CN107011734A - A kind of anti-agglomeration ink - Google Patents

A kind of anti-agglomeration ink Download PDF

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Publication number
CN107011734A
CN107011734A CN201710271328.0A CN201710271328A CN107011734A CN 107011734 A CN107011734 A CN 107011734A CN 201710271328 A CN201710271328 A CN 201710271328A CN 107011734 A CN107011734 A CN 107011734A
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CN
China
Prior art keywords
parts
essential oil
water
ink
agglomeration
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710271328.0A
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Chinese (zh)
Inventor
胡秋生
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Ancient City Huangshan She Yan Co Ltd
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Ancient City Huangshan She Yan Co Ltd
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Application filed by Ancient City Huangshan She Yan Co Ltd filed Critical Ancient City Huangshan She Yan Co Ltd
Priority to CN201710271328.0A priority Critical patent/CN107011734A/en
Publication of CN107011734A publication Critical patent/CN107011734A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/16Writing inks
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/16Writing inks
    • C09D11/17Writing inks characterised by colouring agents

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention provides a kind of anti-agglomeration ink, it is made up of following raw material:Pine soot, gelatine, borneol, water, boric acid, AEO, anti-agglomerating agent, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil.The present invention is by adding special anti-agglomerating agent agent, it is possible to decrease the speed that prepared Chinese ink condenses at low temperature.Meanwhile, by adding a variety of essential oils, increase ink is fragrant, makes user's restoring consciouness, refreshes oneself.

Description

A kind of anti-agglomeration ink
Technical field
The present invention relates to a kind of anti-agglomeration ink, belong to cultural goods field.
Background technology
Ink is the china ink stick that ancient Chinese writing and drawing are used.The primary raw material of ink is carbon black, pine soot, glue etc., is carbon member Element is with the presence of noncrystalline kenel.Prepared Chinese ink for brush writing can be produced by the grinding of inkstone water, with colloid in water Solution is present.
The primary raw material of prepared Chinese ink is soot, sizing material, additive and solution etc., typically processing via machinery.Soot Species it is various, including various ore deposit plants and animal material form through burning or thermal decomposition.
Gelatine is the most frequently used sizing material in prepared Chinese ink, and it is stable higher, can be condensed by freezing, but can still be made after being melted with warm water With gelatine raw material is relatively easy to obtain, and manufacturing process is simpler, has the disadvantage that less than 0 degree easily congeals.
The content of the invention
To overcome above-mentioned technical problem, it is an object of the present invention to provide a kind of anti-agglomeration ink, the special anti-agglomeration by adding Agent agent, it is possible to decrease the speed that prepared Chinese ink condenses at low temperature.Meanwhile, by adding a variety of essential oils, increase ink is fragrant, user is waken up Brain, refresh oneself.
A kind of anti-agglomeration ink, is made up of following raw material:
28-35 parts of pine soot, 6-10 parts of gelatine, 0.3-0.5 parts of borneol, 260-300 parts of water, 3-4 parts of boric acid, aliphatic alcohol polyethenoxy 3-6 parts of ether, 0.4-0.8 parts of anti-agglomerating agent, 0.5-0.8 parts of eucalyptus quintessence oil, 0.3-0.5 parts of Marjoram essential oil, lime essential oil 0.3-0.5 parts.
Further, it is made up of following raw material:
29-33 parts of pine soot, 6-8 parts of gelatine, 0.3-0.5 parts of borneol, 260-300 parts of water, 3-4 parts of boric acid, aliphatic alcohol polyethenoxy 4-6 parts of ether, 2-4 parts of anti-agglomerating agent, 0.6-0.8 parts of eucalyptus quintessence oil, 0.3-0.5 parts of Marjoram essential oil, lime essential oil 0.3-0.5 Part.
Further, it is made up of following raw material:
32 parts of pine soot, 7 parts of gelatine, 0.4 part of borneol, 280 parts of water, 3.6 parts of boric acid, 5 parts of AEO, anti-agglomerating agent 3 parts, 0.7 part of eucalyptus quintessence oil, 0.42 part of Marjoram essential oil, 0.33 part of lime essential oil.
Described anti-agglomerating agent is made by following methods:By percentage by weight ethylene glycol 90.08%, 2- acrylamidos -2- Methyl propane sulfonic acid 1.3%, ethoxylated dodecyl alcohol 0.42%, sodium chloride 2.3%, citrate dihydrate trisodium 4.8%, glycine betaine 1.1% Mixing, stirs 4-5h, produces.
A kind of preparation method of anti-agglomeration ink, comprises the following steps:
A, by gelatine, borneol, boric acid, appropriate amount of water, under the conditions of 85-90 DEG C mix, mixing time is 5-6h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, appropriate amount of water, are mixed under the conditions of 20-25 DEG C, Mixing time is 1-2h;
C, AEO, anti-agglomerating agent, appropriate amount of water are eventually adding, are mixed under the conditions of 30-33 DEG C, during stirring Between be 20-25sec;
After d, filtering, produce.
Ink of the invention, main contributions are embodied at 2 points.One is that with the addition of homemade anti-agglomerating agent, it is ensured that at low temperature, The rate of set of ink is slowed by.Two be that with the addition of pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, allows user can The fragrance of essential oil is smelt, also can arousing brain, raising spirit, raising pleasant feeling.AEO can be by essential oil, anti-agglomerating agent more Rapidly and uniformly it is distributed in solution.
Embodiment
It is prepared by the anti-agglomerating agent of embodiment 1
By ethylene glycol 90.08%, 2- acrylamide-2-methylpro panesulfonic acids 1.3%, ethoxylated dodecyl alcohol 0.42%, sodium chloride 2.3%th, citrate dihydrate trisodium 4.8%, glycine betaine 1.1% is mixed, and is stirred 4.8h, is produced.
Embodiment 2
A kind of anti-agglomeration ink, is made up of following raw material:
32 parts of pine soot, 7 parts of gelatine, 0.4 part of borneol, 280 parts of water, 3.6 parts of boric acid, 5 parts of AEO, anti-agglomerating agent 3 parts, 0.7 part of eucalyptus quintessence oil, 0.42 part of Marjoram essential oil, 0.33 part of lime essential oil.
Comprise the following steps:
A, by gelatine, borneol, boric acid, appropriate amount of water, under the conditions of 88 DEG C mix, mixing time is 5.5h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, appropriate amount of water, mix under the conditions of 23 DEG C, stir The time is mixed for 1.7h;
C, AEO, anti-agglomerating agent, appropriate amount of water are eventually adding, are mixed under the conditions of 32 DEG C, mixing time For 22sec;
After d, filtering, produce.
Embodiment 3
A kind of anti-agglomeration ink, is made up of following raw material:
29 parts of pine soot, 7 parts of gelatine, 0.33 part of borneol, 290 parts of water, 3.8 parts of boric acid, 4 parts of AEO, anti-agglomeration 0.6 part of agent, 0.68 part of eucalyptus quintessence oil, 0.41 part of Marjoram essential oil, 0.47 part of lime essential oil.
Comprise the following steps:
A, by gelatine, borneol, boric acid, appropriate amount of water, under the conditions of 86 DEG C mix, mixing time is 2.6h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, appropriate amount of water, mix under the conditions of 22 DEG C, stir The time is mixed for 1.8h;
C, AEO, anti-agglomerating agent, appropriate amount of water are eventually adding, are mixed under the conditions of 32 DEG C, mixing time For 24sec;
After d, filtering, produce.
Embodiment 4
A kind of anti-agglomeration ink, is made up of following raw material:
35 parts of pine soot, 9 parts of gelatine, 0.45 part of borneol, 290 parts of water, 3.4 parts of boric acid, 5 parts of AEO, anti-agglomeration 0.5 part of agent, 0.6 part of eucalyptus quintessence oil, 0.35 part of Marjoram essential oil, 0.38 part of lime essential oil.
Comprise the following steps:
A, by gelatine, borneol, boric acid, appropriate amount of water, under the conditions of 88 DEG C mix, mixing time is 5.1h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, appropriate amount of water, mix under the conditions of 23 DEG C, stir The time is mixed for 1.4h;
C, AEO, anti-agglomerating agent, appropriate amount of water are eventually adding, are mixed under the conditions of 32 DEG C, mixing time For 23sec;
After d, filtering, produce.
Embodiment 5
A kind of anti-agglomeration ink, is made up of following raw material:
29 parts of pine soot, 8 parts of gelatine, 0.42 part of borneol, 270 parts of water, 3 parts of boric acid, 3.6 parts of AEO, anti-agglomeration 0.4 part of agent, 0.7 part of eucalyptus quintessence oil, 0.3 part of Marjoram essential oil, 0.41 part of lime essential oil.
Comprise the following steps:
A, by gelatine, borneol, boric acid, appropriate amount of water, under the conditions of 88 DEG C mix, mixing time is 5.6h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, appropriate amount of water, mix under the conditions of 24 DEG C, stir The time is mixed for 1.7h;
C, AEO, anti-agglomerating agent, appropriate amount of water are eventually adding, are mixed under the conditions of 31 DEG C, mixing time For 24sec;
After d, filtering, produce.
Embodiment 6
A kind of anti-agglomeration ink, is made up of following raw material:
34 parts of pine soot, 7 parts of gelatine, 0.3 part of borneol, 278 parts of water, 3.2 parts of boric acid, 5.4 parts of AEO, anti-agglomeration 0.5 part of agent, 0.6 part of eucalyptus quintessence oil, 0.35 part of Marjoram essential oil, 0.45 part of lime essential oil.
Comprise the following steps:
A, by gelatine, borneol, boric acid, appropriate amount of water, under the conditions of 90 DEG C mix, mixing time is 5h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, appropriate amount of water, mix under the conditions of 24 DEG C, stir The time is mixed for 2h;
C, AEO, anti-agglomerating agent, appropriate amount of water are eventually adding, are mixed under the conditions of 33 DEG C, mixing time For 24sec;
After d, filtering, produce.
Comparative example 1
Compared with Example 2, difference is in no anti-agglomerating agent.
Experiment:
Under the conditions of 5 DEG C, 20 DEG C, five containers are selected respectively, and the prepared Chinese ink 1cm for pouring into above-described embodiment 2-6 is thick, observes its top layer Start the time condensed, prepared Chinese ink of the setting time than the gained of comparative example 1 of the prepared Chinese ink obtained by acetonideexample 2-6 is than late 25-27 minutes.
All above-mentioned this intellectual properties of primarily implementation, the not this new product of implementation of setting limitation other forms And/or new method.Those skilled in the art will utilize this important information, the above modification, to realize similar execution feelings Condition.But, all modifications or transformation belong to the right of reservation based on new product of the present invention.
The above described is only a preferred embodiment of the present invention, being not the limitation for making other forms to the present invention, appoint What those skilled in the art changed or be modified as possibly also with the technology contents of the disclosure above equivalent variations etc. Imitate embodiment.But it is every without departing from technical solution of the present invention content, the technical spirit according to the present invention is to above example institute Any simple modification, equivalent variations and the remodeling made, still fall within the protection domain of technical solution of the present invention.

Claims (5)

1. a kind of anti-agglomeration ink, it is characterised in that be made up of following raw material:
28-35 parts of pine soot, 6-10 parts of gelatine, 0.3-0.5 parts of borneol, 260-300 parts of water, 3-4 parts of boric acid, aliphatic alcohol polyethenoxy 3-6 parts of ether, 0.4-0.8 parts of anti-agglomerating agent, 0.5-0.8 parts of eucalyptus quintessence oil, 0.3-0.5 parts of Marjoram essential oil, lime essential oil 0.3-0.5 parts.
2. a kind of anti-agglomeration ink according to claim 1, it is characterised in that be made up of following raw material:
29-33 parts of pine soot, 6-8 parts of gelatine, 0.3-0.5 parts of borneol, 260-300 parts of water, 3-4 parts of boric acid, aliphatic alcohol polyethenoxy 4-6 parts of ether, 2-4 parts of anti-agglomerating agent, 0.6-0.8 parts of eucalyptus quintessence oil, 0.3-0.5 parts of Marjoram essential oil, lime essential oil 0.3-0.5 Part.
3. a kind of anti-agglomeration ink according to claim 1, it is characterised in that be made up of following raw material:
32 parts of pine soot, 7 parts of gelatine, 0.4 part of borneol, 280 parts of water, 3.6 parts of boric acid, 5 parts of AEO, anti-agglomerating agent 3 parts, 0.7 part of eucalyptus quintessence oil, 0.42 part of Marjoram essential oil, 0.33 part of lime essential oil.
4. according to a kind of any described anti-agglomeration ink of claim 1-3, it is characterised in that described anti-agglomerating agent is by with lower section Method is made:
By percentage by weight ethylene glycol 90.08%, 2- acrylamide-2-methylpro panesulfonic acids 1.3%, ethoxylated dodecyl alcohol 0.42%th, sodium chloride 2.3%, citrate dihydrate trisodium 4.8%, glycine betaine 1.1% are mixed, and are stirred 4-5h, are produced.
5. according to a kind of preparation method of any described anti-agglomeration ink of claim 1-3, it is characterised in that including following step Suddenly:
A, by gelatine, borneol, boric acid, 3/5ths water, under the conditions of 85-90 DEG C mix, mixing time is 5-6h;
B, addition pine soot, eucalyptus quintessence oil, Marjoram essential oil, lime essential oil, 1/5th water, are mixed under the conditions of 20-25 DEG C Stirring, mixing time is 1-2h;
C, AEO, anti-agglomerating agent, 1/5th water are eventually adding, mix, stir under the conditions of 30-33 DEG C The time is mixed for 20-25sec;
After d, filtering, produce.
CN201710271328.0A 2017-04-24 2017-04-24 A kind of anti-agglomeration ink Pending CN107011734A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110746816A (en) * 2018-07-18 2020-02-04 安徽省绩溪旭龙山庄四宝文化有限公司 Slow-release fragrant ink stick and preparation method thereof
CN114395288A (en) * 2022-01-18 2022-04-26 黄山市歙县徽韵工艺品厂(普通合伙) Pine-tobacco Hui ink and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1167474B1 (en) * 2000-06-23 2005-12-14 Canon Kabushiki Kaisha Ink, ink set, ink-jet recording process, ink cartridge, recording unit and ink-jet recording apparatus
CN101492582A (en) * 2008-02-19 2009-07-29 北京科印近代印刷技术有限公司 Code-jet printing ink modifier
CN102492332A (en) * 2011-12-05 2012-06-13 天津市鸵鸟墨水有限公司 Novel ink and production method thereof
CN104449035A (en) * 2014-11-26 2015-03-25 成都锦汇科技有限公司 Water-based ink with condensation prevention capacity

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1167474B1 (en) * 2000-06-23 2005-12-14 Canon Kabushiki Kaisha Ink, ink set, ink-jet recording process, ink cartridge, recording unit and ink-jet recording apparatus
CN101492582A (en) * 2008-02-19 2009-07-29 北京科印近代印刷技术有限公司 Code-jet printing ink modifier
CN102492332A (en) * 2011-12-05 2012-06-13 天津市鸵鸟墨水有限公司 Novel ink and production method thereof
CN104449035A (en) * 2014-11-26 2015-03-25 成都锦汇科技有限公司 Water-based ink with condensation prevention capacity

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110746816A (en) * 2018-07-18 2020-02-04 安徽省绩溪旭龙山庄四宝文化有限公司 Slow-release fragrant ink stick and preparation method thereof
CN114395288A (en) * 2022-01-18 2022-04-26 黄山市歙县徽韵工艺品厂(普通合伙) Pine-tobacco Hui ink and preparation method thereof

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Application publication date: 20170804

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