CN110327269A - A kind of honey shaddock ferment essential oil shower cream and preparation method thereof - Google Patents
A kind of honey shaddock ferment essential oil shower cream and preparation method thereof Download PDFInfo
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- CN110327269A CN110327269A CN201910771855.7A CN201910771855A CN110327269A CN 110327269 A CN110327269 A CN 110327269A CN 201910771855 A CN201910771855 A CN 201910771855A CN 110327269 A CN110327269 A CN 110327269A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The present invention relates to a kind of sweet shaddock ferment essential oil shower cream and preparation method thereof, the raw material of the honey shaddock ferment essential oil shower cream includes 20 kinds of components such as Fructus Citri grandis extract, saccharomycetes to make fermentation product, orange oil, PEG-7 glyceryl cocoate, laureth sodium sulfovinate, Cocoamidopropyl betaine, glycerol, lauric acid, water.The component is subjected to appropriate weight proportion, is finally prepared to have and improves skin vitality, whitening and moistening skin, promotes skin metabolism, antibacterial bacteriostatic, the sweet shaddock ferment essential oil shower cream for being effectively improved the functions such as dry skin problem.Formula of the present invention improves the safety of product, reduces irritation, and consumer uses safer.Honey shaddock ferment essential oil shower cream of the present invention is colourless, tasteless and nonirritant, antibiotic and hormone is not contained, using safe and effective.
Description
Technical field
The invention belongs to articles for daily use technical fields, and in particular to a kind of honey shaddock ferment essential oil shower cream and its preparation side
Method.
Background technique
Shower cream is a kind of cleaning supplies that modern is common, and the invention of bath oil is primarily to replace tradition cleaning
The sense of touch and effect of soap.Most of existing shower cream is the effect for having played basic moisturizing, having removed body odour, cannot be very
Good plays skin care, antibacterial effect to skin.Traditional shower cream can not improve the vigor of skin, more be unable to improve skin
State, and preparation process is complicated, at high cost, ineffective, is unable to satisfy the market demand.
Summary of the invention
In order to solve the above problems existing in the present technology, the present invention provides a kind of sweet shaddock ferment essential oil shower cream and its
Preparation method.Honey shaddock ferment essential oil shower cream of the present invention, which has, to be improved skin vitality, whitening and moistening skin, promotes skin new old generation
It thanks, antibacterial bacteriostatic, be effectively improved the functions such as dry skin problem.Formula of the present invention improves the safety of product, reduces
Irritation, consumer use safer.
The technical scheme adopted by the invention is as follows:
A kind of honey shaddock ferment essential oil shower cream, raw material components include:
Water 37.64-65.12 parts by weight, laureth sodium sulfovinate 13-17 parts by weight, Cocoamidopropyl betaine
5-11 parts by weight, glycerol 4-6 parts by weight, lauric acid 3-5 parts by weight, acrylic acid esters co-polymer 2-4 parts by weight, coconut oleoyl amine
DEA 1-3 parts by weight, sodium cocoamphoacetate 1-3 parts by weight, sodium lauroyl sarcosine 1-3 parts by weight, trehalose 1-2 weight
Measure part, PEG-7 glyceryl cocoate 1-1.4 parts by weight, Fructus Citri grandis extract 0.5-1.5 parts by weight, saccharomycetes to make fermentation product 0.5-
1.5 parts by weight, orange oil 0.3-0.7 parts by weight, potassium hydroxide 0.8-0.94 parts by weight, sodium chloride 0.5-1.5 parts by weight, DMDM
Hydantoins 0.1-0.3 parts by weight, methyl hydroxybenzoate 0.05-0.15 parts by weight, allantoin 0.1-0.3 parts by weight, EDETATE SODIUM
0.03-0.07 parts by weight.
The raw material components of the further preferably described sweet shaddock ferment essential oil shower cream include:
It is 51.38 parts by weight of water, 15 parts by weight of laureth sodium sulfovinate, 8 parts by weight of Cocoamidopropyl betaine, sweet
Oily 5 parts by weight, 4 parts by weight of lauric acid, 3 parts by weight of acrylic acid esters co-polymer, 2 parts by weight of coconut oleoyl amine DEA, cocounut oil acyl two
2 parts by weight of property guanidine-acetic acid sodium, 2 parts by weight of sodium lauroyl sarcosine, 1.5 parts by weight of trehalose, PEG-7 glyceryl cocoate 1.2
Parts by weight, 1 parts by weight of Fructus Citri grandis extract, 1 parts by weight of saccharomycetes to make fermentation product, 0.5 parts by weight of orange oil, 0.87 weight of potassium hydroxide
Measure part, 1 parts by weight of sodium chloride, 0.2 parts by weight of DMDM hydantoin, 0.1 parts by weight of methyl hydroxybenzoate, 0.2 parts by weight of allantoin,
0.05 parts by weight of EDETATE SODIUM.
The step of preparing Fructus Citri grandis extract include:
(1) the shaddock fruit successively cleaned, cleaned, crushed, filtered and steam after adding soaking in Chinese liquor, wine is then added
Qu Jinhang fermentation, obtains fermentation material；
(2) fermentation material is distilled, obtains the Fructus Citri grandis extract.
Further, in step (1), it is 100-120 mesh that the pomelo powder, which is broken to partial size, and the temperature of the immersion is 25-
27 DEG C, the time of the immersion is 6-8 days, and the Alcohol degree of the white wine is 50-60 degree；The temperature steamed is 100-
120 DEG C, the time steamed is 60-80 minutes, and the additive amount of the distiller's yeast is the 1-3wt% of the Chinese prickly ash fruit weight, institute
Stating fermentation time is 30-60 days, and the temperature of the fermentation is 25-27 DEG C.
The step of preparing orange oil include:
Sweet orange is cleaned, water impregnate, drain after, successively carry out cryo-conservation, crushing, low temperature drying processing, later
It is placed in dehydrated alcohol and impregnates, and extract the oil in sweet orange using supercritical carbon dioxide extraction method, obtain orange oil.
Further, the water impregnates to impregnate 8-10h in 15-18 DEG C of water；The cryo-conservation is in liquid nitrogen
Save 4-6min；It is described to crush to be crushed to 140-150 mesh；The temperature of the low temperature drying is 40-50 DEG C；When water content reaches
After 8%-10%, 4-5h is impregnated in dehydrated alcohol, the addition quality of dehydrated alcohol is 0.8-1.2 times of sweet orange quality；It is described
The extracting pressure of supercritical carbon dioxide extraction method is 23-33Mpa, and extraction temperature is 35-45 DEG C, extraction time 50-
90min, carbon dioxide flow 15-17L/h.
The step of preparing saccharomycetes to make fermentation product include:
Pawpaw pulp, apple pulp and Poria cocos are subjected to boiling, sealing carries out first time hair after mixing with yeast, mature vinegar
Filtrate is then carried out second and fermented, the saccharomycetes to make fermentation product is obtained after filtering by ferment, filtering and collecting filter liquid.
The pawpaw pulp, apple pulp, Poria cocos mass ratio be 1:1:(2-4), the additive amount of the yeast is Poria cocos
The 2%-5% of quality, the additive amount of the mature vinegar are the 1%-3% of Poria cocos quality, and the temperature of the boiling is 100-110 DEG C,
The temperature of the first time fermentation and second of fermentation is 16-28 DEG C, and the time of fermentation is 90-120 days, second for the first time
The time of fermentation is 8-12 days.
The preparation method of the honey shaddock ferment essential oil shower cream, comprising the following steps:
(1) lauric acid, sodium hydroxide are added to the water, are heated after mixing evenly, obtain mixed system A；
(2) laureth sodium sulfovinate, methyl hydroxybenzoate, allantoin and EDETATE SODIUM mixing are added into mixed system A
Uniformly, it heats, obtains mixed system B；
(3) acrylic acid esters co-polymer is added into mixed system B to carry out homogeneous and heat, then adds coconut oleoyl amine
Propyl betaine, glycerol, coconut oleoyl amine DEA, sodium cocoamphoacetate, trehalose, PEG-7 glyceryl cocoate and chlorination
Sodium is uniformly mixed, and obtains mixed system C；
(4) sodium lauroyl sarcosine, Fructus Citri grandis extract, orange oil, saccharomycete hair are added into the mixed system C after cooling
Ferment product and DMDM hydantoin, stir evenly, up to the sweet shaddock ferment essential oil shower cream after detection is qualified.
Further, in step (1)-(3), the heating temperature is 70-90 DEG C；In step (3), the homogenizing time is
30s-90s；In step (4), the temperature of the mixed system C after the cooling is 40-50 DEG C, and the time of the stirring is 15-
25min。
The invention has the benefit that
Honey shaddock ferment essential oil shower cream of the present invention, raw material includes Fructus Citri grandis extract, saccharomycetes to make fermentation product, sweet orange
Oil, PEG-7 glyceryl cocoate, laureth sodium sulfovinate, Cocoamidopropyl betaine, glycerol, lauric acid, water etc. 20
Kind component.Orange oil is one of a small number of contrastimulant essential oils, has sweet tea sweet orange fragrance, can expel intense strain and pressure
Power, improve anxiety caused by insomnia, sweating can be promoted, thus can help the skin blocked be discharged toxin, to oiliness, dark sore or
Dry skin person is all helpful.Due in orange peel contain a large amount of Vitamin C, so sweet orange oil energy preventing cold, to skin
There are moistening effect, the pH-value of energy balance skin, help collagen to be formed, has good function for the growth and reparation of bodily tissue
Effect；Fructus Citri grandis extract has the function of antioxidation, stronger bacteriostasis and improves immunity of organisms；Saccharomycetes to make fermentation produces
Object has the function of moisturizing, moisturizing, except cutin, can also moisten that sebum secretion is prosperous, dry rough skin, helps body flesh
The balance and stability of skin promotes skin to restore elasticity.
Above-mentioned component is subjected to appropriate weight proportion, under the synergistic effect of each component, is finally prepared to have and improve
Skin vitality, promotes skin metabolism, antibacterial bacteriostatic, the sweet shaddock for being effectively improved the functions such as dry skin problem at whitening and moistening skin
Ferment essential oil shower cream.Formula of the present invention improves the safety of product, reduces irritation, and consumer, which uses, more to be pacified
Entirely.Honey shaddock ferment essential oil shower cream of the present invention is colourless, tasteless and nonirritant is had without containing antibiotic and hormone using safe
Effect.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Detailed description.Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained all without making creative work
Other embodiment belongs to the range that the present invention is protected.
1g is represented in following example with 1 parts by weight.
Embodiment 1
The present embodiment provides a kind of sweet shaddock ferment essential oil shower cream, raw material components include:
It is 65.12 parts by weight of water, 13 parts by weight of laureth sodium sulfovinate, 5 parts by weight of Cocoamidopropyl betaine, sweet
Oily 4 parts by weight, 3 parts by weight of lauric acid, 2 parts by weight of acrylic acid esters co-polymer, 1 parts by weight of coconut oleoyl amine DEA, cocounut oil acyl two
1 parts by weight of property guanidine-acetic acid sodium, 1 parts by weight of sodium lauroyl sarcosine, 1 parts by weight of trehalose, 1 weight of PEG-7 glyceryl cocoate
Part, 0.5 parts by weight of Fructus Citri grandis extract, 0.5 parts by weight of saccharomycetes to make fermentation product, 0.3 parts by weight of orange oil, 0.8 weight of potassium hydroxide
Measure part, 0.5 parts by weight of sodium chloride, 0.1 parts by weight of DMDM hydantoin, 0.05 parts by weight of methyl hydroxybenzoate, 0.1 weight of allantoin
Part, 0.03 parts by weight of EDETATE SODIUM.
The preparation of Fructus Citri grandis extract: shaddock fruit successively being cleaned, is cleaned, and being crushed to partial size is 100 mesh, adds 50 degree white
Wine impregnates 6 days at 25 DEG C, filtering, steams 60 minutes at 100 DEG C, and the distiller's yeast of shaddock fruit weight 1wt% is then added at 25 DEG C
Fermentation 30 days, obtains fermentation material, the fermentation material is distilled, obtain the Fructus Citri grandis extract.
The preparation of orange oil: sweet orange is cleaned, and impregnates 8h in 15 DEG C of water, and after draining, 4min is saved in liquid nitrogen,
140 mesh are crushed to, are dried at 40 DEG C, after water content reaches 8%, are impregnated in 0.8 times of sweet orange quality of dehydrated alcohol
4h, and the oil in sweet orange, extracting pressure 23Mpa are extracted using supercritical carbon dioxide extraction method, extraction temperature is 35 DEG C,
Extraction time is 50min, and carbon dioxide flow 15L/h obtains orange oil.
The preparation of saccharomycetes to make fermentation product: by mass ratio be 1:1:2 pawpaw pulp, apple pulp and Poria cocos at 100 DEG C
Lower carry out boiling, seals after mixing with the mature vinegar of the yeast of Poria cocos quality 2%, Poria cocos quality 1%, ferments 90 days at 16 DEG C, mistake
Filtrate is collected after filter, then filtrate is fermented 8 days at 16 DEG C, and the saccharomycetes to make fermentation product is obtained after filtering.
The preparation method of the honey shaddock ferment essential oil shower cream, includes the following steps:
(1) lauric acid, sodium hydroxide are added to the water, are heated to 70 DEG C after mixing evenly, obtain mixed system A；
(2) laureth sodium sulfovinate, methyl hydroxybenzoate, allantoin and EDETATE SODIUM mixing are added into mixed system A
Uniformly, 70 DEG C are heated to, mixed system B is obtained；
(3) acrylic acid esters co-polymer homogeneous 30s is added into mixed system B, is heated to 70 DEG C, then adds cocounut oil
Amido propyl betaine, glycerol, coconut oleoyl amine DEA, sodium cocoamphoacetate, trehalose, PEG-7 glyceryl cocoate and
Sodium chloride is uniformly mixed, and obtains mixed system C；
(4) sodium lauroyl sarcosine, Fructus Citri grandis extract, orange oil, yeast are added into the mixed system C for be cooled to 40 DEG C
Bacterium tunning and DMDM hydantoin stir 15min, up to the sweet shaddock ferment essential oil shower cream after detection is qualified.
Embodiment 2
The present embodiment provides a kind of sweet shaddock ferment essential oil shower cream, raw material components include:
37.64 parts by weight of water, 17 parts by weight of laureth sodium sulfovinate, 11 parts by weight of Cocoamidopropyl betaine,
6 parts by weight of glycerol, 5 parts by weight of lauric acid, 4 parts by weight of acrylic acid esters co-polymer, 3 parts by weight of coconut oleoyl amine DEA, cocounut oil acyl
3 parts by weight of both sexes guanidine-acetic acid sodium, 3 parts by weight of sodium lauroyl sarcosine, 2 parts by weight of trehalose, PEG-7 glyceryl cocoate 1.4
Parts by weight, 1.5 parts by weight of Fructus Citri grandis extract, 1.5 parts by weight of saccharomycetes to make fermentation product, 0.7 parts by weight of orange oil, potassium hydroxide
0.94 parts by weight, 1.5 parts by weight of sodium chloride, 0.3 parts by weight of DMDM hydantoin, 0.15 parts by weight of methyl hydroxybenzoate, allantoin 0.3
Parts by weight, 0.07 parts by weight of EDETATE SODIUM.
The preparation of Fructus Citri grandis extract: shaddock fruit successively being cleaned, is cleaned, and being crushed to partial size is 120 mesh, adds 60 degree white
Wine impregnates 8 days at 27 DEG C, filtering, steams 80 minutes at 120 DEG C, and the distiller's yeast of shaddock fruit weight 3wt% is then added at 27 DEG C
Fermentation 60 days, obtains fermentation material, the fermentation material is distilled, obtain the Fructus Citri grandis extract.
The preparation of orange oil: sweet orange is cleaned, and impregnates 10h in 18 DEG C of water, after draining, is saved in liquid nitrogen
6min is crushed to 150 mesh, is dried at 50 DEG C, after water content reaches 10%, in 1.2 times of dehydrated alcohol of sweet orange quality
Middle immersion 5h, and the oil in sweet orange, extracting pressure 33Mpa, extraction temperature are extracted using supercritical carbon dioxide extraction method
It is 45 DEG C, extraction time 90min, carbon dioxide flow 17L/h and obtains orange oil.
The preparation of saccharomycetes to make fermentation product: by mass ratio be 1:1:4 pawpaw pulp, apple pulp and Poria cocos at 110 DEG C
Lower carry out boiling, seals after mixing with the mature vinegar of the yeast of Poria cocos quality 5%, Poria cocos quality 3%, ferments 120 days at 28 DEG C, mistake
Filtrate is collected after filter, then filtrate is fermented 12 days at 28 DEG C, and the saccharomycetes to make fermentation product is obtained after filtering.
The preparation method of the honey shaddock ferment essential oil shower cream, includes the following steps:
(1) lauric acid, sodium hydroxide are added to the water, are heated to 90 DEG C after mixing evenly, obtain mixed system A；
(2) laureth sodium sulfovinate, methyl hydroxybenzoate, allantoin and EDETATE SODIUM mixing are added into mixed system A
Uniformly, 90 DEG C are heated to, mixed system B is obtained；
(3) acrylic acid esters co-polymer homogeneous 90s is added into mixed system B, is heated to 90 DEG C, then adds cocounut oil
Amido propyl betaine, glycerol, coconut oleoyl amine DEA, sodium cocoamphoacetate, trehalose, PEG-7 glyceryl cocoate and
Sodium chloride is uniformly mixed, and obtains mixed system C；
(4) sodium lauroyl sarcosine, Fructus Citri grandis extract, orange oil, yeast are added into the mixed system C for be cooled to 50 DEG C
Bacterium tunning and DMDM hydantoin stir 25min, up to the sweet shaddock ferment essential oil shower cream after detection is qualified.
Embodiment 3
The present embodiment provides a kind of sweet shaddock ferment essential oil shower cream, raw material components include:
It is 51.38 parts by weight of water, 15 parts by weight of laureth sodium sulfovinate, 8 parts by weight of Cocoamidopropyl betaine, sweet
Oily 5 parts by weight, 4 parts by weight of lauric acid, 3 parts by weight of acrylic acid esters co-polymer, 2 parts by weight of coconut oleoyl amine DEA, cocounut oil acyl two
2 parts by weight of property guanidine-acetic acid sodium, 2 parts by weight of sodium lauroyl sarcosine, 1.5 parts by weight of trehalose, PEG-7 glyceryl cocoate 1.2
Parts by weight, 1 parts by weight of Fructus Citri grandis extract, 1 parts by weight of saccharomycetes to make fermentation product, 0.5 parts by weight of orange oil, 0.87 weight of potassium hydroxide
Measure part, 1 parts by weight of sodium chloride, 0.2 parts by weight of DMDM hydantoin, 0.1 parts by weight of methyl hydroxybenzoate, 0.2 parts by weight of allantoin,
0.05 parts by weight of EDETATE SODIUM.
The preparation of Fructus Citri grandis extract: shaddock fruit successively being cleaned, is cleaned, and being crushed to partial size is 110 mesh, adds 55 degree white
Wine impregnates 7 days at 26 DEG C, filtering, steams 70 minutes at 110 DEG C, and the distiller's yeast of shaddock fruit weight 2wt% is then added at 26 DEG C
Fermentation 45 days, obtains fermentation material, the fermentation material is distilled, obtain the Fructus Citri grandis extract.
The preparation of orange oil: sweet orange is cleaned, and impregnates 9h in 17 DEG C of water, and after draining, 5min is saved in liquid nitrogen,
Be crushed to 145 mesh, be dried at 45 DEG C, after water content reaches 9%, with impregnated in the dehydrated alcohol of the quality such as sweet orange
4.5h, and the oil in sweet orange, extracting pressure 28Mpa, extraction temperature 40 are extracted using supercritical carbon dioxide extraction method
DEG C, extraction time 70min, carbon dioxide flow 16L/h obtain orange oil.
The preparation of saccharomycetes to make fermentation product: by mass ratio be 1:1:3 pawpaw pulp, apple pulp and Poria cocos at 105 DEG C
Lower carry out boiling, seals after mixing with the mature vinegar of the yeast of Poria cocos quality 4%, Poria cocos quality 2%, ferments 105 days at 20 DEG C, mistake
Filtrate is collected after filter, then filtrate is fermented 10 days at 20 DEG C, and the saccharomycetes to make fermentation product is obtained after filtering.
The preparation method of the honey shaddock ferment essential oil shower cream, includes the following steps:
(1) lauric acid, sodium hydroxide are added to the water, are heated to 80 DEG C after mixing evenly, obtain mixed system A；
(2) laureth sodium sulfovinate, methyl hydroxybenzoate, allantoin and EDETATE SODIUM mixing are added into mixed system A
Uniformly, 80 DEG C are heated to, mixed system B is obtained；
(3) acrylic acid esters co-polymer homogeneous 60s is added into mixed system B, is heated to 80 DEG C, then adds cocounut oil
Amido propyl betaine, glycerol, coconut oleoyl amine DEA, sodium cocoamphoacetate, trehalose, PEG-7 glyceryl cocoate and
Sodium chloride is uniformly mixed, and obtains mixed system C；
(4) sodium lauroyl sarcosine, Fructus Citri grandis extract, orange oil, yeast are added into the mixed system C for be cooled to 45 DEG C
Bacterium tunning and DMDM hydantoin stir 20min, up to the sweet shaddock ferment essential oil shower cream after detection is qualified.
Comparative example 1
It is only that the difference of formula components with embodiment 3, does not contain Fructus Citri grandis extract, saccharomycetes to make fermentation in this comparative example 1
Product and orange oil, other raw material components and preparation method are same as Example 3.
Comparative example 2
Be only that the preparation method of Fructus Citri grandis extract is different from embodiment 3, in this comparative example using steam distillation into
Row extracts, other operations are same as Example 3, and wherein steam distillation prepares the concrete operation step of each plant extracts
Are as follows: it takes shaddock fruit successively to be cleaned respectively, dry, pulverize and the water of 2 times of quality is added to 100-200 mesh carries out heating distillation, receive
Collect distillate, obtains Fructus Citri grandis extract.
Comparative example 3
This comparative example is that the difference of embodiment 3 is only that the preparation method of saccharomycetes to make fermentation product is different, in this comparative example
It is only for the first fermentation, second of fermentation operation is removed, other operations are same as Example 3.
Experimental example
One, bacteriostatic test is carried out to sweet shaddock ferment essential oil shower cream obtained by embodiment 1-3 and comparative example 1-3.
Bacterium solution is coated on solid agar plate and is inoculated with, by sweet shaddock ferment obtained by the embodiment 1-3 and comparative example 1-3
Plain essential oil shower cream is separately added on inoculated plate, is done three groups of identical tests in parallel respectively, is cultivated 10min at 25 DEG C, training
Supporting terminates, and detects bacteriostasis rate, three cell means is taken to be recorded in table respectively.
Table 1- bacteriostasis result
| Group | Escherichia coli bacteriostasis rate (%) | Staphylococcus aureus bacteriostasis rate (%) | Candida albicans bacteriostasis rate (%) |
| Embodiment 1 | 86.4 | 76.1 | 78.9 |
| Embodiment 2 | 88.4 | 75.8 | 76.8 |
| Embodiment 3 | 89.8 | 79.9 | 79.3 |
| Comparative example 1 | 50.6 | 43.9 | 42.6 |
| Comparative example 2 | 73.5 | 60.1 | 61.3 |
| Comparative example 3 | 76.3 | 62.3 | 64.2 |
As can be seen from Table 1, sweet shaddock ferment essential oil shower cream obtained by embodiment 1-3 is to Escherichia coli, Staphylococcus aureus
The inhibiting effect of bacterium and Candida albicans is apparently higher than shower cream obtained by comparative example 1-3, also demonstrates 1-3 of embodiment of the present invention institute
Obtaining sweet shaddock ferment essential oil shower cream has good bacteriostasis efficacy.
Two, the moistening effect test of shower cream obtained by embodiment 1-3 and comparative example 1-3
The patient of 60 dry skins is chosen, of all ages, gender is divided into 6 groups, every group of 10 people, respectively embodiment 1-3
Group and comparative example 1-3 group allow subject using the shower cream more than embodiment 1-3 and comparative example 1-3, daily using primary, one
The leg skin moisture content and skin elasticity situation that study subject is tested after month, are averaged, test case is as shown in table 2.
Table 2- skin moisture content and skin elasticity situation test result
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Moisture content of skin | + 52.3% | + 53.5% | + 54.5% | + 23.4% | + 36.6% | + 37.1% |
| Skin elasticity | + 25.7% | + 23.8% | + 26.5% | + 12.5% | + 19.7% | + 17.8% |
By table 2 the results show that sweet shaddock ferment essential oil shower cream is to skin moisture content and skin bullet obtained by the present embodiment 1-3
Property be significantly increased, hence it is evident that be higher than comparative example 1-3 acquired results, illustrate shower cream of the present invention other than cleaning efficacy, also
Can depth nourish skin, keep skin moisturizing it is glossy, lasting moisturizing, improve skin quality.
Three, health chemical testing
Content detection is carried out to lead, arsenic, mercury and the cadmium in the sweet shaddock ferment essential oil shower cream of 3 gained of embodiment, as a result 3 institute of table
Show.
Table 3- health chemical testing result
As can be seen from Table 3, the lead in the sweet shaddock ferment essential oil shower cream of the gained of the embodiment of the present invention 3, arsenic, mercury and cadmium contain
Amount meets the limitation regulation of " cosmetics safety technical specification " 2015 editions.
Four, Micro biological Tests
To the total plate count in the sweet shaddock ferment essential oil shower cream of 3 gained of embodiment, yeast and mold sum, heat-resisting large intestine
Flora, staphylococcus aureus, pseudomonas aeruginosa content detected, as a result shown in table 4.
Table 4- health chemical testing result
| Inspection project | Inspection result | Inspection result |
| Total plate count | < 10 | ≤1000 |
| Yeast and mold sum | < 10 | ≤100 |
| Heat-resisting coliform | It is not detected | It must not detect |
| Staphylococcus aureus | It is not detected | It must not detect |
| Pseudomonas aeruginosa | It is not detected | It must not detect |
As can be seen from Table 4, the total plate count in the sweet shaddock ferment essential oil shower cream of the gained of the embodiment of the present invention 3, mould and
Saccharomycete sum, heat-resisting coliform, staphylococcus aureus, pseudomonas aeruginosa content meet " cosmetics safety skill
Art specification " 2015 editions limitation regulations.
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Those familiar with the art in the technical scope disclosed by the present invention, can easily think of the change or the replacement, and should all contain
Lid is within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. a kind of honey shaddock ferment essential oil shower cream, which is characterized in that raw material components include:
Water 37.64-65.12 parts by weight, laureth sodium sulfovinate 13-17 parts by weight, Cocoamidopropyl betaine 5-11
Parts by weight, glycerol 4-6 parts by weight, lauric acid 3-5 parts by weight, acrylic acid esters co-polymer 2-4 parts by weight, coconut oleoyl amine DEA 1-
3 parts by weight, sodium cocoamphoacetate 1-3 parts by weight, sodium lauroyl sarcosine 1-3 parts by weight, trehalose 1-2 parts by weight,
PEG-7 glyceryl cocoate 1-1.4 parts by weight, Fructus Citri grandis extract 0.5-1.5 parts by weight, saccharomycetes to make fermentation product 0.5-1.5 weight
Measure part, orange oil 0.3-0.7 parts by weight, potassium hydroxide 0.8-0.94 parts by weight, sodium chloride 0.5-1.5 parts by weight, in DMDM second
Uride 0.1-0.3 parts by weight, methyl hydroxybenzoate 0.05-0.15 parts by weight, allantoin 0.1-0.3 parts by weight, EDETATE SODIUM 0.03-
0.07 parts by weight.
2. honey shaddock ferment essential oil shower cream according to claim 1, which is characterized in that raw material components include:
51.38 parts by weight of water, 15 parts by weight of laureth sodium sulfovinate, 8 parts by weight of Cocoamidopropyl betaine, glycerol 5
Parts by weight, 4 parts by weight of lauric acid, 3 parts by weight of acrylic acid esters co-polymer, 2 parts by weight of coconut oleoyl amine DEA, cocounut oil acyl both sexes base
2 parts by weight of sodium acetate, 2 parts by weight of sodium lauroyl sarcosine, 1.5 parts by weight of trehalose, 1.2 weight of PEG-7 glyceryl cocoate
Part, 1 parts by weight of Fructus Citri grandis extract, 1 parts by weight of saccharomycetes to make fermentation product, 0.5 parts by weight of orange oil, 0.87 weight of potassium hydroxide
Part, 1 parts by weight of sodium chloride, 0.2 parts by weight of DMDM hydantoin, 0.1 parts by weight of methyl hydroxybenzoate, 0.2 parts by weight of allantoin, EDTA
0.05 parts by weight of disodium.
3. honey shaddock ferment essential oil shower cream according to claim 1, which is characterized in that the step of preparing Fructus Citri grandis extract packet
It includes:
(1) the shaddock fruit successively cleaned, cleaned, crushed, filtered and steam after adding soaking in Chinese liquor, then be added distiller's yeast into
Row fermentation, obtains fermentation material；
(2) fermentation material is distilled, obtains the Fructus Citri grandis extract.
4. sweet shaddock ferment essential oil shower cream according to claim 3, which is characterized in that in step (1), the pomelo powder is broken to
Partial size is 100-120 mesh, and the temperature of the immersion is 25-27 DEG C, and the time of the immersion is 6-8 days, the alcohol of the white wine
Degree is 50-60 degree；The temperature steamed is 100-120 DEG C, and the time steamed is 60-80 minutes, the distiller's yeast
Additive amount is the 1-3wt% of the shaddock fruit weight, and the fermentation time is 30-60 days, and the temperature of the fermentation is 25-27 DEG C.
5. honey shaddock ferment essential oil shower cream according to claim 1, which is characterized in that the step of preparing orange oil include:
Sweet orange is cleaned, water impregnate, drain after, successively carry out cryo-conservation, crushing, low temperature drying processing, be placed on
It is impregnated in dehydrated alcohol, and extracts the oil in sweet orange using supercritical carbon dioxide extraction method, obtain orange oil.
6. honey shaddock ferment essential oil shower cream according to claim 5, which is characterized in that the water impregnates at 15-18 DEG C
Water in impregnate 8-10h；The cryo-conservation is that 4-6min is saved in liquid nitrogen；It is described to crush to be crushed to 140-150 mesh；Institute
The temperature for stating low temperature drying is 40-50 DEG C；After water content reaches 8%-10%, 4-5h, anhydrous second are impregnated in dehydrated alcohol
The addition quality of alcohol is 0.8-1.2 times of sweet orange quality；The extracting pressure of the supercritical carbon dioxide extraction method is 23-
33Mpa, extraction temperature are 35-45 DEG C, extraction time 50-90min, carbon dioxide flow 15-17L/h.
7. honey shaddock ferment essential oil shower cream according to claim 1, which is characterized in that prepare the step of saccharomycetes to make fermentation product
Suddenly include:
Pawpaw pulp, apple pulp and Poria cocos are subjected to boiling, for the first fermentation, mistake is sealed after mixing with yeast, mature vinegar
Filtrate is collected after filter, and filtrate is then carried out second and is fermented, the saccharomycetes to make fermentation product is obtained after filtering.
8. honey shaddock ferment essential oil shower cream according to claim 7, which is characterized in that the pawpaw pulp, apple pulp,
The mass ratio of Poria cocos is 1:1:(2-4), the additive amount of the yeast is the 2%-5% of Poria cocos quality, the additive amount of the mature vinegar
For the 1%-3% of Poria cocos quality, the temperature of the boiling is 100-110 DEG C, the temperature of the first time fermentation and second of fermentation
Degree is 16-28 DEG C, and the time of fermentation is 90-120 days for the first time, and the time of second of fermentation is 8-12 days.
9. the preparation method of any one of the claim 1-2 sweet shaddock ferment essential oil shower cream, which is characterized in that including following step
It is rapid:
(1) lauric acid, sodium hydroxide are added to the water, are heated after mixing evenly, obtain mixed system A；
(2) laureth sodium sulfovinate, methyl hydroxybenzoate, allantoin and EDETATE SODIUM are added into mixed system A to be uniformly mixed,
Heating, obtains mixed system B；
(3) acrylic acid esters co-polymer is added into mixed system B to carry out homogeneous and heat, then adds cocamidopropyl propyl amide
Glycine betaine, glycerol, coconut oleoyl amine DEA, sodium cocoamphoacetate, trehalose, PEG-7 glyceryl cocoate and sodium chloride are mixed
It closes uniformly, obtains mixed system C；
(4) sodium lauroyl sarcosine, Fructus Citri grandis extract, orange oil, saccharomycetes to make fermentation are added into the mixed system C after cooling to produce
Object and DMDM hydantoin, stir evenly, up to the sweet shaddock ferment essential oil shower cream after detection is qualified.
10. the preparation method of sweet shaddock ferment essential oil shower cream according to claim 9, which is characterized in that step (1)-(3)
In, the heating temperature is 70-90 DEG C；
In step (3), the homogenizing time is 30s-90s；
In step (4), the temperature of the mixed system C after the cooling is 40-50 DEG C, and the time of the stirring is 15-25min.
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| CN115992184A (en) * | 2023-03-23 | 2023-04-21 | 科乐美(广州)生物科技有限公司 | Biological fermentation surfactant, cosmetic and preparation method thereof |
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