CN110603445A - 用于无损测量氢扩散率的设备和方法 - Google Patents

用于无损测量氢扩散率的设备和方法 Download PDF

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Publication number
CN110603445A
CN110603445A CN201880027468.6A CN201880027468A CN110603445A CN 110603445 A CN110603445 A CN 110603445A CN 201880027468 A CN201880027468 A CN 201880027468A CN 110603445 A CN110603445 A CN 110603445A
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China
Prior art keywords
hydrogen
oxidation
diffusivity
chamber
metal structure
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Pending
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CN201880027468.6A
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English (en)
Chinese (zh)
Inventor
A.特雷迪亚
M.沙拉尼
S.A.杜瓦尔
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Saudi Arabian Oil Co
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Saudi Arabian Oil Co
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Publication of CN110603445A publication Critical patent/CN110603445A/zh
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    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20—Metals
    • G01N33/202—Constituents thereof
    • G01N33/2022—Non-metallic constituents
    • G01N33/2025—Gaseous constituents
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N13/00—Investigating surface or boundary effects, e.g. wetting power; Investigating diffusion effects; Analysing materials by determining surface, boundary, or diffusion effects
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/403—Cells and electrode assemblies
    • G01N27/413—Concentration cells using liquid electrolytes measuring currents or voltages in voltaic cells
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen; Reversible storage of hydrogen
    • C01B3/0005—Reversible storage of hydrogen, e.g. by hydrogen getters or electrodes
    • C01B3/001—Reversible storage of hydrogen, e.g. by hydrogen getters or electrodes characterised by the uptaking media; Treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/02—Hydrogen or oxygen
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00—Sampling; Preparing specimens for investigation
    • G01N1/02—Devices for withdrawing samples
    • G01N1/22—Devices for withdrawing samples in the gaseous state
    • G01N1/2226—Sampling from a closed space, e.g. food package, head space
    • G01N2001/2241—Sampling from a closed space, e.g. food package, head space purpose-built sampling enclosure for emissions
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N13/00—Investigating surface or boundary effects, e.g. wetting power; Investigating diffusion effects; Analysing materials by determining surface, boundary, or diffusion effects
    • G01N2013/003—Diffusion; diffusivity between liquids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20—Metals
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/92—Metals of platinum group
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/94—Non-porous diffusion electrodes, e.g. palladium membranes, ion exchange membranes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/32—Hydrogen storage
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Investigating And Analyzing Materials By Characteristic Methods (AREA)
  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
CN201880027468.6A 2017-04-28 2018-04-25 用于无损测量氢扩散率的设备和方法 Pending CN110603445A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US15/530,697 2017-04-28
US15/530,697 US10732163B2 (en) 2017-04-28 2017-04-28 Apparatus and method for the non-destructive measurement of hydrogen diffusivity
PCT/US2018/029298 WO2018200633A1 (en) 2017-04-28 2018-04-25 Apparatus and method for the non-destructive measurement of hydrogen diffusivity

Publications (1)

Publication Number Publication Date
CN110603445A true CN110603445A (zh) 2019-12-20

Family

ID=62152659

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201880027468.6A Pending CN110603445A (zh) 2017-04-28 2018-04-25 用于无损测量氢扩散率的设备和方法

Country Status (8)

Country Link
US (3) US10732163B2 (https=)
EP (1) EP3615930B1 (https=)
JP (1) JP2020517963A (https=)
KR (1) KR20200002857A (https=)
CN (1) CN110603445A (https=)
SA (1) SA519410353B1 (https=)
SG (1) SG11201909860RA (https=)
WO (1) WO2018200633A1 (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110261294B (zh) * 2019-06-04 2022-04-19 中国船舶重工集团公司第七二五研究所 一种模拟深海环境下裂纹区金属腐蚀电化学试验装置
JP7510100B2 (ja) * 2021-03-29 2024-07-03 日本電信電話株式会社 表面水素量解析方法及び表面水素量解析装置並びに表面水素量解析プログラム

Citations (11)

* Cited by examiner, † Cited by third party
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US5405513A (en) * 1994-07-08 1995-04-11 Saudi Arabian Oil Company Method and apparatus for an electrochemical test cell
US6196060B1 (en) * 1998-07-20 2001-03-06 Intevep, S. A. Apparatus and method for monitoring hydrogen permeation
EP1238247A2 (en) * 1999-12-01 2002-09-11 Luiz Augusto Demaria Correa Sensor for measuring hydrogen diffusion differences
US20050238932A1 (en) * 2004-04-26 2005-10-27 Tooru Koyama Fuel cell power source, method of operating thereof and portable electronic equipment
CN101832966A (zh) * 2010-05-28 2010-09-15 东北大学 金属氢渗透性能测定的装置及方法
CN101963569A (zh) * 2010-08-26 2011-02-02 长沙新中大环境科技有限公司 一种检测金属中原子氢扩散渗透速率的双电解液数字传感器
JP2011153897A (ja) * 2010-01-27 2011-08-11 Nippon Telegr & Teleph Corp <Ntt> 水素透過試験システム
GB2490395A (en) * 2011-04-29 2012-10-31 Inst Chemii Fizycznej Polskiej Akademii Nauk Probe for determining rate of hydrogen permeation
CN104950024A (zh) * 2015-06-11 2015-09-30 上海大学 测定氢扩散系数的装置及方法
US20150301010A1 (en) * 2012-10-25 2015-10-22 Letomec S.R.L. A device and a method for permeation hydrogen measurements
RU2586960C1 (ru) * 2015-03-17 2016-06-10 Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский политехнический университет" Способ измерения коэффициентов диффузии водорода в титане

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US3731523A (en) 1971-02-23 1973-05-08 Atomic Energy Commission Hydrogen activity meter
US4065373A (en) 1976-04-26 1977-12-27 Petrolite Corporation Hydrogen patch cell
US4221651A (en) 1979-06-25 1980-09-09 Rockwell International Corporation Electrochemical cell for measuring hydrogen in metal
US4563249A (en) 1983-05-10 1986-01-07 Orbisphere Corporation Wilmington, Succursale De Collonge-Bellerive Electroanalytical method and sensor for hydrogen determination
CA2035105C (en) 1991-01-28 1993-04-27 H. Bruce Freeman Hydrogen monitoring apparatus
US6554981B2 (en) * 1998-09-14 2003-04-29 Saudi Arabian Oil Company Hydrogen permeation probe
US7306951B1 (en) 1999-06-08 2007-12-11 Midwest Research Institute Method and apparatus for determining diffusible hydrogen concentrations
GB2358060B (en) 2000-01-05 2003-09-24 Ion Science Ltd Hydrogen collection and detection
US7552643B2 (en) 2006-12-08 2009-06-30 Centre For Nuclear Energy Research (CNER) Device and system for corrosion detection

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* Cited by examiner, † Cited by third party
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US5405513A (en) * 1994-07-08 1995-04-11 Saudi Arabian Oil Company Method and apparatus for an electrochemical test cell
US6196060B1 (en) * 1998-07-20 2001-03-06 Intevep, S. A. Apparatus and method for monitoring hydrogen permeation
EP1238247A2 (en) * 1999-12-01 2002-09-11 Luiz Augusto Demaria Correa Sensor for measuring hydrogen diffusion differences
US20050238932A1 (en) * 2004-04-26 2005-10-27 Tooru Koyama Fuel cell power source, method of operating thereof and portable electronic equipment
JP2011153897A (ja) * 2010-01-27 2011-08-11 Nippon Telegr & Teleph Corp <Ntt> 水素透過試験システム
CN101832966A (zh) * 2010-05-28 2010-09-15 东北大学 金属氢渗透性能测定的装置及方法
CN101963569A (zh) * 2010-08-26 2011-02-02 长沙新中大环境科技有限公司 一种检测金属中原子氢扩散渗透速率的双电解液数字传感器
GB2490395A (en) * 2011-04-29 2012-10-31 Inst Chemii Fizycznej Polskiej Akademii Nauk Probe for determining rate of hydrogen permeation
US20150301010A1 (en) * 2012-10-25 2015-10-22 Letomec S.R.L. A device and a method for permeation hydrogen measurements
RU2586960C1 (ru) * 2015-03-17 2016-06-10 Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский политехнический университет" Способ измерения коэффициентов диффузии водорода в титане
CN104950024A (zh) * 2015-06-11 2015-09-30 上海大学 测定氢扩散系数的装置及方法

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M.A. MOHTADI-BONAB ET AL.: ""Hydrogen induced cracking susceptibility in different layers of a hot rolled X70 pipeline steel"", 《INTERNATIONAL JOURNAL OF HYDROGEN ENERGY》 *
MANOLATOS, P, ET AL.: "NECESSITY OF A PALLADIUM COATING TO ENSURE HYDROGEN OXIDATION DURING ELECTROCHEMICAL PERMEATION MEASUREMENTS ON IRON", 《ELECTROCHIMICA ACTA》 *
中华人民共和国国家质量监督检验检疫总局 等: "《中华人民共和国标准 GB/T 30074-2013 用电化学技术测量金属中氢渗透（吸收和迁移）的方法》", 17 December 2013 *
欧阳跃军 等: ""氢渗透传感器现场监测应用研究"", 《现代化工》 *
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Also Published As

Publication number Publication date
WO2018200633A1 (en) 2018-11-01
SG11201909860RA (en) 2019-11-28
US10809241B2 (en) 2020-10-20
US20180313806A1 (en) 2018-11-01
EP3615930B1 (en) 2021-06-30
US20190265220A1 (en) 2019-08-29
US10732163B2 (en) 2020-08-04
EP3615930A1 (en) 2020-03-04
US11624743B2 (en) 2023-04-11
US20200200727A1 (en) 2020-06-25
SA519410353B1 (ar) 2022-03-22
KR20200002857A (ko) 2020-01-08
JP2020517963A (ja) 2020-06-18

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Application publication date: 20191220