CN110353073A - A kind of decompression hard candy and preparation method thereof - Google Patents

A kind of decompression hard candy and preparation method thereof Download PDF

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Publication number
CN110353073A
CN110353073A CN201910797502.4A CN201910797502A CN110353073A CN 110353073 A CN110353073 A CN 110353073A CN 201910797502 A CN201910797502 A CN 201910797502A CN 110353073 A CN110353073 A CN 110353073A
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decompression
hard candy
polysaccharides
preparation
plumula nelumbinis
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Inventor
郑俊霞
杨超
王立抗
黄家晋
田文月
赵肃清
张焜
张蓝月
朱展良
胡炎鹏
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Guangdong University of Technology
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Guangdong University of Technology
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Priority to CN201910797502.4A priority Critical patent/CN110353073A/en
Publication of CN110353073A publication Critical patent/CN110353073A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G3/00Sweetmeats; Confectionery; Marzipan; Coated or filled products
    • A23G3/34Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
    • A23G3/36Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G3/00Sweetmeats; Confectionery; Marzipan; Coated or filled products
    • A23G3/34Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
    • A23G3/36Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
    • A23G3/38Sucrose-free products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G3/00Sweetmeats; Confectionery; Marzipan; Coated or filled products
    • A23G3/34Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
    • A23G3/36Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
    • A23G3/42Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G3/00Sweetmeats; Confectionery; Marzipan; Coated or filled products
    • A23G3/34Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
    • A23G3/36Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
    • A23G3/48Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/70Carbohydrates; Sugars; Derivatives thereof
    • A61K31/715Polysaccharides, i.e. having more than five saccharide radicals attached to each other by glycosidic linkages; Derivatives thereof, e.g. ethers, esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/62Nymphaeaceae (Water-lily family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/12Antihypertensives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
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  • Cardiology (AREA)
  • Heart & Thoracic Surgery (AREA)
  • Biotechnology (AREA)
  • Alternative & Traditional Medicine (AREA)
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  • Bioinformatics & Cheminformatics (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
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Abstract

The present invention relates to food technology fields more particularly to a kind of decompression hard candy and preparation method thereof.The invention discloses a kind of decompression hard candy, are made of the following components: Plumula Nelumbinis alkaloid, polysaccharides and xylitol.The decompression hard candy has the effect of decompression, helps to reduce hypertensive patient's blood pressure level, also edible for normal person's leisure for hypertensive patient's daily consumption, is used for preventing hypertension.The decompression hard candy mouthfeel is sweet, overcomes the original bitter taste of Lotus Plumule tea, and fully play the antihypertensive effect of Plumula Nelumbinis alkaloid, and every hard candy independent packaging is easy to carry.

Description

A kind of decompression hard candy and preparation method thereof
Technical field
The present invention relates to food technology fields more particularly to a kind of decompression hard candy and preparation method thereof.
Background technique
Hypertension is one of most common chronic disease and the most important risk factor of cardiovascular and cerebrovascular disease, cerebral apoplexy, Myocardial infarction, heart failure and chronic kidney disease are its major complications.
The equal sugar content of candy on the market is higher, is unfavorable for edible for patients with elevated blood pressure.
Summary of the invention
In view of this, the decompression hard candy can be effectively reduced the present invention provides a kind of decompression hard candy and preparation method thereof Blood pressure level, preventing hypertension, and mouthfeel is good, is suitble to daily consumption.
Its specific technical solution is as follows:
The present invention provides a kind of decompression hard candy, are made of the following components:
Plumula Nelumbinis alkaloid, polysaccharides and xylitol.
In the present invention, Plumula Nelumbinis alkaloid is mainly liensinine, isoliensinine, neferine, and Plumula Nelumbinis alkaloid can The blood pressure level that hypertensive patient can be effectively reduced is effectively reduced, there is good antihypertensive effect.
Polysaccharides not only has effects that enhancing is immune and immunological regulation also has anti-aging, adjusts blood lipid and drop blood The effect of sugar is easily absorbed by the human body, can prevent where the essence of one of most effective ingredient of fructus lycii pulp and fructus lycii The risk of the complication such as hyperlipidemia and hyperglycemia is suffered from reduction hypertensive patient.
Preferably, further includes: fragrance.
Preferably, by weight,
2~5 parts of the Plumula Nelumbinis alkaloid, more preferably 4 parts;
6~8 parts of the polysaccharides, more preferably 6 parts;
87~92 parts of the xylitol, more preferably 90 parts.
Preferably, described fragrance 0.3-0.6 parts, more preferably 0.4 part.
The present invention also provides the preparation methods of above-mentioned decompression hard candy, comprising the following steps:
Step 1: Plumula Nelumbinis alkaloid being mixed with polysaccharides, decocting is extracted, filtered, after concentration, obtains condensed cream;
Step 2: the condensed cream being mixed with xylitol, is stirred off, moulding by casting obtains decompression hard candy.
Preferably, the Plumula Nelumbinis alkaloid preparation method the following steps are included:
Step a: Lotus Plumule is dissolved in refluxing extraction in the first organic solvent, after concentration, obtains medicinal extract;
Step b: it will be eluted after medicinal extract dissolution, after concentration, obtain Plumula Nelumbinis alkaloid.
In the present invention, the first organic solvent is ethanol solution, and the mass concentration of the ethanol solution is 70%-80%;Institute Stating Lotus Plumule to be dissolved in the dissolution time of the first organic solvent is 10-15h;The volume of the Lotus Plumule and first organic solvent Than for 1:(10~12).
In the present invention, the temperature of refluxing extraction described in step a is 45 DEG C -85 DEG C, and the number of the refluxing extraction is 3 times, Each 2h.
In the present invention, the solvent of the dissolution of medicinal extract described in step b is the HCl that mass concentration is 0.1%;What the elution used Eluant, eluent is that 95% ethyl alcohol (contains 1%NH3·H2O);The elution uses D001 type cation exchange resin.
Preferably, the polysaccharides preparation method the following steps are included:
Step c: after the reflux degreasing of fructus lycii powder, fructus lycii residue is obtained;
Step d: the fructus lycii residue is dissolved in the second organic solvent, fructus lycii crude product is obtained;
Step e: the fructus lycii crude product is dissolved in 90~100 DEG C of water, solid matter is removed, is dissolved in third organic solvent In, obtain the polysaccharides.
Preferably, the second organic solvent and third organic solvent are ethyl alcohol.
In the present invention, the solvent of reflux degreasing described in step c is petroleum ether and acetone (1:1, v/v).
In step d, the fructus lycii residue is dissolved in the second organic solvent for sloughing monosaccharide and oligosaccharide.
In step e, the fructus lycii crude product is dissolved in 90~100 DEG C of water for extracting polysaccharide;It is dissolved in third organic solvent In be used for precipitate polysaccharides;Before obtaining the polysaccharides, further includes: use ethyl alcohol and acetone washing, vacuum drying.
As can be seen from the above technical solutions, the invention has the following advantages that
The present invention provides a kind of decompression hard candy, are made of the following components: Plumula Nelumbinis alkaloid, polysaccharides and xylose Alcohol.The decompression hard candy has the effect of decompression, helps to reduce hypertensive patient's blood pressure level, often eat for hypertensive patient day With, it is also edible for normal person's leisure, it is used for preventing hypertension.The decompression hard candy mouthfeel is sweet, and it is original to overcome Lotus Plumule tea Bitter taste, and fully play the antihypertensive effect of Plumula Nelumbinis alkaloid, every hard candy independent packaging is easy to carry.
Detailed description of the invention
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technical description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention without any creative labor, may be used also for those of ordinary skill in the art To obtain other attached drawings according to these attached drawings.
The HPLC figure for the Plumula Nelumbinis alkaloid that Fig. 1 embodiment of the present invention 1 provides, wherein 1 is liensinine, 2 be isoliensinine, 3 be neferine.
Specific embodiment
It in order to make the invention's purpose, features and advantages of the invention more obvious and easy to understand, below will be to of the invention real The technical solution applied in example is clearly and completely described, it is clear that the embodiments described below are only present invention a part Embodiment, and not all embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creation Property labour under the premise of all other embodiment obtained, shall fall within the protection scope of the present invention.
Embodiment 1
The present embodiment is the preparation of Plumula Nelumbinis alkaloid.
Take dry Lotus Plumule appropriate, after impregnating 12h with 12 times of 80% ethyl alcohol of amount, the refluxing extraction 3 times at a temperature of 70 DEG C, often Secondary 2h;Combined extract obtains medicinal extract after concentration;Medicinal extract adds appropriate 0.1% HCl to dissolve, and (contains 1%NH with 95% ethyl alcohol3· H2O) make eluant, eluent, obtain 95% ethanol eluate after the elution of D001 type cation exchange resin, under the conditions of 45 DEG C, depressurize dense Contracting 30min obtains Plumula Nelumbinis alkaloid crude product.
As shown in Figure 1, three peaks in Fig. 1 are respectively liensinine, isoliensinine and neferine.
Embodiment 2
The present embodiment is the preparation of polysaccharides.
The wolfberry fruit powder of dries pulverizing is weighed, with petroleum ether: acetone (1:1) reflux degreasing 20min filters out solvent, residue After air-drying, 80% ethyl alcohol of 10 times of amounts is added, stands 60min at room temperature, filters out solvent, residue water is in 90~100 DEG C of water-baths Polysaccharide is extracted, 40min is concentrated under reduced pressure under the conditions of 65 DEG C in extracting solution, and 95% ethanol precipitation polysaccharide is added in obtained concentrate, so Precipitating is washed with dehydrated alcohol again afterwards, 4h is dried in vacuo under the conditions of 45 DEG C, finally obtains fructus lycii Thick many candies.
Embodiment 3
The present embodiment is the preparation for being depressured hard candy.
The Plumula Nelumbinis alkaloid 20g, 2 polysaccharides 60g of embodiment that Example 1 provides.Xylitol 920g separately is taken, with reality 1 Plumula Nelumbinis alkaloid of example and the mixing of 2 polysaccharides of embodiment are applied, adds suitable quantity of water that dissolution is made to stir off completely, is endured to forefinger contact sugar Close up after slurry with thumb, separates two and refer to the thin sugared line that syrup can be pulled into a retractility, then set syrup on casting machine Casting, demolding after cooling, packaging is to get decompression hard candy.
Embodiment 4
The present embodiment is the preparation for being depressured hard candy.
Take Plumula Nelumbinis alkaloid 50g, polysaccharides 80g.Separately take xylitol 870g, 1 Plumula Nelumbinis alkaloid of embodiment and reality The mixing of 2 polysaccharides of example is applied, adds suitable quantity of water that dissolution is made to stir off, close up after enduring to forefinger contact syrup with thumb completely, separates two Refer to the thin sugared line that syrup can be pulled into a retractility, syrup is then set into casting machine upper, demolding after cooling, packet Dress is to get decompression hard candy.
Embodiment 5
The present embodiment is the preparation for being depressured hard candy.
Take Plumula Nelumbinis alkaloid 30g, polysaccharides 70g.Separately take xylitol 900g, with 1 Plumula Nelumbinis alkaloid of embodiment and The mixing of 2 polysaccharides of embodiment adds suitable quantity of water that dissolution is made to stir off, close up after enduring to forefinger contact syrup with thumb completely, separates Two refer to the thin sugared line that syrup can be pulled into a retractility, and syrup is then set casting machine upper, demolding after cooling, packet Dress is to get decompression hard candy.
Embodiment 6
The present embodiment is the preparation for being depressured hard candy.
Take Plumula Nelumbinis alkaloid 40g, polysaccharides 60g.Xylitol 900g, flavorant 4g separately are taken, with 1 lotus seeds of embodiment Heart alkaloid and 2 polysaccharides of embodiment mixing, add suitable quantity of water make dissolution completely, stir off, after enduring to forefinger contact syrup with thumb Finger closes up, and separates two and refers to the thin sugared line that syrup can be pulled into a retractility, syrup is then set casting machine upper, to cold But it demoulds afterwards, packaging is to get decompression hard candy.
Embodiment 7
The present embodiment is the preparation for being depressured hard candy.
Take Plumula Nelumbinis alkaloid 40g, polysaccharides 65g.Xylitol 890g, flavorant 3g separately are taken, with 1 lotus seeds of embodiment Heart alkaloid and 2 polysaccharides of embodiment mixing, add suitable quantity of water make dissolution completely, stir off, after enduring to forefinger contact syrup with thumb Finger closes up, and separates two and refers to the thin sugared line that syrup can be pulled into a retractility, syrup is then set casting machine upper, to cold But it demoulds afterwards, packaging is to get decompression hard candy.
Embodiment 8
The present embodiment is the preparation for being depressured hard candy.
Take Plumula Nelumbinis alkaloid 30g, polysaccharides 75g.Xylitol 890g, flavorant 5g separately are taken, with 1 lotus seeds of embodiment Heart alkaloid and 2 polysaccharides of embodiment mixing, add suitable quantity of water make dissolution completely, stir off, after enduring to forefinger contact syrup with thumb Finger closes up, and separates two and refers to the thin sugared line that syrup can be pulled into a retractility, syrup is then set casting machine upper, to cold But it demoulds afterwards, packaging is to get decompression hard candy.
Embodiment 9
The present embodiment carries out sensory evaluation to hard candy made from embodiment 3~8, and the results are shown in Table 1.
As shown in Table 1, because Plumula Nelumbinis alkaloid additional amount is less in embodiment 3, the content of xylitol is high, although hard candy Beautiful appearance, but sugariness is big;Plumula Nelumbinis alkaloid additive amount is more in embodiment 4, causes mouthfeel bitter;5 color of embodiment and Good mouthfeel;Embodiment 6 joined fragrance, thus its color and mouthfeel are good;Embodiment 7 is added compared with 6 fragrance of embodiment and reduces, and Plumula Nelumbinis alkaloid increases compared with 5 additional amount of embodiment, causes mouthfeel partially bitter;8 fragrance of embodiment is added excessively, and mouthfeel is caused to be paid no attention to Think.
Hard candy Analyses Methods for Sensory Evaluation Results made from 1 embodiment 3~8 of table
Note: 0~5 poor 6~8 good 9~10 is excellent.
The above, the above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations;Although referring to before Stating embodiment, invention is explained in detail, those skilled in the art should understand that: it still can be to preceding Technical solution documented by each embodiment is stated to modify or equivalent replacement of some of the technical features;And these It modifies or replaces, the spirit and scope for technical solution of various embodiments of the present invention that it does not separate the essence of the corresponding technical solution.

Claims (10)

1. a kind of decompression hard candy, which is characterized in that be made of the following components:
Plumula Nelumbinis alkaloid, polysaccharides and xylitol.
2. decompression hard candy according to claim 1, which is characterized in that further include: fragrance.
3. decompression hard candy according to claim 1 or 2, which is characterized in that by weight,
2~5 parts of the Plumula Nelumbinis alkaloid, 6~8 parts of the polysaccharides, 87~92 parts of the xylitol.
4. decompression hard candy according to claim 3, which is characterized in that by weight, 4 parts of the Plumula Nelumbinis alkaloid, 6 parts of the polysaccharides, 90 parts of the xylitol.
5. decompression hard candy according to claim 3, which is characterized in that described fragrance 0.3-0.6 parts.
6. decompression hard candy according to claim 5, which is characterized in that 0.4 part of the fragrance.
7. being depressured the preparation method of hard candy described in claim 1 to 6 any one, which comprises the following steps:
Step 1: Plumula Nelumbinis alkaloid being mixed with polysaccharides, decocting is extracted, filtered, after concentration, obtains condensed cream;
Step 2: the condensed cream being mixed with xylitol, is stirred off, moulding by casting obtains decompression hard candy.
8. preparation method according to claim 7, which is characterized in that the preparation method of the Plumula Nelumbinis alkaloid include with Lower step:
Step a: Lotus Plumule is dissolved in refluxing extraction in the first organic solvent, after concentration, obtains medicinal extract;
Step b: it will be eluted after medicinal extract dissolution, after concentration, obtain Plumula Nelumbinis alkaloid.
9. preparation method according to claim 7, which is characterized in that the preparation method of the polysaccharides includes following step It is rapid:
Step c: after the reflux degreasing of fructus lycii powder, fructus lycii residue is obtained;
Step d: the fructus lycii residue is dissolved in the second organic solvent, fructus lycii crude product is obtained;
Step e: the fructus lycii crude product is dissolved in 90~100 DEG C of water, solid matter is removed, is dissolved in third organic solvent, obtains To the polysaccharides.
10. preparation method according to claim 9, which is characterized in that the second organic solvent and third organic solvent are Ethyl alcohol.
CN201910797502.4A 2019-08-27 2019-08-27 A kind of decompression hard candy and preparation method thereof Pending CN110353073A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113768021A (en) * 2021-10-29 2021-12-10 绿优品(福建)健康科技研发中心有限公司 A pressed fructose with blood lipid and blood sugar reducing effects, and its preparation method

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1961700A (en) * 2005-11-07 2007-05-16 安徽福康药业有限责任公司 Hard sugar of green tea and preparation method thereof
CN103387620A (en) * 2013-08-08 2013-11-13 福建中医药大学 Polysaccharide, total flavonoid and total alksloid prepared from lotus plumule and preparation method thereof
CN104855663A (en) * 2015-06-02 2015-08-26 湘潭大学 Lotus nut fudge and preparation method thereof
CN105494844A (en) * 2014-10-20 2016-04-20 威海新异生物科技有限公司 Production method of Chinese wolfberry fruit tablet candy
CN106176963A (en) * 2016-07-22 2016-12-07 高华宏 A kind of Plumula Nelumbinis oral cavity disintegration tablet and preparation method thereof
CN108617835A (en) * 2018-05-04 2018-10-09 华东理工大学 A kind of polysaccharides soft sweets and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1961700A (en) * 2005-11-07 2007-05-16 安徽福康药业有限责任公司 Hard sugar of green tea and preparation method thereof
CN103387620A (en) * 2013-08-08 2013-11-13 福建中医药大学 Polysaccharide, total flavonoid and total alksloid prepared from lotus plumule and preparation method thereof
CN105494844A (en) * 2014-10-20 2016-04-20 威海新异生物科技有限公司 Production method of Chinese wolfberry fruit tablet candy
CN104855663A (en) * 2015-06-02 2015-08-26 湘潭大学 Lotus nut fudge and preparation method thereof
CN106176963A (en) * 2016-07-22 2016-12-07 高华宏 A kind of Plumula Nelumbinis oral cavity disintegration tablet and preparation method thereof
CN108617835A (en) * 2018-05-04 2018-10-09 华东理工大学 A kind of polysaccharides soft sweets and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113768021A (en) * 2021-10-29 2021-12-10 绿优品(福建)健康科技研发中心有限公司 A pressed fructose with blood lipid and blood sugar reducing effects, and its preparation method

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