CN110613658A - Acne-removing compound preparation and preparation method thereof - Google Patents
Acne-removing compound preparation and preparation method thereof Download PDFInfo
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61P17/10—Anti-acne agents
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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Abstract
The invention discloses an acne-removing compound preparation which comprises the following raw materials in percentage by weight: humectant: 8-15%, thickening agent: 0.3-1%, emollient: 0-8%, emulsifier: 0-3%, extract of kuh-seng root: 0.1-0.5%, quaternary ammonium salt-73: 0.005-0.01%, extract A: 3-8%, witch hazel extract: 3-10%, saffron extract: 0.1-0.5% and the balance of deionized water; the extract A comprises: 20-30% of phellodendron amurense bark extract, 12-18% of white willow bark extract, 5-10% of phellodendron chinense root extract, 3-5% of scutellaria baicalensis root extract, 3-5% of houttuynia cordata extract, 5-8% of wild soybean seed extract, 5-8% of neem leaf extract and the balance of deionized water. The acne cream is compounded by selecting the components, achieves high-efficiency mild acne removing effect from different layers, can be used for a long time, can quickly remove red skin and detumescence, and can not generate drug resistance to acne bacilli on the surface of a human body.
Description
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to an acne-removing compound preparation and a preparation method thereof.
Background
Along with the continuous improvement of living standard of people, people's eating habits have also changed a lot, and greasy and the higher food of sugar content leads to people's obesity easily, and the life pressure increases, and the endocrine is chaotic, and grease secretes too much, and then more and more people's skin slowly becomes pox muscle, sensitive muscle etc.. However, the acne-removing skin care products on the market at present have many problems, such as poor acne-removing effect, irritation, drug resistance possibly generated after long-term use, and reduced effect.
Therefore, how to provide a safe and effective acne-removing product suitable for sensitive people is a technical problem which needs to be solved urgently by the technical personnel in the field.
Disclosure of Invention
In view of the above, the invention provides an efficient and safe acne-removing preparation suitable for sensitive acne muscle, which can be used for a long time, can quickly remove red skin and reduce swelling, and can not be resistant to acne bacilli on the surface of a human body.
In order to achieve the purpose, the invention adopts the following technical scheme:
an acne-removing compound preparation comprises the following raw materials in percentage by weight: 8-15% of a humectant, 0.3-1% of a thickener, 0-8% of an emollient, 0-3% of an emulsifier, 0.1-0.5% of a sophora flavescens root extract, 0-0.01% of a quaternary ammonium salt-730.005, 3-8% of an extract A, 3-10% of a witch hazel extract, 0.1-0.5% of a saffron extract and the balance of deionized water;
the extract A comprises: 20-30% of phellodendron amurense bark extract, 12-18% of white willow bark extract, 5-10% of phellodendron chinense root extract, 3-5% of scutellaria baicalensis root extract, 3-5% of houttuynia cordata extract, 5-8% of wild soybean seed extract, 5-8% of neem leaf extract and the balance of deionized water.
Preferably, the acne-removing compound preparation comprises the following raw materials in percentage by weight: 10% of humectant, 0.8% of thickener, 0.5% of emollient, 0.1% of emulsifier, 0.2% of sophora flavescens ait root extract, 5% of quaternary ammonium salt-730.01%, 5% of extract A, 5% of witch hazel extract, 0.5% of saffron extract and the balance of deionized water;
the extract A comprises: 25% of phellodendron amurense bark extract, 16% of white willow bark extract, 5% of Chinese rhubarb root extract, 4% of scutellaria root extract, 3% of houttuynia cordata extract, 6% of wild soybean seed extract, 8% of neem leaf extract and the balance of deionized water.
The invention also discloses a preparation method of the acne-removing compound preparation, which comprises the following steps:
the method comprises the following steps: cleaning and disinfecting appliances, weighing articles and machine equipment required by production for standby;
step two: weighing the emollient and the emulsifier in proportion, putting the mixture into an oil phase pot, stirring and heating to 80-85 ℃ to obtain an oil phase for later use;
step three: weighing deionized water, humectant and thickener in proportion, placing into a water phase pot, stirring and heating to 80-85 ℃ (stirring speed 50-100r/min), keeping the temperature for 15-25 min, and homogenizing for 3-5 min (homogenizing speed 1000-;
step four: preheating an emulsifying pot to 45-55 ℃, pumping the water phase obtained in the third step, keeping the temperature at 80-85 ℃, pumping the oil phase obtained in the second step while stirring (the stirring speed is 40-60r/min), starting vacuum negative pressure after pumping, homogenizing and emulsifying for 3-5 minutes (the homogenizing speed is 2000-3000r/min), homogenizing and homogenizing uniformly, and starting stirring and cooling;
step five: when the temperature is reduced to 40-45 ℃, weighing the rest raw materials in proportion, adding the raw materials into an emulsifying pot, uniformly stirring (the stirring speed is 40-60r/min), and then continuously reducing the temperature to 36-38 ℃, wherein the quaternary ammonium salt-73 is completely dissolved by using the polyalcohol in advance;
step six: and after the inspection by an inspector is qualified, filtering the mixture by a 100-mesh filter screen, discharging the mixture, and filling the mixture to obtain a finished product.
Preferably, the vacuum negative pressure in the fourth step is-300 to-400 mbar.
The raw materials used in the invention have the following effects:
extract of kuh-seng root: contains high-efficiency anti-inflammatory and bacteriostatic traditional Chinese medicine components, and can quickly eliminate red swelling;
quaternary ammonium salt-73 (proud): the raw material has super-high activity bacteriostasis capability, can inhibit the activity of acne bacillus under the condition of low concentration, and is negative in tests of skin test, eye irritation test, photosensitivity, phototoxicity, gene mutation type and the like;
the phellodendron amurense bark extract in the extract A can inhibit the growth of acne bacillus; the white willow bark extract contains salicin, which can be converted into salicylic acid, which is an effective exfoliating agent; the extract of radix rehmanniae can inhibit male hormone activity; the Scutellariae radix extract can remove active oxygen in mitochondrial cell system in human body, and has antioxidant effect; the houttuynia cordata extract can inhibit histamine release from mast cells; the extract of semen glycines can inhibit sebaceous gland activity; the neem leaf extract has strong anti-inflammatory effect. The extract A is compounded to achieve the synergistic effect by supplementing each other, thereby inhibiting the activity of sebaceous glands, inhibiting sebum secretion, removing cutin and preventing the abnormal increase of cutin;
witch hazel extract: has excellent oil control and convergence effects;
saffron extract: saffron has the functions of repairing skin barrier, inhibiting skin inflammation and fast eliminating red.
The components are selected for compounding, and the high-efficiency mild acne removing effect is achieved in an auxiliary manner through different action mechanisms.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
an acne-removing compound preparation comprises the following raw materials in percentage by weight: humectant: 8%, thickener: 1%, emollient: 3% and emulsifier: 1%, extract of kuh-seng root: 0.1%, proud (quaternary ammonium salt-73): 0.005%, extract a: 3%, witch hazel extract: 3%, saffron extract: 0.1 percent, and the balance being deionized water;
the extract A comprises: cortex Phellodendri bark extract 30%, cortex Salicis Babylonicae bark extract 12%, radix et rhizoma Rhei sinensis extract 7%, radix Scutellariae extract 3%, herba Houttuyniae extract 4%, semen glycines seed extract 6%, folium Azadirachta indica extract 5%, and deionized water in balance.
Example 2:
an acne-removing compound preparation comprises the following raw materials in percentage by weight: humectant: 10%, thickener: 0.5%, emollient: 5%, emulsifier: 2%, kuh-seng root extract: 0.3%, proud (quaternary ammonium salt-73): 0.008%, extract a: 5%, witch hazel extract: 8%, saffron extract: 0.3 percent, and the balance being deionized water;
the extract A comprises: 20% of phellodendron amurense bark extract, 18% of willow bark extract, 5% of Chinese rhubarb root extract, 5% of scutellaria root extract, 5% of houttuynia cordata extract, 5% of wild soybean seed extract, 8% of neem leaf extract and the balance of deionized water.
Example 3:
an acne-removing compound preparation comprises the following raw materials in percentage by weight: humectant: 15%, thickener: 0.8%, emollient: 8%, emulsifier: 2.5%, extract of kushen root: 0.5%, proud (quaternary ammonium salt-73): 0.01%, extract a: 8%, witch hazel extract: 10%, saffron extract: 0.5 percent, and the balance being deionized water;
the extract A comprises: 25% of phellodendron amurense bark extract, 16% of white willow bark extract, 10% of Chinese rhubarb root extract, 4% of scutellaria root extract, 3% of houttuynia cordata extract, 8% of wild soybean seed extract, 6% of neem leaf extract and the balance of deionized water.
Example 4
An acne-removing compound preparation comprises the following raw materials in percentage by weight: 10% of humectant, 0.8% of thickener, 0.5% of emollient, 0.1% of emulsifier, 0.2% of sophora flavescens ait root extract, 5% of quaternary ammonium salt-730.01%, 5% of extract A, 5% of witch hazel extract, 0.5% of saffron extract and the balance of deionized water;
the extract A comprises: 25% of phellodendron amurense bark extract, 16% of white willow bark extract, 5% of Chinese rhubarb root extract, 4% of scutellaria root extract, 3% of houttuynia cordata extract, 6% of wild soybean seed extract, 8% of neem leaf extract and the balance of deionized water.
Example 5
The acne-removing compound preparation 1-4 is prepared according to the raw material proportion of the embodiment 1-4 and the following preparation steps
The method comprises the following steps: cleaning and disinfecting appliances, weighing articles and machine equipment required by production for standby;
step two: weighing the emollient and the emulsifier in proportion, putting the mixture into an oil phase pot, stirring and heating to 80-85 ℃ to obtain an oil phase for later use;
step three: weighing deionized water, humectant and thickener in proportion, placing into a water phase pot, stirring and heating to 80-85 ℃ (stirring speed 50-100r/min), keeping the temperature for 15-25 min, and homogenizing for 3-5 min (homogenizing speed 1000-;
step four: preheating an emulsifying pot to 45-55 ℃, pumping the water phase obtained in the third step, keeping the temperature at 80-85 ℃, pumping the oil phase obtained in the second step while stirring (the stirring speed is 40-60r/min), starting vacuum negative pressure after pumping, homogenizing and emulsifying for 3-5 minutes (the homogenizing speed is 2000-3000r/min), homogenizing and homogenizing uniformly, and starting stirring and cooling;
step five: when the temperature is reduced to 40-45 ℃, weighing the rest raw materials in proportion, adding the raw materials into an emulsifying pot, uniformly stirring (the stirring speed is 40-60r/min), and then continuously reducing the temperature to 36-38 ℃, wherein the quaternary ammonium salt-73 is completely dissolved by using the polyalcohol in advance;
step six: and after the inspection by an inspector is qualified, filtering the mixture by a 100-mesh filter screen, discharging the mixture, and filling the mixture to obtain a finished product.
Test example 1
And (3) evaluating the product effect:
the acne removing compound preparations 1 to 4 prepared in example 1, example 2, example 3 and example 4 were tested by selecting 50 patients with acne muscle of 18 to 30 years old, respectively, using the following methods: after the face is cleaned, the mung beans are uniformly smeared on the acne affected part, and are gently applied with a spot pressure massage until the acne affected part is completely absorbed, and the mung beans are used once a day in the morning and at night.
The number of people is counted after the filling effect is used for two days, wherein the acne removing effect is very good, the acne removing effect shows that the acne has obvious red fading and detumescence within 24 hours after smearing, the acne removing effect shows that the acne has obvious red fading and detumescence within 48 hours after smearing, the acne removing effect shows that the acne has obvious red fading and detumescence within 72 hours after smearing, the no effect has no obvious change within 72 hours, and the specific statistical result is shown in table 1:
table 1:
from the data in table 1 it can be derived: the high-efficiency mild acne-removing compound preparations prepared in different proportions in examples 1, 2, 3 and 4 have strong acne-removing effects in the using process, and have the user feedback that the effective mild acne-removing compound preparations have already receded from red and subsided swelling in the next day of use, so that the effect of example 4 is better than that of examples 1, 2 and 3 in terms of data, and the acne skin problem can be obviously improved.
The embodiments in the present description are described in a progressive manner, each embodiment focuses on differences from other embodiments, and the same and similar parts among the embodiments are referred to each other.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (4)
1. The acne-removing compound preparation is characterized by comprising the following raw materials in percentage by weight: 8-15% of a humectant, 0.3-1% of a thickener, 0-8% of an emollient, 0-3% of an emulsifier, 0.1-0.5% of a sophora flavescens root extract, 0-0.01% of a quaternary ammonium salt-730.005, 3-8% of an extract A, 3-10% of a witch hazel extract, 0.1-0.5% of a saffron extract and the balance of deionized water;
the extract A comprises: 20-30% of phellodendron amurense bark extract, 12-18% of white willow bark extract, 5-10% of phellodendron chinense root extract, 3-5% of scutellaria baicalensis root extract, 3-5% of houttuynia cordata extract, 5-8% of wild soybean seed extract, 5-8% of neem leaf extract and the balance of deionized water.
2. The acne-removing compound preparation according to claim 1, which is characterized by comprising the following raw materials in percentage by weight: 10% of humectant, 0.8% of thickener, 0.5% of emollient, 0.1% of emulsifier, 0.2% of sophora flavescens ait root extract, 5% of quaternary ammonium salt-730.01%, 5% of extract A, 5% of witch hazel extract, 0.5% of saffron extract and the balance of deionized water;
the extract A comprises: 25% of phellodendron amurense bark extract, 16% of white willow bark extract, 5% of Chinese rhubarb root extract, 4% of scutellaria root extract, 3% of houttuynia cordata extract, 6% of wild soybean seed extract, 8% of neem leaf extract and the balance of deionized water.
3. The preparation method of the acne-removing compound preparation according to any one of claims 1-2, characterized by comprising the following steps:
the method comprises the following steps: cleaning and disinfecting appliances, weighing articles and machine equipment required by production for standby;
step two: weighing the emollient and the emulsifier in proportion, putting the mixture into an oil phase pot, stirring and heating to 80-85 ℃ to obtain an oil phase for later use;
step three: weighing deionized water, a humectant and a thickening agent in proportion, putting the materials into a water phase pot, stirring and heating to 80-85 ℃, preserving heat for 15-25 minutes, and homogenizing for 3-5 minutes to obtain a water phase for later use;
step four: preheating an emulsifying pot to 45-55 ℃, pumping the water phase obtained in the third step, keeping the temperature at 80-85 ℃, pumping the oil phase obtained in the second step while stirring, starting vacuum negative pressure after pumping, homogenizing and emulsifying for 3-5 minutes, homogenizing and uniformly stirring, and cooling;
step five: when the temperature is reduced to 40-45 ℃, weighing the rest raw materials in proportion, adding the raw materials into an emulsifying pot, uniformly stirring, and then continuously reducing the temperature to 36-38 ℃, wherein the quaternary ammonium salt-73 is completely dissolved by using the polyalcohol in advance;
step six: and after the inspection by an inspector is qualified, filtering, discharging and filling to obtain a finished product.
4. The preparation method of the acne-removing compound preparation according to claim 3, characterized in that the vacuum negative pressure in the fourth step is-300 to-400 mbar.
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| CN112516034A (en) * | 2020-12-21 | 2021-03-19 | 广州旭帆生物科技有限公司 | Plant acne removing agent and preparation method and application thereof |
| CN115252501A (en) * | 2022-08-27 | 2022-11-01 | 广州市博之越精细化工有限公司 | Acne-curing composition and preparation method and application thereof |
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Application publication date: 20191227 |