CN110507560A - A kind of facial mask containing Siberian solomonseal rhizome polysaccharide - Google Patents
A kind of facial mask containing Siberian solomonseal rhizome polysaccharide Download PDFInfo
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- CN110507560A CN110507560A CN201910968144.9A CN201910968144A CN110507560A CN 110507560 A CN110507560 A CN 110507560A CN 201910968144 A CN201910968144 A CN 201910968144A CN 110507560 A CN110507560 A CN 110507560A
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- facial mask
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- siberian solomonseal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses a kind of facial masks containing Siberian solomonseal rhizome polysaccharide, belong to facial mask technical field, the facial mask containing Siberian solomonseal rhizome polysaccharide includes facial mask back sheet and coated on the gel glue on back sheet, Chinese herbal medicine active component extract in the gel glue containing 5-50wt%, the Chinese herbal medicine active component extract include Siberian solomonseal rhizome polysaccharide extract.The invention proposes the facial mask containing Siberian solomonseal rhizome polysaccharide, screening 40-60v% Siberian solomonseal rhizome polysaccharide component can be very good the effect for playing removal free radical as active constituent in application process, and facial mask comprehensive maintenance skin is promoted to act on.
Description
Technical field
The present invention relates to a kind of special mask product, in particular to a kind of mask product of active ingredient of Chinese herbs belongs to
Medicine modernizes applied technical field, belongs to facial mask technical field.
Background technique
Facial mask refers to for applying the cosmetics in face management skin youth state, health status.Facial mask generallys use gently
Thin paper or non-woven fabrics applies gelatinous load colloid composition, adds and answer in colloid composition as material of main part, addition
It is made of various nutritional ingredients and moisture.Facial mask is constituting rock-steady structure by attached gels materials such as non-woven fabrics using preceding, so
After apply in skin surface, gel carrier gradually release nutritional ingredient therein and nursing the factor, according to setting for mask product
The effect of meter scheme can use different Essences, reach nourishing skin, maintain moisture, promote skin elasticity acts on.
Facial mask can be formulated difference according to the gel-type vehicle of use, obtain different in the case where application is with skin surface
Active constituent release conditions.On the one hand, the time that can be applied by increasing facial mask, the transfer for improving trophic factors in facial mask are total
Amount has the function that optimization application effect enhancing；On the other hand, the formula of facial mask gel-type vehicle ingredient can be optimized, improved solidifying
The function and effect of gel matrix and skin reach the sorbefacient effect of enhancing.
Rhizoma polygonati (Polygonatum sibiricum) also known as tendrilleaf solomonseal rhizome, chicken head ginger are Liliaceae Polygonatum various plants
Dry tuber.Rhizoma polygonati has nourishing kidney-YIN, and tonifying middle-Jiao and Qi is promoted longevity and other effects.Raw sealwort has intense irritation taste,
Usually used rhizoma polygonati is the rhizoma polygonati that steams by processing processing, the ingredients such as polysaccharide is rich in rhizoma polygonati, modern research shows that rhizoma polygonati
Polysaccharide has antibacterial, anti-inflammatory, adjusting immunity and other effects.
A large amount of planting rhizoma polygonati has great advantage for the downstream industry of rhizoma polygonati, how sufficiently to develop rhizoma polygonati resource, grinds
Study carefully the great demand item that the rhizoma polygonati related industry with Chinese traditional herbs characteristic is Chinese medicine innovation and application field.
Summary of the invention
When it is an object of the invention to overcome the relatively slow facial mask trophic factors transfer velocity in the presence of the prior art, application
Between longer, deficiency that anti-senescence function is weaker, in conjunction with the demand of rhizoma polygonati industry development, provide a kind of innovation contains Siberian solomonseal rhizome polysaccharide
Mask product and preparation method thereof.
The facial mask that the present invention contains Siberian solomonseal rhizome polysaccharide mainly uses Siberian solomonseal rhizome polysaccharide as the active constituent of facial mask, by Siberian solomonseal rhizome polysaccharide
Separating-purifying is carried out, the polysaccharide component for being more applicable for mask product is obtained, the anti-senescence function for giving full play to Siberian solomonseal rhizome polysaccharide is made
With, and realize good promotion trophic factors changing effect, realize the effect of natural face-mask maintaining beauty and keeping young.
In order to achieve the above-mentioned object of the invention, the present invention provides following technical schemes:
A kind of facial mask containing Siberian solomonseal rhizome polysaccharide, it is described including facial mask back sheet and coated on the gel glue on back sheet
Chinese herbal medicine active component extract in gel glue containing 5-50wt%, the Chinese herbal medicine active component extract include rhizoma polygonati
Polyoses extract.
Mask product of the present invention, as Chinese herbal medicine activity extract ingredient, is made full use of natural using Siberian solomonseal rhizome polysaccharide extract
Siberian solomonseal rhizome polysaccharide extract captures free radical efficacy effect, realizes anti-aging effects.In addition, Siberian solomonseal rhizome polysaccharide extract can also promote
Trophic factors transfer utilizes, and can preferably enhance the health-care efficacy of facial mask, improves skin state, promotes skin finish.
Further, the gel glue is to include made of xanthan gum, distilled water, sodium carboxymethylcellulose and water-retaining agent.
Preferably, the weight ratio of the xanthan gum in the gel glue, distilled water, sodium carboxymethylcellulose and water-retaining agent
For 38-42:13-15:14-16:5-7.Preferably, the dosage of water-retaining agent is 5.5-6.5 parts.
Further, the gel glue is prepared by the following method to obtain:
S101, xanthan gum is taken, distilled water is added, is heated to 85-95 DEG C, sufficiently dissolution obtains clear gum liquid.
S102, sodium carboxymethylcellulose is added, stirring and dissolving is abundant, is cooled to 45-55 DEG C, and water-retaining agent is added, and stirring is mixed
It closes uniform.
S103,0.1-0.5wt% methylparaben, 0-0.02wt% essence, preferably 0.01wt% is added, is sufficiently stirred mixed
It closes uniformly, obtains gel glue.
In the process for preparation of gel glue, it is to be dissolved in water xanthan gum at relatively high temperatures first, carboxylic is then added
Sodium carboxymethylcellulose pyce continues to dissolve in relatively lower temperature, is eventually adding the ingredients such as water-retaining agent and methylparaben, essence, real
Existing gel rubber material is sufficiently mixed uniformly, and preparation obtains the good gel glue matrix of transparent homogeneity, loads conduct well
The carrier of natural extract active ingredient.So that active skull cap components can preferably keep lasting stability in gel glue
Property, and realize and the slow release of active constituent is acted on.The gel glue entirety uniformity prepared by the above method is more preferable,
More it is able to maintain the uniformity, consistency and stability of solution.
Preferably, the water-retaining agent is that glycerol and propylene glycol are mixed according to 10:1-1:10 volume ratio.Preferably, institute
It states water-retaining agent and is mixed by glycerol and propylene glycol according to 1-3:1 volume ratio.Such as 2:1.It is preferred that water-retaining agent uses glycerol and third
Glycol cooperates according to a certain percentage, and Water-saving effect is more preferable, and irritation is smaller.
Further, the Chinese herbal medicine active component extract containing 5-40wt% in the facial mask gel glue；Preferably, institute
State the Chinese herbal medicine active component extract in facial mask gel glue containing 10-30wt%, suitable Chinese herbal medicine active constituent addition
Using can not only give full play to the effect of extract, but also will not influence the basic phase stability of gel glue.Such as it can be
12%, 14%, 15%, 17%, 20%, 22%, 25% Chinese herbal medicine active component extract.
Further, the Siberian solomonseal rhizome polysaccharide extract extracts by the following method obtains:
S201, a steaming rhizoma polygonati is taken, the water that 8-20 times is measured is added and decocts 1-4 times, 20-60 minutes each, combined extract is dense
It is reduced to the extracting solution of a 0.7-2 times of weight of steaming rhizoma polygonati；
S202, ethanol precipitation is added the alcohol content of extracting solution is made to reach 40v%, filtering precipitating, filtrate add 95v% with
On ethanol precipitation so that alcohol content is reached 60v%, collect 60v% concentration of alcohol blanking liquid precipitate.
The Siberian solomonseal rhizome polysaccharide extract that application is added in rhizoma polygonati mask product of the present invention is that the extraction of 40-60v% ethyl alcohol separates
The active constituent arrived, active height are more suitable for promoting the effect of trophic factors transfer in facial mask.Extraction obtains this part
Siberian solomonseal rhizome polysaccharide ingredient has radicals scavenging effect well, is more suitably applied in mask product.
Further, the Chinese herbal medicine active component extract also includes Rhizoma Atractylodis Macrocephalae tuckahoe extracts, Fructus Citri Sarcodactylis extract, honeysuckle
At least one of extract.
Further, the Chinese herbal medicine active component extract includes Siberian solomonseal rhizome polysaccharide extract at least 60wt%.
Further, the Chinese herbal medicine active component extract includes the following component of weight percent: Siberian solomonseal rhizome polysaccharide >=
60%, Rhizoma Atractylodis Macrocephalae, tuckahoe extracts 5-30%, Fructus Citri Sarcodactylis extract 0-10%, Honegsukle flower P.E 0-10%.
Preferably, the Chinese herbal medicine activity extract includes weight percent: Siberian solomonseal rhizome polysaccharide 60%, Rhizoma Atractylodis Macrocephalae pachymaran
20%, Fructus Citri Sarcodactylis extract 10%, Honegsukle flower P.E 10%.
Further, the Rhizoma Atractylodis Macrocephalae extract extracts obtain by the following method:
S211, Rhizoma Atractylodis Macrocephalae being taken, cleaned, water decocts 1-3 times, and it is 20-60 minutes each, preferably 30-40 minutes, merges and extract
Liquid, filtrate are concentrated into 0.7-2 times of weight.
S212, addition ethanol precipitation make alcohol content reach 40%, are filtered to remove precipitating, filtrate adds 95v%'s or more
Ethanol precipitation makes alcohol content reach 60%, collects the sediment fraction of 60v% concentration of alcohol, obtains Rhizoma Atractylodis Macrocephalae extract.
Further, the tuckahoe extracts extract obtain by the following method:
S221, Poria cocos medicinal material being taken, cleaned, water decocts 1-3 times, and it is 20-60 minutes each, preferably 30-40 minutes, merges and extract
Liquid, filtrate are concentrated into 0.7-2 times of weight.
S212, addition ethanol precipitation make alcohol content reach 40%, are filtered to remove precipitating, filtrate adds 95v%'s or more
Ethanol precipitation makes alcohol content reach 60%, collects the sediment fraction of 60v% concentration of alcohol, obtains tuckahoe extracts.
Preferably, Rhizoma Atractylodis Macrocephalae extract and tuckahoe extracts are mixed to get Rhizoma Atractylodis Macrocephalae tuckahoe extracts are arrived.
Preferably, Rhizoma Atractylodis Macrocephalae tuckahoe extracts are that Rhizoma Atractylodis Macrocephalae and Poria cocos are extracted to the Rhizoma Atractylodis Macrocephalae Poria cocos being prepared together to extract
Object.The property of the two is close to be extracted together, is conducive to save and is extracted preparation time, improves efficiency.Rhizoma Atractylodis Macrocephalae can also be extracted respectively
Then extract and tuckahoe extracts are mixed to get Rhizoma Atractylodis Macrocephalae tuckahoe extracts.
Preferably, the control of the usage ratio of Rhizoma Atractylodis Macrocephalae and Poria cocos raw material is 1:2-2:1.
Compared with prior art, beneficial effects of the present invention:
1, the invention proposes the facial mask containing Siberian solomonseal rhizome polysaccharide, screening 40-60v% Siberian solomonseal rhizome polysaccharide group is allocated as in application process
For active constituent, the effect for playing removal free radical can be very good, and facial mask comprehensive maintenance skin is promoted to act on.Meanwhile
Siberian solomonseal rhizome polysaccharide can be very good to help trophic factors transfer absorbed, plays a role all and has for the high efficiency of a variety of aging ingredients
There is enhancing facilitation.
2, the present invention is investigated the fit applications of Siberian solomonseal rhizome polysaccharide and other Chinese herbal medicine active constituents, it was found that Siberian solomonseal rhizome polysaccharide
Active constituent with the traditional Chinese medicines extract such as Rhizoma Atractylodis Macrocephalae, Poria cocos as cooperation enhancing, preferably realize facial mask stability and
Trophic factors promotes transferance, has outstanding antioxidation, is of great significance for improving skin quality.
3, the mask product emphasis that the present invention contains Siberian solomonseal rhizome polysaccharide is used as supplement using natural Chinese medicinal herb active component, for
The integrated quality promotion of facial mask is of great significance, and more meets modern consumer and pure natural, natural mode mask product is chased after
It asks, there is great market potential.
4, the present invention is of great significance for the downstream industry exploitation of rhizoma polygonati, changes and is confined to rhizoma polygonati in tradition research
The limitation of dietotherapy application, improves the added value of rhizoma polygonati downstream industry, is conducive to rhizoma polygonati industrialized development, for plantation rhizoma polygonati
Household income increase has fine helping to act on.
Specific embodiment
Below with reference to test example and specific embodiment, the present invention is described in further detail.But this should not be understood
It is all that this is belonged to based on the technology that the content of present invention is realized for the scope of the above subject matter of the present invention is limited to the following embodiments
The range of invention.
Glycerol, propylene glycol analyze pure, Chengdu Ke Long Chemical Co., Ltd..
Fructus Citri Sarcodactylis extract, brand Koeman biology.Appearance: brownish-yellow powder；Effective component: hand lactone, Limettin, orange peel
Glycosides, hottentot tea glycosides etc..Manufacturing enterprise: Shaanxi Koeman Biotechnology Co., Ltd.
Honegsukle flower P.E, brand Koeman biology.Appearance: brownish-yellow powder；Effective component: chlorogenic acid 20%.Production enterprise
Industry: Shaanxi Koeman Biotechnology Co., Ltd.
Lemon extract, Lang Feng, RF001, main constituent component natural lemon are fragrant.Shanghai bright sweetgum material Co., Ltd.
One steams a solarization rhizoma polygonati: taking fresh rhizoma polygonati, cleans, remove palpus, air-dries or dry.Rhizoma polygonati is sliced, thickness 2-4mm.It puts
Enter steamer and steam 4h, then closes the stewing 2h of fire, then take out 40-80 DEG C of drying, obtain a steaming one and shine rhizoma polygonati.Or according to applicant it
(one shines) rhizoma polygonati is steamed in identical method preparation one in preceding report.
Not specified solid material percentage is weight percentage in the present invention, not specified solution percentage
Than for percent by volume.
<embodiment 1>
The basic components of facial mask gel glue design
Cooperate carboxymethyl using xanthan gum as basic colloid with reference to the basic components for preparing gel rubber plaster in the prior art
Sodium cellulosate constitutes gel rubber material, and using glycerol, propylene glycol as water-retaining agent, by formulas optimized design, realizing has well
Stability, the gel matrix material of coating performance.
According to L9(34) orthogonal test carries out facial mask gel glue preparation formula adjusting and optimizing, 4 are used during orthogonal test
The horizontal L of the factor 39Orthogonal test table is designed, select xanthan gum, distilled water, sodium carboxymethylcellulose, water-retaining agent (glycerol:
Propylene glycol=2:1) it is tested, specific each factor level design is as shown in the table.
1 Orthogonal Experiment and Design of table
| The factor | Xanthan gum | Distilled water | Sodium carboxymethylcellulose | Water-retaining agent (glycerol: propylene glycol 2:1) |
| Unit | g | mL | g | mL |
| 1 | 35 | 12 | 12 | 5 |
| 2 | 40 | 14 | 15 | 6 |
| 3 | 45 | 16 | 18 | 7 |
The L designed according to table 19(34) orthogonal test table, it carries out facial mask gel glue and is formulated orthogonal test.
Test method: weighing xanthan gum, and distilled water is added, is heated to 90 DEG C, and sufficiently dissolution obtains clear gum liquid.Add
Enter sodium carboxymethylcellulose, stirring and dissolving is abundant, is cooled to 50 DEG C, and glycerol and propylene glycol (2:1) is added, is uniformly mixed.
0.5wt% methylparaben, 0.01wt% essence is added, is thoroughly mixed uniformly, obtains gel glue.
Gel glue performance of keeping humidity test, the method is as follows: 20mL clear water is contained inside 100mL beaker, then using medical
Breathable adhesive tape closes beaker mouth, covers upper rhizoma polygonati facial mask in medical air-permeable blanket surface, simulates human skin.Get out simulation people
After body skin, dry particle is placed in by 90 DEG C of drying process 3h of hot-air oven, this dry particle is then placed in drying
In device, beaker is smoothly placed in the centre position of drier.
Weigh total weight M when being put into drier of beaker0, for 24 hours, 48h tests obtain M again1、M2, to assess facial mask
Performance of keeping humidity W1%=M1/M0, performance of keeping humidity W2%=M2/M0。
The rhizoma polygonati facial mask glue that above-described embodiment is prepared is respectively applied in medical air-permeable blanket surface, control coating
Uniform thickness 0.2mm is measured, then tests the performance of keeping humidity of different rhizoma polygonati facial mask glues according to the method described above, it is as a result as follows, it takes
For 24 hours, the experiment value that 48h performance of keeping humidity average value is evaluated as orthogonal test, specific test result is as shown in following table 2-3.
2 performance of keeping humidity test result of table
3 orthogonal experiments of table
| Tested number | Xanthan gum | Distilled water | Sodium carboxymethylcellulose | Water-retaining agent | Experiment value | X2 |
| 1 | 1 | 1 | 1 | 1 | 70.75 | 5005.5 |
| 2 | 1 | 2 | 2 | 2 | 69.53 | 4834.4 |
| 3 | 1 | 3 | 3 | 3 | 71.96 | 5178.2 |
| 4 | 2 | 1 | 2 | 3 | 74.00 | 5476.0 |
| 5 | 2 | 2 | 3 | 1 | 75.29 | 5668.6 |
| 6 | 2 | 3 | 1 | 2 | 73.97 | 5471.6 |
| 7 | 3 | 1 | 3 | 2 | 71.22 | 5072.3 |
| 8 | 3 | 2 | 1 | 3 | 72.59 | 5269.3 |
| 9 | 3 | 3 | 2 | 1 | 71.57 | 5122.3 |
| T1 | 204.67 | 209.38 | 206.71 | 210.48 | ||
| T2 | 219.14 | 217.87 | 214.91 | 210.95 | ||
| T3 | 207.54 | 204.10 | 209.73 | 209.92 | ||
| T12 | 41889.81 | 43839.98 | 42729.02 | 44301.83 | ||
| T22 | 48022.34 | 47467.34 | 46186.31 | 44499.90 | ||
| T32 | 43072.85 | 41656.81 | 43986.67 | 44066.41 | ||
| T2 | 44328.33 | 44321.38 | 44300.67 | 44289.38 | ||
| k1 | 68.22 | 69.79 | 68.90 | 70.16 | ||
| k2 | 73.05 | 72.62 | 71.64 | 70.32 | ||
| k3 | 69.18 | 68.03 | 69.91 | 69.97 |
The optimum fiting ratio that the material composition for preparing hydrogel is determined by orthogonal test is xanthan gum 40g, distilled water
14mL, sodium carboxymethylcellulose 15g, water-retaining agent (glycerol 4mL, propylene glycol 2mL).Below to prepare the mixing ratio of hydrogel into
The specific trial-production test of row, analyzes the stability and safety of the hydrogel of different mixing ratios.
<embodiment 101>
The basic components of facial mask gel glue design
It prepares facial mask gel glue: weighing xanthan gum 40g, add 15mL distilled water, be heated to 88 DEG C, sufficiently dissolution obtains
Gelatin-like liquid.Sodium carboxymethylcellulose 14g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, and glycerol 4mL, propylene glycol is added
2mL is uniformly mixed.Methylparaben 0.5g, lemon extract (Lang Feng, similarly hereinafter) 0.01g is added, is thoroughly mixed
It is even, obtain facial mask glue.
<embodiment 102>
The basic components of facial mask gel glue design
It prepares facial mask gel glue: weighing xanthan gum 42g, add 14mL distilled water, be heated to 90 DEG C, sufficiently dissolution obtains
Gelatin-like liquid.Sodium carboxymethylcellulose 15g is added, stirring and dissolving is abundant, is cooled to 55 DEG C, and glycerol 4mL, propylene glycol is added
2mL is uniformly mixed.Methylparaben 0.4g, essence 0.01g is added, is thoroughly mixed uniformly, obtains facial mask glue.<
Embodiment 103 >
The basic components of facial mask gel glue design
It prepares facial mask gel glue: weighing xanthan gum 38g, add 14mL distilled water, be heated to 85 DEG C, sufficiently dissolution obtains
Gelatin-like liquid.Sodium carboxymethylcellulose 13g is added, stirring and dissolving is abundant, is cooled to 48 DEG C, and glycerol 4.5mL, propylene glycol is added
3mL is uniformly mixed.Methylparaben 0.3g, essence 0.01g is added, is thoroughly mixed uniformly, obtains facial mask glue.
The optimal proportion range that above-described embodiment 101-103 is determined according to orthogonal test, then on the basis of optimal parameter
On, small range adjustment realizes a variety of different material dosage addition proportion feasibility verifyings, compares facial mask gel glue quality.It surveys
The performance of viscosity, mobility, adhesive force of hydrogel etc. is analyzed in examination.
<test 1: gel basic characteristic test>
According to 2010 editions two annex IU gelling agent inspections of the Pharmacopoeia of the People's Republic of China.Embodiment 101-103 preparation
Gel rubber material uniformly, it is fine and smooth, keep gluey at room temperature, it is not dry or liquefy, meet regulation of the pharmacopeia about gelling agent.
<test 2: gel is bonded comfort test>
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then facial mask gel glue prepared by above-described embodiment 101-103 is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains
To coating film sample.The facial mask gel glue of non-woven fabrics load every square centimeter is about 1.1-1.3g.
Test result is as follows, by the way that gel made of the raw material of different mixing ratios to be pasted on non-woven fabrics, compares
Paste performance of the corresponding gel rubber material in nonwoven surface.Test method is as follows, and gel rubber material is constituted coated on non-woven fabrics
Patch, cut into the print of 3cm × 3cm, this print be affixed on the outside of upper arm, paste time at least 10min and (it is few to paste the time
Fall off in 10min then unqualified), the paste performance of more different gel rubber plasters, test result is as follows shown in table.
4 gel of table is bonded comfort test result
| Comfort type | Stickiness | Moist feeling | |
| Embodiment 101 | Well | It is outstanding | Moistening effect is good |
| Embodiment 102 | Well | It is outstanding | Moistening effect is good |
| Embodiment 103 | Well | It is outstanding | Moistening effect is good |
Find that corresponding gel rubber plaster basic components have good coating performance by above-mentioned test, it can be very as patch
Good performance is incorporated in the effect of skin surface, and the wetness sensation of patch is good, suitable for answering for facial mask fitting moisturizing moisturizing
Use demand.
<test 3: irritant experiment>
Animal: adult healthy rabbit 4, weight about 1.5kg, 12h is by family's rabbit back backbone diamond wool before irritant experiment
It takes off, unhairing range about 45cm2(being less than rabbit body surface area 10%).
Gel rubber plaster sample: gel rubber plaster (each area about 9cm of above-described embodiment 101-103 preparation2)。
Gel rubber plaster reference substance: the gel mask of commercially available A brand as control (packaging is dismantled before use, cut into 3cm ×
3cm area about 9cm2Control patch).
Test method: on each family's rabbit back skin of unhairing surface, attaching above-mentioned gel rubber plaster sample and reference substance respectively,
Each 2 of left and right amounts to 4.It after the completion of attaching, is fixed with gauze, after keeping gel rubber plaster is stable to be attached at a rabbit back for 24 hours, is taken off
Remove gel rubber plaster, and with warm water cleaning back man rabbit skin.
Whether observer's rabbit back skin there are the irritative responses such as red and swollen, blistering, and 3d is observed continuously.The results show that institute
Some rabbit skin of back no abnormality seens show that the gel rubber plaster product for attaching 101-103 of embodiment of the present invention preparation is nonirritant.
<embodiment 201>
Prepare Siberian solomonseal rhizome polysaccharide extract
100 grams of a steaming rhizoma polygonati is taken, the water that 8 times of amounts are added decocts 2 times, and 40 minutes every time, combined extract, filtrate was concentrated to
100 milliliters, 90v% ethanol precipitation, which is added, makes alcohol content reach 38v%, and filtering precipitating, filtrate, which adds 90v% ethanol precipitation, to be made
Alcohol content reaches 60v%, collects (60v% concentration of alcohol feed liquid newly-generated) precipitating, obtains Siberian solomonseal rhizome polysaccharide.
Prepare Rhizoma Atractylodis Macrocephalae tuckahoe extracts
Rhizoma Atractylodis Macrocephalae and each 50g of Poria cocos are taken, adds water 400mL to decoct 2 times, 25 minutes every time, combined extract, filtrate was concentrated to
100 milliliters, 85v% ethanol precipitation, which is added, makes alcohol content reach 40v%, and filtering precipitating, filtrate, which adds 95v% ethanol precipitation, to be made
Alcohol content reaches 60v%, collects precipitating, obtains Rhizoma Atractylodis Macrocephalae tuckahoe extracts.
<embodiment 202>
Prepare Siberian solomonseal rhizome polysaccharide extract
100 grams of a steaming rhizoma polygonati is taken, the water that 10 times of amounts are added decocts 3 times, and 30 minutes every time, combined extract, filtrate was concentrated
To 100 milliliters, 75% ethanol precipitation, which is added, makes alcohol content reach 40%, and filtering precipitating, filtrate, which adds 95% ethanol precipitation, to be made
Alcohol content reaches 60%, collects this 60% ethanol precipitation part, obtains Siberian solomonseal rhizome polysaccharide.
Prepare Rhizoma Atractylodis Macrocephalae tuckahoe extracts
Rhizoma Atractylodis Macrocephalae and each 50g of Poria cocos are taken, adds water 400mL to decoct 2 times, 25 minutes every time, combined extract, filtrate was concentrated to
100 milliliters, 85v% ethanol precipitation, which is added, makes alcohol content reach 60v%, filters, and collects precipitating, obtains Rhizoma Atractylodis Macrocephalae tuckahoe extracts.
<embodiment 203>
Prepare Siberian solomonseal rhizome polysaccharide extract
100 grams of a steaming rhizoma polygonati is taken, the water that 15 times of amounts are added decocts 2 times, and 20 minutes every time, combined extract, filtrate was concentrated
To 90 milliliters.80v% ethanol precipitation, which is added, makes alcohol content reach 40v%, and precipitating is collected by filtration, obtains Siberian solomonseal rhizome polysaccharide 40v% second
Alcohol precipitate component.Filtrate, which adds 99v% ethanol precipitation, makes alcohol content reach 50v%, is filtered to remove precipitating.Filtrate continuously adds
99v% ethyl alcohol, until feed liquid concentration of alcohol reaches 70%, precipitating is collected in filtering, and obtaining Siberian solomonseal rhizome polysaccharide, (50v%-70v% ethyl alcohol is heavy
Shallow lake part).
Siberian solomonseal rhizome polysaccharide 40v% ethanol precipitation component content is more, and filtrate is dry by 90 DEG C of water-bath rotary evaporations, obtains
Solid powder, powder is more coarse, and finger friction texture is bad.Siberian solomonseal rhizome polysaccharide (50v%-70v% ethanol precipitation part) content
It is less, and polyoses content is less in alcohol precipitation ingredient.
Above-described embodiment 201-203 attempts different feed concentration mixing ratios respectively and extracts, by comparing different
The ethyl alcohol of concentration is precipitated, and the Siberian solomonseal rhizome polysaccharide for selecting 40-60v% concentration ethanol to precipitate is preferable, living at quality is belonged to
The property higher Siberian solomonseal rhizome polysaccharide extract of component content.By comparative analysis, it can determine and preparation height is extracted using water extraction and alcohol precipitation method
The Siberian solomonseal rhizome polysaccharide effect of quality is preferable, can obtain Siberian solomonseal rhizome polysaccharide extract of fine qualities.
<embodiment 3>
Facial mask preparation containing Siberian solomonseal rhizome polysaccharide
It prepares the gel glue of rhizoma polygonati facial mask: weighing xanthan gum 40g, add 14mL distilled water, be heated to 85 DEG C, sufficiently dissolve
Obtain clear gum liquid.Sodium carboxymethylcellulose 15g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, and glycerol 4mL, third is added
Glycol 2mL, is uniformly mixed.Siberian solomonseal rhizome polysaccharide, Rhizoma Atractylodis Macrocephalae tuckahoe extracts prepared by embodiment 201 are added, are uniformly mixed.
Methylparaben 0.5g, essence 0.01g is added, is thoroughly mixed uniformly, obtains gel glue sample.
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then above-mentioned rhizoma polygonati facial mask glue is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains the face containing Siberian solomonseal rhizome polysaccharide
Film.The rhizoma polygonati facial mask glue about 1.2g of non-woven fabrics load every square centimeter.
According to above-mentioned Siberian solomonseal rhizome polysaccharide facial mask preparation method, following addition Siberian solomonseal rhizome polysaccharide, Rhizoma Atractylodis Macrocephalae tuckahoe extracts are prepared respectively
The gel glue sample containing Siberian solomonseal rhizome polysaccharide of adding proportion.
301, Siberian solomonseal rhizome polysaccharide gel glue A, using the preparation of 201 method of embodiment: Siberian solomonseal rhizome polysaccharide 13g and Rhizoma Atractylodis Macrocephalae Poria cocos mention
Take object 6g.
302, Siberian solomonseal rhizome polysaccharide gel glue liquid B, using the preparation of 201 method of embodiment: Siberian solomonseal rhizome polysaccharide 13g.
303, Rhizoma Atractylodis Macrocephalae tuckahoe extracts gel glue C, using the preparation of 201 method of embodiment: Rhizoma Atractylodis Macrocephalae tuckahoe extracts 6g.
304, Siberian solomonseal rhizome polysaccharide gel glue D, using 203 method of embodiment preparation Siberian solomonseal rhizome polysaccharide 40v% ethanol precipitation at
Point, total 13g.
305, Siberian solomonseal rhizome polysaccharide gel glue E, the Siberian solomonseal rhizome polysaccharide 13g prepared using 203 method of embodiment.This Siberian solomonseal rhizome polysaccharide is
50v%-70v% ethanol precipitation part.
Preparation embodiment 201,203 is repeated to extract for several times, it is appropriate to obtain 50-70v% ethanol precipitation Siberian solomonseal rhizome polysaccharide, for
State the glue sample preparation of gel containing Siberian solomonseal rhizome polysaccharide of multiple and different adding proportions.
<test of test 4:DPPH free radical scavenging activity>
DPPH (1,1- diphenyl -2- trinitrophenyl-hydrazine) standard items 20mg is weighed, is settled to dehydrated alcohol dissolution
500mL obtains the standard solution that concentration is 0.04mg/mL.
It takes gel glue A-E sample 4mL to be added in colorimetric cylinder, DPPH standard solution 1mL is added, it is fixed to prepare addition distilled water
Hold to 10mL.After shaking up, colorimetric cylinder is placed in light protected environment reaction 30min, then measures suction at 520nm with spectrophotometer
Luminosity A1。
Using dehydrated alcohol as blank sample, 4mL dehydrated alcohol and DPPH standard solution 1mL is added, it is fixed that distilled water is then added
Hold to 10ml and standard items A is made0。
Compare different absorbance changes, ratio=A that DPPH free radical is removed can be reacted1/A0× 100%.
The rhizoma polygonati facial mask glue that above-described embodiment is prepared is subjected to free radical scavenging activity test according to the method described above, is tied
Fruit is as shown in the table.
The test of 5 rhizoma polygonati facial mask glue free radical scavenging activity of table
| Clearance rate % | |
| Gel glue A | 91.5 |
| Gel glue liquid B | 72.3 |
| Gel glue C | 16.6 |
| Gel glue D | 35.3 |
| Gel glue E | 61.8 |
The gel glue of test result display addition Siberian solomonseal rhizome polysaccharide has good radicals scavenging effect, shows corresponding
Siberian solomonseal rhizome polysaccharide extract has the function of protecting the skin from free radical destruction well.Using Siberian solomonseal rhizome polysaccharide extracting solution by not
Ingredient with concentration ethanol precipitating differs greatly for the scavenging effect of free radical, when using the precipitating analysis of 40-60v% concentration of alcohol
Siberian solomonseal rhizome polysaccharide component out for free radical clearance rate highest, and 40% ethanol precipitation be precipitated Siberian solomonseal rhizome polysaccharide for free radical
Scavenging effect it is then weaker, be unable to reach ideal level.
<embodiment 4>
Facial mask preparation containing Siberian solomonseal rhizome polysaccharide
It prepares the gel glue of rhizoma polygonati facial mask: weighing xanthan gum 40g, add 14mL distilled water, be heated to 90 DEG C, sufficiently dissolve
Obtain clear gum liquid.Sodium carboxymethylcellulose 15g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, and glycerol 4mL, third is added
Glycol 2mL, is uniformly mixed.Natural Chinese medicinal herb active component extract is added, is uniformly mixed.Methylparaben is added
0.5g, essence 0.01g are thoroughly mixed uniformly, obtain gel glue sample.
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then above-mentioned rhizoma polygonati facial mask glue is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains the face containing Siberian solomonseal rhizome polysaccharide
Film.The rhizoma polygonati facial mask glue of non-woven fabrics load every square centimeter is about 1.2g.
Natural Chinese medicinal herb active component according to addition application is different, respectively obtains the more containing rhizoma polygonati of following 401-404
The mask product of sugar.Wherein, the natural Chinese medicinal herb active component that application is added in each rhizoma polygonati mask product is as follows.
401, gel glue sample addition application: Siberian solomonseal rhizome polysaccharide 16g, the Rhizoma Atractylodis Macrocephalae Poria cocos of 202 method of embodiment preparation extract
Object 4g.
402, gel glue sample addition application: Siberian solomonseal rhizome polysaccharide 12g, the Rhizoma Atractylodis Macrocephalae Poria cocos of 202 method of embodiment preparation extract
Object 6g.
403, gel glue sample addition application: Siberian solomonseal rhizome polysaccharide 14g, the Rhizoma Atractylodis Macrocephalae Poria cocos of 202 method of embodiment preparation extract
Object 3g, Fructus Citri Sarcodactylis extract 2g.
404, gel glue sample addition application: Siberian solomonseal rhizome polysaccharide 14g, the Rhizoma Atractylodis Macrocephalae Poria cocos of 202 method of embodiment preparation extract
Object 3g, Fructus Citri Sarcodactylis extract 1.5g, Honegsukle flower P.E 1.5g.
<test 5: antibacterial test>
The preparation of culture medium: by 10g peptone, 5gNaCl is put into beaker, and water 1000mL is added to boil, and 5g beef is added
Cream after thawing, is sub-packed in after conical flask packages, high pressure sterilization (121 DEG C) 20min after taking-up, is placed in 80 DEG C of water-baths, standby
With.
Test method: this culture medium is added into 5 times of distilled water dilutions of water, heating and melting, the volume coated on embodiment 3-4 preparation
The gel mask surface containing Siberian solomonseal rhizome polysaccharide of number 301-305,401-405, culture medium coated weight is about 0.1g/cm2.It has coated
Cheng Hou is cooled to room temperature, in sample surfaces streak inoculation.Keep each sample scribing line dynamics, length consistent.
Evaluation of result: it after inoculation, is placed in 37 DEG C of constant incubators and is incubated for 12h.It takes out, observation statistics colony counts, root
Gel glue facial mask bacteriostasis is assessed according to colony counts, as a result as shown in the table.
The 6 antibacterial test of rhizoma polygonati facial mask glue of table
Antibacterial test result shows that the Siberian solomonseal rhizome polysaccharide facial mask glue that the present invention uses has good bacteriostasis, for
Various pathogens have good inhibiting effect, can be good at the growth for inhibiting staphylococcus aureus and Escherichia coli.It is single
Pure application Siberian solomonseal rhizome polysaccharide facial mask glue fungistatic effect is poor, and the facial mask rejection of both fit applications is more excellent.
<test 6: irritant experiment two>
The student enrollment of 16 skin healths is invited, boy student, schoolgirl are fifty-fifty, are respectively 401- by the number of above-mentioned preparation
404 film sample containing Siberian solomonseal rhizome polysaccharide, is pasted on the skin surface of left/right Medial upper arm softness, and other side arm is same
Alcohol wipe cleaning in position is used as blank control, and the change of skin at two is observed after 6h.
Positive controls: skin surface, as control, pastes time 6h using medical gelatin patch.Bonding method, sticky position
Set same Siberian solomonseal rhizome polysaccharide gel mask product.
After the test, it is independently scored by subject, code of points is as follows.
Nonirritant: skin keeps moist, it is no it is rubescent, play rash, get blister, without itch, pain, allergy phenomena such as.
It is given a mark 9-10 points according to skin state assessment.
Minimal irritation: after 12h, slight change, such as rubescent, rash, bubble, slight itch or mistake occur for skin colour
It is quick etc., belong in the degree that subject can endure, 4-8 points of assessment marking.
Serious irritation is detached from experiment: in experimentation, there is more serious irritation problem in subject, and experiment is automatic
Stop, subject voluntarily throws off face-mask material, seeking medical attention in necessary situation.Scoring 0-3 points of serious irritation result..
The marking for counting each subject is allocated as a result, being averaged as final irritant experiment appraisal result, specific feelings
Condition is as shown in the table.
7 rhizoma polygonati facial mask glue irritation test result of table corresponds to number
The irritation test result of rhizoma polygonati mask product shows the gel rubber plaster product of the invention containing rhizoma polygonati active constituent
With good skin compatibility, irritation adverse reaction will not be generated, for being of great significance according to application.With it is commercially available
Medical gelatin patch is compared, and the skin compatibility of gel rubber plaster product of the invention is more preferable, has more safety as mask product application
Advantage.
<embodiment 5>
Facial mask containing Siberian solomonseal rhizome polysaccharide
It prepares the gel glue of rhizoma polygonati facial mask: weighing xanthan gum 45g, add 20mL distilled water, be heated to 85 DEG C, sufficiently dissolve
Obtain clear gum liquid.Sodium carboxymethylcellulose 12g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, glycerol 4.2mL is added,
Propylene glycol 2.1mL, is uniformly mixed.Be added prepared by embodiment 201: Siberian solomonseal rhizome polysaccharide 13g, Rhizoma Atractylodis Macrocephalae tuckahoe extracts 6g are stirred
It mixes uniformly mixed.Methylparaben 0.4g is added, appropriate amount of essence is thoroughly mixed uniformly, obtains rhizoma polygonati facial mask glue.
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then above-mentioned rhizoma polygonati facial mask glue is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains the face containing Siberian solomonseal rhizome polysaccharide
Film.The rhizoma polygonati facial mask glue of non-woven fabrics load every square centimeter is about 1.2g.
<embodiment 6>
Facial mask containing Siberian solomonseal rhizome polysaccharide
It prepares the gel glue of rhizoma polygonati facial mask: weighing xanthan gum 55g, add 20mL distilled water, be heated to 90 DEG C, sufficiently dissolve
Obtain clear gum liquid.Sodium carboxymethylcellulose 13g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, it is added glycerol 4mL, third
Glycol 2mL, is uniformly mixed.The preparation of 202 method of embodiment is added: Siberian solomonseal rhizome polysaccharide 16g and Rhizoma Atractylodis Macrocephalae tuckahoe extracts 8g is stirred
It mixes uniformly mixed.Methylparaben 0.5g is added, appropriate amount of essence is thoroughly mixed uniformly, obtains rhizoma polygonati facial mask glue.
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then above-mentioned rhizoma polygonati facial mask glue is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains the face containing Siberian solomonseal rhizome polysaccharide
Film.The rhizoma polygonati facial mask glue of non-woven fabrics load every square centimeter is about 1.2g.
<embodiment 7>
Facial mask containing Siberian solomonseal rhizome polysaccharide
It prepares the gel glue of rhizoma polygonati facial mask: weighing xanthan gum 52g, add 20mL distilled water, be heated to 83 DEG C, sufficiently dissolve
Obtain clear gum liquid.Sodium carboxymethylcellulose 15g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, it is added glycerol 4mL, third
Glycol 2mL, is uniformly mixed.202 method of embodiment preparation: Siberian solomonseal rhizome polysaccharide 16g and Rhizoma Atractylodis Macrocephalae tuckahoe extracts 5g, Buddhist is added
Hand extract 4g, is uniformly mixed.Methylparaben 0.4g is added, appropriate amount of essence is thoroughly mixed uniformly, obtains rhizoma polygonati
Facial mask glue.
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then above-mentioned rhizoma polygonati facial mask glue is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains the face containing Siberian solomonseal rhizome polysaccharide
Film.The rhizoma polygonati facial mask glue of non-woven fabrics load every square centimeter is about 1.3g.
<embodiment 8>
Facial mask containing Siberian solomonseal rhizome polysaccharide
It prepares the gel glue of rhizoma polygonati facial mask: weighing xanthan gum 40g, add 15mL distilled water, be heated to 88 DEG C, sufficiently dissolve
Obtain clear gum liquid.Sodium carboxymethylcellulose 14g is added, stirring and dissolving is abundant, is cooled to 50 DEG C, it is added glycerol 4mL, third
Glycol 2mL, is uniformly mixed.203 method of embodiment preparation: Siberian solomonseal rhizome polysaccharide 15g and Rhizoma Atractylodis Macrocephalae tuckahoe extracts 4g, gold is added
Honeysuckle flower extract 4g, is uniformly mixed.Methylparaben 0.5g is added, appropriate amount of essence is thoroughly mixed uniformly, obtains Huang
Smart facial mask glue.
Prepare non-woven fabrics, by non-woven fabrics as heating disinfection 15min in boiled water, takes out, scrape off water extra on non-woven fabrics
Point；Then above-mentioned rhizoma polygonati facial mask glue is cooled to 30 DEG C or so, is coated on non-woven fabrics, obtains the face containing Siberian solomonseal rhizome polysaccharide
Film.The rhizoma polygonati facial mask glue of non-woven fabrics load every square centimeter is about 1.1g.
Claims (10)
1. a kind of facial mask containing Siberian solomonseal rhizome polysaccharide, which is characterized in that including facial mask back sheet and coated on the gel on back sheet
Glue, the Chinese herbal medicine active component extract containing 5-50wt% in the gel glue, the Chinese herbal medicine active component extract
Include Siberian solomonseal rhizome polysaccharide extract.
2. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that the gel glue be include xanthan gum,
Made of distilled water, sodium carboxymethylcellulose and water-retaining agent.
3. as claimed in claim 2 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that xanthan gum, steaming in the gel glue
The ratio of distilled water, sodium carboxymethylcellulose and water-retaining agent is 38-42:13-15:14-16:5-7.
4. as claimed in claim 2 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that the gel glue is made by the following method
It is standby to obtain:
S101, xanthan gum is taken, distilled water is added, is heated to 85-95 DEG C, sufficiently dissolution obtains clear gum liquid；
S102, sodium carboxymethylcellulose is added, stirring and dissolving is abundant, is cooled to 45-55 DEG C, and water-retaining agent is added, and is stirred
It is even；
S103,0.1-0.5wt% methylparaben, 0-0.02wt% essence is added, is thoroughly mixed uniformly, obtains gel glue
Liquid.
5. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that contain 5- in the facial mask gel glue
The Chinese herbal medicine active component extract of 40wt%.
6. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that the Siberian solomonseal rhizome polysaccharide extract be by with
What lower method was extracted:
S201, a steaming rhizoma polygonati is taken, the water that 8-20 times is measured is added and decocts 1-4 times, 20-60 minutes each, combined extract is concentrated into
One steams the extracting solution of 0.7-2 times of weight of rhizoma polygonati；
S202, addition ethanol precipitation make the alcohol content of extracting solution reach 40v%, filtering precipitating, and filtrate adds the second of 95v% or more
Alcohol precipitating makes alcohol content reach 60v%, collects 60v% concentration of alcohol blanking liquid precipitate.
7. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that the Chinese herbal medicine active component extract is also
Include at least one of Rhizoma Atractylodis Macrocephalae tuckahoe extracts, Fructus Citri Sarcodactylis extract, Honegsukle flower P.E.
8. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that the Chinese herbal medicine active component extract packet
It includes: Siberian solomonseal rhizome polysaccharide at least 60%.
9. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that the Rhizoma Atractylodis Macrocephalae extract is by with lower section
What method was extracted:
S211, Rhizoma Atractylodis Macrocephalae is taken, cleaned, water decocts 1-3 times, and 20-60 minutes each, combined extract, filtrate is concentrated into 0.7-2
Times weight；
S212, addition ethanol precipitation make alcohol content reach 40%, are filtered to remove precipitating, and the ethyl alcohol that filtrate adds 95v% or more is heavy
Shallow lake makes alcohol content reach 60%, collects the sediment fraction of 60v% concentration of alcohol, obtains Rhizoma Atractylodis Macrocephalae extract.
10. as described in claim 1 containing the facial mask of Siberian solomonseal rhizome polysaccharide, which is characterized in that Rhizoma Atractylodis Macrocephalae tuckahoe extracts be by Rhizoma Atractylodis Macrocephalae and
Poria cocos extracts the extract being prepared together.
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| CN108451862A (en) * | 2018-06-26 | 2018-08-28 | 成都中医药大学 | A kind of facial cleanser and preparation method thereof containing sealwort with moisturizing repair function |
| CN109652239A (en) * | 2018-11-27 | 2019-04-19 | 安徽省玉兔日用化学品有限公司 | A kind of amino acid perfumed soap and its processing technology containing Rhizoma Polygonati extract |
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| CN105153319A (en) * | 2014-06-05 | 2015-12-16 | 上海家化联合股份有限公司 | Rhizoma polygonati beta-galactan, preparation method thereof, and application to anti-inflammatory aspect |
| CN106243241A (en) * | 2015-06-03 | 2016-12-21 | 上海家化联合股份有限公司 | The preparation of a kind of Rhizoma Polygonati Pectic polysaccharides and application |
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