CN110693737B - High-pearly-luster isolating and brightening emulsion and preparation method thereof - Google Patents
High-pearly-luster isolating and brightening emulsion and preparation method thereof Download PDFInfo
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- CN110693737B CN110693737B CN201911065941.2A CN201911065941A CN110693737B CN 110693737 B CN110693737 B CN 110693737B CN 201911065941 A CN201911065941 A CN 201911065941A CN 110693737 B CN110693737 B CN 110693737B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/75—Anti-irritant
Abstract
The invention belongs to the field of cosmetics, and particularly relates to high-pearly isolating brightening emulsion and a preparation method thereof. The active component, polyhydric alcohol, humectant, emulsifier, emollient oil and modified bismuth oxychloride dispersion slurry. The modified bismuth oxychloride dispersion slurry treated by the treating agent is added into the isolation brightening emulsion, and the plant extract is added as an active ingredient, so that the prepared isolation brightening emulsion has better stability, improves skin feel and reduces irritation. The preparation method of the emulsion is simple and easy to implement and easy to popularize and apply.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to high-pearly isolating brightening emulsion and a preparation method thereof.
Background
Along with the environmental pollution and the destruction of the atmospheric ozone layer, the quantity of ultraviolet rays emitted to the ground surface is greatly increased. Long-term scientific research proves that ultraviolet rays can change the structure or function of single cell components, and the radiation of a large amount of ultraviolet rays to cells can cause the cells to lose the communication power with surrounding cells or to be apoptotic together. Ultraviolet rays in sunlight are one of the main causes of human skin aging, and direct irradiation of the ultraviolet rays on the skin can cause a series of skin problems such as skin spots, burns, dermatitis, even skin cancer and the like.
Nowadays, sun protection is a great trend of the development of cosmetics, in the process of developing sun protection products, certain natural plant components with sun protection and ultraviolet resistance functions have the advantages of mild performance, high efficiency and the like, and people pay attention to the sun protection cream mainly for protecting skin and relieving irritation of adverse factors to the skin. The sun screen also has the function of isolating ultraviolet rays. Uv screening is not a unique function of a sunscreen, and sunscreens used in sunscreens are the same as those used in sunscreens.
As a core raw material of an isolation cosmetic, the isolation sunscreen active ingredients are various, such as a physical ultraviolet screening agent, a chemical ultraviolet absorbent, a living active substance for resisting ultraviolet radiation, and a compound use of various sunscreen active ingredients, but most of the active ingredients are absorbed very little, and some active ingredients have the defects of poor stability, low permeability, certain irritation and the like.
The isolation sunscreen cosmetics in the prior art have the condition that the water resistance durability and the skin feeling cannot be compatible. In addition to pursuing the highest level of protection for female consumers, sun block texture remains the most important decision consideration. Many people dislike the use of sunscreen products, but the reason for this is that they feel thick and heavy, and in addition, the weather is hot in summer, and then the sunscreen product is applied to the skin, which causes sticky feeling. Some sunscreen products have a refreshing feel on the skin, are poorly water resistant, and are hot in summer, and the applied sunscreen texture on the skin is easily washed away by sweat, and has to be applied periodically at intervals. The current commercial isolation brightening products, such as emulsion or BB cream, are basically rich in powder, white after use, thick and heavy in skin feel, and make up.
Chinese patent application CN109199954A is a sunscreen lotion and its preparation method, wherein the sunscreen lotion comprises the following components in parts by weight: 0.2-3 parts of neopentyl glycol diheptanoate, 1-5 parts of caprylic propyl heptyl ester, 0.1-5 parts of cetearyl alcohol, 3-10 parts of organic sunscreen agent, 1-2.5 parts of emulsifier, 0.5-10 parts of titanium dioxide, 0.1-5 parts of polymethylsilsesquioxane, 35-65 parts of water, 1-15 parts of butanediol, 1-15 parts of glycerol, 0.1-3 parts of p-hydroxyacetophenone, 01-0.5 part of potassium cetyl phosphate, 0.1-1 part of triethanolamine, 0.1-5 parts of thickening agent, 0.1-1 part of preservative, 0.1-10 parts of humectant and 0.1-10 parts of skin conditioning agent; the sunscreen emulsion component has a certain anti-isolation effect, but the stability of the sunscreen emulsion component is still to be examined, and the glossiness, the irritation to the skin and the like of the sunscreen emulsion component after being used need to be further improved.
Disclosure of Invention
In order to overcome the technical problems, the invention provides the high-pearly-luster isolating and brightening emulsion which is simple in preparation method, and the prepared emulsion has better glossiness, better stability and better anti-allergic effect, and further reduces the damage to the skin.
In order to achieve the above purpose, the technical scheme provided by the invention is as follows:
a high pearly luster isolated brightening emulsion comprises the following components: active ingredients, polyhydric alcohol, a humectant, an emulsifier, emollient oil and modified bismuth oxychloride dispersion slurry;
the modified bismuth oxychloride dispersion slurry modification treatment method comprises the following steps: dissolving the treating agent in ethanol, adding bismuth oxychloride powder, stirring, and uniformly dispersing to obtain bismuth oxychloride dispersion slurry;
preferably, the treating agent used for the modified bismuth oxychloride is a homopolymer or a copolymer of styrene, acrylic acid (ester) and ammonium methacrylate;
preferably, the high-pearly isolating brightening emulsion comprises the following components in parts by weight: 8-10 parts of active ingredients, 8-15 parts of polyhydric alcohol, 1-5 parts of humectant, 3-5 parts of emulsifier, 0.1-15 parts of emollient oil and 3-5 parts of modified bismuth oxychloride dispersion slurry;
preferably, the active ingredients include: one or more of herba Dendrobii extract, stigma croci Sativi extract, yeast lysate extract, flos Matricariae Chamomillae extract, Malva sylvestris extract, radix Paeoniae extract, flos Lonicerae extract, herba Taraxaci rhizome/root extract, herba Violae extract and Aloe Barbadensis leaf juice;
preferably, the raw materials of the active ingredients comprise: one or more of herba Dendrobii, stigma croci, yeast lysate, flos Matricariae Chamomillae, flos Malloti Apeltae, radix Paeoniae, flos Lonicerae, rhizome/root of Taraxacum officinale, herba Violae, and Aloe Barbadensis leaf;
preferably, the active ingredients are mixed extracts of dendrobium officinale, peony roots and honeysuckle flowers;
preferably, the mass ratio of the dendrobium officinale to the peony root to the honeysuckle flower in the raw materials of the mixed extract of the dendrobium officinale and the peony root to the honeysuckle flower is 1-6: 2-3: 4-5;
preferably, the preparation method of the mixed extract of dendrobium officinale, the peony root and the honeysuckle flower comprises the following preparation processes,
s1: pulverizing herba Dendrobii, radix Paeoniae and flos Lonicerae, adding into water, performing enzymolysis, filtering, and concentrating to obtain filtrate concentrate;
s2: adding ethanol into the concentrated solution, reflux-extracting, and drying to obtain mixed extract of herba Dendrobii, radix Paeoniae and flos Lonicerae.
Preferably, the enzyme for enzymolysis in step S1 is a mixture of cellulase and aldolase;
preferably, the mass ratio of the cellulase to the aldehyde enzyme is 1-5: 1;
preferably, the enzyme for enzymolysis is 0.5-2% of the total mass of the crushed dendrobium officinale, the crushed peony root and the crushed honeysuckle;
preferably, the concentration in step S1 is carried out until the solid content of the concentrated solution is 30-50%;
preferably, the ethanol is added in the step S2 in an amount of 4-6 times the volume of the concentrated solution;
preferably, the reflux extraction time is 2-3 h.
Preferably, the polyhydric alcohol is any one or more of propylene glycol, 1, 3 propylene glycol, butylene glycol, dipropylene glycol, sorbitol, polyglycerol-10 and polyglycerol-6;
preferably, the polyol is propylene glycol or 1, 3 propylene glycol or a mixture of both;
preferably, the humectants are: any one or more of polyglutamic acid, hyaluronic acid, trehalose, lodestone and sodium PCA;
preferably, the humectant is a mixture of hyaluronic acid, polyglutamic acid, sodium PCA and lodestone;
preferably, the mass ratio of the hyaluronic acid to the polyglutamic acid to the sodium PCA to the lodestone is 1-2: 1:1: 1-3;
preferably, the emulsifier has an HLB value of 3 to 5;
preferably, the emulsifier is any one or more of PEG-30 dipolyhydroxystearate, cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG-9 dimethiconoethyl polydimethylsiloxane, PEG-10 polydimethylsiloxane and PEG-9 dimethiconoethyl polydimethylsiloxane;
preferably, the emulsifier is a mixture of PEG-10 polydimethylsiloxane and PEG-9 polydimethylsiloxane ethyl polydimethylsiloxane;
preferably, the weight ratio of the PEG-10 polydimethylsiloxane to the PEG-9 polydimethylsiloxane is 1-2: 1-5, preferably 2: 5;
preferably, the emollient oil is one or more of polydimethylsiloxane, cyclomethicone, cyclopentadimethicone, dimethicone, cyclohexadimethicone, alkyl dimethicone and phenyl dimethicone;
preferably, the emollient oil may also be one or more of C12-15 alcohol benzoate, myristyl myristate, trimethylolpropane triisostearate, pentaerythritol tetraisostearate, caprylic/capric triglyceride, C13-16 isoparaffin, hydrogenated polydecene, ethylhexyl palmitate, butylene glycol dicaprylate/dicaprate, coco-caprylate/caprate, propylene glycol dicaprylate/dicaprate, cetyl ethyl hexanoate, neopentyl glycol dicaprylate/dicaprate, isononyl isononanoate and isopropyl palmitate;
preferably, the emollient grease is a mixture of phenyl polydimethylsiloxane and cyclomethicone;
preferably, the mass ratio of the phenyl polydimethylsiloxane to the cyclic polydimethylsiloxane is 1-4: 1;
preferably, the emollient oil is cyclopenta dimethyl siloxane, a mixture of cyclohexa dimethyl siloxane and dimethyl siloxane;
preferably, the weight ratio of the cyclopentadimethylsiloxane, the cyclohexadimethylsiloxane and the polydimethylsiloxane is 1: 1-2: 1;
preferably, the emollient oil is any one or more of cyclopentadimethylsiloxane, coco-caprylate/caprate, cetyl ethylhexanoate and C13-16 isoparaffin.
Another object of the present invention is to provide a method for preparing a high pearlescent isolating brightening emulsion:
(1) dissolving emulsifier in water, stirring, and heating to 70-90 deg.C to obtain emulsifier solution;
(2) taking a water phase pot, sequentially adding the polyhydric alcohol and the humectant into the water phase pot, stirring and heating;
(3) adding the emulsifier solution into a water phase pot, and adding the emulsifier solution while stirring;
(4) cooling to 40-50 deg.C, adding active ingredients and emollient oil, and homogenizing;
(5) cooling, and adding the modified bismuth oxychloride dispersion slurry and auxiliary materials to obtain the high-pearly-luster isolating and brightening emulsion.
Preferably, in the step (1), the heating temperature is 85 ℃;
preferably, in the step (2), the heating temperature is 80-90 ℃, preferably 85-90 ℃;
preferably, in the step (4), the temperature is reduced to 45 ℃;
preferably, in the step (5), the temperature of the reduced temperature is 30-35 ℃.
Preferably, in the step (5), the auxiliary materials comprise essence and preservative.
Compared with the prior art, the invention has the technical advantages that:
(1) the special treated dispersion slurry of bismuth oxychloride is used in the invention, so that the appearance, brightness and waterproof effects of the product are improved;
(2) the active ingredients in the application are preferably mixed extracts of dendrobium officinale, the peony roots and the honeysuckle flowers, and the three have good synergistic effect, so that the brightening effect and the waterproof effect of the high-pearly-luster isolating brightening emulsion can be promoted;
(3) the extraction method of the active ingredients in the application can better extract the active ingredients of the active ingredients, and the active ingredients can play better effects of moisturizing, protecting skin, brightening and the like under the condition of limited raw materials;
(4) the prepared emulsion is prepared by adding the oil phase into the water phase, so that the arrangement of the bismuth oxychloride is more uniform and the stability is better;
(5) the plant extract is added as an active ingredient, so that the moisturizing and anti-allergy effects of the emulsion can be improved, the prepared emulsion has good skin feel while being isolated and brightened, and the irritation of the emulsion to the skin is reduced.
Detailed Description
Example 1
In this embodiment, the modification treatment method of the modified bismuth oxychloride dispersed slurry comprises: dissolving the treating agent in ethanol, adding bismuth oxychloride powder, stirring, and uniformly dispersing to obtain bismuth oxychloride dispersion slurry;
the modified bismuth oxychloride treating agent is a homopolymer of styrene;
in this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 1 composition of components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and honeysuckle flower comprises the following preparation processes,
s1: pulverizing Dendrobium officinale, radix paeoniae alba and honeysuckle flower, adding into water, and mixing according to a mass ratio of 5: 1, performing enzymolysis with cellulase and aldehydic acid enzyme (enzyme for enzymolysis is 0.5% of the total mass of pulverized herba Dendrobii, radix Paeoniae and flos Lonicerae), filtering, and concentrating to obtain concentrated filtrate with solid content of 50%;
s2: adding ethanol 6 times the volume of the concentrated solution into the concentrated solution, reflux-extracting for 3h, and drying to obtain mixed extract of herba Dendrobii, radix Paeoniae and flos Lonicerae.
The preparation method of the high-pearly isolating brightening emulsion provided by the embodiment comprises the following steps:
(1) dissolving an emulsifier in water, stirring, and heating to 85 ℃ to obtain an emulsifier solution;
(2) taking a water phase pot, sequentially adding the polyhydric alcohol and the humectant into the water phase pot, stirring, and heating at 85 ℃;
(3) adding the emulsifier solution into a water phase pot, and adding the emulsifier solution while stirring;
(4) cooling to 45 deg.C, adding active ingredients and skin caring oil, and homogenizing;
(5) cooling to 35 ℃, and adding the modified bismuth oxychloride dispersion slurry and the auxiliary materials to obtain the high-pearly-luster isolating and brightening emulsion.
Example 2
In this embodiment, the modification treatment method of the modified bismuth oxychloride dispersed slurry comprises: dissolving the treating agent in ethanol, adding bismuth oxychloride powder, stirring, and uniformly dispersing to obtain bismuth oxychloride dispersion slurry;
the modified bismuth oxychloride treating agent is a copolymer of styrene, acrylic acid (acrylate) and ammonium methacrylate in a mass ratio of 1:1: 1;
in this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 2 composition of components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and honeysuckle flower comprises the following preparation processes,
s1: pulverizing Dendrobium officinale, radix paeoniae alba and honeysuckle flower, adding into water, and mixing according to a mass ratio of 1:1, performing enzymolysis with cellulase and aldehydic acid enzyme (enzyme for enzymolysis is 2% of the total mass of pulverized herba Dendrobii, radix Paeoniae and flos Lonicerae), filtering, and concentrating until the solid content of the concentrated solution is 30% to obtain concentrated solution of filtrate;
s2: adding ethanol with volume 4 times of the concentrated solution into the concentrated solution, reflux-extracting for 2 hr, and drying to obtain mixed extract of herba Dendrobii, radix Paeoniae and flos Lonicerae.
The preparation method of the high-pearly isolating brightening emulsion provided by the embodiment comprises the following steps:
(1) dissolving an emulsifier in water, stirring, and heating to 70 ℃ to obtain an emulsifier solution;
(2) taking a water phase pot, sequentially adding the polyhydric alcohol and the humectant into the water phase pot, stirring, and heating at 90 ℃;
(3) adding the emulsifier solution into a water phase pot, and adding the emulsifier solution while stirring;
(4) cooling to 50 deg.C, adding active ingredients and skin caring oil, and homogenizing;
(5) cooling to 30 ℃, and then adding the modified bismuth oxychloride dispersion slurry and the auxiliary materials to obtain the high-pearly-luster isolating and brightening emulsion.
Example 3
In this embodiment, the modification treatment method of the modified bismuth oxychloride dispersed slurry comprises: dissolving the treating agent in ethanol, adding bismuth oxychloride powder, stirring, and uniformly dispersing to obtain bismuth oxychloride dispersion slurry;
the modified bismuth oxychloride treating agent is a homopolymer of ammonium methacrylate;
in this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 3 composition of the components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and honeysuckle flower comprises the following preparation processes,
s1: pulverizing Dendrobium officinale, radix paeoniae alba and honeysuckle flower, adding into water, and mixing according to a mass ratio of 1:1, performing enzymolysis with cellulase and aldehydic acid enzyme (enzyme for enzymolysis is 1% of the total mass of pulverized herba Dendrobii, radix Paeoniae and flos Lonicerae), filtering, and concentrating until the solid content of the concentrated solution is 40% to obtain concentrated solution of filtrate;
s2: adding ethanol 5 times the volume of the concentrated solution into the concentrated solution, reflux-extracting for 2-3 hr, and drying to obtain mixed extract of herba Dendrobii, radix Paeoniae and flos Lonicerae.
The preparation method of the high-pearly isolating brightening emulsion provided by the embodiment comprises the following steps:
(1) dissolving an emulsifier in water, stirring, and heating to 90 ℃ to obtain an emulsifier solution;
(2) taking a water phase pot, sequentially adding the polyhydric alcohol and the humectant into the water phase pot, stirring, and heating at 85 ℃;
(3) adding the emulsifier solution into a water phase pot, and adding the emulsifier solution while stirring;
(4) cooling to 45 deg.C, adding active ingredients and skin caring oil, and homogenizing;
(5) cooling to 30 ℃, and then adding the modified bismuth oxychloride dispersion slurry and the auxiliary materials to obtain the high-pearly-luster isolating and brightening emulsion.
Example 4
In this example, the modification treatment method of the modified bismuth oxychloride dispersion slurry was the same as in example 1.
In this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 4 composition of components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and chamomile flower comprises the following preparation processes,
s1: taking dendrobium officinale, radix paeoniae alba and chamomile flower, crushing, adding into water, and mixing according to a mass ratio of 1:1, performing enzymolysis with cellulase and aldehyde acid enzyme (enzyme for enzymolysis is 1% of the total mass of pulverized herba Dendrobii, radix Paeoniae and flos Matricariae Chamomillae), filtering, and concentrating until the solid content of the concentrated solution is 40% to obtain concentrated solution of filtrate;
s2: adding ethanol 5 times the volume of the concentrated solution into the concentrated solution, reflux-extracting for 2-3 hr, and drying to obtain mixed extract of herba Dendrobii, radix Paeoniae and flos Matricariae Chamomillae.
The preparation method of the high-pearly isolating brightening emulsion provided by the embodiment comprises the following steps: the same as in example 1.
Example 5
In this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 5 composition of the components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and chamomile flower is the same as that in embodiment 4.
The embodiment provides a preparation method of a high-pearly isolating brightening emulsion, which comprises the following steps: the same as in example 1.
Example 6
In this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 6 composition of components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and chamomile flower is the same as that in embodiment 4.
The embodiment provides a preparation method of a high-pearly isolating brightening emulsion, which comprises the following steps: the same as in example 1.
Example 7
In this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 7 composition of components
In this embodiment, the preparation method of the mixed extract of dendrobium officinale, radix paeoniae alba and chamomile flower is the same as that in embodiment 4.
The embodiment provides a preparation method of a high-pearly isolating brightening emulsion, which comprises the following steps: the same as in example 1.
Example 8
Compared with example 1, the difference is only that the active ingredients adopt the extracts of commercially available dendrobium officinale, peony root and honeysuckle flower;
in this embodiment, the high pearlescent isolating brightening emulsion comprises the following components in parts by weight:
TABLE 8 compositional Components
The preparation method of the high-pearly isolated brightening emulsion provided by the embodiment is the same as that of the embodiment 1.
Comparative example 1
The difference compared to example 1 is only the method of extraction of the active ingredient.
The modification treatment method of the modified bismuth oxychloride dispersion slurry is the same as that of example 1;
in the comparative example, the high-pearly isolating brightening emulsion comprises the components of example 1 in parts by weight;
in the comparative example, the preparation method of the mixed extract of the dendrobium officinale, the peony root and the honeysuckle flower comprises the following preparation processes,
s1: pulverizing herba Dendrobii, radix Paeoniae and flos Lonicerae, adding into water, performing enzymolysis with cellulase (enzyme for enzymolysis is 0.5% of total mass of pulverized herba Dendrobii, radix Paeoniae and flos Lonicerae), filtering, and concentrating to obtain concentrated filtrate with solid content of 50%;
s2: adding ethanol 6 times the volume of the concentrated solution into the concentrated solution, reflux-extracting for 3h, and drying to obtain mixed extract of herba Dendrobii, radix Paeoniae and flos Lonicerae.
The preparation method of the high-pearly isolated brightening emulsion provided by the comparative example is the same as that of example 1.
Comparative example 2
The only difference compared to example 1 is the preparation method.
The modification treatment method of the modified bismuth oxychloride dispersion slurry is the same as that of example 1;
in the comparative example, the high pearly isolated brightening emulsion comprises the same components as example 1 in parts by weight
In the comparative example, the preparation method of the mixed extract of the dendrobium officinale, the peony root and the honeysuckle flower is the same as that of the example 1;
the preparation method of the high-pearly isolating brightening emulsion provided by the comparative example comprises the following steps:
(1) dissolving an emulsifier in water, stirring, and heating to 50 ℃ to obtain an emulsifier solution;
(2) taking a water phase pot, sequentially adding the polyhydric alcohol and the humectant into the water phase pot, and stirring;
(3) adding the emulsifier solution into a water phase pot, and adding the emulsifier solution while stirring;
(4) cooling to 45 deg.C, adding active ingredients and skin caring oil, and homogenizing;
(5) cooling to 35 ℃, and adding the modified bismuth oxychloride dispersion slurry and the auxiliary materials to obtain the high-pearly-luster isolating and brightening emulsion.
Effect example brightening and Water proofing test
The test method comprises the following steps: volunteers were selected, aged between 20-40, and divided into 10 groups, each requiring 5 subjects to complete the test. Screening qualified test subjects, cleaning whole face with facial cleanser, sitting for 20min at constant temperature and humidity, and keeping the whole face exposed and relaxed, wherein water and beverage can not be drunk in the sitting period. Subjects were photographed by Visia-CR by the laboratory. The subject was applied with a sample by the laboratory technician and photographed by Visia-CR. The experimenter uses a hand-held shower nozzle to wash the face of the experimenter for 1min by clean water at the flow rate of 30-40ml/s, and the Visia-CR photographs. The photographs were compared before and after each other by a laboratory specialist, and the Lab value (L by color measurement) of the specified part (cheek) was measuredtThe value represents the brightness of the skin, the larger the value, the brighter the skin. a istRepresenting the degree of reddish greenness, the greater the number, the more red the skin is. btRepresenting blue-yellow, the greater the number, the more yellow the skin is; l is0、a0、b0All refer to data obtained before the emulsion was used) and calculated therefrom
△ E is the comparison of the skin color after washing before rinsing, and the closer the value is to 0, the less makeup is removed, the better the makeup effect is, the effect is shown in Table 9.
TABLE 9 brightening and water-proof effect scoring table
Note that: in the same row, the significant difference P between different son and mother is less than 0.05.
Therefore, the high-pearly luster isolating and brightening emulsion prepared by the invention has better brightening effect and waterproof effect.
The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.
Claims (7)
1. The high-pearly luster isolating and brightening emulsion comprises the following components in parts by weight: 8-10 parts of active ingredients, 8-15 parts of polyhydric alcohol, 1-5 parts of humectant, 3-5 parts of emulsifier, 0.1-15 parts of emollient oil and 3-5 parts of modified bismuth oxychloride dispersion slurry;
the modified bismuth oxychloride dispersion slurry modification treatment method comprises the following steps: dissolving the treating agent in ethanol, adding bismuth oxychloride powder, stirring, and uniformly dispersing to obtain bismuth oxychloride dispersion slurry;
the treating agent used for the modified bismuth oxychloride is a homopolymer of styrene, a copolymer of styrene, acrylic acid (ester) and ammonium methacrylate or a homopolymer of ammonium methacrylate;
the active ingredients comprise: one or more of herba Dendrobii extract, stigma croci Sativi extract, yeast lysate extract, flos Matricariae Chamomillae extract, Malva sylvestris extract, radix Paeoniae extract, flos Lonicerae extract, herba Taraxaci rhizome/root extract, herba Violae extract and Aloe Barbadensis leaf juice.
2. The high pearlescent barrier highlight emulsion of claim 1, wherein the polyol is any one or more of propylene glycol, butylene glycol, dipropylene glycol, sorbitol, polyglycerol-10 and polyglycerol-6.
3. The high pearlescent barrier lightening emulsion of claim 1 wherein the humectant is: any one or more of polyglutamic acid, hyaluronic acid, trehalose, lodestone and sodium PCA.
4. The high pearlescent insulated lightening emulsion of claim 1 wherein the emulsifier is any one or more of PEG-30 dipolyhydroxystearate, cetyl PEG/PPG-10/1 dimethicone, lauryl PEG-9 dimethicoxyethyldimethicone, PEG-10 dimethicone, and PEG-9 dimethicoxyethyldimethicone.
5. The high pearlescent insulated lightening emulsion of claim 1 wherein the emollient grease is any one or more of polydimethylsiloxane, cyclomethicone, alkyl dimethicone and phenyl dimethicone.
6. The high pearlescent barrier lightening emulsion of claim 1 wherein the emollient oil is one or more of C12-15 alcohol benzoate, myristyl myristate, trimethylolpropane triisostearate, pentaerythritol tetraisostearate, caprylic/capric triglyceride, C13-16 isoparaffin, hydrogenated polydecene, ethylhexyl palmitate, butanediol dicaprylate/dicaprate, coco-caprylate/caprate, propylene glycol dicaprylate/dicaprate, cetyl ethylhexanoate, neopentyl glycol dicaprylate/dicaprate, isononyl isononanoate and isopropyl palmitate.
7. A process for the preparation of a highly pearlescent isolated lightening emulsion according to any one of claims 1 to 6: the method is characterized by comprising the following steps:
(1) dissolving emulsifier in water, stirring, and heating to 70-90 deg.C to obtain emulsifier solution;
(2) taking a water phase pot, sequentially adding the polyhydric alcohol and the humectant into the water phase pot, stirring and heating;
(3) adding the emulsifier solution into a water phase pot, and adding the emulsifier solution while stirring;
(4) cooling to 40-50 deg.C, adding active ingredients and emollient oil, and homogenizing;
(5) cooling, and adding the modified bismuth oxychloride dispersion slurry and auxiliary materials to obtain the high-pearly-luster isolating brightening emulsion;
wherein, the auxiliary materials comprise essence and preservative.
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