CN104559391A - Colorful ink composition and preparation method thereof for traditional Chinese paintings - Google Patents
Colorful ink composition and preparation method thereof for traditional Chinese paintings Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
- C09D11/17—Writing inks characterised by colouring agents
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Abstract
The invention provides a colorful ink composition for traditional Chinese paintings. The colorful ink composition comprises the following raw materials in percentage by weight: 10-20% of pigments, 10-15% of colloids, 0.1-1% of a surfactant, 1-5% of additives, 1-10% of a dispersing agent, 0.2-1% of spice, 1-1.5% of an antiseptic, and the balance of water. The preparation method comprises the following steps: firstly, adding deionized water accounting for 10%-15% of total weight in a heating container, and adding the additives in a stirring manner, completely dissolving the additives; heating the dissolved additives to above 90 DEG C, and adding the colloids in the heated container until the colloids are completely dissolved; rolling or grinding the added pigments, and gradually adding the prepared colloid solution in the rolled or ground pigments until the pigment fineness reaches 5-10 micrometers so as to form a basic ink pulp; adding the surfactant and the spice in the basic ink pulp, and stirring the surfactant, the spice, and the basic ink pulp; preparing a solution of which the concentration is 8%-13% by using the antiseptic, adding the prepared solution in the basic ink pulp, adding the balance of the deionized water in the mixture, stirring the deionized water and the mixture so as to enable the mixture to be completely dissolved; lowering the temperature, leaving the obtained composition to stand, and canning the obtained composition.
Description
Technical field:
The present invention relates to a kind of traditional Chinese Painting colored ink composition and making method.
Background technology:
As everyone knows, prepared Chinese ink is all black, at present also not with the colored prepared Chinese ink of merit in prepared Chinese ink.Black prepared Chinese ink is develop according to black block grinding, is the thick liquid containing a large amount of carbon element and glue; Its ink marks write is shiny black, strong covering power.Because carbon structure is comparatively soft, roll relatively good control in dispersion processing process grinding, auxiliary join that a certain amount of natural glue body can be fairly simple hold carbon black, be namely scattered in solution and form prepared Chinese ink solution.Be used as colored prepared Chinese ink at present and use various pigment, pigment used mostly is mineral color, chemical color, organic synthesis pigment; Its close structure, primary structure particle differs, both bad dispersion, not easily grinds again and rolls processing, is difficult to form colloidal solution, particularly very difficult colloid and holds the stabilising system forming solution.All traditional Chinese Paintings add and much more color all adopt acrylic paints lotion or solid pigment for this reason, with water transfer dilution use voluntarily, avoid the formation of the deficiency of liquid.Owing to adding propylene class synthetic resins in coloured pigment lotion; in the rare process of tune; usually can not evenly can play up because of different from the solidification point of tusche; particularly propylene class and synthetic resins; after dry solidification, water just dissolves and does not know clearly; resin incrustation can not renew, and also makes troubles to user.
Summary of the invention:
What the present invention innovated provides a kind of traditional Chinese Painting colored ink composition and making method.
The colored ink composition of traditional Chinese Painting, mainly comprise the raw material of following weight per-cent: pigment 10-20%, colloid 10-15%, tensio-active agent 0.1-1%, additive 1-5%, dispersion agent 1-10%, spices 0.2-1%, sanitas 1-1.5%, its surplus is water.
The colored prepared Chinese ink making method of traditional Chinese Painting: first first add the deionized water accounting for gross weight 10% ~ 15% in heating container, under agitation adding additive makes it dissolve completely, be heated to more than 90 DEG C, drop into colloid, heating holding temperature is dissolved completely to it and is become hydrosol more than 90 DEG C while stirring, with deionized water, dispersion agent is mixed with the solution that concentration is 30% ~ 40% again, add pigment to mix thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5-10 μM, form prepared Chinese ink base paste. add tensio-active agent again, essence and flavoring agent stirs, finally with 80-90 DEG C of deionized water sanitas is mixed with concentration be 8% ~ 13% solution join in base paste, the deionized water of surplus adds to standard weights, continue stirring and make its abundant solution, cooling, leave standstill, filling.
This invention utilizes dispersion agent and colloid is auxiliary joins as dispersion medium, coloured pigment is stably scatter, and roll pigment fineness reach less than 5 μm by grinding, coloured pigment is made to be dispersed in solution, thus formation is suitable for traditional Chinese Painting use, and the colored prepared Chinese ink identical with black prepared Chinese ink system.
Embodiment
The colored prepared Chinese ink of traditional Chinese Painting, mainly comprise the raw material of following weight per-cent: pigment 10-20%, colloid 10-15%, tensio-active agent 0.1-1%, additive 1-5%, dispersion agent 1-10%, spices 0.2-1%, sanitas 1-1.5%, its surplus is deionized water, making method: first first add the deionized water accounting for gross weight 10% ~ 15% in heating container, under agitation adding additive makes it dissolve completely, be heated to more than 90 DEG C, drop into colloid, heating holding temperature is dissolved completely to it and is become hydrosol more than 90 DEG C while stirring, with deionized water, dispersion agent is mixed with the solution of concentration 30% ~ 40% again, add pigment to mix thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5-10 μm, form prepared Chinese ink base paste. add tensio-active agent again, essence and flavoring agent stirs, finally with 80-90 DEG C of deionized water, sanitas being mixed with concentration 8% ~ 13% solution joins in base paste, the deionized water of surplus adds to standard weights, continue stirring and make its abundant solution, cooling, leave standstill, filling.
Described pigment is permanent bordeaux F5R, bronze red C, Pigment red A3B, Pigment red 2GL, Pigment red RT, Pigment red HF2B, Pigment red BP, Pigment red 5G, Pigment red FP, Pigment red RE, Pigment red B, Pigment red F3C, Pigment red PT, organic red 420, organic red 6B, organic red 5034, organic red BK, organic red 2R, organic red 2BR, organic red 2BM, organic red RN, organic red BR, organic red FB, organic red F5R, organic red F6B, organic red F4C, organic yellow GH, organic yellow 10G, organic yellow GF, organic yellow GR, organic yellow G, organic yellow 203, organic yellow F10G, organic yellow 104, organic yellow GG, organic yellow HR, organic yellow 103, organic yellow H4G, organic yellow H3G, organic yellow GRY, Pigment Yellow 73 AR, Pigment Yellow 73 HD, Pigment Yellow 73 HG, Pigment Yellow 73 H3R, Pigment Yellow 73 3R, Pigment Yellow 73 16, organic blue B, organic blue BGS, organic blue 4920, organic blue 7090, organic blue BS, organic blue BG, organic green G, organic green 8730, ferric oxide, red lead chrome yellow, zinc-chrome yellow, cadmium yellow, iron oxide yellow, barba hispanica, cobalt blue, ultramarine, chromoxide green, lead chrome green, gamboge, sodium alizarinsulfonate, indigo-blue any one or two or more.
Described pigment can add carbon black allotment color and luster.
Described colloid be animal gelatine, animal skin glue, vegetable jelly, Sudan Gum-arabic any one.
Described tensio-active agent is sodium alkyl benzene sulfonate, tetradecyl sodium sulfonate, alkylpolyoxyethylene sodium sulfate, sodium soap, alkyl ether phosphates ester ammonium salt, succsinic acid two (2-Ethyl-butyl) sodium sulfonate, sodium metnylene bis-naphthalene sulfonate, surfactant AS, thunder rice side A, triethanolamine oleate, fatty alcohol-polyoxyethylene ether phosphate monoester, lipid acid sodium phosphate salt, polyol ester (single R-Glyceric acid of lipid acid, sorbitan ester), lauryl alcohol list or bis phosphoric acid acid potassium salt, the auxiliary of one or more of alkyl glycoside joins use.
Described additive comprises synthetic resins, described synthetic resins be resol, polyvinyl chloride (PVC) RESINS, epoxy resin, acrylic resin unsaturated polyester resin, urea-formaldehyde resin, urethane resin, furane resin any one.
Described additive comprises PH adjusting agent, described PH adjusting agent be citric acid, hexanodioic acid, lemon acid potassium, lactic acid, fumaric acid, sodium sesquicarbonate, Tartaric acid, sodium dihydrogen citrate, oxysuccinic acid, salt of wormwood, lemon acid potassium, phosphoric acid, sodium carbonate, Trisodium Citrate, acetic acid, Trisodium Citrate, hydrochloric acid, lime, sulfuric acid, sulfurous gas, caustic soda, trolamine, sodium hydroxide, sodium carbonate, sodium bicarbonate any one.
Described dispersion agent be 4,8-dibutyl a kind of apple sulfonic acid a kind of apple, 2-Naphthol cresoform sulfonation condensate sulfonates, diffusion agent N B, sodium laurylsulfonate, dodecyl sodium sulfonate ammonium, sulfonated castor oil, alkylphosphonic acid carboxylic acid list or dibasic acid esters salt, lauryl alcohol phosphoric acid ester, lauryl alcohol phosphoric acid ester potassium, polyoxyethylene monoalkyl phosphoric acid esters, sorbitan ester, sucrose ester, Nepal, 6501,2: 1 type alcohol amide any one.
Described essence and flavoring agent is natural essence spices, as cloves, santal, Moschus, the banksia rose, camphor, peppermint or compound essence spices any one.
Described sanitas comprise PHENOL 99.8 MIN ((CARBOLIC ACID)), borneol, Sodium Benzoate, borneol, GERMALL IS 45 (propylene glycol-diazonium alkyl urea-Nepal's methyl esters-iodine proyl n-butyl carbamate) any one.
Following methods is adopted to detect depth of color, water logging fastness, capillary test, biological test, the winter hardiness of the colored prepared Chinese ink of traditional Chinese Painting:
Test is carried out under envrionment temperature is the condition of 15 DEG C ~ 25 DEG C.
1.1 depth of color tests
1.1.1 instrument and material
A) 10mL centrifuge tube
B) 120g/m
2plumbous drawing paper bar (long 100mm, wide 10mm)
C) standard model: standard model prepared Chinese ink, get every year initial batch with the standard model comparison check of previous year after, the qualified same product standard model prepared Chinese ink as the current year.(that is: what the standard substance of every money prepared Chinese ink were same money prepared Chinese ink deposits product.)
1.1.2 Methods and steps
Getting the immersion of plumbous drawing paper bar has been added with in the centrifuge tube of sample prepared Chinese ink, immerse the about long 70mm of part, take out immediately after 1min, after being vertically placed to complete drying, cut off a section of 20mm bottom, do two so altogether, and in kind make vitta with standard model prepared Chinese ink, then get two kinds of vittas, intuition observes contrast, determines its depth of color.The method is intended to the stable case of testing the colored prepared Chinese ink product colour degree of depth of traditional Chinese Painting.
1.2 water logging fastness tests
1.2.1 instrument and material
A) vitta prepared of depth of color inspection institute
B) 500mL beaker
1.2.2 Methods and steps
Get sample prepared Chinese ink and each one of standard model prepared Chinese ink vitta prepared by depth of color inspection institute, be immersed in and be added with in the beaker of distilled water, take out after 24h, after complete seasoning, its water logging fastness is determined in contrast.
1.3 capillary test
1.3.1 instrument and material
A) pipette
B) middling speed qualitative filter paper
1.3.2 Methods and steps
Materials prepared Chinese ink in right amount by pipette, and in qualitative filter paper centre, same position drips three continuously, gives free rein to diffusion, and after complete drying, intuition observes capillary figure center has free of glue spots and periphery to have no-watermark to ooze out.
1.4 biological test
1.4.1 instrument and material
A) flat culture dish (￠ 80mm)
B) thermostat container
C) 100ml graduated cylinder (scale value 1ml)
1.4.2 Methods and steps
Materials prepared Chinese ink 20ml, puts into flat culture dish, add a cover, and is placed in 35 DEG C ± 2 DEG C thermostat containers, takes out after continuing 72h, and intuition is observed with or without mould evil idea and corrupt smell.
1.5 freezing test
1.5.1 instrument and material
A) refrigerator
B) refrigerator thermometer
C) sample 2-4 bottle
D) 100ml beaker
1.5.2 Methods and steps
A. the prepared Chinese ink 50ml that materialses puts into the beaker of 100ml, puts into refrigerator, is adjusted to standard gauge fixed temperature, takes out prepared Chinese ink visual inspection after insulation 6h.
B. sample prepared Chinese ink is put into refrigerator, under refrigerator temperature being adjusted to-6 DEG C ± 1 DEG C condition, taking out after insulation 6h, under 25 DEG C ± 2 DEG C conditions, make it naturally melt, then with hand even, do Physicochemical test after leaving standstill 10min and measure
Example 1: the red prepared Chinese ink of traditional Chinese Painting
The traditional Chinese Painting making method of red prepared Chinese ink: the deionized water first first adding 10g in heating container, under agitation adding sodium bicarbonate makes it dissolve completely, be heated to more than 90 DEG C, drop into gelatine, to dissolving completely, to become hydrosol stand-by 90 DEG C more than to heat holding temperature while stirring.With 5g deionized water, sulfonated castor oil is diluted again, add Pigment red RT, organic yellow 203 is mixed thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5-10 μm, form prepared Chinese ink base paste. add sodium alkyl benzene sulfonate again, santal stirs, finally will join in base paste after Sodium Benzoate dissolving completely with more than 80-90 DEG C deionized water 8g, the deionized water of surplus adds to standard weights, continues stirring and makes its abundant solution; Cooling, leave standstill, filling.
General data:
Example 2: the yellow prepared Chinese ink of traditional Chinese Painting
The traditional Chinese Painting making method of yellow prepared Chinese ink: the deionized water first first adding 14g in heating container, under agitation adding epoxy resin makes it dissolve completely, be heated to more than 90 DEG C, drop into hide glue, to dissolving completely, to become hydrosol stand-by 90 DEG C more than to heat holding temperature while stirring.With 8g deionized water, diffusion agent N B is dissolved again, add Pigment Yellow 73 HG to mix thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5 10 μm, form prepared Chinese ink base paste. add sodium metnylene bis-naphthalene sulfonate again, the banksia rose stirs, finally will join in base paste after PHENOL 99.8 MIN ((CARBOLIC ACID)) dissolving completely with more than 80-90 DEG C deionized water 12g, the deionized water of surplus adds to standard weights, continues stirring and makes its abundant solution; Cooling, leave standstill, filling.
General data:
Example 3: the blue prepared Chinese ink of traditional Chinese Painting
The traditional Chinese Painting making method of blue prepared Chinese ink: the deionized water first first adding 17g in heating container, under agitation adding sodium hydroxide makes it dissolve completely, be heated to more than 90 DEG C, drop into vegetable jelly, to dissolving completely, to become hydrosol stand-by 90 DEG C more than to heat holding temperature while stirring.With 17g deionized water, lauryl alcohol phosphoric acid ester is dissolved again, add organic blue BGS, carbon black mixes thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5-10 μm, form prepared Chinese ink base paste. add thunder rice side A, alkyl glycoside, cloves stirring again, finally will join in base paste after borneol dissolving completely with more than 80-90 DEG C deionized water 8g, the deionized water of surplus adds to standard weights, continues stirring and makes its abundant solution; Cooling, leave standstill, filling.
General data:
Example 4: the green prepared Chinese ink of traditional Chinese Painting
The traditional Chinese Painting making method of green prepared Chinese ink: the deionized water first first adding 20g in heating container, under agitation adding sodium carbonate makes it dissolve completely, be heated to more than 90 DEG C, drop into Sudan Gum-arabic, to dissolving completely, to become hydrosol stand-by 90 DEG C more than to heat holding temperature while stirring.With 20g deionized water, sorbitan ester is dissolved again, add organic green G to mix thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5-10 μm, form prepared Chinese ink base paste. add alkylpolyoxyethylene sodium sulfate again, peppermint stirs, finally being dissolved by GERMALL IS 45 completely with more than 80-90 DEG C deionized water 10g joins in base paste, the deionized water of surplus adds to standard weights, continues stirring and makes its abundant solution; Cooling, leave standstill, filling.
General data:
Experiment shows, the present invention has bright in luster, smell delicate fragrance, heavy ink is sedate, and light ink is distinct, and residual ink is solidified, self-dissolving of dripping, and can directly use together with tusche, grisaille painting one integrated mass shows level fully, have convert various, the effect got close to nature.Itself and black prepared Chinese ink dissolve each other and soak mutually, and painting and calligraphy are all suitable.
Claims (10)
1. the colored ink composition of traditional Chinese Painting, it is characterized in that, mainly comprise the raw material of following weight per-cent: pigment 10-20%, colloid 10-15%, tensio-active agent 0.1-1%, additive 1-5%, dispersion agent 1-10%, spices 0.2-1%, sanitas 1-1.5%, its surplus is water.
2. the colored ink composition of traditional Chinese Painting according to claim 1, is characterized in that, described water is ionized water; Described dispersion agent be 4,8-dibutyl a kind of apple sulfonic acid a kind of apple, 2-Naphthol cresoform sulfonation condensate sulfonates, diffusion agent N B, sodium laurylsulfonate, dodecyl sodium sulfonate ammonium, sulfonated castor oil, alkylphosphonic acid carboxylic acid list or dibasic acid esters salt, lauryl alcohol phosphoric acid ester, lauryl alcohol phosphoric acid ester potassium, polyoxyethylene monoalkyl phosphoric acid esters, sorbitan ester, sucrose ester, Nepal, 6501,2: 1 type alcohol amide any one; Described essence and flavoring agent is natural essence spices, as cloves, santal, Moschus, the banksia rose, camphor, peppermint or compound essence spices any one; Described sanitas comprise PHENOL 99.8 MIN ((CARBOLIC ACID)), borneol, Sodium Benzoate, borneol, GERMALL IS45 (propylene glycol-diazonium alkyl urea-Nepal's methyl esters-iodine proyl n-butyl carbamate) any one.
3. the colored ink composition of traditional Chinese Painting according to claim 1, is characterized in that, described pigment is permanent bordeaux F5R, bronze red C, Pigment red A3B, Pigment red 2GL, Pigment red RT, Pigment red HF2B, Pigment red BP, Pigment red 5G, Pigment red FP, Pigment red RE, Pigment red B, Pigment red F3C, Pigment red PT, organic red 420, organic red 6B, organic red 5034, organic red BK, organic red 2R, organic red 2BR, organic red 2BM, organic red RN, organic red BR, organic red FB, organic red F5R, organic red F6B, organic red F4C, organic yellow GH, organic yellow 10G, organic yellow GF, organic yellow GR, organic yellow G, organic yellow 203, organic yellow F10G, organic yellow 104, organic yellow GG, organic yellow HR, organic yellow 103, organic yellow H4G, organic yellow H3G, organic yellow GRY, Pigment Yellow 73 AR, Pigment Yellow 73 HD, Pigment Yellow 73 HG, Pigment Yellow 73 H3R, Pigment Yellow 73 3R, Pigment Yellow 73 16, organic blue B, organic blue BGS, organic blue 4920, organic blue 7090, organic blue BS, organic blue BG, organic green G, organic green 8730, ferric oxide, red lead chrome yellow, zinc-chrome yellow, cadmium yellow, iron oxide yellow, barba hispanica, cobalt blue, ultramarine, chromoxide green, lead chrome green, gamboge, sodium alizarinsulfonate, indigo-blue any one or two or more.
4. the colored ink composition of the traditional Chinese Painting according to claim 1 or 3, is characterized in that, described pigment can add carbon black allotment color and luster.
5. the colored ink composition of traditional Chinese Painting according to claim 1, is characterized in that, described colloid be animal gelatine, animal skin glue, vegetable jelly, Sudan Gum-arabic any one.
6. the colored ink composition of traditional Chinese Painting according to claim 1, it is characterized in that, described tensio-active agent is sodium alkyl benzene sulfonate, tetradecyl sodium sulfonate, alkylpolyoxyethylene sodium sulfate, sodium soap, alkyl ether phosphates ester ammonium salt, succsinic acid two (2-Ethyl-butyl) sodium sulfonate, sodium metnylene bis-naphthalene sulfonate, surfactant AS, thunder rice side A, triethanolamine oleate, fatty alcohol-polyoxyethylene ether phosphate monoester, lipid acid sodium phosphate salt, polyol ester (single R-Glyceric acid of lipid acid, sorbitan ester), lauryl alcohol list or bis phosphoric acid acid potassium salt, the auxiliary of one or more of alkyl glycoside joins use.
7. the colored ink composition of traditional Chinese Painting according to claim 1, it is characterized in that, described additive comprises synthetic resins, described synthetic resins be resol, polyvinyl chloride (PVC) RESINS, epoxy resin, acrylic resin unsaturated polyester resin, urea-formaldehyde resin, urethane resin, furane resin any one.
8. the colored ink composition of traditional Chinese Painting according to claim 1, it is characterized in that, described additive comprises PH adjusting agent, described PH adjusting agent be citric acid, hexanodioic acid, lemon acid potassium, lactic acid, fumaric acid, sodium sesquicarbonate, Tartaric acid, sodium dihydrogen citrate, oxysuccinic acid, salt of wormwood, lemon acid potassium, phosphoric acid, sodium carbonate, Trisodium Citrate, acetic acid, Trisodium Citrate, hydrochloric acid, lime, sulfuric acid, sulfurous gas, caustic soda, trolamine, sodium hydroxide, sodium carbonate, sodium bicarbonate any one.
9. the colored ink composition of traditional Chinese Painting according to claim 1, it is characterized in that, described dispersion agent be 4,8-dibutyl a kind of apple sulfonic acid a kind of apple, 2-Naphthol cresoform sulfonation condensate sulfonates, diffusion agent N B, sodium laurylsulfonate, dodecyl sodium sulfonate ammonium, sulfonated castor oil, alkylphosphonic acid carboxylic acid list or dibasic acid esters salt, lauryl alcohol phosphoric acid ester, lauryl alcohol phosphoric acid ester potassium, polyoxyethylene monoalkyl phosphoric acid esters, sorbitan ester, sucrose ester, Nepal, 6501,2: 1 type alcohol amide any one.
10. the colored prepared Chinese ink making method of traditional Chinese Painting: first first add the deionized water accounting for gross weight 10% ~ 15% in heating container, under agitation adding additive makes it dissolve completely, be heated to more than 90 DEG C, drop into colloid, heating holding temperature is dissolved completely to it and is become hydrosol more than 90 DEG C while stirring, with deionized water, dispersion agent is mixed with the solution that concentration is 30% ~ 40% again, add pigment to mix thoroughly, rare paste is become to be rolled or to grind, the hydrosol prepared progressively is added along with grinding the carrying out of rolling, until pigment fineness reaches 5-10 μM, form prepared Chinese ink base paste. add tensio-active agent again, essence and flavoring agent stirs, finally with 80-90 DEG C of deionized water sanitas is mixed with concentration be 8% ~ 13% solution join in base paste, the deionized water of surplus adds to standard weights, continue stirring and make its abundant solution, cooling, leave standstill, filling.
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| CN105017829A (en) * | 2015-06-30 | 2015-11-04 | 河南行知专利服务有限公司 | Biological environmental-friendly pigment used for artistic designing |
| CN105062212A (en) * | 2015-10-08 | 2015-11-18 | 苏州市永津彩印包装有限公司 | High-performance aromatic ink |
| CN105482532A (en) * | 2015-12-31 | 2016-04-13 | 苏州冰心文化用品有限公司 | Anti-aging traditional Chinese painting pigment and preparation method thereof |
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| CN105017829A (en) * | 2015-06-30 | 2015-11-04 | 河南行知专利服务有限公司 | Biological environmental-friendly pigment used for artistic designing |
| CN105062212A (en) * | 2015-10-08 | 2015-11-18 | 苏州市永津彩印包装有限公司 | High-performance aromatic ink |
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| CN105839215B (en) * | 2016-04-11 | 2018-02-09 | 浙江纳美新材料股份有限公司 | A kind of preparation method for being used to prepare the three primary colors colorant of coloured polyester fiber |
| CN108707367A (en) * | 2017-04-06 | 2018-10-26 | 上海大学 | A kind of prepared Chinese ink and preparation method thereof |
| CN107459870A (en) * | 2017-08-31 | 2017-12-12 | 黄太海 | A kind of method done raw material with tradition system ink, black cream is produced using wall breaking technology |
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| CN110373066A (en) * | 2019-07-24 | 2019-10-25 | 杨英才 | A kind of ceramics dizzy dye glaze and preparation method thereof |
| CN114591642A (en) * | 2020-12-03 | 2022-06-07 | 濮阳职业技术学院 | Process for preparing environment-friendly odorless pigment for art |
| CN115044235A (en) * | 2022-02-15 | 2022-09-13 | 九江学院 | Formaldehyde-free art painting pigment and preparation method thereof |
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