CN105132173A - Mango essence for oil-based ink and preparation method of mango essence - Google Patents
Mango essence for oil-based ink and preparation method of mango essence Download PDFInfo
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- CN105132173A CN105132173A CN201510611298.4A CN201510611298A CN105132173A CN 105132173 A CN105132173 A CN 105132173A CN 201510611298 A CN201510611298 A CN 201510611298A CN 105132173 A CN105132173 A CN 105132173A
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Abstract
The invention relates to mango essence for oil-based ink. The mango essence consists of mango essence, maltodextrin and starch sodium octenylsuccinate, wherein the mango essence consists of 3-hydroxyl-2- butanone, trans-2-hexenic acid, hexanol, benzenepropanal with the mass percentage concentration being 1 percent, hexyl hexanoate, beta-caryophyllene, delta-dodecalactone, furanone, nerol, rose oxide with the mass percentage concentration being 1 percent, alpha-pinene, leaf alcohol, citronellyl propionate, styrax, lemon oil and glycerol triacetate. The invention also provides a preparation method of the mango essence for the oil-based ink. The mango essence, the maltodextrin, the starch sodium octenylsuccinate and deionized water are uniformly mixed; homogenizing and emulsification are performed; then, spray drying is carried out; particular mango essence is formed, so that the aroma retaining effect and the oil solubility of the essence are improved; the mango essence is applicable to perfuming of the oil-based ink. The mango essence for the oil-based ink obtained by the method provided by the invention has the advantages of intense and vivid fragrance, strong natural feeling and permanent fragrance.
Description
Technical field
The invention belongs to chemical field, relate to a kind of essence, specifically a kind of oil-based ink mango essence and preparation method thereof.
Background technology
Along with China's rapid development of economy, under the drive of the industries such as printing, journalism, packing and decorating, exploitation, ink industry is also developed rapidly.Oil-based ink is that pigment grind is become very trickle particle, is dissolved in the ink in a kind of special solvent, is adapted at unlike material prints, such as plastics, leather, timber, glass, the materials such as acrylic.Advantage is ink of can not spreading and sinking in, and water tolerance is strong, fast light, not fugitive color, is suitable for industry extensive.
Oil-based ink does not generally have fragrance or has slight peculiar smell, if make oil-based ink with the fragrance of certain feature, will greatly promote added value and the result of use of oil-based ink.This just needs in ink, add the essence with certain odor type.In general, essence is a kind of by the artificial redeployed mixture containing multiple spices, and spices is all have volatile organic compound, easily volatilizees in direct use procedure, and fragrance remaining time is short.Therefore, development that have Longaacting fragrance-aretaining, that can be applicable to oil-based ink essence has very important significance.The preparation that can be applicable to oil-based ink mango essence has no report.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of oil-based ink mango essence and preparation method thereof, described this oil-based ink mango essence and preparation method thereof solves the short technical problem of fragrant ink fragrance remaining time of the prior art.
The invention provides a kind of oil-based ink mango essence, count by weight percentage, composition and the content of its raw material are as follows:
Mango essence 10%-25%,
Maltodextrin 55%-80%,
Starch Sodium Octenyl Succinate 10%-20%;
Described mango essence counts by weight percentage, its composition and content as follows:
Present invention also offers the preparation method of above-mentioned a kind of oil-based ink mango essence, comprise the steps:
1) 3-hydroxy-2-butanone is taken according to mass percent, trans-2-hexenoic acid, hexanol, mass percent concentration is the phenylpropyl aldehyde of 1%, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration is the rose oxide of 1%, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate, by 3-hydroxy-2-butanone, trans-2-hexenoic acid, hexanol, mass percent concentration is the phenylpropyl aldehyde of 1%, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration is the rose oxide of 1%, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate Homogeneous phase mixing, namely mango essence is obtained,
2) take mango essence, maltodextrin and starch Sodium Octenyl Succinate, in a reaction vessel, add maltodextrin and starch Sodium Octenyl Succinate, then add deionized water, heated and stirred, until become settled solution system completely;
3) mango essence is joined in obtained settled solution, continue to stir, essence is uniformly dispersed, shear 5-15 minute with 5000-8000r/min;
4) obtained homogeneous solution is carried out spraying dry, the inlet temperature of spray-drying tower is 150-200 DEG C, and temperature out is 80-120 DEG C, obtains oil-based ink mango essence from outlet.
Present invention also offers a kind of oil-based ink with mango characteristic perfume, be made up of above-mentioned oil-based ink mango essence and oil-based ink, described oil-based ink mango essence and the mass ratio of oil-based ink are 1 ~ 10:90 ~ 99.
Present invention also offers a kind of mango essence, count by weight percentage, its composition and content as follows:
The present invention, according to the odour characteristics of natural mango and note structure, chooses suitable raw material, modulate give off a strong fragrance, fine and smooth, natural mango essence true to nature.Then mango essence is mixed with maltodextrin, starch Sodium Octenyl Succinate and deionized water, carry out homogenizing emulsifying, then spraying dry, form particulate state mango essence, thus improve lasting and the oil soluble of essence, make it be applicable to the perfuming of oil-based ink.
A kind of particulate state mango essence of the present invention, can be applied to the perfuming of oil-based ink better, thus improves added value and the result of use of oil-based ink.This particulate state mango essence adds in oil-based ink and layering does not occur, stable system, and lasting is lasting.
Embodiment
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of oil-based ink mango essence, count by weight percentage, composition and the content of its raw material are as follows:
Mango essence 10g (10%)
Maltodextrin 80g (80%)
Starch Sodium Octenyl Succinate 10g (10%)
Above-mentioned mango essence, counts by weight percentage, its composition and content as follows:
The preparation method of above-mentioned mango essence comprises the steps:
Be the phenylpropyl aldehyde of 1% by 3-hydroxy-2-butanone, trans-2-hexenoic acid, hexanol, mass percent concentration, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration be 1% rose oxide, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate Homogeneous phase mixing, namely obtain mango essence.The essence fragrant aroma obtained, has the characteristic perfume of mango, and natural sense is strong.
The preparation method of above-mentioned a kind of oil-based ink mango essence comprises the steps:
(1), in 250ml beaker, add 80g maltodextrin and 10g starch Sodium Octenyl Succinate, then add the deionized water of 90g, heated and stirred, until become settled solution system completely.
(2), by 10g mango essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shears 15 minutes with 5000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 150 DEG C, and temperature out is 80 DEG C, from outlet can be given off a strong fragrance, particulate state mango essence true to nature.
The particulate state mango essence obtained is added in 99g oil-based ink with the perfuming amount of 1g, obtains the stay-in-grade oil-based ink with mango characteristic perfume.
The particulate state mango essence steady quality of above-mentioned gained, gives off a strong fragrance, natural true to nature, and lasting is lasting, has the characteristic perfume of mango.
Embodiment 2
A kind of oil-based ink mango essence, count by weight percentage, composition and the content of its raw material are as follows:
Mango essence 25g (25%)
Maltodextrin 55g (55%)
Starch Sodium Octenyl Succinate 20g (20%)
Above-mentioned mango essence, counts by weight percentage, its composition and content as follows:
The preparation method of above-mentioned mango essence comprises the steps:
Be the phenylpropyl aldehyde of 1% by 3-hydroxy-2-butanone, trans-2-hexenoic acid, hexanol, mass percent concentration, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration be 1% rose oxide, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate Homogeneous phase mixing, namely obtain mango essence.The essence fragrant aroma obtained, has the characteristic perfume of mango.
The preparation method of above-mentioned a kind of oil-based ink mango essence comprises the steps:
(1), in 250ml beaker, add 55g maltodextrin and 25g starch Sodium Octenyl Succinate, then add the deionized water of 80g, heated and stirred, until become settled solution system completely.
(2), by 20g mango essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shears 5 minutes with 8000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 200 DEG C, and temperature out is 120 DEG C, from outlet can be given off a strong fragrance, particulate state mango essence true to nature.
The particulate state mango essence obtained is added in 90g oil-based ink with the perfuming amount of 10g, obtains the stay-in-grade oil-based ink with mango characteristic perfume.
The particulate state mango essence steady quality of above-mentioned gained, fragrant aroma, lasting is lasting, has the characteristic perfume of mango.
Embodiment 3
A kind of oil-based ink mango essence, count by weight percentage, composition and the content of its raw material are as follows:
Mango essence 12g (12%)
Maltodextrin 70g (70%)
Starch Sodium Octenyl Succinate 18g (18%)
Above-mentioned mango essence, counts by weight percentage, its composition and content as follows:
The preparation method of above-mentioned mango essence comprises the steps:
Be the phenylpropyl aldehyde of 1% by 3-hydroxy-2-butanone, trans-2-hexenoic acid, hexanol, mass percent concentration, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration be 1% rose oxide, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate Homogeneous phase mixing, namely obtain mango essence.The essence fragrance obtained is sent out thoroughly, has the characteristic perfume of mango, and natural sense is strong.
The preparation method of above-mentioned a kind of oil-based ink mango essence comprises the steps:
(1), in 250ml beaker, add 70g maltodextrin and 18g starch Sodium Octenyl Succinate, add the water of 88g, heated and stirred, until hydration becomes settled solution system completely.
(2), by 12g mango essence, join in the settled solution that step (1) obtains, continue to stir, essence is uniformly dispersed, shears 10 minutes with 6000r/min.
(3), by the homogeneous solution that step (2) obtains carry out spraying dry, the inlet temperature of spray-drying tower is 180 DEG C, and temperature out is 100 DEG C, can obtain fragrant aroma, particulate state mango essence true to nature from outlet.
The particulate state mango essence obtained is added in 95g oil-based ink with the perfuming amount of 5g, obtains the stay-in-grade oil-based ink with mango characteristic perfume.
The particulate state mango essence steady quality of above-mentioned gained, fragrance is sent out thoroughly, and lasting is lasting, has the characteristic perfume of mango.
Above affiliated content be only the present invention conceive under basic explanation, and any equivalent transformation that technical scheme according to the present invention is done, all belongs to the scope of protection of the invention.
Claims (4)
1. an oil-based ink mango essence, is characterized in that counting by weight percentage, and composition and the content of its raw material are as follows:
Mango essence 10%-25%,
Maltodextrin 55%-80%,
Starch Sodium Octenyl Succinate 10%-20%;
Described mango essence counts by weight percentage, its composition and content as follows:
3-hydroxy-2-butanone 1%-5%,
Trans-2-hexenoic acid 1%-5%,
Hexanol 5%-10%,
Mass percent concentration is the phenylpropyl aldehyde 1%-5% of 1%,
Hexyl hexanoate 1%-5%,
β-caryophyllene 10%-15%,
Fourth position dodecalactone 1%-5%,
Furanone 1%-5%,
Vernol 1%-5%,
Mass percent concentration is the rose oxide 1%-5% of 1%,
α-pinene 2%-10%,
Leaf-alcohol 10%-30%,
Citronellyl propionate 0.5%-2%,
Styracin 0.5%-2%,
Lemon oil 5%-15%,
Surplus is glycerine triacetate.
2. the preparation method of a kind of oil-based ink mango essence according to claim 1, is characterized in that comprising the steps:
1) 3-hydroxy-2-butanone is taken according to mass percent, trans-2-hexenoic acid, hexanol, mass percent concentration is the phenylpropyl aldehyde of 1%, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration is the rose oxide of 1%, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate, by 3-hydroxy-2-butanone, trans-2-hexenoic acid, hexanol, mass percent concentration is the phenylpropyl aldehyde of 1%, hexyl hexanoate, β-caryophyllene, fourth position dodecalactone, furanone, vernol, mass percent concentration is the rose oxide of 1%, α-pinene, leaf-alcohol, citronellyl propionate, styracin, lemon oil, glycerine triacetate Homogeneous phase mixing, namely mango essence is obtained,
2) take mango essence, maltodextrin and starch Sodium Octenyl Succinate, in a reaction vessel, add maltodextrin and starch Sodium Octenyl Succinate, then add deionized water, heated and stirred, until become settled solution system completely;
3) mango essence is joined in obtained settled solution, continue to stir, essence is uniformly dispersed, shear 5-15 minute with 5000-8000r/min;
4) obtained homogeneous solution is carried out spraying dry, the inlet temperature of spray-drying tower is 150-200 DEG C, and temperature out is 80-120 DEG C, obtains oil-based ink mango essence from outlet.
3. have an oil-based ink for mango characteristic perfume, it is characterized in that: be made up of oil-based ink mango essence according to claim 1 and oil-based ink, described oil-based ink mango essence and the mass ratio of oil-based ink are 1 ~ 10:90 ~ 99.
4. a mango essence, is characterized in that counting by weight percentage, its composition and content as follows:
3-hydroxy-2-butanone 1%-5%,
Trans-2-hexenoic acid 1%-5%,
Hexanol 5%-10%,
Mass percent concentration is the phenylpropyl aldehyde 1%-5% of 1%,
Hexyl hexanoate 1%-5%,
β-caryophyllene 10%-15%,
Fourth position dodecalactone 1%-5%,
Furanone 1%-5%,
Vernol 1%-5%,
Mass percent concentration is the rose oxide 1%-5% of 1%,
α-pinene 2%-10%,
Leaf-alcohol 10%-30%,
Citronellyl propionate 0.5%-2%,
Styracin 0.5%-2%,
Lemon oil 5%-15%,
Surplus is glycerine triacetate.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510611298.4A CN105132173A (en) | 2015-09-23 | 2015-09-23 | Mango essence for oil-based ink and preparation method of mango essence |
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| CN201510611298.4A CN105132173A (en) | 2015-09-23 | 2015-09-23 | Mango essence for oil-based ink and preparation method of mango essence |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107011709A (en) * | 2017-05-22 | 2017-08-04 | 和县科嘉阀门铸造有限公司 | A kind of valve surface protection formula of delicate fragrance coating and preparation method thereof |
| WO2018116142A1 (en) * | 2016-12-20 | 2018-06-28 | Victoria Link Limited | Synthetic lures |
| CN111632562A (en) * | 2020-06-15 | 2020-09-08 | 上海应用技术大学 | Starch-based supramolecular vesicle and preparation method thereof |
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| CN101818007A (en) * | 2010-02-21 | 2010-09-01 | 苏州科斯伍德油墨股份有限公司 | Antibacterial and bacteriostatic oily ink |
| CN103695177A (en) * | 2013-12-27 | 2014-04-02 | 广东江大和风香精香料有限公司 | Red jujube flavor and preparation method thereof |
| US20140255080A1 (en) * | 2013-03-11 | 2014-09-11 | Crayola Llc | Scratch and sniff delivery systems and methods of using the same |
| CN104708933A (en) * | 2013-12-14 | 2015-06-17 | 上海泉灵信息科技有限公司 | Novel new-formula fragrance microcapsule printing ink |
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Patent Citations (4)
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| CN101818007A (en) * | 2010-02-21 | 2010-09-01 | 苏州科斯伍德油墨股份有限公司 | Antibacterial and bacteriostatic oily ink |
| US20140255080A1 (en) * | 2013-03-11 | 2014-09-11 | Crayola Llc | Scratch and sniff delivery systems and methods of using the same |
| CN104708933A (en) * | 2013-12-14 | 2015-06-17 | 上海泉灵信息科技有限公司 | Novel new-formula fragrance microcapsule printing ink |
| CN103695177A (en) * | 2013-12-27 | 2014-04-02 | 广东江大和风香精香料有限公司 | Red jujube flavor and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018116142A1 (en) * | 2016-12-20 | 2018-06-28 | Victoria Link Limited | Synthetic lures |
| AU2017381742B2 (en) * | 2016-12-20 | 2023-02-02 | Victoria Link Limited | Synthetic lures |
| AU2017381742C1 (en) * | 2016-12-20 | 2023-06-15 | Victoria Link Limited | Synthetic lures |
| CN107011709A (en) * | 2017-05-22 | 2017-08-04 | 和县科嘉阀门铸造有限公司 | A kind of valve surface protection formula of delicate fragrance coating and preparation method thereof |
| CN111632562A (en) * | 2020-06-15 | 2020-09-08 | 上海应用技术大学 | Starch-based supramolecular vesicle and preparation method thereof |
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