CN110786340A - Method for preparing water-soluble liquid turpentine sulfur and using method thereof - Google Patents

Method for preparing water-soluble liquid turpentine sulfur and using method thereof Download PDF

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Publication number
CN110786340A
CN110786340A CN201911116629.1A CN201911116629A CN110786340A CN 110786340 A CN110786340 A CN 110786340A CN 201911116629 A CN201911116629 A CN 201911116629A CN 110786340 A CN110786340 A CN 110786340A
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China
Prior art keywords
sulfur
rosin
water
component
turpentine
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CN201911116629.1A
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Chinese (zh)
Inventor
张圣寅
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Hanyouli Biotechnology Shanghai Co Ltd
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Hanyouli Biotechnology Shanghai Co Ltd
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Priority to CN201911116629.1A priority Critical patent/CN110786340A/en
Publication of CN110786340A publication Critical patent/CN110786340A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/06—Coniferophyta [gymnosperms], e.g. cypress
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Mycology (AREA)
  • Biotechnology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to the technical field of turpentine sulfur preparation, and discloses a preparation method and a use method of water-soluble liquid turpentine sulfur, wherein the water-soluble liquid turpentine sulfur is composed of a turpentine batter A component and an additive B component according to a proportion, wherein the turpentine batter A component is 25-50% of turpentine powder and 10-20% of ethanol in a specific ratio; the specific mixture ratio of the component B of the additive is 30-50% of water, 3-10% of potassium hydroxide and 1-5% of sulfur. In addition, liquefaction with rosin has the effects of preventing natural pests and reducing the amount of pesticides used, and the technology treats liquid rosin stabilized by heating by treating solid rosin with ethanol to form a dough-like liquid and mixing a mixture of water, potassium hydroxide and sulfur.

Description

Method for preparing water-soluble liquid turpentine sulfur and using method thereof
Technical Field
The invention relates to the technical field of turpentine sulfur preparation, in particular to a method for preparing water-soluble liquid turpentine sulfur and a using method thereof.
Background
Chemical pesticides with high control values are commonly used for pest control of crops. However, control with pesticides can cause side effects such as damage to livestock and damage to non-target organisms, residual toxicity and ecosystem disturbances.
Therefore, there is an urgent need to develop environmentally friendly control agents, and thus, environmentally friendly products such as nimum oil, pyrethrin, gosames, oregano, peppermint oil, and the like. Although various attempts have been made to develop environmentally friendly control agents using mainly raw materials, the raw materials have a disadvantage in that they are still expensive due to high production costs.
The invention relates to a sterilization and insecticide taking natural substances as main components, in particular to a sterilization and insecticide taking rosin and sulfur as main components, which is used for solving the problem of food and has made a lot of efforts by human beings. Many chemical studies and attempts are being made to improve the productivity per unit area, to supply nutrient salts such as fertilizers, and to control pests.
However, in recent years, agricultural chemicals such as fertilizers, insecticides, and fungicides have been produced and used in large quantities by chemical synthesis, which is a major cause of disruption of the ecological balance and environmental destruction. Chemical fertilizers and pesticides have been used to promote abnormal growth of plants and to temporarily control pests, but in the long run they are becoming more and more resistant to pesticides and pathogens. It causes a problem that must be solved.
In addition, chemical pesticides are destroying the natural food chain and destroying microorganisms beneficial to natural organisms and plants. In addition, the continued use of chemical fertilizers and pesticides raises secondary pollution problems with soil and water. In order to solve the above problems, many studies on microbial pesticides have been recently conducted.
However, microbial pesticides have not been widely used, and a great deal of research on natural pesticides is required. Anthracnose is a disease that occurs in crops such as apples, grapes, peppers and watermelons, in plants in warm and humid areas. These fungi produce spores in conidia. This disease causes the appearance of multicolored spots on the leaves, stems, fruits and flowers of the plant, which grow and shrink tissues, causing the plant to wilt and die.
To prevent anthracnose, ticks and insects are removed to remove the affected area, fungicides are sprayed or anthracnose is spread between plants. Incidentally, pepper anthracnose starts to flower when it starts to bloom in the middle 6 th month, and the fungus causing the anthracnose rapidly grows in a humid environment, so that it is necessary to spray a pesticide after rain. Typically, pepper growers spray an average of 15 or more fungicides between 6 and 8 months to control anthracnose. However, anthrax causing fungi are increasingly resistant to fungicides and are readily spread throughout the field from areas where no pesticide is applied. The frequent spraying of toxic pesticide can also aggravate the pesticide poisoning phenomenon in farmers, and the prevention and treatment effect of reducing plant diseases and insect pests and the phenomenon of pesticide mixing are achieved.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the preparation method and the application method of the water-soluble liquid turpentine sulfur, which have the advantages of reducing the prevention and treatment effect of plant diseases and insect pests, the phenomenon of pesticide mixing and the like, and solve the problem that the pesticide poisoning phenomenon in farmers is aggravated by frequently spraying toxic pesticide.
(II) technical scheme
In order to achieve the purpose of reducing the prevention and control effect of plant diseases and insect pests and the phenomenon of mixing pesticides, the invention provides the following technical scheme: the water-soluble liquid turpentine sulfur is composed of a turpentine batter A component and an additive B component according to a proportion, wherein the turpentine batter A component comprises 25-50% of turpentine powder and 10-20% of ethanol in a specific ratio; wherein the component B of the additive comprises 30-50% of water, 3-10% of potassium hydroxide and 1-5% of sulfur.
The preparation method of the water-soluble liquid turpentine sulfur comprises the following specific steps:
the specific preparation steps of the component A are as follows:
a) putting solid rosin into a stirrer to be stirred and crushed to prepare rosin powder;
b) putting the rosin powder and the ethanol in a corresponding proportion into a stirrer, fully mixing, and stirring until rosin paste A is formed;
the specific preparation steps of the component B are as follows:
a) adding water, potassium hydroxide and sulfur in corresponding proportion into a stirrer, heating in the stirrer, keeping the temperature at 80-100 ℃, and continuously stirring for 1-2h to fully reflect and mix the raw materials to finally obtain an additive B;
mixing the rosin paste A component and the additive B according to a corresponding proportion, stirring, keeping the temperature of the raw materials in the stirrer at 80-100 ℃, continuously stirring for 2-4h, and then cooling at normal temperature to obtain a liquid rosin sulfur product.
Preferably, the rosin powder is obtained by grinding and stirring solid rosin.
Preferably, the ethanol is high-purity ethanol with the concentration of over 99 percent.
Preferably, when the rosin sulfur is used, the first: mixing liquid rosin sulfur in a ratio of 1: 500 is diluted in water and sprayed to crops, can achieve the effect of preventing plant diseases and insect pests, can be mixed with pesticide, and can improve the effect of pesticide components.
Preferably, the rosin sulfur is used in a second method of mixing liquid rosin sulfur and pesticide component natural penicillin extracted from the pest control office at a ratio of 1:2, and diluting the mixture by 500 times with water to prevent harmful bacteria and pests.
(III) advantageous effects
Compared with the prior art, the invention provides a method for preparing water-soluble liquid rosin sulfur and a using method thereof, and the method has the following beneficial effects:
1. the invention has the advantages that the liquidation of the sulfur improves the absorptivity, is beneficial to the planting of crops, and utilizes the sulfur which is difficult to treat as industrial waste, thereby being beneficial to environmental protection. In addition, the liquefaction by rosin has the functions of preventing natural pests and reducing the using amount of pesticides.
2. The method for preparing sulfur from water-soluble liquid rosin comprises treating solid rosin with ethanol to obtain dough-like liquid, mixing with water, potassium hydroxide, and sulfur to obtain mixture, and treating the liquid rosin stabilized by heating.
3. The natural substance processing technology can apply the antibacterial effect and the strong coating effect of the rosin to crops, and the sulfur is added in the manufacturing process, so that the crops can grow healthily in the breeding period, and the effect of preventing plant diseases and insect pests is achieved.
4. The preparation method and the application method of the water-soluble liquid turpentine sulfur comprise the following steps: mixing liquid rosin sulfur in a ratio of 1: 500 is diluted in water and sprayed to crops to reach the effect of preventing diseases and pests, and the application method of improving the effect of pesticide components by mixing it with pesticide component natural penicillin extracted from the plant, 1:2, and then diluting 500 times with water to prevent and treat harmful bacteria and pests.
Drawings
FIG. 1 is a frame diagram of the manufacturing process of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example one
The water-soluble liquid turpentine sulfur is composed of a turpentine batter A component and an additive B component according to a proportion;
wherein the component A of the rosin paste comprises 25 percent of rosin powder and 20 percent of ethanol;
wherein the component B of the additive comprises 50 parts of water, 3 parts of potassium hydroxide and 5 parts of sulfur.
Example two
The water-soluble liquid turpentine sulfur is composed of a turpentine batter A component and an additive B component according to a proportion;
wherein the component A of the rosin paste comprises 40 percent of rosin powder and 15 percent of ethanol;
wherein the component B of the additive comprises 40% of water, 7% of potassium hydroxide and 2% of sulfur.
EXAMPLE III
The water-soluble liquid turpentine sulfur is composed of a turpentine batter A component and an additive B component according to a proportion;
wherein the component A of the rosin paste comprises 50 percent of rosin powder and 10 percent of ethanol;
wherein the component B of the additive comprises 30 percent of water, 10 percent of potassium hydroxide and 1 percent of sulfur.
Wherein the content of the first and second substances,
the rosin powder is obtained by grinding and stirring solid rosin.
The ethanol is high-purity ethanol with concentration of over 99%.
The preparation method of the water-soluble liquid turpentine sulfur comprises the following specific steps:
the specific preparation steps of the component A are as follows:
a) putting solid rosin into a stirrer to be stirred and crushed to prepare rosin powder;
b) putting the rosin powder and the ethanol in a corresponding proportion into a stirrer, fully mixing, and stirring until rosin paste A is formed;
the specific preparation steps of the component B are as follows:
a) adding water, potassium hydroxide and sulfur in corresponding proportion into a stirrer, heating in the stirrer, keeping the temperature at 80-100 ℃, and continuously stirring for 1-2h to fully reflect and mix the raw materials to finally obtain an additive B;
mixing the rosin paste A component and the additive B according to a corresponding proportion, stirring, keeping the temperature of the raw materials in the stirrer at 80-100 ℃, continuously stirring for 2-4h, and then cooling at normal temperature to obtain a liquid rosin sulfur product.
The use method of the water-soluble liquid turpentine sulfur comprises the following steps: when rosin sulfur is used, the first: mixing liquid rosin sulfur in a ratio of 1: 500 is diluted in water and sprayed to crops to reach the effect of preventing diseases and pests, and the application method of improving the effect of pesticide components by mixing it with pesticide component natural penicillin extracted from the plant, 1:2, and then diluting 500 times with water to prevent and treat harmful bacteria and pests.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (5)

1. The water-soluble liquid rosin sulfur is characterized in that: the water-soluble liquid turpentine sulfur is composed of a turpentine batter A component and an additive B component according to a proportion, wherein the turpentine batter A component is 25-50% of turpentine powder and 10-20% of ethanol in a specific ratio; wherein the component B of the additive comprises 30-50% of water, 3-10% of potassium hydroxide and 1-5% of sulfur.
2. The water-soluble liquid rosin sulfur according to claim 1, wherein: the rosin powder is obtained by grinding and stirring solid rosin.
3. The water-soluble liquid rosin sulfur according to claim 1, wherein: the ethanol is high-purity ethanol with the concentration of over 99 percent.
4. The preparation method of the water-soluble liquid turpentine sulfur comprises the following specific steps:
the specific preparation steps of the component A are as follows:
a) putting solid rosin into a stirrer to be stirred and crushed to prepare rosin powder;
b) putting the rosin powder and the ethanol in a corresponding proportion into a stirrer, fully mixing, and stirring until rosin paste A is formed;
the specific preparation steps of the component B are as follows:
a) adding water, potassium hydroxide and sulfur in corresponding proportion into a stirrer, heating in the stirrer, keeping the temperature at 80-100 ℃, and continuously stirring for 1-2h to fully reflect and mix the raw materials to finally obtain an additive B;
mixing the rosin paste A component and the additive B according to a corresponding proportion, stirring, keeping the temperature of the raw materials in the stirrer at 80-100 ℃, continuously stirring for 2-4h, and then cooling at normal temperature to obtain a liquid rosin sulfur product.
5. The use method of the water-soluble liquid turpentine sulfur is characterized in that: when the rosin sulfur is used, the first is as follows: mixing liquid rosin sulfur in a ratio of 1: 500 is diluted in water and sprayed to crops to reach the effect of preventing diseases and pests, and the application method of improving the effect of pesticide components by mixing it with pesticide component natural penicillin extracted from the plant, 1:2, and then diluting 500 times with water to prevent and treat harmful bacteria and pests.
CN201911116629.1A 2019-11-15 2019-11-15 Method for preparing water-soluble liquid turpentine sulfur and using method thereof Pending CN110786340A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103120190A (en) * 2011-11-18 2013-05-29 大连得达科技发展有限公司 Plant pesticide for controlling crop pesticides and pests and preparation method thereof
CN103766403A (en) * 2012-10-23 2014-05-07 大连鹤菲英博科技有限公司 Method for preparing rosin mixture
CN105850999A (en) * 2016-05-06 2016-08-17 广西师范大学 Preparation method and application of rosin-source pesticide synergist
CN107258833A (en) * 2017-07-13 2017-10-20 曲翠平 A kind of preparation method of rosin mixture biological pesticide

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103120190A (en) * 2011-11-18 2013-05-29 大连得达科技发展有限公司 Plant pesticide for controlling crop pesticides and pests and preparation method thereof
CN103766403A (en) * 2012-10-23 2014-05-07 大连鹤菲英博科技有限公司 Method for preparing rosin mixture
CN105850999A (en) * 2016-05-06 2016-08-17 广西师范大学 Preparation method and application of rosin-source pesticide synergist
CN107258833A (en) * 2017-07-13 2017-10-20 曲翠平 A kind of preparation method of rosin mixture biological pesticide

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
四川省农业科学研究所植物保护系: "含硫松脂合剂的介绍", 《昆虫知识》 *

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Application publication date: 20200214