CN111700321A - Method for manufacturing negative oxygen ion mask - Google Patents
Method for manufacturing negative oxygen ion mask Download PDFInfo
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- CN111700321A CN111700321A CN202010562563.5A CN202010562563A CN111700321A CN 111700321 A CN111700321 A CN 111700321A CN 202010562563 A CN202010562563 A CN 202010562563A CN 111700321 A CN111700321 A CN 111700321A
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- negative oxygen
- rare earth
- oxygen ion
- later use
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- 229910052760 oxygen Inorganic materials 0.000 title claims abstract description 57
- 239000001301 oxygen Substances 0.000 title claims abstract description 57
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 9
- -1 oxygen ion Chemical class 0.000 claims abstract description 56
- 229910052761 rare earth metal Inorganic materials 0.000 claims abstract description 47
- 150000002910 rare earth metals Chemical class 0.000 claims abstract description 47
- GZCRRIHWUXGPOV-UHFFFAOYSA-N terbium atom Chemical compound [Tb] GZCRRIHWUXGPOV-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910052771 Terbium Inorganic materials 0.000 claims abstract description 17
- NAWDYIZEMPQZHO-UHFFFAOYSA-N ytterbium Chemical compound [Yb] NAWDYIZEMPQZHO-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229910052769 Ytterbium Inorganic materials 0.000 claims abstract description 15
- 241000894006 Bacteria Species 0.000 claims abstract description 10
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910000420 cerium oxide Inorganic materials 0.000 claims abstract description 8
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 claims abstract description 8
- QJVKUMXDEUEQLH-UHFFFAOYSA-N [B].[Fe].[Nd] Chemical compound [B].[Fe].[Nd] QJVKUMXDEUEQLH-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910001172 neodymium magnet Inorganic materials 0.000 claims abstract description 7
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052746 lanthanum Inorganic materials 0.000 claims abstract description 5
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000011435 rock Substances 0.000 claims abstract description 5
- 239000004575 stone Substances 0.000 claims abstract description 5
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 5
- 229940070527 tourmaline Drugs 0.000 claims abstract description 5
- 229910052613 tourmaline Inorganic materials 0.000 claims abstract description 5
- 239000011032 tourmaline Substances 0.000 claims abstract description 5
- 229910052726 zirconium Inorganic materials 0.000 claims abstract description 5
- 239000004744 fabric Substances 0.000 claims description 29
- 239000002245 particle Substances 0.000 claims description 18
- 238000001816 cooling Methods 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 229920000742 Cotton Polymers 0.000 claims description 7
- 238000005520 cutting process Methods 0.000 claims description 6
- 239000004745 nonwoven fabric Substances 0.000 claims description 5
- 229910052692 Dysprosium Inorganic materials 0.000 claims description 4
- 238000001354 calcination Methods 0.000 claims description 4
- KBQHZAAAGSGFKK-UHFFFAOYSA-N dysprosium atom Chemical compound [Dy] KBQHZAAAGSGFKK-UHFFFAOYSA-N 0.000 claims description 4
- 238000003825 pressing Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 3
- 229910000831 Steel Inorganic materials 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 238000007731 hot pressing Methods 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 239000008213 purified water Substances 0.000 claims description 2
- 238000009958 sewing Methods 0.000 claims description 2
- 239000010959 steel Substances 0.000 claims description 2
- 239000011162 core material Substances 0.000 claims 4
- 238000003756 stirring Methods 0.000 claims 1
- 241000700605 Viruses Species 0.000 abstract description 5
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract 1
- 210000000805 cytoplasm Anatomy 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 238000004887 air purification Methods 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000029058 respiratory gaseous exchange Effects 0.000 description 2
- 241000711573 Coronaviridae Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 230000009385 viral infection Effects 0.000 description 1
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D13/00—Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
- A41D13/05—Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches protecting only a particular body part
- A41D13/11—Protective face masks, e.g. for surgical use, or for use in foul atmospheres
- A41D13/1192—Protective face masks, e.g. for surgical use, or for use in foul atmospheres with antimicrobial agent
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D31/00—Materials specially adapted for outerwear
- A41D31/02—Layered materials
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D31/00—Materials specially adapted for outerwear
- A41D31/04—Materials specially adapted for outerwear characterised by special function or use
- A41D31/30—Antimicrobial, e.g. antibacterial
- A41D31/305—Antimicrobial, e.g. antibacterial using layered materials
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/45—Oxides or hydroxides of elements of Groups 3 or 13 of the Periodic System; Aluminates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic System; Titanates; Zirconates; Stannates; Plumbates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/80—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with boron or compounds thereof, e.g. borides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/83—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D2500/00—Materials for garments
- A41D2500/30—Non-woven
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Biochemistry (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Physical Education & Sports Medicine (AREA)
- Respiratory Apparatuses And Protective Means (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Filtering Materials (AREA)
Abstract
The invention provides a method for manufacturing a negative oxygen ion mask, which comprises the following core raw materials in percentage by weight: 10 parts of high-purity germanite, 5 parts of cerium oxide, 40 parts of high-purity tourmaline, 10 parts of conductive titanium dioxide, 5 parts of volcanic rock, 5 parts of medical stone, 10 parts of neodymium iron boron, 2 parts of rare earth zirconium, 1 part of rare earth lanthanum, 5 parts of cerium oxide, 1 part of rare earth terbium and 1 part of rare earth ytterbium; 2. the invention has the beneficial effects that: according to the negative oxygen ion mask, the negative oxygen ion raw pulp is implanted into the mask, so that high-concentration negative oxygen ions can be released, all viruses and bacteria harmful to human bodies are positive charges, and the viruses and the bacteria can be automatically neutralized when encountering the negative oxygen ions, so that the negative oxygen ion mask has the functions of removing formaldehyde, resisting bacteria and preventing haze. The negative oxygen ion mask can effectively resist bacteria and haze and purify the air breathed by a wearer after being used for a long time.
Description
Technical Field
The technology belongs to the technical field of health care, and relates to a manufacturing method of a negative oxygen ion mask.
Background
With the appearance of haze and the novel coronavirus which is outbreaked in 2020, a large number of people suffer great pain, and simultaneously immeasurable economic loss is caused to various industries. Although the conventional mask has a certain protection effect, the quality problem of the breathing air cannot be effectively improved.
In view of the above, the invention discloses a negative oxygen ion mask, wherein the negative oxygen ion raw pulp is implanted into the mask, so that high-concentration negative oxygen ions can be released, all viruses and bacteria harmful to human bodies are positive charges, and the viruses and the bacteria can be automatically neutralized when encountering the negative oxygen ions, so that the negative oxygen ion mask has the functions of removing formaldehyde, resisting bacteria and preventing haze.
Disclosure of Invention
The invention provides a manufacturing method of a negative oxygen ion mask, which improves the structure of the mask, designs a movable multilayer negative oxygen ion filter chip, enables the mask to be repeatedly used by washing, simultaneously perfectly melts a negative oxygen ion material into high-grade cotton cloth, enables the mask to release high-concentration negative oxygen ions for a long time, and enables bacteria and viruses to be positive charges, and the negative oxygen ions in the negative oxygen ion mask to be automatically neutralized once meeting. Therefore, the negative oxygen ion mask can prevent various virus infections and effectively protect and repair respiratory tracts after being used for a long time.
In order to achieve the purpose, the invention adopts the following technical scheme:
1. the negative oxygen ion raw stock is prepared by a special technology, so that the negative oxygen ion raw stock is non-toxic, harmless and free of radiation pollution;
2. placing the original pulp of negative oxygen ions on high-grade cotton cloth fabric to enable the original pulp to release negative oxygen ions efficiently;
3. through improving gauze mask inner structure, increase filter chip, make the gauze mask can the washing use repeatedly to let the anti-bacterial antifog haze function and the air purification function obtain the performance of maximize.
The beneficial effect of this patent technique lies in:
1. through the effect of negative oxygen ion to and N95 melt-blown cloth and non-woven fabrics, can effectively resist the antifog haze of fungus, and purify the respiratory air of wearer.
2. Through improving gauze mask inner structure, increase filter chip, make the gauze mask can the washing use repeatedly to let the anti-bacterial antifog haze function and the air purification function obtain the performance of maximize, greatly reduced consumer's use cost simultaneously.
Drawings
FIG. 1 is a flow chart of the preparation of the negative oxygen ion raw stock.
FIG. 2 is a flow chart of the fabrication of a filter chip.
The method comprises the following specific implementation steps:
the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiment is only one embodiment of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
1. The preparation steps of the negative oxygen ion protoplasm are shown in figure 1:
BZ 1: preparing materials: preparing the following materials in percentage by weight: 10 parts of high-purity germanite, 5 parts of cerium oxide, 40 parts of high-purity tourmaline, 10 parts of conductive titanium dioxide, 5 parts of volcanic rock, 5 parts of medical stone, 10 parts of neodymium iron boron, 2 parts of rare earth zirconium, 1 part of rare earth lanthanum, 5 parts of cerium oxide, 1 part of rare earth terbium and 1 part of rare earth ytterbium;
BZ2 grinding: respectively placing the rare earth ytterbium and the rare earth terbium in a grinder to grind the particle size of the rare earth terbium to be not more than 300 meshes to obtain 300 meshes of rare earth terbium and rare earth ytterbium powder for later use;
BZ3 preparation of rare earth terbium and rare earth ytterbium particles: making the rare earth ytterbium into particles with the particle size of 0.8-1mmd, and making the rare earth terbium powder into particles with the particle size of 2-3 mmd for later use;
BZ 4: putting 10 parts of neodymium iron boron (N4OSH) into a high-temperature nano grinder, heating to 400 ℃, keeping the temperature for 24 hours, and grinding to 1250 meshes for later use;
BZ 5: 5 parts of rare earth dysprosium is taken and crushed to about 100 meshes for standby;
BZ 6: preparing a mixture: according to the set weight parts, 10 parts of high-purity germanite, 5 parts of cerium oxide, 40 parts of high-purity tourmaline, 5 parts of volcanic rock, 5 parts of medical stone, 2 parts of rare earth zirconium and 1 part of rare earth lanthanum are weighed for standby application of BZ1, crushed to about 100 meshes and put into a stirrer to be stirred for 15-30 minutes at 600r/min to obtain a uniform mixture for standby application;
calcining the BZ7 mixture: calcining the mixture for later use of BZ6 in a vacuum heating furnace, heating to 2950-3000 ℃, keeping the temperature constant for 120 hours, cooling to 2550 ℃, injecting BZ5 rare earth dysprosium particles for later use, keeping the temperature constant for 24 hours, cooling to 1350 ℃, injecting BZ3 by weight of rare earth terbium particles for later use, keeping the temperature constant for 24 hours, cooling to 800 ℃, injecting 1 part by weight of BZ3 by weight of rare earth ytterbium particles and 10 parts by weight of conductive titanium dioxide, keeping the temperature constant for 12 hours, cooling to 420 ℃, injecting 10 parts by weight of BZ4 by weight of neodymium iron boron powder for later use, continuously cooling to 20 ℃, injecting 40 parts by weight of purified water, opening a furnace cover after half an hour, and filtering by using a 50-mesh steel net to obtain the crude negative oxygen ion stock.
BZ8 grinding: and (3) grinding the coarse material obtained from the BZ7 in a grinder to 1250 meshes to obtain the high-concentration negative oxygen ion raw stock.
BZ9 recovering rare earth ytterbium and terbium: recovering rare earth ytterbium and rare earth terbium from the residue of BZ 7.
2. The steps of manufacturing the filter chip based on the negative oxygen ion raw stock are shown in fig. 2:
s1: preparing a fabric: cutting the high-grade pure cotton fabric into pieces with the width of 1 meter for later use;
cutting the N95 melt-blown fabric according to the size of (125mm multiplied by 85mm) and processing the selvedges; cutting high-grade non-woven fabric according to the size of (125mm multiplied by 85mm) and processing the edge;
s2: implanting negative oxygen ions: heating the primary negative oxygen ion pulp to 40 ℃, adding the pure cotton cloth fabric prepared in S1, heating to 60 ℃, keeping the temperature for 20 hours, and cooling to normal temperature;
s3: making ofNegative oxygen ion protoplasm cloth: taking out the fabric from S2, drying by pressing to remove water, and obtaining the negative oxygen ion release amount of 1500-3"negative oxygen ion protoplasm cloth;
s4: manufacturing an inner core: pressing the non-woven fabric prepared in the step S1 outside the two layers of melt-blown fabric by a hot pressing method to form a four-layer inner core;
s5: manufacturing a filter chip: sewing the negative oxygen ion raw pulp cloth of S3 on the outer surface of the four-layer inner core of S4 to wrap the outer surface of the four-layer inner core, thereby obtaining a negative oxygen ion filter chip;
the filter chip manufactured by the steps can achieve the purposes of resisting bacteria and haze and purifying the breathing air.
3. Manufacturing a chip sleeve:
the pure cotton cloth is cut into small blocks of 130mm x 110mm, the small blocks are sewn inside the mask, and the left end and the right end are not sewn, namely the chip sleeve. When in use, the filter chip is inserted into the chip sleeve, and the filter chip is taken out when the mask is cleaned.
Claims (3)
1. A manufacturing method of a negative oxygen ion mask is characterized in that negative oxygen ion cloth manufactured based on negative oxygen ion raw stock is used as a core material for generating negative oxygen ions, N95 melt-blown cloth and non-woven cloth are arranged in the negative oxygen ion cloth to form six layers of filter chips, and the effects of resisting bacteria, preventing haze, purifying air and the like are achieved.
2. The method for manufacturing a negative oxygen ion mask according to claim 1, wherein the negative oxygen ion raw pulp manufacturing step comprises:
BZ 1: preparing materials: preparing the following materials in percentage by weight: 10 parts of high-purity germanite, 5 parts of cerium oxide, 40 parts of high-purity tourmaline, 10 parts of conductive titanium dioxide, 5 parts of volcanic rock, 5 parts of medical stone, 10 parts of neodymium iron boron, 2 parts of rare earth zirconium, 1 part of rare earth lanthanum, 5 parts of cerium oxide, 1 part of rare earth terbium and 1 part of rare earth ytterbium;
BZ 2: grinding: respectively placing the rare earth ytterbium and the rare earth terbium in a grinder to grind the particle size of the rare earth terbium to be not more than 300 meshes to obtain 300 meshes of rare earth terbium and rare earth ytterbium powder for later use;
BZ 3: preparing rare earth terbium and rare earth ytterbium particles: making the rare earth ytterbium into particles with the particle size of 0.8-1mmd, and making the rare earth terbium powder into particles with the particle size of 2-3 mmd for later use;
BZ 4: putting 10 parts of neodymium iron boron (N40SH) into a high-temperature nano grinder, heating to 400 ℃, keeping the temperature for 24 hours, and grinding to 1250 meshes for later use;
BZ 5: 5 parts of rare earth dysprosium is taken and crushed to about 100 meshes for standby;
BZ 6: preparing a mixture: crushing 10 parts of high-purity germanite, 5 parts of cerium oxide, 40 parts of high-purity tourmaline, 5 parts of volcanic rock, 5 parts of medical stone, 2 parts of rare earth zirconium and 1 part of rare earth lanthanum which are prepared by BZ1 according to the set weight parts to 100 meshes, and stirring the crushed materials in a stirrer at a speed of 100r/min for 15 to 30 minutes to obtain a uniform mixture for later use;
BZ 7: and (3) calcining the mixture: calcining a mixture for later use of BZ6 in a vacuum heating furnace, heating to 2950-3000 ℃, keeping the temperature constant for 120 hours, cooling to 2550 ℃, injecting BZ5 rare earth dysprosium particles for later use, keeping the temperature constant for 24 hours, cooling to 1350 ℃, injecting BZ3 by 1 part by weight of rare earth terbium particles for later use, keeping the temperature constant for 24 hours, then cooling to 800 ℃, injecting BZ3 by 1 part by weight of rare earth ytterbium particles and 10 parts by weight of conductive titanium dioxide, keeping the temperature constant for 12 hours, cooling to 420 ℃, injecting BZ4 by 10 parts by weight of neodymium iron boron powder for later use, continuously cooling to 20 ℃, injecting 40 parts by weight of purified water, opening a furnace cover after half an hour, and filtering by using a 50-mesh steel net to obtain the crude negative oxygen ion stock;
BZ 8: grinding: grinding the coarse material obtained from the BZ7 in a grinder to 1250 meshes to obtain high-concentration negative oxygen ion raw stock;
BZ 9: recovering ytterbium and terbium: recovering rare earth ytterbium and rare earth terbium from the residue of BZ 7.
3. The method comprises the following steps of preparing a negative oxygen ion mask filter chip based on negative oxygen ion raw stock:
s1: preparing a fabric: cutting the high-grade pure cotton fabric into pieces with the width of 1 meter for later use;
cutting the N95 melt-blown fabric according to the size of (125mm multiplied by 85mm) and processing the selvedges; cutting high-grade non-woven fabric according to the size of (125mm multiplied by 85mm) and processing the edge;
s2: implanting negative oxygen ions: heating the primary negative oxygen ion pulp to 40 ℃, adding the pure cotton cloth fabric prepared in S1, heating to 60 ℃, keeping the temperature for 20 hours, and cooling to normal temperature;
s3: manufacturing negative oxygen ion cloth: taking out the fabric from S2, drying by pressing to remove water to obtain negative oxygen ion release amount of 1500/cm3"finished negative oxygen ion cloth;
s4: manufacturing an inner core: pressing the non-woven fabric prepared in the step S1 outside the two layers of melt-blown fabric by a hot pressing method to form a four-layer inner core;
s5: manufacturing a filter chip: and sewing the negative oxygen ion cloth of S3 on the outer surface of the four-layer core of S4 to wrap the negative oxygen ion mask filter chip.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111876078A (en) * | 2020-08-07 | 2020-11-03 | 蒋勰 | Method for manufacturing negative oxygen ion wall sticker |
CN112263027A (en) * | 2020-10-26 | 2021-01-26 | 康源健康科技有限公司 | Efficient antibacterial and antiviral anion mask and manufacturing method thereof |
CN112335957A (en) * | 2020-10-30 | 2021-02-09 | 吴溪元 | Negative oxygen ion functional high polymer material mask and preparation process thereof |
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CN113080545A (en) * | 2021-03-04 | 2021-07-09 | 重庆中膜科技集团有限公司 | Negative oxygen ion mask processing technology |
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