CN110638667A - Safe and stable single-agent hair dye and preparation method thereof - Google Patents
Safe and stable single-agent hair dye and preparation method thereof Download PDFInfo
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- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q5/10—Preparations for permanently dyeing the hair
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Abstract
The invention belongs to the technical field of hair dyes, and particularly relates to a safe and stable single-agent hair dye. The hair dye comprises 2,4,5, 6-tetraaminopyrimidine sulfate, plant extract, graphene oxide, dimethyl polysiloxane, 1, 3-butanediol, xanthan gum, monoethanolamine, ascorbic acid, polyoxyethylene (20) oleyl alcohol ether and essence, wherein the plant extract comprises tea extract, jasmine extract, mulberry extract and gallnut extract. Compared with the prior art, the hair dye avoids stimulation and allergy symptoms caused by hydrogen peroxide or p-phenylenediamine during the hair dyeing process, and after the hair dye is dyed, the hair can restore the original hair color without changing the original color, so that the hair dye can prove that the hair dye is safe, environment-friendly and healthy in performance and can adapt to and meet the safe selection and use of hair dyes for middle-aged and elderly people.
Description
Technical Field
The invention belongs to the technical field of hair dyes, and particularly relates to a safe and stable single-agent hair dye.
Background
Hair dye is a cosmetic for dyeing hair, and dyeing hair with colors can improve the quality and the image of the hair.
Hair dyes can be currently classified into four types: oxidative permanent hair dyes, ionic hair dyes, temporary hair dyes, and semi-permanent hair dyes. The existing hair dye mainly has the following three problems, on one hand, most of the hair dye generally needs to be split into a plurality of doses in order to show the effect of the hair dye, and the hair dye is mixed for use when in use, so that the inconvenience in use is caused; on the other hand, the hair dye generally contains chemical substances such as hydrogen peroxide or p-phenylenediamine which can cause irritation or allergy to the scalp, and can bring a series of sequelae to the scalp and even the body after long-term use; on the other hand, most people use the hair dye, the pigment fades along with hair washing, the original hair can turn yellow, the original hair quality can not be recovered, more people are inclined to dye white hair into black aiming at middle-aged and old people, and middle-aged and old people pay more attention to the selection and use of the hair dye, so that the hair dye is prevented from hurting hair and scalp.
Disclosure of Invention
In view of the above problems, the present invention aims to provide a safe and stable single-agent hair dye and a preparation method thereof, wherein the color of the single-agent hair dye is biased to be purple, the pigment is mainly derived from plant extracts, and other plant extracts with different colors can be selected for replacement.
The technical content of the invention is as follows:
the invention provides a safe and stable single-agent hair dye, which comprises 2,4,5, 6-tetraaminopyrimidine sulfate (colorant), plant extract, graphene oxide, dimethyl polysiloxane (anti-sweat and deodorant), 1, 3-butanediol (odorless, low-toxicity, good water-solubility, wetting agent, softening agent and flavoring agent), xanthan gum (emulsifier and stabilizer), monoethanolamine (bactericide, emulsifier, preservative and foaming agent), ascorbic acid, polyoxyethylene (20) oleyl ether and essence;
the plant extract comprises tea extract, jasmine extract, mulberry extract and gallnut extract;
the cleaning agent comprises, by mass, 3-4% of 2,4,5, 6-tetraaminopyrimidine sulfate, 9-12% of a plant extract, 3-5% of graphene oxide, 3-4% of dimethylpolysiloxane, 2-4% of 1, 3-butanediol, 3-6% of xanthan gum, 4-7% of monoethanolamine, 2-4% of ascorbic acid, 3-5% of polyoxyethylene (20) oleyl ether, 0.5-2% of essence and the balance of deionized water.
The invention also provides a preparation method of the safe and mild single-agent hair dye, which sequentially comprises the following steps:
1) mixing 2,4,5, 6-tetraaminopyrimidine sulfate, folium Camelliae sinensis extract, Mori fructus extract and polyoxyethylene (20) oleyl alcohol ether, adding DMF and propylene glycol, mixing and dissolving, stirring at constant temperature, heating, and evaporating to remove DMF and propylene glycol to obtain mixture A;
2) mixing and dissolving dimethyl polysiloxane, butanediol and monoethanolamine, adding jasmine extract, gallnut extract and DMF, mixing and dissolving, stirring at constant temperature for emulsification reaction, and heating to evaporate DMF to obtain a mixture B;
3) mixing the mixture A, the mixture B, xanthan gum and ascorbic acid, and stirring at constant temperature for emulsification reaction;
4) and adding water and graphene oxide, mixing and stirring, cooling to room temperature for reaction, and finally dripping essence, mixing and stirring uniformly to obtain the hair dye.
Step 1) the use ratio of DMF and propylene glycol is 1: (1-1.5);
the temperature of the constant-temperature stirring in the steps 1) to 3) is 45-70 ℃.
The invention has the following beneficial effects:
the single-agent hair dye does not contain chemical substances which stimulate the skin, such as hydrogen peroxide, p-phenylenediamine and other metal salt components, and the like, and is prepared mainly by using substances such as plant extraction components, graphene oxide, 2,4,5, 6-tetraaminopyrimidine sulfate and the like, and an emulsifying agent formed by the single-agent hair dye can be directly used on human hair, and has the characteristics of higher dyeing stability, higher uniformity and good film forming property; after the hair is dyed, the hair is smoother and glossier, and the conditions of dry hair, frizziness, unsmooth hair and the like can not occur;
compared with the prior art, the scalp irritation and allergy symptoms caused by hydrogen peroxide or p-phenylenediamine in the hair dyeing process are avoided, after the product is dyed, the original hair color can be recovered after the pigment is completely faded, the original color cannot be changed, the product has the performance which is safe, environment-friendly and healthy, and can be suitable for and meet the safe selection and use of hair dyes by middle-aged and elderly people.
Detailed Description
The present invention is described in further detail in the following detailed description with reference to specific embodiments, which are intended to be illustrative only and not to be limiting of the scope of the invention, as various equivalent modifications of the invention will become apparent to those skilled in the art after reading the present invention and are intended to be included within the scope of the appended claims.
All the raw materials and reagents of the invention are conventional market raw materials and reagents unless otherwise specified.
Example 1
A preparation method of a safe and mild single-agent hair dye sequentially comprises the following steps:
1) mixing 2g, 4g, 5g, 6 g-tetraaminopyrimidine sulfate, 3g tea extract, 2g mulberry extract and 5g polyoxyethylene (20) oleyl ether in an emulsifying pot, adding 10g DMF and 10g propylene glycol, mixing and dissolving, slowly heating to 50 ℃, stirring at constant temperature for 1.5h, then heating to 185-190 ℃, and evaporating to remove DMF and propylene glycol to obtain a mixture A;
2) mixing and dissolving 4g of dimethyl polysiloxane, 2g of butanediol and 7g of monoethanolamine, adding 2g of jasmine extract, 2g of nutgall extract and 25g of DMF, mixing and dissolving in an emulsifying pot, slowly heating to 45 ℃, stirring at a constant temperature for 1.5h, carrying out an emulsification reaction, heating to 185-190 ℃, and evaporating to remove DMF to obtain a mixture B;
3) mixing the mixture A, the mixture B, 3g of xanthan gum and 3g of ascorbic acid, slowly heating to 55 ℃, stirring at constant temperature, and carrying out an emulsion reaction for 1 h;
4) and adding 58g of water and 5g of graphene oxide, mixing and stirring for 0.5h, cooling to room temperature for reaction, and finally dripping 1g of essence, mixing and stirring uniformly for 2h to obtain the hair dye.
Example 2
A preparation method of a safe and mild single-agent hair dye sequentially comprises the following steps:
1) mixing 2g, 4g, 5g, 6 g-tetraaminopyrimidine sulfate, 3g tea extract, 3g mulberry extract and 3g polyoxyethylene (20) oleyl ether in an emulsifying pot, adding 10g of DMF and 12g of propylene glycol for mixing and dissolving, slowly heating to 55 ℃, stirring for 1.5h at constant temperature, then heating to 185-190 ℃, and evaporating to remove DMF and propylene glycol to obtain a mixture A;
2) mixing and dissolving 3g of dimethyl polysiloxane, 4g of butanediol and 4g of monoethanolamine, adding 2g of jasmine extract, 2g of nutgall extract and 25g of DMF, mixing and dissolving in an emulsifying pot, slowly heating to 50 ℃, stirring at constant temperature for 1.5h, carrying out an emulsification reaction, heating to 185-190 ℃, and evaporating to remove DMF to obtain a mixture B;
3) mixing the mixture A, the mixture B, 5g of xanthan gum and 4g of ascorbic acid, slowly heating to 50 ℃, stirring at constant temperature, and carrying out an emulsion reaction for 1 h;
4) and adding 58g of water and 3g of graphene oxide, mixing and stirring for 0.5h, then cooling to room temperature for reaction, and finally dripping 1g of essence, mixing and stirring uniformly for 2h to obtain the hair dye.
Example 3
A preparation method of a safe and mild single-agent hair dye sequentially comprises the following steps:
1) mixing 2g, 4g, 5g, 6-tetraaminopyrimidine sulfate, 4g tea extract, 2g mulberry extract and 4g polyoxyethylene (20) oleyl ether in an emulsifying pot, adding 10g of DMF and 13g of propylene glycol, mixing and dissolving, slowly heating to 55 ℃, stirring at constant temperature for 1.5h, then heating to 185-190 ℃, and evaporating to remove DMF and propylene glycol to obtain a mixture A;
2) mixing and dissolving 3g of dimethyl polysiloxane, 4g of butanediol and 5g of monoethanolamine, adding 3g of jasmine extract, 2g of nutgall extract and 26g of DMF, mixing and dissolving in an emulsifying pot, slowly heating to 50 ℃, stirring at constant temperature for 1.5h, carrying out an emulsification reaction, heating to 185-190 ℃, and evaporating to remove DMF to obtain a mixture B;
3) mixing the mixture A, the mixture B, 6g of xanthan gum and 2g of ascorbic acid, slowly heating to 50 ℃, stirring at constant temperature, and carrying out an emulsion reaction for 1 h;
4) and adding 56g of water and 4g of graphene oxide, mixing and stirring for 0.5h, cooling to room temperature for reaction, and finally dripping 1g of essence, mixing and stirring uniformly for 2h to obtain the hair dye.
Example 4
A preparation method of a safe and mild single-agent hair dye sequentially comprises the following steps:
1) mixing 2g, 4g, 5g, 6-tetraaminopyrimidine sulfate, 3g tea extract, 3g mulberry extract and 4g polyoxyethylene (20) oleyl ether in an emulsifying pot, adding 10g of DMF and 15g of propylene glycol for mixing and dissolving, slowly heating to 55 ℃, stirring for 1.5h at constant temperature, then heating to 185-190 ℃, and evaporating to remove DMF and propylene glycol to obtain a mixture A;
2) mixing and dissolving 3g of dimethyl polysiloxane, 4g of butanediol and 5g of monoethanolamine, adding 3g of jasmine extract, 2g of nutgall extract and 28g of DMF, mixing and dissolving in an emulsifying pot, slowly heating to 50 ℃, stirring at a constant temperature for 1.5h, carrying out an emulsification reaction, heating to 185-190 ℃, and evaporating to remove DMF to obtain a mixture B;
3) mixing the mixture A, the mixture B, 5g of xanthan gum and 4g of ascorbic acid, slowly heating to 50 ℃, stirring at constant temperature, and carrying out an emulsion reaction for 1 h;
4) and adding 56g of water and 4g of graphene oxide, mixing and stirring for 0.5h, cooling to room temperature for reaction, and finally dripping 1g of essence, mixing and stirring uniformly for 2h to obtain the hair dye.
Comparative example 1
A single-agent hair dye containing p-phenylenediamine is prepared by replacing graphene oxide in example 1 with p-phenylenediamine, and keeping the other components unchanged;
comparative example 2
A single-agent hair dye containing hydrogen peroxide and p-phenylenediamine is prepared by replacing 2,4,5, 6-tetraaminopyrimidine sulfate in example 2 with hydrogen peroxide, replacing graphene oxide with p-phenylenediamine, and keeping the rest unchanged;
comparative example 3
A single-agent hair dye adopting a chemical colorant is prepared by replacing all plant extracts in example 3 with colorants, and the colorants are prepared by mixing Chinese gall pigment liquid, tea pigment liquid, sodium carboxymethylcellulose, 1, 3-butanediol, triethanolamine, glycerol, essence, preservative and deionized water, and the rest are unchanged.
Comparative example 4
A single-agent hair dye containing p-phenylenediamine and a chemical colorant is prepared by replacing graphene oxide in example 4 with p-phenylenediamine and replacing all plant extracts with the colorant prepared in comparative example 3, and the rest is not changed.
The essences of the above examples and comparative examples include rose essential oil, jasmine essential oil, and the like.
Test examples
The hair dye products prepared in the examples 1 to 4 and the hair dye products prepared in the comparative examples 1 to 4 are taken as follows:
a. by smelling the smell of the hair dye, the products of comparative examples 1, 2,4 were more pungent in taste, while the product of comparative example 2 was more pungent;
b. color retention test: the 7 hair dye products of examples 1 to 4 and comparative examples 1 to 4 are used for respectively dyeing white hair of middle and old aged people, standing for 30 to 40 minutes, then putting the hair dye products into an aqueous solution containing 5 percent shampoo, then putting the hair dye products into an eddy current rotating machine, rotating at a controlled rotating speed of 40r/min, repeating the test and observing the color effect of the hair, and the results are shown in the following table:
TABLE 1 color retention test results for dyed hair
| Dyeing effect | Number of washes for first fade | Hair color development after hair color fading | |
| Example 1 | Bright black color | 91 | Original color |
| Example 2 | Bright black color | 85 | Original color |
| Example 3 | Bright black color | 93 | Original color |
| Example 4 | Bright black color | 90 | Original color |
| Comparative example 1 | Black color | 75 | A little bit yellow |
| Comparative example 2 | Black color | 79 | Light yellow belt |
| Comparative example 3 | Black color | 70 | Yellow with partial color |
| Comparative example 4 | Black color | 80 | Light yellow belt |
From the results shown in table 1, the hair dye of the example of the present invention has a brilliant black and glossy dyeing effect, and a better color retention than the hair dye of the comparative example, which indicates that the hair dye of the present invention has a better stability, and the hair after use still retains the original color after fading, indicating that the hair dye does not damage the hair, and the hair quality is still more flexible, and the hair dye of the comparative example, which contains hydrogen peroxide or p-phenylenediamine, protects the hair after fading to be yellow, indicating that the hair dye of the comparative example causes a certain degree of damage to the hair.
Claims (8)
1. A safe and stable single-agent hair dye is characterized by comprising 2,4,5, 6-tetraaminopyrimidine sulfate, plant extract, graphene oxide, dimethyl polysiloxane, 1, 3-butanediol, xanthan gum, monoethanolamine, ascorbic acid, polyoxyethylene (20) oleyl alcohol ether and essence.
2. The one-part hair dye composition of claim 1, wherein the plant extract comprises tea leaf extract, jasmine extract, mulberry extract, and gallnut extract.
3. The one-part hair dye according to claim 1, wherein the one-part hair dye comprises, by mass, 3 to 4% of 2,4,5, 6-tetraaminopyrimidine sulfate, 9 to 12% of a plant extract, 3 to 5% of graphene oxide, 3 to 4% of dimethylpolysiloxane, 2 to 4% of 1, 3-butanediol, 3 to 6% of xanthan gum, 4 to 7% of monoethanolamine, 2 to 4% of ascorbic acid, 3 to 5% of polyoxyethylene (20) oleyl ether, 0.5 to 2% of an essence, and the balance deionized water.
4. A preparation method of a safe and stable single-agent hair dye is characterized by sequentially comprising the following steps:
1) mixing 2,4,5, 6-tetraaminopyrimidine sulfate, folium Camelliae sinensis extract, Mori fructus extract and polyoxyethylene (20) oleyl alcohol ether, adding DMF and propylene glycol, mixing and dissolving, stirring at constant temperature, heating, and evaporating to remove DMF and propylene glycol to obtain mixture A;
2) mixing and dissolving dimethyl polysiloxane, butanediol and monoethanolamine, adding jasmine extract, gallnut extract and DMF, mixing and dissolving, stirring at constant temperature for emulsification reaction, and heating to evaporate DMF to obtain a mixture B;
3) mixing the mixture A, the mixture B, xanthan gum and ascorbic acid, and stirring at constant temperature for emulsification reaction;
4) and adding water and graphene oxide, mixing and stirring, cooling to room temperature for reaction, and finally dripping essence, mixing and stirring uniformly to obtain the hair dye.
5. The method for preparing a one-part hair dye according to claim 4, wherein the DMF and propylene glycol used in the step 1) are in a ratio of 1: (1-1.5).
6. The method for preparing the one-part hair dye according to claim 4, wherein the amount of DMF added in the step 2) is 60-63% of the amount of the mixture B.
7. The method for preparing the one-part hair dye according to claim 4, wherein the constant-temperature stirring temperature in the steps 1) to 3) is 45-70 ℃.
8. The method for preparing the single-agent type hair dye according to claim 4, wherein the graphene oxide in the step 4) is ground and sieved into particles with the pore size of 10-20 nm before use.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| IT202100031967A1 (en) * | 2021-12-21 | 2023-06-21 | Beauty & Business S P A | COMPOSITIONS FOR HAIR DYEING IN GEL OR GEL-EMULSION FORM |
| CN116763672A (en) * | 2022-05-13 | 2023-09-19 | 佛山市喜妆化妆品有限公司 | Preparation formula and method of air-oxidized single-agent hair dyeing product |
| CN117017809A (en) * | 2023-07-07 | 2023-11-10 | 珠海横琴一果投资合伙企业(有限合伙) | Dioxygen-free hair dye paste and preparation method thereof |
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|---|---|---|---|---|
| IT202100031967A1 (en) * | 2021-12-21 | 2023-06-21 | Beauty & Business S P A | COMPOSITIONS FOR HAIR DYEING IN GEL OR GEL-EMULSION FORM |
| US11813349B2 (en) | 2021-12-21 | 2023-11-14 | Beauty & Business S.P.A. | Hair colouring compositions in gel or emulsion-gel form |
| CN116763672A (en) * | 2022-05-13 | 2023-09-19 | 佛山市喜妆化妆品有限公司 | Preparation formula and method of air-oxidized single-agent hair dyeing product |
| CN117017809A (en) * | 2023-07-07 | 2023-11-10 | 珠海横琴一果投资合伙企业(有限合伙) | Dioxygen-free hair dye paste and preparation method thereof |
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Application publication date: 20200103 |