剂、漂白剂、浸泡剂、去污剂;织物柔软剂;洗涤皂;洗涤片;消毒剂;表面消毒剂、呈液体、凝胶样或施加在固态的载体上形式的包括使厕所清香的空气清新剂;气溶胶喷雾剂;蜡、抛光剂优选家具抛光剂、地板蜡、鞋油、身体护理产品优选固体肥皂和液体肥皂、沐浴露、洗发水、剃须皂、剃须泡沫、沐浴油;水包油、油包水和水包油包水型的化妆品乳液优选护肤霜和乳液、面霜和乳液、防晒霜和乳液、晒后霜和乳液、护手霜和乳液、足霜和乳液、脱毛霜和乳液、须后、须后霜和乳液、须前、晒黑霜和乳液;头发护理产品优选头发喷雾剂、发胶、头发乳液、护发素、永久和半永久性染发剂;头发变形剂例如冷波和直发剂、生发水、发霜和乳液;清新纸巾、除臭剂、止汗剂优选腋下喷雾剂、滚涂剂、除臭棒和除臭霜;以及装饰性化妆品优选彩妆化妆品。
包含在根据本发明的加香制品中的一种或多种另外的组分(ii),优选包含在其中的添加剂、助剂和/或活性物质,优选是防腐剂;研磨剂、抗痤疮剂;抗老化剂;抗菌剂、消脂剂、去头皮屑剂;抗炎剂、防刺激剂、抑制刺激剂;抗微生物剂;抗氧化剂;收敛剂、止汗剂、防腐剂、抗静电剂、黏合剂、缓冲剂、载体材料;螯合剂;细胞刺激剂、清洁剂、护理剂、脱毛剂、表面活性剂、除臭剂、止汗剂;柔软剂、乳化剂;酶、精油;纤维、成膜剂、固定剂、发泡剂、泡沫稳定剂、防泡剂、泡沫促进剂、杀真菌剂、凝胶剂、凝胶形成剂;头发护理剂、头发变形剂、头发拉直剂、保湿剂、润湿物质、水分保持物质;漂白剂、强化剂、去污剂、光学增白剂、浸渍剂、防污剂、减摩剂、润滑剂、保湿霜、软膏、遮光剂、增塑剂、遮瑕剂、抛光剂、增亮剂、聚合物;粉末、蛋白质;再脂化剂、磨料、有机硅、皮肤舒缓剂、皮肤清洁剂、皮肤护理剂、皮肤修复剂;皮肤提亮剂;皮肤保护剂、皮肤柔软剂、清凉剂、皮肤清凉剂;温热剂、皮肤温热剂;稳定剂、UV吸收剂、UV过滤剂;洗涤剂、织物柔软剂、混悬剂、皮肤美黑剂;增稠剂、维生素;油、蜡、脂肪;磷脂;饱和脂肪酸、一元或多元不饱和脂肪酸、α-羟基酸、多羟基脂肪酸;液化剂、染料、颜色保护剂、颜料;抗腐蚀剂、香料、矫味剂、芳香剂、多元醇;表面活性剂;电解质、有机溶剂;或有机硅衍生物。优选地,根据本发明待应用的式(I)的化合物与这些物质具有高的相容性。
除了在溶液或乳液中用作为液体之外,根据本发明待应用的式(I)的化合物或根据本发明的芳香剂组合物可被吸附在固体上或以(微)胶囊的方式在载体物质中使用。这些剂型能够不仅保证式(I)的化合物或芳香剂组合物在产品中的精细分布而且保证在使用期间可控释放。这样的固体能够优选是多孔的无机材料,例如轻质硫酸盐、硅胶、沸石、石膏、黏土、黏土颗粒、加气混凝土等;或有机材料,例如木材、基于纤维素的物质、糖或塑料,例如PVC、聚乙酸乙烯酯或聚氨酯。
胶囊产品例如能够喷雾干燥,作为包合物或作为挤出产品存在。根据本发明待应用的式(I)的化合物或根据本发明的芳香剂组合物的微囊化例如能够通过借助于胶囊材料,例如由类聚氨酯物质或软明胶制成的胶囊材料的所谓的凝聚方法来实现。
根据本发明待应用的式(I)的喷雾干燥的化合物或根据本发明的芳香剂组合物例如能够通过喷雾干燥包含以下的乳液或分散体来制备:根据本发明待应用的式(I)的化合物或根据本发明的芳香剂组合物,其中能够使用改性淀粉、蛋白质、糊精和植物胶作为载体。
包合物例如能够通过将根据本发明待应用的式(I)的化合物或根据本发明的芳香剂组合物的分散体和环糊精或脲衍生物并入合适的溶剂例如水中来制备。
挤出产品能够通过将根据本发明待应用的式(I)的化合物或根据本发明的芳香剂组合物与合适的蜡质物质融合并通过挤出与接下来如果需要的话在合适的溶剂,例如异丙醇中的固化来获得。
吸附物以及胶囊产品能够通过用适合的材料进行所谓的“涂布”来进一步优化关于更有针对性的释放香味,为此优选可使用蜡类塑料例如聚乙烯醇。
还优选的是根据本发明的加香制品,其中组分(i)以感官有效量包含在内,优选以如下量包含在内,所述量足以使消费者感知一种或多种选自龙涎香、吲哚和木质的香调。
更优选的是根据本发明的加香的制品,其中按制品的总重量计,式(I)的化合物的总量的份额在0.0001重量%至5重量%的范围中,更优选在0.001重量%至2重量%的范围中,特别优选在0.001重量%至1重量%的范围中。
根据另一方面,本发明涉及一种用于给制品加香的方法,所述方法包括以下步骤或由其组成:
(a)提供
(a.1)根据本发明的芳香剂组合物(如本文中所述),
或
(a.2)式(I)的一种或多种化合物
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选地,式(Ia)和/或(Ib)和/或(Ic)的化合物中的一种或多种,
和任选地一种或多种溶剂,优选地如上所述的一种或多种溶剂,和/或一种或多种其他芳香剂,
(b)将芳香剂组合物(a.1)或式(I)的化合物/溶剂(如果存在的话)/其他芳香剂(如果存在的话)(a.2)以感官有效量添加给待加香的物品,优选以如下量添加,所述量足以赋予、强化和/或改变选自龙涎香、吲哚和木质调的一种或多种香调,优选以如下量添加,所述量足以修饰、调和和/或改善一种或多种其他芳香剂(如果存在的话)的天然的嗅觉印象和/或赋予、强化和/或改变龙涎香类和/或木质的和/或吲哚类的嗅觉前调。
在上文中结合根据本发明的用途或根据本发明的芳香剂组合物或根据本发明的制品所陈述的内容再次适用于该方法的一些优选的设计方案。
在下文中,根据所选的实施例更详细地解释本发明。除非另有说明,否则所有数据均指重量。
如下所述,根据本发明待应用的式(I)的化合物例如能够如下获得:从4-叔丁基环己酮开始,通过格氏反应,并且如果需要的话,随后进行醚化。
具体实施方式
实施例1:4-叔丁基-1-甲基-环己醇的合成(格氏反应)
将200ml的甲基氯化镁溶液(在THF中为3M)和100ml的THF在氮气气氛下置于具有磁力搅拌器的搅拌机中。随后,在20℃至25℃下在1小时至2小时内滴入83.2g(0.54mol)溶于200ml的THF中的4-叔丁基环己酮中。将混合物在室温下再搅拌2至3小时。将沉积物倒入0℃至5℃的冷饱和氯化铵溶液中,然后用MTBE振摇萃取,并且将有机相用苏打溶液洗涤并且然后用NaCl溶液洗涤。在蒸发之后,获得84.6g的粗产物。
原料在小柱中蒸馏。
产率:77.8g(理论值的84.7%)
实施例2:4-叔丁基-1-甲基-环己醇甲基醚的合成(醚化)
在具有磁力搅拌器的搅拌机中,在20℃时,将由42.5g的(0.25mol)4-叔丁基-1-甲基-环己醇在100ml的无水THF中构成的溶液在氮气气氛下滴入给在无水THF中的0.3mol的60%氢化钠。然后在室温下再搅拌5小时。随后,在室温下在30分钟内滴入在100ml无水THF中的42.6g(0.3mol)的甲基碘。然后将其在室温下再搅拌2小时。将反应混合物在冷却下小心地与250ml的冰冷的水混合,并且在分离水相之后,分别用50ml饱和盐溶液中性地再洗涤两次。在蒸出溶剂之后,将剩余物在小柱中蒸馏。
产率:28.8g(理论值的62.8%)
在制备根据本发明待应用的其他的式(I)的化合物时,能够使用相同的助剂、设备和参数。
根据本发明的芳香剂组合物的一些实例:
香油1(左:对比,右:根据本发明的)
随着添加(Ia)或(b)或(Ic)的化合物,香油(右栏)闻起来更加和谐、更有花香和更天然,并且具有更强烈的龙涎香调。
香油2(左:对比,右:根据本发明的)
随着添加(Ia)或(Ib)或(Ic)的化合物,香油(右栏)除了具有更强烈的龙涎香调以外,还具有更强的花香散发性,并且表现地更加圆润和和谐。
Claims (13)
2.根据权利要求1所述的用途,其中式(I)的一种、多种或所有的化合物选自式(Ia)的化合物、式(Ib)的化合物和式(Ic)的化合物
3.根据权利要求1或2所述的用途,所述用途用于赋予、改变和/或强化选自龙涎香、吲哚和木质调的一种或多种香调,优选用于修饰、调和和/或改善一种或多种另外的芳香剂的天然的嗅觉印象和/或用于赋予、改变和/或增强龙涎香类和/或木质和/或吲哚类的嗅觉前调。
4.一种芳香剂组合物,其包含以下或由以下组成:式(I)的一种或多种化合物
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选地包含式(Ia)的和/或(Ib)的和/或(Ic)的化合物中的一种或多种或者由其组成,
和
一种或多种溶剂,其中优选地,一种、多种或所有溶剂选自乙醇、异丙醇、二乙二醇单乙醚、甘油、丙二醇、1,2-丁二醇、二丙二醇、邻苯二甲酸二乙酯、柠檬酸三乙酯和肉豆蔻酸异丙酯,
和/或
一种或多种另外的芳香剂,
其中优选地,芳香剂混合物中的式(I)的化合物的总质量与所述芳香剂混合物中如果存在的话一种或多种另外的芳香剂的总质量的比例为1:999至999:1,优选1:99至1:1,尤其优选1:99至1:2,更优选1:90至1:5,并且尤其优选1:80至1:10。
5.根据权利要求4所述的芳香剂组合物,其中按所述芳香剂组合物的总重量计,所述芳香剂组合物中式(I)的化合物的总量的份额为0.1重量%至50重量%,更优选0.5重量%至15重量%,更优选0.75重量%至2重量%。
7.根据权利要求4至6中任一项所述的芳香剂组合物的用途,其用于赋予、改变和/或强化选自龙涎香、吲哚和木质调的一种或多种香调,优选用于修饰、调和和/或改善一种或多种另外的芳香剂的天然的嗅觉印象和/或用于赋予、改变和/或强化龙涎香类和/或木质和/或吲哚类的嗅觉前调。
8.一种用于赋予、改变和/或强化选自龙涎香、吲哚和木质调的一种或多种香调的方法,所述方法优选用于修饰、调和和/或改善一种或多种另外的芳香剂的天然的嗅觉印象和/或用于赋予、改变和/或强化龙涎香类和/或木质和/或吲哚类的嗅觉前调,所述方法包括以下步骤或由以下步骤组成:
(a)提供
(a.1)式(I)的一种或多种化合物
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选式(Ia)和/或(Ib)和/或(Ic)化合物中的一种或更多种,
和
(a.2)一种、两种、三种、四种、五种、六种、七种、八种、九种、十种或更多种另外的芳香剂,
(b)将式(I)的化合物(a.1)以感官有效量添加给一种或多种所述另外的芳香剂(a.2),优选以如下量添加,所述量足以赋予、强化和/或改变选自龙涎香、吲哚和木质调的一种或多种香调,优选以如下量添加,所述量足以修饰、调和和/或改善所述一种或多种另外的芳香剂的天然的嗅觉印象和/或足以赋予、强化和/或改变龙涎香类和/或木质和/或吲哚类的嗅觉前调。
10.根据权利要求9所述的加香制品,其中所述加香制品选自化妆品;洗涤剂和清洁剂;织物软化剂;漂白剂;消毒剂;香味释放系统;皮肤防晒霜;头发护理产品;除臭剂;酸性、碱性和中性清洁剂,优选地板清洁剂、窗户玻璃清洁剂、餐具洗涤剂、浴室和卫生清洁剂、擦拭乳、固体和液体WC清洁剂、粉末和泡沫地毯清洁剂、液体洗涤剂、粉末洗涤剂;洗衣预处理剂、漂白剂、浸泡剂、去污剂;织物软化剂;洗涤皂;洗涤片;消毒剂;表面消毒剂,呈液体、凝胶样或施加在固态的载体上形式的包括使厕所清香的空气清新剂;气溶胶喷雾剂;蜡、抛光剂优选家具抛光剂、地板蜡、鞋油和身体护理产品优选固体肥皂和液体肥皂、沐浴露、洗发水、剃须皂、剃须泡沫、沐浴油;水包油、油包水和水包油包水型的化妆品乳液优选护肤霜和乳液、面霜和乳液、防晒霜和乳液、晒后霜和乳液、护手霜和乳液、足霜和乳液、脱毛霜和乳液、须后、须后霜和乳液、须前、晒黑霜和乳液;头发护理产品优选头发喷雾剂、发胶、头发乳液、护发素、永久和半永久性染发剂;头发变形剂如冷波和直发剂、生发水、发霜和乳液;清新纸巾、除臭剂、止汗剂优选腋下喷雾剂、滚涂剂、除臭棒和除臭霜;以及装饰性化妆品优选彩妆化妆品。
11.根据权利要求9或10所述的加香制品,其中组分(i)以感官有效量包含在内,优选以如下量包含在内,所述量足以使消费者感知到选自龙涎香、吲哚和木质调的一种或多种香调。
12.根据权利要求9至11中任一项所述的加香制品,其中按所述制品的总重量计,式(I)的化合物的总量的份额在0.0001重量%至5重量%的范围中,更优选在0.001重量%至2重量%的范围中,特别优选在0.001重量%至1重量%的范围中。
13.一种用于对制品进行加香的方法,其包括以下步骤或由以下步骤组成:
(a)提供
(a.1)根据权利要求4至6中任一项所述的芳香剂组合物,或者
(a.2)式(I)的一种或多种化合物
其中R是甲基或乙基,并且R1是H、甲基或乙基,
优选式(Ia)的和/或(Ib)的和/或(Ic)的化合物中的一种或多种,
和任选地一种或多种溶剂,优选如在权利要求4中所限定的,和/或一种或多种另外的芳香剂,
(b)将芳香剂组合物(a.1)或式(I)的化合物/溶剂(如果存在的话)/另外的芳香剂(如果存在的话)(a.2)以感官有效量添加给待经加香制品,优选以如下量添加,所述量足以赋予、强化和/或改变选自龙涎香、吲哚和木质调的一种或多种香调,优选以如下量添加,所述量足以修饰、调和和/或改善所述一种或多种另外的芳香剂(如果存在的话)的天然的嗅觉印象,和/或足以赋予、强化和/或改变龙涎香类和/或木质和/或吲哚类的嗅觉前调。
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