CN110478262A - Sea-buckthorn shampoo and preparation method thereof - Google Patents
Sea-buckthorn shampoo and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/00—Cosmetics or similar toiletry preparations
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Abstract
The invention discloses a kind of sea-buckthorn shampoos and preparation method thereof, belong to shampoo technical field.The present invention extracts flavones and other nutriments in Leaves of Hippophae L powder using in-situ extraction technology and Micellar Solubilization method, develops shampoo using Leaves of Hippophae L and Seabuckthorn Oil as main component.This method not only improves flavonoids extraction rate of seabuckthorn leave, and a kind of environmentally protective, natural, efficient seabuckthorn leaf flavonoid extraction method.The sea-buckthorn shampoo comprehensive performance that the present invention develops is good, feeds back after most triers experience, sea-buckthorn leaves shampoo is the advanced shampoo for integrating cleaning, anticreep, conditioning and maintenance.
Description
Technical field
The invention belongs to shampoo technical fields, and in particular to a kind of sea-buckthorn shampoo and preparation method thereof.
Background technique
Sea-buckthorn (Sea-Buckthorn) is commonly called as arrow-leaved oleaster, black thorn, sour thorn willow etc., is a kind of Elaeangnaceae acid thorn category fallen leaves filling
Wood or dungarunga；Branch is grey, spinosity, orange-yellow oval fruits.Sea-buckthorn is a kind of non-pulse family nitrogen-fixing plants, root system is complicated,
It is cold-resistant, drought-enduring, sprouting ability is very strong.Usually as the important selection for soil erosion of checking winds and fixing drifting sand, reduce, to improvement soil texture
With stablize ecosystem ecological significance with higher.Simultaneously again because the bioactive substance content of sea-buckthorn is very high, nutrition
Composition is extremely abundant, is often taken as a kind of function plant of integration of drinking and medicinal herbs.Research shows that the flavones and flavonoids that contain in sea-buckthorn
Substance has antibacterial, antiviral, antiulcer, anti-aging, anti-radiation effect, also has to cardiovascular disease and tumour good pre-
Anti- effect was once widely used in Chinese medicine, Tibetan medicine and anaesthetic in Ancient Times in China, and modern sea-buckthorn also develops the battalion of many high assignments
Product is supported, there are many health care product, fruit drink, jam, candy, fruit wine, fruit tea and the fructus hippophaes using sea-buckthorn exploitation in the market
The products such as powder.In recent years, the characteristics of many chemical product researchers have nourishing and maintenance effect to skin according to Seabuckthorn Oil, develops
Many daily necessities, such as sea-buckthorn nurse oil, seabuckthorn essential oil, sea-buckthorn bath foam, sea-buckthorn handmade soap, these products are also because its is good anti-
Welcome of the advantages that aging, anti-oxidant, Nantural non-toxic are done harm to by the majority of consumers.
Currently, returning ecology, return to naturally, nutriment is extracted from natural plants, using green made of herbal essences
Color plant shampoo, more by the favor of numerous consumers.Analogy educates red et al. use microwave method and has obtained the effective ingredient of Chinese herbal medicine, and
Shampoo is added it to, Chinese medicinal herb nutrient scalp care hair shampoo has been made；Luo Mengjun et al. is extracted using Hot water extraction
Nutritional ingredient in green tea, and the extracting solution is added in shampoo, it has developed the good green tea of a comprehensive performance and washes
Hair-care shampoo；Zhao Yongguang et al. uses total flavonoids from platycladus orientalis leaves extracting solution for curative effect agent, is developed into the anti-dandruff anti-drop function of cacumen biotae and washes
Hair-care shampoo.Research shows that injection Vitamin B_6 can do good hair quality nutrient solution in sea-buckthorn, flavonoids can promote in hair shampoo article
Natural on-off cycles of hair growth prevents hair loss, and improves hair quality.Seabuckthorn Oil main component is tocopherol, carrotene and a large amount of unsaturated fat
Acid, phytosterol and free amino acid etc., while also containing the microelement of multiple beneficial.The tocopherol pair contained in Seabuckthorn Oil
Human skin and scalp have protective effect, can prevent quilt under the conditions of light, heat and radiation of the unsaturated fatty acid in cell membrane
Oxidation, to prevent the accumulation of lipofuscin；Beta carotene can be directly entered epidermal cell by scalp, and be converted into dimension life
Plain E and nourish hair quality, the cuticula of maintenance hair；Free amino acid has good nutrition and protection to make skin and hair
With.One of root of hair blood flow is obstructed the main reason for being most people alopecia.The oriented hair follicle tissue of blood of human body is defeated
Blood can be transported to papilla by the effect for sending nutriment, the netted capillary for surrounding hair follicle, if by extraneous thorn
Swashing and interference, the quantity of netted capillary will be reduced, conveys the function reduction of nutrition, hair follicle will lack nutrition,
To suffer from baldness, main nutrient composition is flavones and flavonoid substances in Leaves of Hippophae L, and flavones can activate hair root
Hair matricyte strengthens blood circulation, brings back to life hair follicle, restore and improve the ability of hair growth, after promoting blood circulation
Nutritional ingredient is provided to hair follicle tissue, to play the effect of hair care, hair tonic.Therefore after Leaves of Hippophae L is added in shampoo,
Its effective component acts on scalp surface, makes scalp surface relaxation, so as to make the netted capillary vessel number of hair root tip
The effect of amount increases, and the blood flow of conveying increases, generates Anti-hair loss.The mechanism of anti-dandruff and itching-relieving is to inhibit hair epidermal cell
The speed of degeneration, delay fall off.Though the heavy metallic salts such as general anti-dandruff and itching-relieving agent selenium class can achieve the goal, increase depilation phenomenon
It is more, antibacterial anti-inflammatory, antipruritic anti-dandruff Anti-hair loss and side effect can be generated with natural plants herbal substances.
Currently, existing shampoo is primarily present following deficiency, and first, it is unreasonable due to being formulated, it is easy scurf of starting；
Second, only have single hair washing function, it is obvious to wash the dry withered sense in back；Third lacks the nursing function to scalp, often goes out
Existing itching of the scalp and hair loss phenomenon.
Summary of the invention
The purpose of the present invention is to solve the deficiencies in the prior art, and provide a kind of sea-buckthorn shampoo and its preparation side
Method.
The present invention adopts the following technical scheme:
Sea-buckthorn shampoo, in terms of every 500mL sea-buckthorn shampoo, including following component:
Sodium sulfate of polyethenoxy ether of fatty alcohol 45-50g, the Cocoamidopropyl betaine aqueous solution that mass fraction is 35%
20g, the CAD cocounut oil acyl both sexes diethyl acid disodium 30g of content 40%, cocounut oil diglycollic amide 12g, coconut monoethanol amide 9g,
Pungent Plantacare 818 aqueous solution 30g, glycerol 9-15g, pearly-lustre raw material 30g, olive oil 10g, dimethylbenzene of the mass fraction for 60%
Sodium sulfonate 15g, cationic melon rubber 0.9g, Polyquaternium-10 1.5g, PEG-120 methyl glucosamine dioleate 1.5g, sun
Ion panthenol 2.5mL, disodium EDTA 0.3-0.5g, essence 4mL, Leaves of Hippophae L powder 12.5-15g, Kathon CG CG
15-20mL, Seabuckthorm Seed Oil 5g, water surplus, appropriate citric acid, the citric acid are used for regulation system pH.
In some of embodiments, the pearly-lustre raw material is pearlescent flake or pearlite slurry.
The present invention also provides a kind of sea-buckthorn shampoos, further include lauryl sodium sulfate 12g, sodium lauroyl sarcosine
6g。
The present invention also provides a kind of sea-buckthorn shampoos, further include dried peppermint leaf powder 10g.
The present invention also provides the preparation methods of the sea-buckthorn shampoo described in one kind, include the following steps:
Step 1: being first added to the water dissolution for EDTA, sequentially adds primary surfactant fatty alcohol polyoxyethylene ether sulfuric acid
Sodium, CAD cocounut oil acyl both sexes diethyl acid disodium, cocounut oil diglycollic amide, coconut monoethanol amide, are heated to 65-70 while stirring
DEG C, constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirring and dissolving；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl that mass fraction is 60% is sequentially added
Glucoside aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternary amine of the mass fraction for 35%
Salt -10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: it is cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then uses lemon
Acid for adjusting pH adds deionized water to 480mL scale, stirs to 6.3-6.8；
Step 4: being cooled to 35-40 DEG C, and Leaves of Hippophae L powder is added in batches under constant stirring, then is added in batches
Seabuckthorm Seed Oil, then plus deionized water to 500mL scale, after charging, continue to stir 40-50min, can discharge.
In some of embodiments, the cation guar gum of every 0.9g is dissolved by pre-dispersed finger described in step 1 in advance
In the water of 10g.
When using lemon acid for adjusting pH in some of embodiments, described in step 3, first citric acid is dissolved with water.
The present invention also provides a kind of preparation methods of sea-buckthorn shampoo, include the following steps:
Step 1: being first added to the water dissolution for EDTA, sequentially adds primary surfactant fatty alcohol polyoxyethylene ether sulfuric acid
Sodium, CAD cocounut oil acyl both sexes diethyl acid disodium, lauryl sodium sulfate, sodium lauroyl sarcosine, cocounut oil diglycollic amide, cocounut oil
Single ethanol amide, is heated to 65-70 DEG C while stirring, and constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirs
Mix dissolution；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl that mass fraction is 60% is sequentially added
Glucoside aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternary amine of the mass fraction for 35%
Salt -10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: it is cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then uses lemon
Acid for adjusting pH adds deionized water to 480ml scale, stirs to 6.3-6.8；
Step 4: being cooled to 35-40 DEG C, and Leaves of Hippophae L powder is added in batches under constant stirring, then is added in batches
Seabuckthorm Seed Oil, then plus deionized water to 500ml scale, after charging, continue to stir 40-50min, can discharge.
The present invention also provides a kind of preparation methods of sea-buckthorn shampoo, include the following steps:
Step 1: being first added to the water dissolution for EDTA, sequentially adds primary surfactant fatty alcohol polyoxyethylene ether sulfuric acid
Sodium, CAD cocounut oil acyl both sexes diethyl acid disodium, lauryl sodium sulfate, sodium lauroyl sarcosine, cocounut oil diglycollic amide, cocounut oil
Single ethanol amide, is heated to 65-70 DEG C while stirring, and constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirs
Mix dissolution；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl that mass fraction is 60% is sequentially added
Glucoside aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternary amine of the mass fraction for 35%
Salt -10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: it is cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then uses lemon
Acid for adjusting pH adds deionized water to 480ml scale, stirs to 6.3-6.8；
Step 4: being cooled to 35-40 DEG C, and Leaves of Hippophae L powder, dried peppermint leaf powder are added in batches under constant stirring, then
Be added Seabuckthorm Seed Oil in batches, then plus deionized water to 500ml scale, after charging, continue to stir 40-50min, can go out
Material.
Compared with prior art, the present invention has the advantages that: shampoo of the invention is by a variety of surfactants
It compounds, the composition of surfactant has conclusive effect to the colloidal nature of shampoo, foam property.The present invention passes through
Comparative test is selected with sodium sulfate of polyethenoxy ether of fatty alcohol, Cocoamidopropyl betaine, cocounut oil acyl both sexes diethyl acid disodium
For primary surfactant, cocounut oil diglycollic amide, coconut monoethanol amide are as stabilizer, not only foam uniform and smooth, but also
This micella composition is conducive to the dissolution of Leaves of Hippophae L active constituent, realizes the in-situ extraction of active seabuckthorn ingredient, realizes Leaves of Hippophae L
The powder even direct use of dried peppermint leaf powder.
Detailed description of the invention
Fig. 1 is primary SEM figure；
Fig. 2 is the SEM figure that 4 gained shampoo of the embodiment of the present invention washes hair.
Specific embodiment
The preferred embodiment of the present invention is described in detail with reference to the accompanying drawing, so that advantages and features of the invention energy
It is easier to be readily appreciated by one skilled in the art, so as to make a clearer definition of the protection scope of the present invention.
Sea-buckthorn shampoo, in terms of every 500mL sea-buckthorn shampoo, including following component:
Sodium sulfate of polyethenoxy ether of fatty alcohol 45-50g, the Cocoamidopropyl betaine aqueous solution that mass fraction is 35%
20g, the CAD cocounut oil acyl both sexes diethyl acid disodium 30g of content 40%, cocounut oil diglycollic amide 12g, coconut monoethanol amide 9g,
Pungent Plantacare 818 aqueous solution 30g, glycerol 9-15g, pearly-lustre raw material 30g, olive oil 10g, dimethylbenzene of the mass fraction for 60%
Sodium sulfonate 15g, cationic melon rubber 0.9g, Polyquaternium-10 1.5g, PEG-120 methyl glucosamine dioleate 1.5g, sun
Ion panthenol 2.5mL, disodium EDTA 0.3-0.5g, essence 4mL, Leaves of Hippophae L powder 12.5-15g, Kathon CG CG
15-20mL, Seabuckthorm Seed Oil 5g, water surplus, appropriate citric acid, the citric acid are used for regulation system pH.
In some of embodiments, the pearly-lustre raw material is pearlescent flake or pearlite slurry.
The present invention also provides a kind of sea-buckthorn shampoos, further include lauryl sodium sulfate 12g, sodium lauroyl sarcosine
6g。
The present invention also provides a kind of sea-buckthorn shampoos, further include dried peppermint leaf powder 10g.
The present invention also provides the preparation methods of the sea-buckthorn shampoo described in one kind, include the following steps:
Step 1: being first added to the water dissolution for EDTA, sequentially adds primary surfactant fatty alcohol polyoxyethylene ether sulfuric acid
Sodium, CAD cocounut oil acyl both sexes diethyl acid disodium, cocounut oil diglycollic amide, coconut monoethanol amide, are heated to 65-70 while stirring
DEG C, constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirring and dissolving；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl that mass fraction is 60% is sequentially added
Glucoside aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternary amine of the mass fraction for 35%
Salt -10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: it is cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then uses lemon
Acid for adjusting pH adds deionized water to 480mL scale, stirs to 6.3-6.8；
Step 4: being cooled to 35-40 DEG C, and Leaves of Hippophae L powder is added in batches under constant stirring, then is added in batches
Seabuckthorm Seed Oil, then plus deionized water to 500mL scale, after charging, continue to stir 40-50min, can discharge.
In one embodiment, the cation guar gum of every 0.9g is dissolved by pre-dispersed finger described in step 1 in advance
In the water of 10g.
In one embodiment, when using lemon acid for adjusting pH described in step 3, first citric acid is dissolved with water.
The present invention also provides the preparation methods of another sea-buckthorn shampoo, include the following steps:
Step 1: being first added to the water dissolution for EDTA, sequentially adds primary surfactant fatty alcohol polyoxyethylene ether sulfuric acid
Sodium, CAD cocounut oil acyl both sexes diethyl acid disodium, lauryl sodium sulfate, sodium lauroyl sarcosine, cocounut oil diglycollic amide, cocounut oil
Single ethanol amide, is heated to 65-70 DEG C while stirring, and constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirs
Mix dissolution；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl that mass fraction is 60% is sequentially added
Glucoside aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternary amine of the mass fraction for 35%
Salt -10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: it is cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then uses lemon
Acid for adjusting pH adds deionized water to 480ml scale, stirs to 6.3-6.8；
Step 4: being cooled to 35-40 DEG C, and Leaves of Hippophae L powder is added in batches under constant stirring, then is added in batches
Seabuckthorm Seed Oil, then plus deionized water to 500ml scale, after charging, continue to stir 40-50min, can discharge.
The present invention also provides the preparation methods of another sea-buckthorn shampoo, include the following steps:
Step 1: being first added to the water dissolution for EDTA, sequentially adds primary surfactant fatty alcohol polyoxyethylene ether sulfuric acid
Sodium, CAD cocounut oil acyl both sexes diethyl acid disodium, lauryl sodium sulfate, sodium lauroyl sarcosine, cocounut oil diglycollic amide, cocounut oil
Single ethanol amide, is heated to 65-70 DEG C while stirring, and constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirs
Mix dissolution；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl that mass fraction is 60% is sequentially added
Glucoside aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternary amine of the mass fraction for 35%
Salt -10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: it is cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then uses lemon
Acid for adjusting pH adds deionized water to 480ml scale, stirs to 6.3-6.8；
Step 4: being cooled to 35-40 DEG C, and Leaves of Hippophae L powder, dried peppermint leaf powder are added in batches under constant stirring, then
Be added Seabuckthorm Seed Oil in batches, then plus deionized water to 500ml scale, after charging, continue to stir 40-50min, can go out
Material.
Primary raw material and reagent used in the present invention are as shown in the table:
1 primary raw material of table and reagent
Wherein, pearlescent flake CAS NO.:111-60-4, Guangzhou Hua Zhiwang Chemical Co., Ltd., 500g.
Pearlite slurry: Shandong You Suo Chemical Industry Science Co., Ltd, content 35%, 500g.
Sodium xylene sulfonate CAS NO.:1300-72-7, Shandong You Suo Chemical Industry Science Co., Ltd, content 40%, 600g.
Raw materials used proportion is as follows in each embodiment:
The 2 raw materials used proportion of each embodiment of table
The configuration criteria of shampoo of the invention: 1. safety is good, and pH value control is 6.5 or so (with human body scalp pH
It is close) it is non-stimulated to eyes, skin；2. foam performance is good, foaming abundancy；3. moderate viscosity, appearance exquisiteness is soft, and fragrance is pure and fresh
Comfortably；4. Anti-hair loss has good maintenance function；5. have good hair conditioning, can make hair it is submissive it is smooth, do not knot；6. having
Good moisture retention nourishes hair, keeps hair glossy.
It is found during completing the present invention, during finished product storage, observes the solid for having white in bottom of bottle portion
Always it is not dissolved, very influences the beauty of shampoo and using feeling.The dosage of the fine or not and pearling agent of pearl effect adds
Enter that speed, cooling velocity, raw material composition etc. has relationship in formula.The pearling agent of sheet, following factor are used in the present invention
It is bad all to may cause pearly-lustre: the 1. effect quality of surface active agent solubilization；It, cannot be sufficiently molten 2. the medium oil ingredient of system is excessive
Solve pearlescent flake；3. temperature when being added is too low, dissolve insufficient；4. mixing time is not enough or pearlescent flake particle too greatly cannot be complete
It is complete to melt.To solve the problems, such as that pearlescent flake dissolves, many measures are taken.Firstly, temperature when this ingredient is added is improved,
The time that order of addition shifts to an earlier date to make to stir and dissolve extends, but there is no this phenomenon is thoroughly changed, then by pearlescent flake
The problem of grinding ratio that is finely ground, and improving cosolvent using advance, being just addressed pearlescent flake dissolution.
Therefore it should be noted that the compatibility between addition temperature, order of addition and each component of additive in component design,
Strict control technique is answered in preparation.
Meanwhile after carrying out test of many times, the preference temperature of discovery addition Leaves of Hippophae L is 35~37 DEG C.Leaves of Hippophae L is being had one's hair wash
Otherwise additive amount in shampoo formula is easy to appear layering no more than 10-12%.
The quality of shampoo, fine and smooth degree are related to the degree that it is emulsified, the mixing speed of magnetic stirrer when production
Control it is very crucial.Mixing speed is faster, and the solution rate of various additives is faster, and the interior phase dispersion of the product of synthesis is got over
It is good, but mixing speed is too fast, can bring numerous air-bubble into lotion, generate a large amount of foams, and then influence the stability of product；
Mixing speed is excessively slow, and additive cannot be sufficiently mixed uniformly, and will appear agglomeration lamination.Therefore it to be controlled in emulsification
Mixing speed is in 180r/min or so.
It finds, is placed in after the completion of production in brown bottle than being placed in black plastic bag covering during the experiment
Wide-mouth bottle color change more slowly, can preferably keep be added Leaves of Hippophae L activity, preferably extraction Leaves of Hippophae L in battalion
Support substance and effective component.This under the conditions of also side light is protected from light storage be a pass for preferably maintaining shampoo stability
Key factor.
Following performance detection is carried out to sea-buckthorn shampoo made from the embodiment of the present invention 4:
1, stability (pH, stickiness)
Product is placed on during wide-mouth bottle is kept in dark place from completing, and is measured a pH value every three days, is had no obvious change
Change, and viscosity also keeps stable, phenomena such as suspending, layering do not occur, illustrates that pH, stickiness keep stablizing.
2, heat resistance
Sea-buckthorn hair washing sample is poured into respectively in 2 clean test tubes, a test tube to be checked is put in tune after sealing up for safekeeping
In section to 50 DEG C of insulating box.It takes out, after restoring room temperature, is compared with the sample of any processing of another Zhi Weijing two days later,
Range estimation does not occur being layered and suspension phenomenon, and color, fragrance, appearance, viscosity and the pH state of shampoo are without influence, explanation
Product is heat-resist.
3, cold resistance
Sea-buckthorn shampoo sample is packed into two clean test tubes, seals up for safekeeping and is put into -4 DEG C of refrigerator cold-storage afterwards, two days
After take out, after restoring room temperature, the two by contrast after, range estimation occurs without layering and suspension phenomenon, the color of shampoo, fragrance, appearance,
Viscosity and pH state illustrate that product cold resistance is good without influence.
4, foaminess, hair conditioning
In the present invention other than anionic surfactant, it is also added into amino acid foaming agent sodium lauroyl sarcosine,
Measurement through Roche foam meter, as the content of amino acid foaming agent increases, the foam height of system is first increased and is reduced afterwards, explanation
Increase the content of amino acid foaming agent in a small range and AES, K12 are compounded, than anionic surfactant is used alone
Better foaming properties can be reached.Content through Experimental Research sodium lauroyl sarcosine in hair washing formula is advisable with 3%.
The indices testing result of 4 gained sea-buckthorn shampoo of embodiment is as shown in table 1 below:
1 indices testing result of table
| Index name | Index request | Sample evaluation result |
| Appearance | Foreign | Foreign |
| Fragrance | It is pure | It is pure |
| PH value | 4.0~8.0 | 6.3~6.8 |
| Viscosity (25 DEG C, Pas) | ≥0.4 | ≥0.4 |
| Effective substance (%) | ≥10.0 | ≥10.0 |
| Foam height (40 DEG C, cm) | ≥50.0 | ≥50.0 |
| Heat-resisting (50 DEG C, 48h) | Without precipitation and separation metachromatism | Without precipitation and separation metachromatism |
| Cold-resistant (- 4 DEG C, 48h) | It is normal to restore RT sample | It is normal to restore RT sample |
5, the using effect evaluation of sea-buckthorn shampoo
Product is on probation through 40 subjects, experiences its hair conditioning, moisture retention and Anti-hair loss effect etc..As the result is shown 87.5%
Trier's reflection it is good, Leaves of Hippophae L on the hair conditioning of shampoo, pH value, using feeling etc. substantially without influence；Sea-buckthorn is added
It can be reduced depilation phenomenon after leaf, maintenance conditioning effect is more preferable.It the results are shown in Table 2
Product is after 40 people's uses, and 96% reflects that the shampoo foaminess is good, and hair is washed rear submissive smooth, and scalp is salubrious
It is non-stimulated.Whatsoever crowd uses, and all generates without dandruff, has good opsonic action to hair.
Maintenance anticreep effect statistical form of 2 sea-buckthorn shampoo of table
The effect of in order to further verify shampoo of the present invention, by scanning electron microscope (SEM) to primary and through the present invention
The 4 processed hair of gained shampoo of embodiment is observed, as a result as depicted in figs. 1 and 2, it is seen that primary hair cuticula watt sample squama
Piece close-packed arrays, and through the processed hair of sea-buckthorn shampoo, surface is smooth, glossy, illustrates that the product correct can initiate
Nutrition, moisten effect.
The embodiments of the present invention are described in detail for above-described embodiment, but the present invention is not limited to above-mentioned embodiment party
Formula can also be done without departing from the purpose of the present invention within the knowledge of a person skilled in the art
Various change out.
Claims (9)
1. sea-buckthorn shampoo, which is characterized in that in terms of every 500mL sea-buckthorn shampoo, including following component:
Sodium sulfate of polyethenoxy ether of fatty alcohol 45-50g, mass fraction be 35% Cocoamidopropyl betaine aqueous solution 20g,
CAD cocounut oil acyl both sexes diethyl acid disodium 30g, cocounut oil diglycollic amide 12g, coconut monoethanol amide 9g, mass fraction 60%
Pungent Plantacare 818 aqueous solution 30g, glycerol 9-15g, pearly-lustre raw material 30g, olive oil 10g, sodium xylene sulfonate 15g, sun from
Sub- melon rubber 0.9g, Polyquaternium-10 1.5g, PEG-120 methyl glucosamine dioleate 1.5g, cationic panthenol 2.5mL,
Disodium EDTA 0.3-0.5 g, 4 mL of essence, Leaves of Hippophae L powder 12.5-15g, Kathon CG CG 15-20mL, seabuckthorn seeds
Oily 5g, water surplus, appropriate citric acid, the citric acid are used for regulation system pH.
2. sea-buckthorn shampoo according to claim 1, which is characterized in that the pearly-lustre raw material is pearlescent flake or pearl
Light slurry.
3. sea-buckthorn shampoo according to claim 1, which is characterized in that further include lauryl sodium sulfate 12g,
Sodium lauroyl sarcosine 6g.
4. sea-buckthorn shampoo according to claim 1, which is characterized in that further include dried peppermint leaf powder 10g.
5. the preparation method of sea-buckthorn shampoo described in claim 1, which comprises the steps of:
Step 1: being first added to the water dissolution for EDTA, sequentially add primary surfactant sodium sulfate of polyethenoxy ether of fatty alcohol,
CAD cocounut oil acyl both sexes diethyl acid disodium, cocounut oil diglycollic amide, coconut monoethanol amide, are heated to 65-70 DEG C while stirring,
Constant temperature adds pre-dispersed cationic melon rubber, stirring and dissolving to whole dissolutions；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl glucose that mass fraction is 60% is sequentially added
Glycosides aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternium-of the mass fraction for 35%
10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: being cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then with citric acid tune
PH to 6.3-6.8 is saved, adds deionized water to 480mL scale, stirs；
Step 4: being cooled to 35-40 DEG C, Leaves of Hippophae L powder is added in batches under constant stirring, then sea-buckthorn is added in batches
Seed oil, then plus deionized water to 500mL scale, after charging, continue to stir 40-50min, can discharge.
6. the preparation method of sea-buckthorn shampoo according to claim 5, which is characterized in that pre- described in step 1
Dispersion, which refers to, is in advance dissolved into the cation guar gum of every 0.9g in the water of 10g.
7. the preparation method of sea-buckthorn shampoo according to claim 5, which is characterized in that used described in step 3
When lemon acid for adjusting pH, first citric acid is dissolved with water.
8. the preparation method of sea-buckthorn shampoo as claimed in claim 3, which comprises the steps of:
Step 1: being first added to the water dissolution for EDTA, sequentially add primary surfactant sodium sulfate of polyethenoxy ether of fatty alcohol,
CAD cocounut oil acyl both sexes diethyl acid disodium, lauryl sodium sulfate, sodium lauroyl sarcosine, cocounut oil diglycollic amide, cocounut oil list second
Alkylolamides is heated to 65-70 DEG C while stirring, and constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirs molten
Solution；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl glucose that mass fraction is 60% is sequentially added
Glycosides aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternium-of the mass fraction for 35%
10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: being cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then with citric acid tune
PH to 6.3-6.8 is saved, adds deionized water to 480ml scale, stirs；
Step 4: being cooled to 35-40 DEG C, Leaves of Hippophae L powder is added in batches under constant stirring, then sea-buckthorn is added in batches
Seed oil, then plus deionized water to 500ml scale, after charging, continue to stir 40-50min, can discharge.
9. the preparation method of sea-buckthorn shampoo as claimed in claim 4, which comprises the steps of:
Step 1: being first added to the water dissolution for EDTA, sequentially add primary surfactant sodium sulfate of polyethenoxy ether of fatty alcohol,
CAD cocounut oil acyl both sexes diethyl acid disodium, lauryl sodium sulfate, sodium lauroyl sarcosine, cocounut oil diglycollic amide, cocounut oil list second
Alkylolamides is heated to 65-70 DEG C while stirring, and constant temperature to whole dissolutions adds pre-dispersed cationic melon rubber, stirs molten
Solution；
Step 2: when step 1 gained lotion is cooled to 55-60 DEG C, the pungent decyl glucose that mass fraction is 60% is sequentially added
Glycosides aqueous solution, pearly-lustre raw material, olive oil, Cocoamidopropyl betaine aqueous solution, polyquaternium-of the mass fraction for 35%
10, PEG-120 methyl glucosamine dioleate and glycerol, stirring and dissolving；
Step 3: being cooled to 43-48 DEG C of addition sodium xylene sulfonate, cationic panthenol, essence, Kathon CG CG, then with citric acid tune
PH to 6.3-6.8 is saved, adds deionized water to 480ml scale, stirs；
Step 4: being cooled to 35-40 DEG C, Leaves of Hippophae L powder, dried peppermint leaf powder is added in batches under constant stirring, then in batches
Secondary addition Seabuckthorm Seed Oil, then plus deionized water to 500ml scale, after charging, continue to stir 40-50min, can discharge.
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1490036A (en) * | 2003-08-27 | 2004-04-21 | 王敏达 | Chemical for promoting growth of hairs and preventnig sinility |
| CN1931124A (en) * | 2005-09-14 | 2007-03-21 | 戚善龙 | All-effect liquid shampoo |
| CN101474136A (en) * | 2009-01-16 | 2009-07-08 | 徐艳萍 | Shampoo composition |
| CN102885742A (en) * | 2012-11-06 | 2013-01-23 | 蒋亚飞 | Fleece flower root wet wipe for wiping hair and scalp and preparation method of fleece flower root wet wipe |
| CN103054779A (en) * | 2013-01-15 | 2013-04-24 | 李玉兰 | Bath foam and preparation method thereof |
| US20130344178A1 (en) * | 2012-06-22 | 2013-12-26 | Eun Joo KO | Natural shampoo using herbal medicine mature decoction having a function of preventing hair loss and stimulating hair growth, and method of preparing the same |
| CN108186511A (en) * | 2018-03-31 | 2018-06-22 | 佛山娇芙生物科技有限公司 | A kind of hippophae rhamnoides fruit oil Haircare composition |
-
2019
- 2019-09-18 CN CN201910883817.0A patent/CN110478262A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1490036A (en) * | 2003-08-27 | 2004-04-21 | 王敏达 | Chemical for promoting growth of hairs and preventnig sinility |
| CN1931124A (en) * | 2005-09-14 | 2007-03-21 | 戚善龙 | All-effect liquid shampoo |
| CN101474136A (en) * | 2009-01-16 | 2009-07-08 | 徐艳萍 | Shampoo composition |
| US20130344178A1 (en) * | 2012-06-22 | 2013-12-26 | Eun Joo KO | Natural shampoo using herbal medicine mature decoction having a function of preventing hair loss and stimulating hair growth, and method of preparing the same |
| CN102885742A (en) * | 2012-11-06 | 2013-01-23 | 蒋亚飞 | Fleece flower root wet wipe for wiping hair and scalp and preparation method of fleece flower root wet wipe |
| CN103054779A (en) * | 2013-01-15 | 2013-04-24 | 李玉兰 | Bath foam and preparation method thereof |
| CN108186511A (en) * | 2018-03-31 | 2018-06-22 | 佛山娇芙生物科技有限公司 | A kind of hippophae rhamnoides fruit oil Haircare composition |
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