CN110743194A - Double-tunnel type countercurrent ultrasonic-homogenization combined extraction system - Google Patents
Double-tunnel type countercurrent ultrasonic-homogenization combined extraction system Download PDFInfo
- Publication number
- CN110743194A CN110743194A CN201911067284.5A CN201911067284A CN110743194A CN 110743194 A CN110743194 A CN 110743194A CN 201911067284 A CN201911067284 A CN 201911067284A CN 110743194 A CN110743194 A CN 110743194A
- Authority
- CN
- China
- Prior art keywords
- extraction
- tunnel type
- countercurrent ultrasonic
- extraction system
- ultrasonic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
- B01J19/10—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing sonic or ultrasonic vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D2011/002—Counter-current extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Organic Chemistry (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a double-tunnel type countercurrent ultrasonic-homogenization combined extraction system. Consists of two parts, 1) a primary tunnel type countercurrent ultrasonic extraction system. Comprises a solvent storage tank (1), a raw material box (2), a screw transmission device (3 a), a tunnel type countercurrent ultrasonic extraction device (4 a), a horizontal centrifuge (9) and an extraction liquid storage tank (11) which are connected in sequence; 2) a secondary tunnel type countercurrent ultrasonic-homogeneous combined extraction system. The primary extraction residue tank (5), the screw transmission device (3 b), the stirring tank (6), the homogenizer (7), the screw pump (8), the tunnel type countercurrent ultrasonic extraction equipment (4 b), the horizontal centrifuge (9), the secondary residue storage tank (10) and the extraction liquid storage tank (11) are connected in sequence. The extraction temperature of the extraction system is room temperature, the extraction system is suitable for extracting heat-sensitive components, and the extraction rate is greatly improved through ultrasonic secondary countercurrent extraction.
Description
Technical Field
The invention belongs to the field of natural product active ingredient extraction, and particularly relates to a double-tunnel type countercurrent ultrasonic-homogenization combined extraction system.
Background
In northeast China, the method has wide regions and complex topography, is a green treasury of wild plant resources in China, and breeds abundant wild small berry resources with various varieties. The small berries such as vitis amurensis, vaccinium uliginosum, actinidia kolomikta, sea buckthorn, lonicera edulis, black currant and the like are bright in color, unique in flavor and high in nutritional value; the health-care food also has medicinal efficacy, contains rich polyphenol and flavonoid compounds, has good effects of reducing blood sugar, reducing blood pressure, resisting oxidation, preventing radiation, inhibiting bacteria and diminishing inflammation and the like, can also prevent and assist in treating cardiovascular and cerebrovascular diseases, and is an ideal natural health-care nutritional food raw material; in addition, some flavone components are widely used in the field of cosmetics for moisturizing, whitening, anti-wrinkle, delaying aging and the like. In order to ensure the application value, the method is very important for obtaining functional active ingredients.
At present, the extraction method of functional active ingredients in small berries mainly comprises the following steps: steam extraction technology, supercritical carbon dioxide extraction technology, ultrasonic-assisted extraction technology, microwave-assisted extraction technology, enzymolysis-assisted extraction technology and the like. Most of the extraction technologies have the problems of low extraction rate, high consumption of extraction solvent, high extraction temperature (unsuitable for extraction of heat-sensitive components), complex extraction process, long extraction time, high cost and the like.
Disclosure of Invention
In order to solve the problems, the invention provides a double-tunnel type countercurrent ultrasonic-homogenization combined extraction system. In the extraction process, the active ingredients are extracted by utilizing the ultrasonic cavitation, and the homogenization-ultrasonic combination technology is adopted for secondary extraction, so that the extraction effect is obviously improved. The whole system is carried out at normal temperature, is suitable for extracting thermosensitive components, is carried out continuously, and greatly saves time and production cost.
The double-tunnel type countercurrent ultrasonic-homogenization combined extraction system consists of two parts: a primary tunnel type countercurrent ultrasonic extraction system and a secondary tunnel type countercurrent ultrasonic-homogenization combined extraction system. Wherein:
the primary tunnel type countercurrent ultrasonic extraction system mainly comprises a solvent storage tank, a raw material tank, a screw transmission device, tunnel type countercurrent ultrasonic extraction equipment, a horizontal centrifuge and an extraction liquid storage tank. The material enters the tunnel type countercurrent ultrasonic extraction equipment through the screw transmission device, and the extract liquid centrifugally enters the extract liquid storage tank.
The secondary tunnel type countercurrent ultrasonic-homogenizing combined extraction system mainly comprises a primary extraction residue box, a screw transmission device, a stirring tank, a homogenizer, a screw pump, tunnel type countercurrent ultrasonic extraction equipment, a horizontal centrifuge, a secondary residue storage box and an extraction liquid storage tank. The primary extraction slag enters a stirring tank through a screw transmission device, after homogenization, the primary extraction slag is conveyed through a screw pump for secondary extraction, and the extraction liquid centrifugally enters an extraction liquid storage tank.
The invention has the following advantages:
1. the active ingredients are fully released by adopting an ultrasonic-homogenizing-ultrasonic extraction mode, and the extraction rate is increased from 70% to 96%.
2. The whole system operates at normal temperature and is suitable for extracting heat-sensitive components.
3. And the extraction continuity is realized by using double-tunnel extraction.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a dual-tunnel countercurrent ultrasonic-homogeneous extraction system.
Detailed Description
The technical solution of the present invention is further described below with reference to the accompanying drawings, but not limited thereto, and any modification or equivalent replacement of the technical solution of the present invention without departing from the spirit and scope of the technical solution of the present invention shall be covered by the protection scope of the present invention.
The first embodiment is as follows: the embodiment is described with reference to fig. 1, and the dual-tunnel type countercurrent ultrasonic-homogeneous extraction system of the embodiment is composed of two parts: a primary tunnel type countercurrent ultrasonic extraction system and a secondary tunnel type countercurrent ultrasonic-homogenization combined extraction system. Wherein:
the primary tunnel type countercurrent ultrasonic extraction system mainly comprises a solvent storage tank (1), a raw material tank (2), a screw transmission device (3 a), tunnel type countercurrent ultrasonic extraction equipment (4 a), a horizontal centrifuge (9) and an extraction liquid storage tank (11). The primary extraction system is started by opening the valve (12 a) and the valve (12 b). The material enters a tunnel type countercurrent ultrasonic extraction device through a screw transmission device, and the centrifuged extraction liquid enters an extraction liquid storage tank.
The secondary tunnel type countercurrent ultrasonic-homogenizing combined extraction system mainly comprises a primary extraction residue box (5), a screw transmission device (3 b), a stirring tank (6), a homogenizer (7), a screw pump (8), tunnel type countercurrent ultrasonic extraction equipment (4 b), a horizontal centrifuge (9), a secondary residue storage box (10) and an extraction liquid storage tank (11). The primary extraction slag enters a stirring tank through a screw transmission device, a valve (12 c) is opened, a solvent is injected and uniformly stirred, then the primary extraction slag is uniformly sheared at a high speed through a homogenizer and then is conveyed to tunnel type countercurrent ultrasonic extraction equipment through a screw pump for secondary extraction, and the extraction liquid enters an extraction liquid storage tank in a centrifugal mode.
Claims (6)
1. A double-tunnel type countercurrent ultrasonic-homogenization combined extraction system is characterized by comprising two parts: primary tunnel type countercurrent ultrasonic extraction system and secondary tunnel type countercurrent ultrasonic-homogeneous combined extraction system, wherein:
the primary tunnel type countercurrent ultrasonic extraction system is mainly formed by sequentially connecting a solvent storage tank (1), a raw material tank (2), a spiral transmission device (3 a), tunnel type countercurrent ultrasonic extraction equipment (4 a), a horizontal centrifuge (9) and an extract storage tank (11), wherein materials enter the tunnel type countercurrent ultrasonic extraction equipment through the spiral transmission device, and extract is centrifuged and enters the extract storage tank;
the secondary tunnel type countercurrent ultrasonic-homogeneous combined extraction system is mainly formed by sequentially connecting a primary extraction residue box (5), a screw transmission device (3 b), a stirring tank (6), a homogenizer (7), a screw pump (8), tunnel type countercurrent ultrasonic extraction equipment (4 b), a horizontal centrifuge (9), a secondary residue storage box (10) and an extract storage tank (11), wherein primary extraction residues enter the stirring tank through the screw transmission device, secondary extraction is transmitted through the screw pump after homogenization, and extract centrifugally enters the extract storage tank.
2. The dual-tunnel type countercurrent ultrasonic-homogenization combined extraction system as claimed in claim 1, which is characterized in that the dual-tunnel type countercurrent ultrasonic extraction is adopted to realize secondary extraction and improve extraction rate.
3. The dual-tunnel countercurrent ultrasonic-homogeneous combined extraction system of claim 1, wherein the extraction agent is fully contacted with the material by using a tunnel countercurrent ultrasonic countercurrent extraction device.
4. The dual-tunnel countercurrent ultrasonic-homogenization combined extraction system of claim 1, wherein a homogenizer is used, the material is sheared at high speed, and the extractant and the material are mixed uniformly.
5. The dual-tunnel countercurrent ultrasonic-homogeneous combined extraction system according to claim 1, wherein the system is suitable for extracting active ingredients of small berries with high water content and abundant polyphenol and flavone compounds.
6. The dual-tunnel countercurrent ultrasonic-homogenization extraction system of claim 1, which is operated at normal temperature and is suitable for extraction of heat-sensitive components.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911067284.5A CN110743194A (en) | 2019-11-04 | 2019-11-04 | Double-tunnel type countercurrent ultrasonic-homogenization combined extraction system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911067284.5A CN110743194A (en) | 2019-11-04 | 2019-11-04 | Double-tunnel type countercurrent ultrasonic-homogenization combined extraction system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110743194A true CN110743194A (en) | 2020-02-04 |
Family
ID=69282037
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201911067284.5A Pending CN110743194A (en) | 2019-11-04 | 2019-11-04 | Double-tunnel type countercurrent ultrasonic-homogenization combined extraction system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110743194A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1579592A (en) * | 2003-08-17 | 2005-02-16 | 王锡康 | New-type technological equipment and method for plant extraction |
| CN202570152U (en) * | 2012-06-06 | 2012-12-05 | 万绍平 | Tunnel type microwave plant cell wall breaking device |
| CN103830932A (en) * | 2012-11-28 | 2014-06-04 | 东北林业大学 | Tunnel type ultrasonic triple-effect reflux extraction system |
| CN204865072U (en) * | 2015-08-14 | 2015-12-16 | 象山医疗精密仪器有限公司 | Pipeline spinning formula ultrasonic wave extracts unit |
| CN107469380A (en) * | 2017-07-28 | 2017-12-15 | 哈尔滨工业大学 | A kind of tunnel type ultrasonic wave-screw extrusion cycling extraction equipment |
| US20190153013A1 (en) * | 2017-11-22 | 2019-05-23 | Tci Co., Ltd | Method for extracting active ingredients |
-
2019
- 2019-11-04 CN CN201911067284.5A patent/CN110743194A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1579592A (en) * | 2003-08-17 | 2005-02-16 | 王锡康 | New-type technological equipment and method for plant extraction |
| CN202570152U (en) * | 2012-06-06 | 2012-12-05 | 万绍平 | Tunnel type microwave plant cell wall breaking device |
| CN103830932A (en) * | 2012-11-28 | 2014-06-04 | 东北林业大学 | Tunnel type ultrasonic triple-effect reflux extraction system |
| CN204865072U (en) * | 2015-08-14 | 2015-12-16 | 象山医疗精密仪器有限公司 | Pipeline spinning formula ultrasonic wave extracts unit |
| CN107469380A (en) * | 2017-07-28 | 2017-12-15 | 哈尔滨工业大学 | A kind of tunnel type ultrasonic wave-screw extrusion cycling extraction equipment |
| US20190153013A1 (en) * | 2017-11-22 | 2019-05-23 | Tci Co., Ltd | Method for extracting active ingredients |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101194713B (en) | Method for processing edible camellia oil | |
| CN104351869A (en) | Aronia melenocarpa composite juice beverage and preparation method thereof | |
| CN103431256B (en) | A kind of black bean jam and preparation method thereof | |
| CN103463123A (en) | Method for extracting effective constituents from maca | |
| CN108541847A (en) | A kind of raw squeezing drinks and preparation method of enrichment anthocyanidin | |
| CN104432339A (en) | Method for preparing dragon fruit and lychee drink | |
| CN103653151A (en) | Production method for tomato juice beverage prepared with enzymatic method | |
| CN105558506A (en) | Marinating material for stewed duck with bean sauce | |
| CN106726910A (en) | A kind of green papaya shin moisturizer | |
| CN105231376A (en) | Processing method of trichosanthes kirilowi and fructu broussonetiae fruit butter | |
| CN104921217A (en) | Lycium ruthenicum fruit, haw and lemon compound beverage preparation method | |
| CN104489114A (en) | Grape seed polyphenol soya-bean milk and preparation method thereof | |
| CN104886330A (en) | Soft candy prepared from okra scraps as well as preparation method of soft candy | |
| JP2008156287A (en) | Collagen production promoter | |
| CN104447897B (en) | A kind of method that persimmon tannin is extracted from persimmon | |
| CN106343295A (en) | Raspberry drink with slimming and beautifying functions and preparation method thereof | |
| CN109054992A (en) | A method of extracting Seabuckthorm Seed Oil | |
| CN109430605A (en) | A kind of sea-buckthorn mulberries Chinese wolfberry fruit drink and preparation method thereof | |
| CN110743194A (en) | Double-tunnel type countercurrent ultrasonic-homogenization combined extraction system | |
| CN101703539A (en) | Method for extracting okra by using supercritical carbon dioxide | |
| CN101096627B (en) | Loquat flower wine and method for making same | |
| CN106666633A (en) | Fruit-flavor additive and preparation method thereof | |
| CN104489821A (en) | Preparation method of litchi and dragon fruit beverage | |
| KR20050122190A (en) | The manufacturing method for gochujang with onion | |
| CN103611333A (en) | Method for supercritical extraction of super natural factors of propolis by using CO2 fluid in combination with solid-state enzymolysis |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200204 |
|
| RJ01 | Rejection of invention patent application after publication |