CN110396323A - A kind of high-concentration negative oxygen ion material and preparation method thereof - Google Patents
A kind of high-concentration negative oxygen ion material and preparation method thereof Download PDFInfo
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- CN110396323A CN110396323A CN201910727916.XA CN201910727916A CN110396323A CN 110396323 A CN110396323 A CN 110396323A CN 201910727916 A CN201910727916 A CN 201910727916A CN 110396323 A CN110396323 A CN 110396323A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/221—Oxides; Hydroxides of metals of rare earth metal
- C08K2003/2213—Oxides; Hydroxides of metals of rare earth metal of cerium
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Abstract
The present invention relates to a kind of high-concentration negative oxygen ion materials, by weight, including following raw material components: 15-40 parts of germanium, 1-5 parts of cerium oxide, 1-5 parts of rare earth ytterbium, 1-5 parts of rare earth terbium, Tourmaline 10-40,10-40 parts of pelelith；Preparation method includes step 1 grinding；Step 2 prepares rare earth terbium, rare earth ytterbium particle；Step 3 prepares mixture；Step 4 mixture pelleting；Step 5 mixture calcines to obtain a kind of high-concentration negative oxygen ion material.The beneficial effects of the present invention are: high-concentration negative oxygen ion of the invention, which generates material itself, can give off high-frequency energy shock wave, release high-concentration negative oxygen ion, pass through neutralization, remove the intracorporal free radical of people, promote the metabolic function of human body cell, it delays senescence, enhances Lymphatic Circulation, promote blood circulation of human body.
Description
Technical field
The invention belongs to field of material technology, and in particular to a kind of high-concentration negative oxygen ion material and preparation method thereof and answer
With.
Background technique
It is exactly to aoxidize that life science, which has solved bright disease and the basic reason of aging, and preventing the substance of oxidation is exactly reducing agent,
For life science, antioxidant is exactly healthy material.The indispensable grain of the mankind, meat, sugar and food additives etc. are sour
Property substance be actually sometimes also oxide harmful to health.The reason of excessive fatigue is also oxidation, cation accelerated oxidation
Reaction, pollution air contain a large amount of cation.So people feel very ill, people is allowed to feel comfortable and be conducive to health
Be negative oxygen ion.
Negative oxygen ion plays an important role to the physiological function of people, when negative oxygen ion concentration is greater than 1000/cm3When, have
Beneficial to human health and longevity, sleeps, reduces blood pressure, boosting metabolism, improve immunity, mitigate because it can play improvement
Many wholesome effects such as fatigue, raising working efficiency, pure and fresh purification air.
The functional material of releasing negative oxygen ion is the very useful far infrared emitting material of a kind of pair of human health, can quilt
Applied to multiple fields such as building, environmental protection, weavings, provided for daily life a kind of actual, completely new, multi-faceted
Health care.At present common negative oxygen ion material use negative oxygen ion generation material is directly added into ceramics be made bear from
Sub- ceramic material, since common negative oxygen ion generates, the places of production such as material such as tourmaline, opal are rare, and it is expensive
And it radiates exceeded etc..This just significantly limits the large-scale application that the negative oxygen ions such as tourmaline generate material.Using artificial
Synthesis negative oxygen ion, which generates material, can not only reduce the production cost of negative oxygen ion ceramic material, will also greatly promote negative oxygen from
The large-scale application of subfunction material.
Summary of the invention
For an object of the present invention there is provided a kind of high-concentration negative oxygen ion material, it is negative which can release high concentration
Oxonium ion, this high-concentration negative oxygen ion remove the intracorporal free radical of people, promote the metabolism of human body cell by neutralization
Function delays senescence, and enhances Lymphatic Circulation, promotes blood circulation of human body；Simultaneously because 3000 degree of high temperature puffing techniques are used,
The radioactivity in minerals is effectively removed, the safety of product is improved.
To achieve the goals above, the present invention adopts the following technical scheme that:
A kind of high-concentration negative oxygen ion material, it is characterised in that: by weight, including following raw material components: 35 parts of germanium, dilute
1 part of native ytterbium, 2 parts of rare earth terbium, 35 parts of Tourmaline, 30 parts of pelelith.
Preferably, a kind of high-concentration negative oxygen ion material, it is characterised in that: by weight, including following components: germanium
35 parts, 5 parts of cerium oxide, 1 part of rare earth ytterbium, 2 parts of rare earth terbium, 30 parts of Tourmaline, 30 parts of pelelith.
The second object of the present invention is to provide a kind of preparation method of high-concentration negative oxygen ion material.It is characterized by:
Include the following steps:
Step 1 grinding: rare earth ytterbium, rare earth terbium are respectively placed in grinder fineness of grind partial size no more than 300 mesh, obtained
300 mesh rare earth terbiums, rare earth ytterbium powder, it is spare；
Step 2 prepares rare earth terbium, rare earth ytterbium particle: rare earth ytterbium is made to the particle of partial size 0.8-1mmd, rare earth terbium powder system
It is spare at the particle of 2--3mmd；
Step 3 prepares mixture: by setting parts by weight by spare 35 parts of the germanium that weighs of step 1,5 parts of cerium oxide, support
30 parts of Ma beautiful jade, 30 parts of pelelith be crushed to 100 mesh or so be placed in blender with 600r/min stirring 15-30 minutes, obtain uniformly
Mixture, it is spare；
Step 4 mixture: by weight percentage by step 3 preliminary mixture, step 3 preliminary mixture mixture weight
70 parts of amount adds 30 parts of tap water to be uniformly mixed, spare；
The calcining of step 5 mixture: the spare mixture of step 4 is placed in 2950-3000 DEG C of vacuum furnace and is forged
Spare 1 part of rare earth terbium particle weight of injection step two when being cooled to 1350 DEG C after burning 8-10 hours, note when being cooled to 800 DEG C
Enter 1 part of the spare rare earth ytterbium particle weight of step 2, injects 60 parts of water when being cooled to 20 DEG C, 50 mesh steel of bell are opened after half an hour
Net filtration is up to a kind of high-concentration negative oxygen ion material coarse fodder.
Step 6 grinding: coarse fodder obtained by step 5 is placed in grinder and is ground to 1250 mesh and remembers one needed for the present invention
Kind high-concentration negative oxygen ion material.
Step 7 recovering rare earth ytterbium and rare earth terbium: recovering rare earth ytterbium and rare earth terbium from the residue of step 5.
The beneficial effects of the present invention are: 1, of the invention high-concentration negative oxygen ion, which generate material itself, can give off high frequency
Energy shock wave, this material can release high-concentration negative oxygen ion, and this high-concentration negative oxygen ion is acted on by charge neutrality,
The intracorporal free radical of people is removed, the metabolic function of human body cell is promoted, is delayed senescence, Lymphatic Circulation is enhanced, promotes blood of human body
Circulation.2, high-concentration negative oxygen ion material of the invention can release negative oxygen ion, per cubic centimeter to can reach 60000-90000
It is a, reach as high as 90000 or more.It is equivalent to the concentration of our negative oxygen ions in virgin forest.This material can release
High-concentration negative oxygen ion, this high-concentration negative oxygen ion remove the intracorporal free radical of people by neutralization, promote human body thin
The metabolic function of born of the same parents delays senescence, and enhances Lymphatic Circulation, promotes blood circulation of human body；Can effective human activin enzyme system, it is extensive
Multiple cell proper motion, to promote removing toxic substances and the functions of expelling toxin of human body itself；General nutriment can be easily passed through to be not easy
By blood-brain barrier, it is oxidation resistant especially into playing the role of in brain hence into the inside of various tissues.3, and often
The negative oxygen ion ceramic material seen is compared, and negative oxygen ion ceramic material releasing negative oxygen ion concentration per cubic centimeter generally exists
3000 hereinafter, the negative oxygen ion energy that discharges of high-concentration negative oxygen ion material of the invention is strong, concentration is high, it is per cubic centimeter
Concentration reaches as high as 60000 or more.And the duration is longer.
There are 32 electronics around germanium atom core, 4 electronics on outermost siding track do irregular movement.Once in temperature
It rises, an electronics on outermost siding track will leave the right or normal track because stimulated.And facilitate adjustment biology departing from the electronics of track
Ionic equilibrium, keep the abnormal restoring of body neuron circuit normal, have prevent and improve body sense of discomfort and massage hot spring
Effect and other effects.Germanium is there are also the function of the abnormal current potential of adjustment human body, and when cancer cell current potential is ramping up, Germanium can be captured
The electronics of cancer cell declines its current potential, inhibits the deterioration of illness.
Germanium itself can releasing negative oxygen ion, but the duration is not grown, and only higher (when 40 or more) Celsius in temperature
It could releasing negative oxygen ion.After rare earth is added in formula, since rare earth material has very strong energy, germanium, cerium can be activated
The activity of equal substances, make its at normal temperature material also can sustained release negative oxygen ion, this material can release the negative oxygen of high concentration
Ion, this high-concentration negative oxygen ion remove the intracorporal free radical of people, promote the metabolism function of human body cell by neutralization
Can, it delays senescence, enhances Lymphatic Circulation, promote blood circulation of human body.
Specific embodiment
Property content is described in further detail for the essence of the present invention With reference to embodiment.
Embodiment 1
Releasing negative oxygen ion is prepared up to 3000-3200 negative oxygen ion negative oxygen ion dope for inner wall of architecture:
Material component: A material (high-concentration negative oxygen ion material): by weight, including following components: 35 parts of germanium, oxygen
Change 5 parts of cerium, 1 part of rare earth ytterbium, 2 parts of rare earth terbium, 30 parts of Tourmaline, 30 parts of pelelith.
B material (dope for inner wall of architecture): by weight, including following components: 260 parts of styrene-acrylic emulsion, partial size are not more than
The anatase titanium dioxide titanium of 800 mesh is not more than the wollastonite of 800 mesh from 180 parts of powder, partial size no more than 100 parts of kaolin, the partial size of 800 mesh
80 parts, partial size no more than 50 parts of the dicalcium powders of 800 mesh, partial size no more than 800 mesh (5040) 8 parts of 50 parts of talcum powder, dispersing agent,
12 parts of alcohol ester, 4 parts of thickener (TT-935), defoaming agent, 2,2 parts of pH adjusting agent (AMP-95), 220 parts of tap water.
Preparation method
A material (high-concentration negative oxygen ion material) preparation method: include the following steps:
Step 1 grinding: rare earth ytterbium, rare earth terbium are respectively placed in grinder fineness of grind partial size no more than 300 mesh, obtained
300 mesh rare earth terbiums, rare earth ytterbium powder, it is spare；
Step 2 prepares rare earth terbium, rare earth ytterbium particle: rare earth ytterbium is made to the particle of partial size 0.8-1mmd, rare earth terbium powder system
It is spare at the particle of 2--3mmd；
Step 3 prepares mixture: by setting parts by weight by spare 35 parts of the germanium that weighs of step 1,5 parts of cerium oxide, support
30 parts of Ma beautiful jade, 30 parts of pelelith be crushed to 100 mesh or so be placed in blender with 600r/min stirring 15-30 minutes, obtain uniformly
Mixture, it is spare；
Step 4 mixture: by weight percentage by step 3 preliminary mixture, step 3 preliminary mixture mixture weight
70 parts of amount adds 30 parts of tap water to be uniformly mixed, spare；
The calcining of step 5 mixture: the spare mixture of step 4 is placed in 2950-3000 DEG C of vacuum furnace and is forged
Spare 1 part of rare earth terbium particle weight of injection step two when being cooled to 1350 DEG C after burning 8-10 hours, note when being cooled to 800 DEG C
Enter 1 part of the spare rare earth ytterbium particle weight of step 2, injects 60 parts of water when being cooled to 20 DEG C, 50 mesh steel of bell are opened after half an hour
Net filtration is up to a kind of high-concentration negative oxygen ion material coarse fodder.
Step 6 grinding: coarse fodder obtained by step 5 is placed in grinder and is ground to 1250 mesh and remembers one needed for the present invention
Kind high-concentration negative oxygen ion material.
Step 7 recovering rare earth ytterbium and rare earth terbium: recovering rare earth ytterbium and rare earth terbium from the residue of step 5.
B material (dope for inner wall of architecture) preparation method: include the following steps:
Step 1 prepares water-borne dispersions: by the parts by weight tap water 220kg of setting, dispersing agent (5040) 8kg, defoaming
Agent 2kg is mixed evenly, and the height that partial size is not more than 800 mesh no more than anatase thpe white powder 180kg, the partial size of 800 mesh is added
Dicalcium powder 50kg, the partial size that ridge soil 100kg, partial size are not more than 800 mesh no more than wollastonite 80kg, the partial size of 800 mesh are not more than
It is spare to obtain homogeneous aqueous's dispersion with 1300- 1700r/min high-speed stirred 30 minutes by the talcum powder 50kg of 800 mesh；
The preparation of step 3 finished product: styrene-acrylic emulsion (styrene-the third is added in the spare water-borne dispersions of step 2 under stiring
Olefin(e) acid ester lotion) 220kg, it adds 12 10kg of alcohol ester, thickener (TT-935) 4kg, pH adjusting agent (AMP-95) 2kg and stirs
30 minutes are mixed to get a kind of white nano rare earth dope for inner wall of architecture；Or red, yellow and other color pigment are added as needed
Or colorant stirs evenly the nano rare earth dope for inner wall of architecture to get a kind of red color or yellow color and other colors.
By above-mentioned A material (high-concentration negative oxygen ion material) and B material (dope for inner wall of architecture): (high concentration is negative for A material
Oxonium ion material) 10 parts 90 parts of B material (dope for inner wall of architecture) is added and obtains releasing negative oxygen ion up to 3000 negative oxygen
Ion dope for inner wall of architecture.
Embodiment 2
Releasing negative oxygen ion is prepared up to 4000-4200 negative oxygen ion negative oxygen ion dope for inner wall of architecture:
A material (high-concentration negative oxygen ion material) and B material (dope for inner wall of architecture) and preparation preparation method and embodiment 1
It is identical.
By above-mentioned A material (high-concentration negative oxygen ion material) and B material (dope for inner wall of architecture): (high concentration is negative for A material
Oxonium ion material) 12 parts 88 parts of B material (dope for inner wall of architecture) is added and obtains releasing negative oxygen ion up to 4000 negative oxygen
Ion dope for inner wall of architecture.
Embodiment 3
Releasing negative oxygen ion is prepared up to 6000-6200 negative oxygen ion negative oxygen ion dope for inner wall of architecture:
A material (high-concentration negative oxygen ion material) and B material (dope for inner wall of architecture) and preparation 1 phase of preparation method embodiment
Together.
By above-mentioned A material (high-concentration negative oxygen ion material) and B material (dope for inner wall of architecture): (high concentration is negative for A material
Oxonium ion material) 15 parts 85 parts of B material (dope for inner wall of architecture) is added and obtains releasing negative oxygen ion up to 6000 negative oxygen
Ion dope for inner wall of architecture.
The embodiments of the present invention have been described in detail above, but content is only the preferred embodiment of the present invention,
It should not be considered as limiting the scope of the invention.Any changes and modifications in accordance with the scope of the present application,
It should still be within the scope of the patent of the present invention.
Claims (3)
1. a kind of high-concentration negative oxygen ion material, it is characterised in that: by weight, including following raw material components: 15-40 parts of germanium,
1-5 parts of cerium oxide, 1-5 parts of rare earth ytterbium, 1-5 parts of rare earth terbium, Tourmaline 10-40,10-40 parts of pelelith.
2. a kind of high-concentration negative oxygen ion material according to claim 1, it is characterised in that: by weight, including with
Lower component: 35 parts of germanium, 5 parts of cerium oxide, 1 part of rare earth ytterbium, 2 parts of rare earth terbium, 30 parts of Tourmaline, 30 parts of pelelith.
3. a kind of preparation method of high-concentration negative oxygen ion material.It is characterized by comprising following steps:
Step 1 grinding: rare earth ytterbium, rare earth terbium are respectively placed in grinder fineness of grind partial size no more than 300 mesh, it is dilute to obtain 300 mesh
Native terbium, rare earth ytterbium powder, it is spare；
Step 2 prepares rare earth terbium, rare earth ytterbium particle: rare earth ytterbium being made to the particle of partial size 0.8-1mmd, rare earth terbium powder is made
The particle of 2--3mmd, it is spare；
Step 3 prepares mixture: by the parts by weight of setting by spare 35 parts of the germanium that weighs of step 1,5 parts of cerium oxide, Tourmaline
30 parts, 30 parts of pelelith are crushed to 100 mesh or so and are placed in blender with 600r/min stirring 15-30 minutes, obtain and uniformly mix
Object, it is spare；
Step 4 mixture: by weight percentage by step 3 preliminary mixture, step 3 preliminary mixture mixture weight 70
Part, add 30 parts of tap water to be uniformly mixed, it is spare；
The calcining of step 5 mixture: the spare mixture of step 4 is placed in 2950-3000 DEG C of vacuum furnace and calcines 8-
Spare 1 part of rare earth terbium particle weight of injection step two, injection step when being cooled to 800 DEG C when being cooled to 1350 DEG C after 10 hours
Two spare 1 part of rare earth ytterbium particle weight, 60 parts of water are injected when being cooled to 20 DEG C, bell is opened after half an hour and is filtered with 50 mesh steel meshes
Up to a kind of high-concentration negative oxygen ion material coarse fodder.
Step 6 grinding: coarse fodder obtained by step 5 is placed in grinder be ground to 1250 mesh remember it is a kind of high needed for the present invention
Concentration negative oxygen ion material.
Step 7 recovering rare earth ytterbium and rare earth terbium: recovering rare earth ytterbium and rare earth terbium from the residue of step 5.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111607265A (en) * | 2020-07-03 | 2020-09-01 | 成都菩提高能科技有限公司 | Preparation method of negative oxygen ion waterproof emulsion paint |
| CN111700321A (en) * | 2020-06-19 | 2020-09-25 | 成都菩提高能科技有限公司 | Method for manufacturing negative oxygen ion mask |
| CN111728213A (en) * | 2020-07-20 | 2020-10-02 | 哈尔滨惠缘量子科技有限公司 | Method for preparing ion calcium pine pollen peptidase nutrition emulsion |
| CN111744112A (en) * | 2020-07-31 | 2020-10-09 | 成都菩提高能科技有限公司 | Method for manufacturing negative ion self-heating cloth |
| CN111876078A (en) * | 2020-08-07 | 2020-11-03 | 蒋勰 | Method for manufacturing negative oxygen ion wall sticker |
| CN112012010A (en) * | 2020-08-31 | 2020-12-01 | 蒋勰 | Method for manufacturing negative oxygen ion wall cloth |
| CN112125578A (en) * | 2020-09-17 | 2020-12-25 | 上海多礼新材料研究中心 | Negative oxygen ion material with good waterproof performance |
| CN112140263A (en) * | 2020-09-17 | 2020-12-29 | 上海多礼新材料研究中心 | Negative oxygen ion material capable of efficiently releasing and preparation method thereof |
| CN112136832A (en) * | 2020-09-17 | 2020-12-29 | 上海多礼新材料研究中心 | Antibacterial negative oxygen ion material and preparation process thereof |
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| CN105838956A (en) * | 2016-05-04 | 2016-08-10 | 成都市思燕电子科技有限公司 | Negative oxygen ion generation material containing germanium rare earth |
| CN109737511A (en) * | 2018-12-29 | 2019-05-10 | 深圳我氧你绿色科技有限公司 | A kind of domestic air conditioning mask that release negative ion antibiotic eliminates the unusual smell |
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| CN105838956A (en) * | 2016-05-04 | 2016-08-10 | 成都市思燕电子科技有限公司 | Negative oxygen ion generation material containing germanium rare earth |
| CN109737511A (en) * | 2018-12-29 | 2019-05-10 | 深圳我氧你绿色科技有限公司 | A kind of domestic air conditioning mask that release negative ion antibiotic eliminates the unusual smell |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111700321A (en) * | 2020-06-19 | 2020-09-25 | 成都菩提高能科技有限公司 | Method for manufacturing negative oxygen ion mask |
| CN111607265A (en) * | 2020-07-03 | 2020-09-01 | 成都菩提高能科技有限公司 | Preparation method of negative oxygen ion waterproof emulsion paint |
| CN111728213A (en) * | 2020-07-20 | 2020-10-02 | 哈尔滨惠缘量子科技有限公司 | Method for preparing ion calcium pine pollen peptidase nutrition emulsion |
| CN111744112A (en) * | 2020-07-31 | 2020-10-09 | 成都菩提高能科技有限公司 | Method for manufacturing negative ion self-heating cloth |
| CN111876078A (en) * | 2020-08-07 | 2020-11-03 | 蒋勰 | Method for manufacturing negative oxygen ion wall sticker |
| CN112012010A (en) * | 2020-08-31 | 2020-12-01 | 蒋勰 | Method for manufacturing negative oxygen ion wall cloth |
| CN112125578A (en) * | 2020-09-17 | 2020-12-25 | 上海多礼新材料研究中心 | Negative oxygen ion material with good waterproof performance |
| CN112140263A (en) * | 2020-09-17 | 2020-12-29 | 上海多礼新材料研究中心 | Negative oxygen ion material capable of efficiently releasing and preparation method thereof |
| CN112136832A (en) * | 2020-09-17 | 2020-12-29 | 上海多礼新材料研究中心 | Antibacterial negative oxygen ion material and preparation process thereof |
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