CN110522818A - A kind of concocting method of Rehmannia glutinosa medicine materical crude slice - Google Patents
A kind of concocting method of Rehmannia glutinosa medicine materical crude slice Download PDFInfo
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- CN110522818A CN110522818A CN201910977604.4A CN201910977604A CN110522818A CN 110522818 A CN110522818 A CN 110522818A CN 201910977604 A CN201910977604 A CN 201910977604A CN 110522818 A CN110522818 A CN 110522818A
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- rehmannia glutinosa
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/80—Scrophulariaceae (Figwort family)
- A61K36/804—Rehmannia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a kind of concocting methods of Rehmannia glutinosa medicine materical crude slice, first radix rehmanniae recen is washed, to reduce total ash and acid-insoluble ash content, again to bake drying, it avoids tradition from steaming and fries duration and degree of heating drawback not easy to control, mode is steamed using wine later, and parameter is steamed to wine and is optimized, the operation steamed while pressurizeed by wine, convenient for controlling the time, the influence factors such as temperature, and concocted time can be shortened, reduce the loss of the effective components such as medical fluid, yellow rice wine is set sufficiently to moisturize radix rehmanniae recen, improve Rehmannia glutinosa yield, sliced natural drying later, obtain finished product, entire process flow is simple to operation, compared with traditional handicraft compared with, it is shorter with the period, the utilization of resources is more abundant and lower advantage is lost, strong technical support is provided for Rehmannia glutinosa production and processing, it is suitble to the industrial-scale production of Rehmannia glutinosa medicine materical crude slice preparation.
Description
Technical field
The present invention relates to Chinese medicine preparation technical field more particularly to a kind of concocting methods of Rehmannia glutinosa medicine materical crude slice.
Background technique
The prepared slices of Chinese crude drugs are that Chinese medicine passes through by traditional Chinese medical theory, Chinese medicine preparation method, can be direct after Processing methods
Chinese medicine for tcm clinical practice.
Rehmannia glutinosa is the Preparata of glutinous rehmannia, and gas is micro-, sweet, enriching yin of enriching blood, beneficial to spirit and marrow.For blood deficiency chlorosis,
Palpitation and severe palpitation, irregular menstruation, metrostaxis, the deficiency of liver-yin and kidney-yin, soreness and weakness of waist and knees, osteopyrexia and fever, night sweat spermatorrhea, Heat Diabetes, dizziness,
Tinnitus, poliosis.Rehmannia glutinosa medicine materical crude slice is widely used, and Rehmannia glutinosa process of preparation method domestic at present is largely using tradition
The concocting method of Chinese medicine, including stock, slice, drying and other steps, some can also be plus boiling, these traditional systems
Not only prepared slice quality is poor for the Rehmannia glutinosa that Preparation Method obtains, and differs greatly between batch in industrialization process, and effective component
Dissolution is slow, and degree of absorption is low, and curative effect is difficult to reach demand.
Summary of the invention
The object of the invention is to remedy the disadvantages of known techniques, provides a kind of concocting method of Rehmannia glutinosa medicine materical crude slice.
The present invention is achieved by the following technical solutions:
A kind of concocting method of Rehmannia glutinosa medicine materical crude slice, comprising the following specific steps
(1) radix rehmanniae recen is taken, is put into stir in clear water and clean, fish for medicinal material after standing 5-10 minutes and drain, divided in disk
In, it is sent into an oven and is dried for standby；
(2) step 1 gained medicinal material is put into steamer, then the yellow rice wine of quality of medicinal material 10-15% is added thereto, in 120-130 DEG C
Lower pressurization steams 60-90 minutes, takes out after the completion spare；
(3) medicinal material steamed is divided in baking pan, is put into drying chamber and is baked at 50-60 DEG C, it is every during baking
A medicinal material was stirred every 60-90 minutes, until medicinal material drying to moisture content is no more than 15%；
(4) medicinal material completed will be baked to be sliced with slicer, and the glutinous rehmannia after slice is placed in natural drying in glass sunlight house
12-24 hours, up to medicine materical crude slice of the present invention after sealed package.
Control mixing speed is 50-80 revs/min when washing in the step 1, is washed 5-6 minutes.
Drying temperature is 55-65 DEG C in the step 1, and the time is 150-180 minutes.
Yellow rice wine alcoholic strength is 12-14 degree in the step 2.
Pressure control is 0.26-0.30MPa when pressurization steams in the step 2.
It is repeated 6 times in the step 2 in the process that the bored mild laxation pressurization of yellow rice wine steams.
It is 4-6cm that thickness control is divided during baking in the step 3.
Slice thickness is 3-4mm in the step 4.
The invention has the advantages that
The present invention first washes radix rehmanniae recen, to reduce total ash and acid-insoluble ash content, then to bake drying, avoids tradition
Steam and fry duration and degree of heating drawback not easy to control, mode is steamed using wine later, and parameter is steamed to wine and is optimized, by wine steam simultaneously into
The operation of row pressurization convenient for control time, the influence factors such as temperature, and can shorten concocted time, reduce medical fluid etc. effectively at
The loss divided, makes yellow rice wine sufficiently moisturize radix rehmanniae recen, improves Rehmannia glutinosa yield, later sliced natural drying, obtain finished product, whole
A process flow is simple to operation, compared with traditional handicraft compared with the period is shorter, the utilization of resources is more abundant and loss is lower
Advantage provides strong technical support for Rehmannia glutinosa production and processing, is suitble to the industrial-scale production of Rehmannia glutinosa medicine materical crude slice preparation.
Specific embodiment
Below in conjunction with specific example, technical scheme is described further:
A kind of concocting method of Rehmannia glutinosa medicine materical crude slice, comprising the following specific steps
(1) take radix rehmanniae recen, be put into clear water with 60 revs/min stirring and washing 5 minutes, standing fish for medicinal material after ten minutes and drip
It is dry, divided in disk, be sent into an oven, 60 DEG C drying 180 minutes it is spare；
(2) step 1 gained medicinal material is put into steamer, then 13 degree of yellow rice wine of quality of medicinal material 12% is added thereto, at 125 DEG C
It is forced into 0.28MPa to steam 70 minutes, pressurization steams process and is repeated 6 times, and takes out after the completion spare；
(3) medicinal material steamed is divided in baking pan, thickness control 5cm, is put into drying chamber and is baked at 55 DEG C, dried
A medicinal material was stirred during system every 60 minutes, until medicinal material drying to moisture content is no more than 15%；
(4) medicinal material completed will be baked to be sliced with slicer, slice thickness 3mm, and the glutinous rehmannia after slice is placed in sun
Natural drying 24 hours in light room, up to medicine materical crude slice of the present invention after sealed package.
Gained finished product is irregular block piece, and not of uniform size, surface corvinus, glossy, stickiness is big, matter it is soft and with tough
Property, it is not easily broken, section corvinus, glossy, gas is micro-, sweet.
Identification:
Reference substance solution preparation: taking acteoside reference substance appropriate, accurately weighed, adds mobile phase that every 1ml is made containing 10 μ g's
Solution to get.
Test solution preparation: taking this product most coarse powder 2g, accurately weighed, sets in round-bottomed flask, and methanol is added in precision
100ml, weighed weight are heated to reflux 30 minutes, let cool, then weighed weight, and the weight of less loss is supplied with methanol, is shaken up, filtration,
Precision measures subsequent filtrate 50ml, and it is closely dry to be recovered under reduced pressure solvent, and residue flowing phased soln is transferred in 10ml measuring bottle, adds flowing
Mutually to scale, shake up, filter, take subsequent filtrate to get.
This product (C containing acteoside after measured29H36O15) it is no less than 0.020%.
Claims (8)
1. a kind of concocting method of Rehmannia glutinosa medicine materical crude slice, which is characterized in that comprising the following specific steps
(1) radix rehmanniae recen is taken, is put into stir in clear water and clean, fish for medicinal material after standing 5-10 minutes and drain, divided in disk
In, it is sent into an oven and is dried for standby；
(2) step 1 gained medicinal material is put into steamer, then the yellow rice wine of quality of medicinal material 10-15% is added thereto, in 120-130 DEG C
Lower pressurization steams 60-90 minutes, takes out after the completion spare；
(3) medicinal material steamed is divided in baking pan, is put into drying chamber and is baked at 50-60 DEG C, it is every during baking
A medicinal material was stirred every 60-90 minutes, until medicinal material drying to moisture content is no more than 15%；
(4) medicinal material completed will be baked to be sliced with slicer, and the glutinous rehmannia after slice is placed in natural drying in glass sunlight house
12-24 hours, up to medicine materical crude slice of the present invention after sealed package.
2. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that wash time control in the step 1
Mixing speed processed is 50-80 revs/min, is washed 5-6 minutes.
3. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that drying temperature in the step 1
It is 55-65 DEG C, the time is 150-180 minutes.
4. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that yellow rice wine alcohol in the step 2
Degree is 12-14 degree.
5. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that pressurization steams in the step 2
When pressure control be 0.26-0.30MPa.
6. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that bored in yellow rice wine in the step 2
The process that mild laxation pressurization steams is repeated 6 times.
7. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that bake process in the step 3
In divide thickness control be 4-6cm.
8. the concocting method of Rehmannia glutinosa medicine materical crude slice according to claim 1, which is characterized in that slice thickness in the step 4
For 3-4mm.
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| CN201910977604.4A CN110522818A (en) | 2019-10-15 | 2019-10-15 | A kind of concocting method of Rehmannia glutinosa medicine materical crude slice |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638901A (en) * | 2019-10-15 | 2020-01-03 | 安徽协和成药业饮片有限公司 | Preparation method of prepared rehmannia root traditional Chinese medicine decoction pieces steamed with high-pressure wine |
| CN114081914A (en) * | 2021-12-28 | 2022-02-25 | 河北仁心药业有限公司 | High-pressure processing method of prepared rehmannia root |
| CN115770756A (en) * | 2022-12-01 | 2023-03-10 | 九信(武汉)中药研究院有限公司 | Method for reducing ash content of cassia seed |
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| CN114081914A (en) * | 2021-12-28 | 2022-02-25 | 河北仁心药业有限公司 | High-pressure processing method of prepared rehmannia root |
| CN115770756A (en) * | 2022-12-01 | 2023-03-10 | 九信(武汉)中药研究院有限公司 | Method for reducing ash content of cassia seed |
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Application publication date: 20191203 |