CN110731392A - method for preparing Chinese prickly ash oil - Google Patents

method for preparing Chinese prickly ash oil Download PDF

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Publication number
CN110731392A
CN110731392A CN201911043075.7A CN201911043075A CN110731392A CN 110731392 A CN110731392 A CN 110731392A CN 201911043075 A CN201911043075 A CN 201911043075A CN 110731392 A CN110731392 A CN 110731392A
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China
Prior art keywords
zanthoxylum
oil
mixture
pepper
powder
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CN201911043075.7A
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Chinese (zh)
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樊轩
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Individual
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Individual
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D9/00Other edible oils or fats, e.g. shortenings, cooking oils
    • A23D9/02Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
    • A23D9/04Working-up
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/10Production of fats or fatty oils from raw materials by extracting
    • C11B1/108Production of fats or fatty oils from raw materials by extracting after-treatment, e.g. of miscellae
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/008Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Fats And Perfumes (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a preparation method of zanthoxylum oil, which comprises the following steps of drying collected fresh zanthoxylum, removing zanthoxylum seeds, leaving dry zanthoxylum shells for standby, crushing the zanthoxylum shells, pouring vegetable oil into a pot, heating, boiling zanthoxylum powder, cooling, standing for layering, separating supernatant liquid from precipitate for standby, mixing the supernatant liquid, the precipitate, the zanthoxylum powder and sesame oil, squeezing the mixture in a squeezer to obtain a mixture, filtering the mixture, adding the mixture into a centrifugal oil filter, rotating the mixture for precipitation, and obtaining the obtained zanthoxylum oil, wherein the preparation method of the zanthoxylum oil has the advantages of forcing out the fragrance of zanthoxylum through boiling, enabling the zanthoxylum oil to be more fragrant, removing the zanthoxylum seeds harmful to human bodies through drying, ensuring smooth performance in the pressing process through adding the sesame oil, simultaneously increasing the nutrition and the taste of the zanthoxylum oil, and improving the utilization rate of the zanthoxylum oil through setting the squeezing temperature and centrifugal separation, and having good practical value.

Description

method for preparing Chinese prickly ash oil
Technical Field
The invention belongs to the technical field of edible oil squeezing, and particularly relates to a preparation method of zanthoxylum oil.
Background
The fructus Zanthoxyli is Rutaceae, Laxylum deciduous tree, and has height of 7 m; short thorns exist on the branches of the thorns on the stems, and the branches growing in the current year are short and soft; the blade shaft is often provided with very narrow blade wings; the lobules are opposite, oval, elliptical and thin in needle shape, the leaf margin has fine fissures, and the tooth gaps have oil spots. The leaf back is soft hair, and the leaf back is dry and has reddish brown stripes; the inflorescence grows from the top of the lateral branch or grows from the top of the lateral branch, the perianth sheet is yellow green, and the shape and the size are approximately the same; the flower pillar is bent back obliquely; purple red fruit, scattered micro-convex oil spots, 4-5 months of flowering period, 8-9 months or 10 months of fruit period.
The pricklyash peel can be used as a traditional Chinese medicine and has the effects of warming the middle-jiao and promoting the circulation of qi, expelling cold, relieving pain, killing insects and the like; it is used to treat stomach and abdominal psychroalgia, emesis, diarrhea, schistosomiasis, ascariasis, etc. Also used as an epidermal anesthetic. The medical treatise is also recorded in the book "medical treatise on property of medicine": treating aversion to wind, obstinate arthralgia of the whole body and limbs, mouth and teeth edema and shaking; it is mainly used for treating postpartum dysuria and dysentery with blood, and has the effects of promoting hair growth and treating abdominal psychroalgia. It is indicated for wind-cold syndrome of head-wind with tearing, lumbar and foot paralysis, deficiency and retention of blood, edema of lower urinary system, cold and pain in abdomen, and toothache.
Modern people pay more attention to health, and the food therapy method is more favored, pepper is used as traditional Chinese medicines, the taste is slightly rough in the eating process, and the pepper can be used as pepper oil to be added into daily diet for treatment in step .
Disclosure of Invention
The invention aims to provide a preparation method of zanthoxylum oil, which solves the problems of low oil yield and serious waste in the existing zanthoxylum oil preparation method.
The technical scheme adopted by the invention is that the preparation method of zanthoxylum oil comprises the following steps:
step 1, pepper pretreatment
Drying the collected fresh pepper, removing pepper seeds, removing impurities by using a blower fan, and leaving a dried pepper shell for later use;
step 2, pulverizing
Putting the pericarpium zanthoxyli of the step 1 into a crusher to be crushed, and collecting pericarpium zanthoxyli powder;
step 3, decocting
Pouring vegetable oil into a pot, heating, decocting the pepper powder obtained in the step 2, cooling, standing for layering, and separating supernatant and precipitate for later use;
step 4, mixing the supernatant liquid and the precipitate in the step 3, the pepper powder and the sesame oil in the step 2, and putting the mixture into a squeezer for squeezing to obtain a mixture;
step 5, centrifugal filtration
And (4) filtering the mixture obtained in the step (4), adding the mixture into a centrifugal oil filter, and carrying out rotary precipitation to obtain clear liquid, namely the obtained zanthoxylum oil.
The present invention is also characterized in that,
2. the method for preparing zanthoxylum oil according to claim 1, wherein the drying parameters in step 1 are 70-80 ℃ and 4-6 h.
The mesh number of the pepper powder in the step 2 is 40-60 meshes.
In the step 3, the mass ratio of the vegetable oil to the pepper powder is 5:1, and the decocting parameters are as follows: the oil temperature is 100-.
In the step 4, the parameters of the pressing are as follows: squeezing temperature is 60-80 deg.C, and squeezing time is 20-30 min.
The centrifugal filtration parameters in step 5 are as follows: the rotation speed is 1000-.
In the step 4, the proportion of the pepper powder to the sesame oil is 1: 2.
the preparation method of zanthoxylum oil has the advantages that the fragrance of zanthoxylum is forced out by boiling, so that the zanthoxylum oil is more aromatic, zanthoxylum seeds harmful to human bodies are removed by drying, the pressing process can be carried out smoothly by adding sesame oil, the nutrition and the blending taste of the zanthoxylum oil are increased, the utilization rate of the zanthoxylum oil is improved by setting the pressing temperature and centrifugal separation, and the preparation method has good practical value.
Detailed Description
The present invention will be described in detail below with reference to specific embodiments.
The invention relates to a preparation method of zanthoxylum oil, which comprises the following steps:
step 1, pepper pretreatment
Drying the collected fresh pepper, removing pepper seeds and other impurities (rhizomes, leaves and the like), and then removing the impurities by using a blower fan, and leaving a dried pepper shell for later use;
the drying parameters are as follows: the drying temperature is 70-80 ℃, and the drying time is 4-6 h.
Step 2, pulverizing
Putting the pericarpium zanthoxyli of the step 1 into a crusher to be crushed, and collecting pericarpium zanthoxyli powder;
the mesh number of the pricklyash peel powder is 40-60 meshes.
Step 3, decocting
Pouring vegetable oil into a pot, heating, decocting the pepper powder obtained in the step 2, cooling, standing for layering, and separating supernatant and precipitate for later use;
the mass ratio of the vegetable oil to the pepper powder is 5:1, and the decocting parameters are as follows: the oil temperature is 100-.
Step 4, mixing the supernatant liquid and the precipitate in the step 3, the pepper powder and the sesame oil in the step 2, and putting the mixture into a squeezer for squeezing to obtain a mixture;
the proportion of the pepper powder to the sesame oil is 1: 2.
the squeezing parameters are as follows: squeezing temperature is 60-80 deg.C, and squeezing time is 20-30 min.
Step 5, centrifugal filtration
Filtering the mixture obtained in the step (4), adding the mixture into a centrifugal oil filter, and carrying out rotary precipitation to obtain clear liquid, namely the obtained zanthoxylum oil;
the centrifugal filtration parameters were: the rotation speed is 1000-.
Example 1
Step 1, drying collected fresh pepper, removing pepper seeds and other impurities, and then removing the impurities through a blower fan, and leaving dried pepper shells for later use; the drying parameters are as follows: the drying temperature is 70 ℃, and the drying time is 6 h.
And 2, putting the pericarpium zanthoxyli of the step 1 into a crusher to be crushed, and collecting pericarpium zanthoxyli powder with 40-60 meshes.
Step 3, pouring vegetable oil into a pot, heating, decocting the pepper powder obtained in the step 2, cooling, standing for layering, and separating supernatant and precipitate for later use; the mass ratio of the vegetable oil to the pepper powder is 5:1, and the decocting parameters are as follows: the oil temperature is 100 deg.C, and the decocting time is 30 min.
Step 4, mixing the supernatant liquid and the precipitate in the step 3, the pepper powder and the sesame oil in the step 2, and putting the mixture into a squeezer for squeezing to obtain a mixture; the proportion of the pepper powder to the sesame oil is 1: 2; the squeezing parameters are as follows: squeezing temperature is 80 deg.C, and squeezing time is 20 min.
Step 5, filtering the mixture obtained in the step 4, adding the mixture into a centrifugal oil filter, and carrying out rotary precipitation to obtain clear liquid, namely the obtained zanthoxylum oil; the centrifugal filtration parameters were: the rotation speed is 1000 rad/min.
Example 2
Step 1, drying collected fresh pepper, removing pepper seeds and other impurities, and then removing the impurities through a blower fan, and leaving dried pepper shells for later use; the drying parameters are as follows: the drying temperature is 80 ℃, and the drying time is 4 h.
And 2, putting the pericarpium zanthoxyli of the step 1 into a crusher to be crushed, and collecting pericarpium zanthoxyli powder with 40-60 meshes.
Step 3, pouring vegetable oil into a pot, heating, decocting the pepper powder obtained in the step 2, cooling, standing for layering, and separating supernatant and precipitate for later use; the mass ratio of the vegetable oil to the pepper powder is 5:1, and the decocting parameters are as follows: the oil temperature is 120 deg.C, and the decocting time is 20 min.
Step 4, mixing the supernatant liquid and the precipitate in the step 3, the pepper powder and the sesame oil in the step 2, and putting the mixture into a squeezer for squeezing to obtain a mixture; the proportion of the pepper powder to the sesame oil is 1: 2; the squeezing parameters are as follows: squeezing temperature is 80 deg.C, and squeezing time is 20 min.
Step 5, filtering the mixture obtained in the step 4, adding the mixture into a centrifugal oil filter, and carrying out rotary precipitation to obtain clear liquid, namely the obtained zanthoxylum oil; the centrifugal filtration parameters were: the rotation speed is 1500 rad/min.
Example 3
Step 1, drying collected fresh pepper, removing pepper seeds and other impurities, and then removing the impurities through a blower fan, and leaving dried pepper shells for later use; the drying parameters are as follows: the drying temperature is 75 ℃, and the drying time is 5 h.
And 2, putting the pericarpium zanthoxyli of the step 1 into a crusher to be crushed, and collecting pericarpium zanthoxyli powder with 40-60 meshes.
Step 3, pouring vegetable oil into a pot, heating, decocting the pepper powder obtained in the step 2, cooling, standing for layering, and separating supernatant and precipitate for later use; the mass ratio of the vegetable oil to the pepper powder is 5:1, and the decocting parameters are as follows: the oil temperature is 110 deg.C, and the decocting time is 25 min.
Step 4, mixing the supernatant liquid and the precipitate in the step 3, the pepper powder and the sesame oil in the step 2, and putting the mixture into a squeezer for squeezing to obtain a mixture; the proportion of the pepper powder to the sesame oil is 1: 2; the squeezing parameters are as follows: squeezing temperature is 70 deg.C, and squeezing time is 25 min.
Step 5, filtering the mixture obtained in the step 4, adding the mixture into a centrifugal oil filter, and carrying out rotary precipitation to obtain clear liquid, namely the obtained zanthoxylum oil; the centrifugal filtration parameters were: the rotation speed is 1300 rad/min.
The zanthoxylum oil prepared by the embodiments 1-3 has pure taste, and the test shows that the utilization rate of the zanthoxylum is improved by 20-25%.

Claims (7)

1, kinds of pepper oil preparation method, characterized by, including the following steps:
step 1, pepper pretreatment
Drying the collected fresh pepper, removing pepper seeds, removing impurities by using a blower fan, and leaving a dried pepper shell for later use;
step 2, pulverizing
Putting the pericarpium zanthoxyli of the step 1 into a crusher to be crushed, and collecting pericarpium zanthoxyli powder;
step 3, decocting
Pouring vegetable oil into a pot, heating, decocting the pepper powder obtained in the step 2, cooling, standing for layering, and separating supernatant and precipitate for later use;
step 4, mixing the supernatant liquid and the precipitate in the step 3, the pepper powder and the sesame oil in the step 2, and putting the mixture into a squeezer for squeezing to obtain a mixture;
step 5, centrifugal filtration
And (4) filtering the mixture obtained in the step (4), adding the mixture into a centrifugal oil filter, and carrying out rotary precipitation to obtain clear liquid, namely the obtained zanthoxylum oil.
2. The method for preparing zanthoxylum oil according to claim 1, wherein the drying parameters in step 1 are 70-80 ℃ and 4-6 h.
3. The method for preparing zanthoxylum oil according to claim 1, wherein the mesh number of the zanthoxylum powder in step 2 is 40-60 mesh.
4. The preparation method of zanthoxylum oil as claimed in claim 1, wherein the mass ratio of the vegetable oil to the zanthoxylum powder in step 3 is 5:1, and the parameters of the decoction are oil temperature of 100 ℃ and temperature of 120 ℃ and the decoction time of 20-30 min.
5. The method for preparing zanthoxylum oil according to claim 1, wherein the squeezing parameters in step 4 are 60-80 ℃ and 20-30 min.
6. The method for preparing zanthoxylum oil as claimed in claim 1, wherein the centrifugal filtration parameter in step 5 is 1000-1500 rad/min.
7. The method for preparing zanthoxylum oil according to claim 1, wherein the ratio of the zanthoxylum powder to the sesame oil in step 4 is 1: 2.
CN201911043075.7A 2019-10-30 2019-10-30 method for preparing Chinese prickly ash oil Pending CN110731392A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101653173A (en) * 2009-09-01 2010-02-24 河北锦秀果业有限公司 Bunge pricklyash seed edible oil and production method thereof
CN103549035A (en) * 2013-10-23 2014-02-05 贵州省关岭自治县板贵花椒食品香料有限公司 Processing technology for zanthoxylum oil
CN103749742A (en) * 2013-12-31 2014-04-30 安顺市西秀区百岁陈德文牌食品加工厂 Production method of zanthoxylum oil
KR20160097396A (en) * 2015-02-06 2016-08-18 경상남도 Purification and Conservation extension method of Zanthoxylum schinifolium oil
CN109548892A (en) * 2018-11-15 2019-04-02 习水县绵盛农业发展有限公司 A kind of Chinese prickly ash oil making technology

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101653173A (en) * 2009-09-01 2010-02-24 河北锦秀果业有限公司 Bunge pricklyash seed edible oil and production method thereof
CN103549035A (en) * 2013-10-23 2014-02-05 贵州省关岭自治县板贵花椒食品香料有限公司 Processing technology for zanthoxylum oil
CN103749742A (en) * 2013-12-31 2014-04-30 安顺市西秀区百岁陈德文牌食品加工厂 Production method of zanthoxylum oil
KR20160097396A (en) * 2015-02-06 2016-08-18 경상남도 Purification and Conservation extension method of Zanthoxylum schinifolium oil
CN109548892A (en) * 2018-11-15 2019-04-02 习水县绵盛农业发展有限公司 A kind of Chinese prickly ash oil making technology

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
赵宝峰等: "《调味品(下) 608例》", 科学技术文献出版社, pages: 158 - 159 *

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