CN110577763B - Oil painting pigment with lasting fragrance and preparation method thereof - Google Patents
Oil painting pigment with lasting fragrance and preparation method thereof Download PDFInfo
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- CN110577763B CN110577763B CN201910876243.4A CN201910876243A CN110577763B CN 110577763 B CN110577763 B CN 110577763B CN 201910876243 A CN201910876243 A CN 201910876243A CN 110577763 B CN110577763 B CN 110577763B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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Abstract
The invention discloses an oil painting pigment with lasting fragrance, which is prepared from the following components in percentage by mass: 40-80% of pigment powder, 15-58% of linseed oil, 1-5% of essence and 1-5% of fragrance retention agent. The oil painting pigment with lasting fragrance provided by the invention has an excellent oil painting effect, has lasting pleasant fragrance, and can give good experience in smell except vision while painting.
Description
Technical Field
The invention belongs to the technical field of oil painting pigments, and particularly relates to an oil painting pigment with lasting fragrance and a preparation method thereof.
Background
The oil painting pigment is a special painting pigment for oil painting and is prepared by adding oil and glue into pigment powder, stirring and grinding. The basic components of the oil painting pigment are the same as those of other painting pigments, and the oil painting pigment consists of a pigment, an extender pigment, a vehicle and certain auxiliary materials such as a shaping agent, a stabilizer, a drying retardant or a drier and the like. Pigment powder used by ancient master is partly derived from soil and minerals, and partly derived from plants or animals.
The oil painting pigment is widely applied in various forms, while painting expression, the rich color of the oil painting can convey various information, people can experience and enjoy the oil painting pigment through vision, but the oil painting pigment generally has monotonous and unpleasant smell.
In view of the above, the development of an oil painting pigment with lasting fragrance has positive significance for the preparation and application of the pigment.
Disclosure of Invention
The first purpose of the invention is to provide an oil painting pigment with lasting fragrance.
The second purpose of the invention is to provide a preparation method of the oil painting pigment with lasting fragrance.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the invention provides an oil painting pigment with lasting fragrance, which is prepared from the following components in percentage by mass: 40-80% of pigment powder, 15-58% of linseed oil, 1-5% of essence and 1-5% of fragrance retention agent.
Preferably, the oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 42-75% of pigment powder, 19-52% of linseed oil, 3-4% of essence and 3-4% of fragrance retention agent.
Preferably, the oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 42% of pigment powder, 52% of linseed oil, 3% of essence and 3% of fragrance retention agent.
Preferably, the oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 70% of pigment powder, 23% of linseed oil, 4% of essence and 3% of fragrance retention agent.
Preferably, the oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 75% of pigment powder, 19% of linseed oil, 3% of essence and 3% of fragrance retention agent.
Preferably, the oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 70% of pigment powder, 25% of linseed oil, 3% of essence and 2% of fragrance retention agent.
The pigment powder is ferric oxide color powder.
The linseed oil is refined linseed oil.
The essence is at least one of aldehyde compounds, ketone compounds, alcohol compounds, ester compounds and acid compounds; further, the aldehyde compound is selected from at least one of benzaldehyde, cinnamaldehyde, citral, acetaldehyde, butyraldehyde, hexanal, octanal and decanal; the ketone compound is at least one of beta-ionone, muscone, civetone and carvone; the alcohol compound is at least one selected from ethanol, phenethyl alcohol, n-propyl alcohol, n-butyl alcohol, isobutyl alcohol, n-amyl alcohol, isoamyl alcohol, hexanol, heptanol, 2-octanol, 1-octen-3-ol, nonanol, decanol, cis-3-hexenol (leaf alcohol), linalool, geraniol and cis-6-nonenol; the ester compound is at least one selected from ethyl butyrate, ethyl acetate, ethyl 2-methyl butyrate, isoamyl acetate and allyl caproate; the acid compound is at least one selected from acetic acid, propionic acid, butyric acid, valeric acid, caproic acid, enanthic acid, pelargonic acid, capric acid, undecanoic acid, dodecanoic acid, tetradecanoic acid, phenylacetic acid and lactic acid.
The fragrance-retaining agent is cation mono-quaternary ammonium salt compound (such as CTAB) and double quaternary ammonium salt compound (such as cardanol polyoxyethylene ether quaternary ammonium salt).
The second aspect of the invention provides a preparation method of the oil painting pigment with lasting fragrance, which comprises the following steps:
according to the proportion, the linseed oil, the essence and the fragrance retention agent are fully mixed, then the uniformly dispersed pigment powder is added, and grinding and stirring are carried out, so as to obtain the oil painting pigment with lasting fragrance.
Due to the adoption of the technical scheme, the invention has the following advantages and beneficial effects:
the oil painting pigment with lasting fragrance provided by the invention has the vividness and excellent use feeling of the oil painting pigment, has pleasant and lasting fragrance, the used essence components are tested by utilizing a template reaction to influence the substrate, and whether the essence components influence the pigment substrate or not is observed (whether a chemical substance in a single essence component is added, other components are not changed, whether the coloring power, light resistance, covering power, transparency, oil absorption, toughness, dryness, plasticity, leveling property and the like of a final pigment finished product are influenced or not is observed, so that acid substances can obviously influence the dryness and oil absorption of the pigment and have a clustering phenomenon, 2-3 times of linseed oil is required to obtain the pigment with good properties, and the pigments obtained by other substances have similar and good properties), and has excellent expansibility and wide applicability.
The essence used by the oil painting pigment with lasting fragrance provided by the invention does not influence the tinting strength, light resistance, covering power, transparency, oil absorption, toughness, dryness, plasticity, leveling property and the like of the oil painting pigment.
The oil painting pigment with lasting fragrance provided by the invention has an excellent oil painting effect, has lasting pleasant fragrance, and can give good experience in smell except vision while painting.
The oil painting pigment with lasting fragrance provided by the invention is safe and nontoxic, has lasting pleasant fragrance, overcomes the defect of single odor of the existing oil painting pigment, and endows oil painting pictures with multi-sense enjoyment while keeping the stable character of the pigment.
The oil painting pigment with lasting fragrance provided by the invention is added with the cationic quaternary ammonium salt substance as a fragrance retention agent, so that the release time of the fragrance can be prolonged on the premise of not influencing the volatilization of the fragrance and the shape of the pigment, and the state of the pigment can be optimized.
Detailed Description
In order to more clearly illustrate the invention, the invention is further described below in connection with preferred embodiments. It is to be understood by persons skilled in the art that the following detailed description is illustrative and not restrictive, and is not to be taken as limiting the scope of the invention.
The reagents used in the invention: iron oxide color powder was purchased from Zhengzhou Pengying chemical commerce and trade; the flaxseed oil is of French Bei Bi European Bopu series and purchased from the creative art article wholesale department; fragrance-retaining agents were purchased from Shanghai Mass. chemical technology, Inc.
The linseed oil used in the examples of the present invention is refined linseed oil.
Example 1
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 42% of ferric oxide color powder, 52% of linseed oil, 3% of essence (phenethyl alcohol) and 3% of fragrance retention agent (CTAB cetyl trimethyl ammonium bromide).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 100 days.
Example 2
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 70% of ferric oxide color powder, 23% of linseed oil, 4% of essence (muscone) and 3% of a fragrance retention agent (CTAB cetyl trimethyl ammonium bromide).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 90 days.
Example 3
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 75% of iron oxide color powder, 19% of linseed oil, 3% of essence (acetic acid) and 3% of fragrance retention agent (cetyl trimethyl ammonium bromide).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 60 days. However, the acid substances are contained, the oil absorption of the pigment is influenced, the finished product is in a cluster shape, the leveling property is not good, and the linseed oil which is 2 to 3 times more than the pigment needs to be added to obtain the pigment with good properties.
Example 4
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 40% of iron oxide color powder, 58% of linseed oil, 1% of essence (butyraldehyde) and 1% of fragrance retention agent (cetyl trimethyl ammonium bromide).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 90 days.
Example 5
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 75% of iron oxide color powder, 15% of linseed oil, 5% of essence (carvone) and 5% of fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 80 days.
Example 6
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 60% of iron oxide color powder, 36% of linseed oil, 2% of essence (isoamylol) and 2% of fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 80 days.
Example 7
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 40% of iron oxide color powder, 53% of linseed oil, 3% of essence (propionic acid) and 4% of fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 60 days. However, the acid substances affect the oil absorption of the pigment, the finished product is in a cluster shape, the leveling property is not good, and the pigment with good properties can be obtained only by adding 2-3 times of linseed oil.
Example 8
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 80% of iron oxide color powder, 16% of linseed oil, 2% of essence (benzaldehyde) and 2% of fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 80 days.
Example 9
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 60% of iron oxide color powder, 34% of linseed oil, 5% of essence (beta-ionone) and 1% of a fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 90 days.
Example 10
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 50% of iron oxide color powder, 44% of linseed oil, 2% of essence (n-propanol) and 4% of fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 70 days.
Example 11
An oil painting pigment with lasting fragrance is prepared from the following components in percentage by mass: 70% of iron oxide color powder, 25% of linseed oil, 3% of essence (n-propanol) and 2% of a fragrance retention agent (cardanol polyoxyethylene ether quaternary ammonium salt).
The preparation method of the oil painting pigment with lasting fragrance comprises the following steps:
adding the linseed oil, the essence and the fragrance retaining agent into a grinding dish according to the proportion, then adding the iron oxide color powder by using a sieve, grinding and stirring for one minute until an oil phase and the powder are uniformly mixed and no large particles exist, obtaining the oil painting pigment with lasting fragrance, and bottling and storing the ground oil painting pigment with lasting fragrance.
The oil painting pigment prepared by the embodiment has lasting fragrance and can last for 80 days.
Comparative example 1
Compared with the example 1, the perfume is not contained, and the rest is the same as the example 1.
The pigment obtained in this example had an unpleasant odor such as greasiness and metallic odor. The other properties were similar to those of the pigment of example 1.
Comparative example 2
Compared with the example 1, the perfume-retaining agent is not contained, and the rest is the same as the example 1.
The pigment prepared in the embodiment has no added fragrance retention agent, and the fragrance can last for 20 days. At the same time, the pigment tinting strength and leveling were less good than the pigment of example 1.
Comparative example 3
Compared with the example 1, the perfume does not contain essence and a perfume-retaining agent, and the rest is the same as the example 1.
The pigment obtained in this example had an unpleasant odor such as greasiness and metallic odor. The pigment tinting strength and leveling were less good than the example 1 pigment.
Methods of testing the performance of examples and comparative examples were tested according to oil paint color standard QB T1335.1-1991, color difference using a colorimeter, fineness using a blade fineness gauge, and data shown in Table 1:
TABLE 1
Although the present invention has been described with reference to a preferred embodiment, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (3)
1. The oil painting pigment with lasting fragrance is characterized by being prepared from the following components in percentage by mass:
40 to 80 percent of pigment powder
15 to 58 percent of linseed oil
1 to 5 percent of essence
1 to 5 percent of fragrance retention agent
The pigment powder is ferric oxide color powder, the essence is an alcohol compound, and the fragrance retention agent is cetyl trimethyl ammonium bromide;
the oil painting pigment is prepared by the following preparation method mainly comprising the following steps:
fully mixing the linseed oil, the essence and the fragrance-retaining agent according to the proportion, then adding the uniformly dispersed pigment powder, grinding and stirring to obtain the target product.
2. The oil paint pigment of claim 1, wherein the alcohol compound is selected from the group consisting of: at least one of phenethyl alcohol, n-propanol or isoamyl alcohol.
3. The oil paint pigment according to claim 1 or 2, wherein the linseed oil used is refined linseed oil.
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| CN201910876243.4A CN110577763B (en) | 2019-09-17 | 2019-09-17 | Oil painting pigment with lasting fragrance and preparation method thereof |
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| CN201910876243.4A CN110577763B (en) | 2019-09-17 | 2019-09-17 | Oil painting pigment with lasting fragrance and preparation method thereof |
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| CN110577763B true CN110577763B (en) | 2021-09-24 |
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| CN113583502B (en) * | 2021-08-04 | 2023-01-03 | 上海马利画材股份有限公司 | Medium agent and preparation method and application thereof |
| CN113999719A (en) * | 2021-10-21 | 2022-02-01 | 上海应用技术大学 | Method for comprehensively utilizing kettle bottoms after beta-ionone rectification |
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| FR2831549B3 (en) * | 2001-10-26 | 2003-09-12 | Catherine Claire Carol Barraud | AROMATIC PAINTS FOR THE ARTISTIC AREA COMPOSED OF GOUACHE, WATERCOLOR, OIL, PASTEL, INCORPORATING ESSENTIAL OILS OR NATURAL OR SYNTHETIC FLAVORS |
| CN1164694C (en) * | 2002-01-29 | 2004-09-01 | 吴雯菲 | Composite compounding agent for amphiphilic active pigment |
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