CN111876078A - Method for manufacturing negative oxygen ion wall sticker - Google Patents
Method for manufacturing negative oxygen ion wall sticker Download PDFInfo
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- CN111876078A CN111876078A CN202010786293.6A CN202010786293A CN111876078A CN 111876078 A CN111876078 A CN 111876078A CN 202010786293 A CN202010786293 A CN 202010786293A CN 111876078 A CN111876078 A CN 111876078A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F13/00—Coverings or linings, e.g. for walls or ceilings
- E04F13/07—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor
- E04F13/08—Coverings or linings, e.g. for walls or ceilings composed of covering or lining elements; Sub-structures therefor; Fastening means therefor composed of a plurality of similar covering or lining elements
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/221—Oxides; Hydroxides of metals of rare earth metal
- C08K2003/2213—Oxides; Hydroxides of metals of rare earth metal of cerium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
- E04F2290/00—Specially adapted covering, lining or flooring elements not otherwise provided for
- E04F2290/04—Specially adapted covering, lining or flooring elements not otherwise provided for for insulation or surface protection, e.g. against noise, impact or fire
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Organic Chemistry (AREA)
- Architecture (AREA)
- Plant Pathology (AREA)
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Abstract
The invention provides a method for manufacturing a negative oxygen ion wall sticker, which comprises the following core raw material of negative oxygen ion raw pulp: 30 parts of high-purity germanite, 5 parts of cerium oxide, 35 parts of high-purity tourmaline, 5 parts of conductive titanium dioxide, 10 parts of neodymium iron boron, 5 parts of rare earth zirconium, 5 parts of rare earth dysprosium, 3 parts of rare earth lanthanum, 1 part of rare earth terbium, 1 part of rare earth ytterbium and a plurality of purified water; the invention has the beneficial effects that: the negative oxygen ion wall sticker uses market mature technology environment-friendly waterproof emulsion TFX (produced by Sichuan sunrise chemical Co., Ltd.), the core raw material negative oxygen ion protoplasm is prepared from high-purity mineral components, and the negative oxygen ion protoplasm is calcined at the high temperature of about 3000 ℃, so that harmful components such as sulfur, phosphorus, radiation and the like in the mineral are effectively removed, and the negative oxygen ion wall sticker is environment-friendly, healthy and free of radiation pollution. The substrate adopts the ordinary environmental protection wall subsides of selling in a large number on the market, through the effect of negative oxygen ion, can effectively disinfect antibiotic and establish green oxygen bar space, guarantees to possess the fresh air as nature in the application range. The high-concentration negative oxygen ions can clear free radicals in human bodies, promote the metabolism function of human cells, enhance lymphatic circulation and promote the blood circulation of the human bodies and are beneficial to body health (the function of the hundred-concentration negative oxygen ions is known) through the electric neutralization effect.
Description
Technical Field
The technology belongs to the technical field of novel building materials, and relates to a manufacturing method of a negative oxygen ion wall sticker.
Background
With the improvement of living standard and the change of life style in recent years, people live in the room for a longer time, and the quality of indoor air directly influences the work and life of people. Poor air qualityThe traditional Chinese medicine preparation can disperse attention, reduce work efficiency and cause symptoms of headache, nausea, fatigue, skin red swelling and the like in severe cases, which are collectively called as 'sick building syndrome'. People are eagerly expected to improve increasingly severe living and office environments and improve living quality. Various coatings, paints, wall coverings, adhesives, etc. are used for interior decoration,Artificial boardPhenol, formaldehyde, asbestos dust, radioactive substances and the like are emitted from marble floors, newly purchased furniture and the like, and can cause reactions such as headache, insomnia, dermatitis, allergy and the like of people to reduce the immunologic function of human bodies, so that the international cancer research institute lists the substances as suspicious carcinogens. According to incomplete statistics, 210 thousands of children die from decoration pollution every year in China, the lung cancer fatality rate is high, and the fatality rate is related to indoor air quality, and the negative oxygen ion wall sticker is invented.
After the product is used, the concentration of negative oxygen ions in a room can reach 5000 pieces/cm3Above, 5000-10000 pieces/cm according to the identification of the indoor air freshening standard of the world health organization3Is especially fresh and can prevent diseases (known in every degree).
Disclosure of Invention
The invention provides a manufacturing method of a negative oxygen ion wall sticker, which is characterized in that a negative oxygen ion material is perfectly fused on the surface of the wall sticker to release high-concentration negative oxygen ions for a long time, so that the wall sticker can effectively sterilize and resist bacteria, and has the effects of water resistance and moisture resistance.
In order to achieve the purpose, the invention adopts the following technical scheme:
1. the negative oxygen ion raw stock is prepared by a special technology, so that the negative oxygen ion raw stock is non-toxic, harmless and free of radiation pollution;
2. the original negative oxygen ion pulp and the waterproof emulsion are perfectly fused by a high-tech process and then sprayed on the surface of a common wall sticker so as to release high-concentration negative oxygen ions.
The beneficial effect of this patent technique lies in:
1. high-purity mineral components are selected, and radioactive substances are volatilized through a high-temperature calcination (about 3000 ℃) manufacturing process, so that the primary pulp is guaranteed to efficiently release negative oxygen ions, and the environment-friendly, healthy and radiation-free pollution is realized;
2. through the action of negative oxygen ions, the antibacterial and waterproof paint has the functions of effectively sterilizing and resisting bacteria and preventing water and moisture.
Description of the drawings:
FIG. 1 is a flow chart of the preparation of a primary pulp of negative oxygen ions
FIG. 2 is a flow chart of the manufacture of negative oxygen ion wall sticker
The method comprises the following specific implementation steps:
the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiment is only one embodiment of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
1. As shown in fig. 1, the process of making the negative oxygen ion raw stock comprises:
p1 preparation: the following materials were prepared separately: 30 parts of high-purity germanite, 5 parts of cerium oxide, 35 parts of high-purity tourmaline, 5 parts of conductive titanium dioxide, 10 parts of neodymium iron boron, 5 parts of rare earth zirconium, 5 parts of rare earth dysprosium, 3 parts of rare earth lanthanum, 1 part of rare earth terbium, 1 part of rare earth ytterbium and a plurality of purified water;
p2 preparing rare earth terbium and rare earth ytterbium balls: respectively grinding the rare earth ytterbium and the rare earth terbium in a grinder until the fineness particle size is not more than 300 meshes, then preparing the rare earth ytterbium powder into small balls with the diameter of 3-3.5mm, and preparing the rare earth terbium into small balls with the diameter of 1.5-2mm for later use;
p3 grinding neodymium iron boron powder: putting 10 parts of neodymium iron boron (N40SH) into a high-temperature nano grinder, heating to 400 ℃, keeping the temperature for 24 hours, and grinding to 1250 meshes for later use;
p4 preparation of rare earth dysprosium particles: 5 parts of rare earth dysprosium is taken and crushed to about 100 meshes for standby;
p5 preparation of the mixture: crushing 30 parts of the high-purity germanite, 5 parts of cerium oxide, 35 parts of high-purity tourmaline, 5 parts of rare earth zirconium and 3 parts of rare earth lanthanum which are prepared in the first step to 100 meshes by weight according to the set parts by weight, and stirring the crushed materials in a stirrer at a speed of 100r/min for 15 to 30 minutes to obtain a uniform mixture for later use;
calcining the P6 mixture: calcining the mixture of P5 in a vacuum heating furnace, heating to 2950-3000 ℃, keeping the temperature constant for 120 hours, cooling to 2550 ℃, injecting P4 rare earth dysprosium particles, keeping the temperature constant for 24 hours, cooling to 1330 ℃, injecting 1 part by weight of P2 rare earth terbium microspheres, keeping the temperature constant for 24 hours, cooling to 800 ℃, injecting 1 part by weight of P2 rare earth ytterbium particles and 5 parts by weight of conductive titanium dioxide, keeping the temperature constant for 12 hours, cooling to 400 ℃, injecting P3 neodymium iron boron powder, keeping the temperature constant for 12 hours, cooling to 20 ℃, injecting 150 parts by weight of water, opening a furnace cover after half an hour, and filtering with a 50-mesh steel net to obtain the crude negative oxygen ion protoplasm;
p7 grind coarse: grinding the coarse material obtained from the P6 in a grinder to 1250 meshes to obtain high-concentration negative oxygen ion primary pulp;
p8 recovering rare earth ytterbium and terbium: recovery of the rare earths ytterbium and terbium from the residue of P6: pouring the residues into a stainless steel screen with the diameter of 2.5mm, and shaking the screen to obtain rare earth ytterbium spheres in the screen; and putting the remainder of the step into a screen with the diameter of 1mm, and shaking the screen to obtain the rare earth terbium spheres.
2. The method for manufacturing the negative oxygen ion wall sticker based on the negative oxygen ion raw stock comprises the following steps: as shown in fig. 2:
s1: stock preparation
Taking 100 parts of the original negative oxygen ion pulp obtained from P7;
260 parts of TFX environment-friendly waterproof emulsion of Sichuan sunrise chemical Co.Ltd;
5 parts of dispersant, 2 parts of thickener, 10 parts of film-forming assistant, 10 parts of alkaline regulator, 2 parts of cellulose and 800 parts of purified water;
proper amount of common wall paste.
S2: preparing an auxiliary agent:
respectively taking 100 parts of purified water, adding the dispersant, the thickening agent and the film-forming aid of the S1 into the purified water, and respectively stirring uniformly;
s3: emulsifying primary pulp:
pouring the dispersant solution obtained in the step S2 into the raw stock prepared in the step S1, stirring the mixture for 30 minutes at the speed of 500 rpm, and then adding the thickener solution obtained in the step S2, and stirring the mixture for 30 minutes at the same speed;
s4: the emulsion helps the membrane:
adding the film forming aid solution obtained in the step S2 into the TFX emulsion prepared in the step S1, and stirring for 90 minutes at 300 revolutions per minute;
s5: mixing:
mixing the emulsified raw stock obtained in the step S3 with the liquid obtained in the step S4, uniformly stirring at 30 revolutions per minute, adding the cellulose prepared in the step S1, stirring at 30 revolutions per minute for 30 minutes, adding purified water to 1000 parts, and stirring at 30 revolutions per minute for 15 minutes;
s6: adjusting the pH value:
and (5) testing the pH value of the product obtained in the step S5, and gradually adding an alkaline regulator for later use in the step S1 until the pH value reaches 8-9.5 to obtain the negative oxygen ion stock solution.
S7-spraying: uniformly spraying the stock solution obtained in the step S6 on the surface of the ordinary wall sticker prepared in the step S1, wherein the dosage is 100 g/square meter, and drying to obtain the negative oxygen ion release amount of 10000/cm in 5000-3The negative oxygen ion wall plaster finished product.
The negative oxygen ion wall sticker manufactured by the steps can efficiently release negative oxygen ions beneficial to human bodies, and has efficient sterilization and antibacterial effects. Meanwhile, the waterproof and moistureproof structure has the advantages of convenience in installation and waterproof and moistureproof functions.
Claims (3)
1. The method for making negative oxygen ion wall plaster is characterized by that it uses the original negative oxygen ion pulp as core, and implants the negative oxygen ion into the surface of general wall plaster by using special method.
2. The method for manufacturing a negative oxygen ion waterproof wall sticker as claimed in claim 1, wherein the following steps of manufacturing the negative oxygen ion raw stock are included:
as shown in fig. 1, the process of making the negative oxygen ion raw stock comprises:
p1 preparation: the following materials were prepared separately: 30 parts of high-purity germanite, 5 parts of ceria, 35 parts of high-purity tourmaline, 5 parts of conductive titanium dioxide, 10 parts of neodymium iron boron, 5 parts of rare earth zirconium, 5 parts of rare earth dysprosium, 3 parts of rare earth lanthanum, 1 part of rare earth terbium, 1 part of rare earth ytterbium and a plurality of purified water;
p2 preparing rare earth terbium and rare earth ytterbium balls: respectively grinding the rare earth ytterbium and the rare earth terbium in a grinder until the fineness particle size is not more than 300 meshes, then preparing the rare earth ytterbium powder into small balls with the diameter of 3-3.5mm, and preparing the rare earth terbium into small balls with the diameter of 1.5-2mm for later use;
p3 grinding neodymium iron boron powder: putting 10 parts of neodymium iron boron (N40SH) into a high-temperature nano grinder, heating to 400 ℃, keeping the temperature for 24 hours, and grinding to 1250 meshes for later use;
p4 preparation of rare earth dysprosium particles: 5 parts of rare earth dysprosium is taken and crushed to about 100 meshes for standby;
p5 preparation of the mixture: grinding 30 parts of high-purity germanite, 5 parts of ceria, 35 parts of high-purity tourmaline, 5 parts of rare earth zirconium and 3 parts of rare earth lanthanum which are weighed for standby in the first step according to the set weight parts to 100 meshes, putting the ground materials into a stirrer, and stirring the materials for 15-30 minutes at a speed of 100r/min to obtain a uniform mixture for standby;
calcining the P6 mixture: calcining the mixture of P5 in a vacuum heating furnace, heating to 2950-3000 ℃, keeping the temperature constant for 120 hours, cooling to 2550 ℃, injecting P4 rare earth dysprosium particles, keeping the temperature constant for 24 hours, cooling to 1330 ℃, injecting 1 part by weight of P2 rare earth terbium microspheres, keeping the temperature constant for 24 hours, cooling to 800 ℃, injecting 1 part by weight of P2 rare earth ytterbium particles and 5 parts by weight of conductive titanium dioxide, keeping the temperature constant for 12 hours, cooling to 400 ℃, injecting P3 neodymium iron boron powder, keeping the temperature constant for 12 hours, cooling to 20 ℃, injecting 150 parts by weight of water, opening a furnace cover after half an hour, and filtering with a 50-mesh steel net to obtain the crude negative oxygen ion protoplasm;
p7 grind coarse: grinding the coarse material obtained from the P6 in a grinder to 1250 meshes to obtain high-concentration negative oxygen ion primary pulp;
p8 recovering rare earth ytterbium and terbium: recovery of the rare earths ytterbium and terbium from the residue of P6: pouring the residues into a stainless steel screen with the diameter of 2.5mm, and shaking the screen to obtain rare earth ytterbium spheres in the screen; and putting the remainder of the step into a screen with the diameter of 1mm, and shaking the screen to obtain the rare earth terbium spheres.
3. The method for manufacturing the negative oxygen ion wall sticker based on the negative oxygen ion raw stock comprises the following steps: as shown in fig. 2:
s1: stock preparation
Taking 100 parts of the original negative oxygen ion pulp obtained from P7;
260 parts of TFX environment-friendly waterproof emulsion of Sichuan sunrise chemical Co.Ltd;
5 parts of dispersant, 2 parts of thickener, 10 parts of film-forming assistant, 10 parts of alkaline regulator, 2 parts of cellulose and 800 parts of purified water;
proper amount of common wall paste.
S2: preparing an auxiliary agent:
respectively taking 100 parts of purified water, adding the dispersant, the thickening agent and the film-forming aid of the S1 into the purified water, and respectively stirring uniformly;
s3: emulsifying primary pulp:
pouring the dispersant solution obtained in the step S2 into the raw stock prepared in the step S1, stirring the mixture for 30 minutes at the speed of 500 rpm, and then adding the thickener solution obtained in the step S2, and stirring the mixture for 30 minutes at the same speed;
s4: the emulsion helps the membrane:
adding the film forming aid solution obtained in the step S2 into the TFX emulsion prepared in the step S1, and stirring for 90 minutes at 300 revolutions per minute;
s5: mixing:
mixing the emulsified raw stock obtained in the step S3 with the liquid obtained in the step S4, uniformly stirring at 30 revolutions per minute, adding the cellulose prepared in the step S1, stirring at 30 revolutions per minute for 30 minutes, adding purified water to 1000 parts, and stirring at 30 revolutions per minute for 15 minutes;
s6: adjusting the pH value:
and (5) testing the pH value of the product obtained in the step S5, and gradually adding an alkaline regulator for later use in the step S1 until the pH value reaches 8-9.5 to obtain the negative oxygen ion stock solution.
S7-spraying: uniformly spraying the stock solution obtained in the step S6 on the surface of the ordinary wall sticker prepared in the step S1, wherein the dosage is 100 g/square meter, and drying to obtain the negative oxygen ion release amount of 10000/cm in 5000-3The negative oxygen ion wall plaster finished product.
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| CN202010786293.6A CN111876078A (en) | 2020-08-07 | 2020-08-07 | Method for manufacturing negative oxygen ion wall sticker |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111154407A (en) * | 2020-02-12 | 2020-05-15 | 常德集智生物科技有限公司 | Green antibacterial bactericidal negative oxygen ion releasing coating and preparation method thereof |
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| CN111744112A (en) * | 2020-07-31 | 2020-10-09 | 成都菩提高能科技有限公司 | Method for manufacturing negative ion self-heating cloth |
| CN112012010A (en) * | 2020-08-31 | 2020-12-01 | 蒋勰 | Method for manufacturing negative oxygen ion wall cloth |
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2020
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|---|---|---|---|---|
| WO2005073463A1 (en) * | 2004-01-30 | 2005-08-11 | Dsg Daedong Wallpaper Co., Ltd. | Functional wallpaper emitting anions and far infrared rays and method for manufacturing the same |
| CN110396323A (en) * | 2019-08-07 | 2019-11-01 | 四川省中源惠量子科技有限公司 | A kind of high-concentration negative oxygen ion material and preparation method thereof |
| CN110565372A (en) * | 2019-09-26 | 2019-12-13 | 成都康源量子生物技术研究院 | Negative oxygen ion energy brocade roll and preparation method thereof |
| CN111139691A (en) * | 2019-12-24 | 2020-05-12 | 安徽掌融通讯科技有限公司 | Functional negative ion anti-formaldehyde ecological wallpaper and preparation process thereof |
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| CN111154407A (en) * | 2020-02-12 | 2020-05-15 | 常德集智生物科技有限公司 | Green antibacterial bactericidal negative oxygen ion releasing coating and preparation method thereof |
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