CN109288768A - A kind of Chinese torreya shampoo and preparation method thereof - Google Patents

A kind of Chinese torreya shampoo and preparation method thereof Download PDF

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CN109288768A
CN109288768A CN201811106921.0A CN201811106921A CN109288768A CN 109288768 A CN109288768 A CN 109288768A CN 201811106921 A CN201811106921 A CN 201811106921A CN 109288768 A CN109288768 A CN 109288768A
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骆冠军
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Zhejiang Guanlide Health Industry Co Ltd
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Zhejiang Guanlide Health Industry Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9755Gymnosperms [Coniferophyta]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00Drugs for dermatological disorders
    • A61P17/04Antipruritics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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Abstract

The invention discloses a kind of Chinese torreya shampoos and preparation method thereof, including Chinese torreyanut extract, chelating agent, moisturizer, bleeding agent, surfactant, film forming agent, aromatic, preservative, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, emollients, hair restorer, acid-base modifier, hair conditioner, cosolvent and water, the weight ratio of the Chinese torreyanut extract is 0.25-0.45 parts, the weight ratio of the skin conditioning agent is 0.04-0.06 parts of monkey-bread tree seed extract, 0.04-0.06 parts of dried tremella extract, 0.04-0.06 parts of Radix Salviae Miltiorrhizae root extract, 0.04-0.06 parts of Black Ganoderma extract, 0.04-0.06 parts of black tea extract, 0.04-0.06 parts of kuh-seng root extract, lotus flower water 0.04 - 0.06 part, 0.04-0.06 parts of Chinese herbaceous peony root extract, 0.04-0.06 parts of white pond lily flower extract, 0.04-0.06 parts of tuckahoe extracts and 0.04-0.06 parts of coptis extract, the effect of Chinese torreyanut inhibits the growth of acne pathogenic bacteria, antipruritic and adjusting grease glandular secretion is given full play of, scalp dandruff and long acne problem are effectively slowed down.

Description

A kind of Chinese torreya shampoo and preparation method thereof
[technical field]
The present invention relates to the technical field of shampoo, the technology of especially a kind of Chinese torreya shampoo and preparation method thereof is led Domain.
[background technique]
Chinese torreya also known as Chinese torreyanut, goat's horn Chinese torreya and thin Chinese torreya etc. are taxaceae Chinese torreya category aiphylliums, belong to kind of an interior natural variation by Chinese torreya The excellent variety that type is cultivated through vegetative propagation, be distributed in China more save, be collection it is edible, medicinal, oily use, material use and The multipurpose rare tree of ornamental greening.Chinese torreya whole body be it is precious, be commonly called as only " green peel " aril allow number of people pain not , the exosper of Chinese torreya aril system taxaceae Chinese torreya platymiscium Chinese torreya fruit, but account for about its seed fresh weight 50~60%, always Since people can not find to its reasonable utilization approach, green peel is deposited in Around the house and streams side as processing waste, It not only results in waste of resources, also pollution environment.
Chinese torreya aril oil content is high, and the plants essential oil therefrom extracted is not only with high purity, and active constituent is more, and with special Fragrance and significant pharmacological effect, be mainly manifested in mosquito dispersing, antibacterial, anti-oxidant etc., be rare cosmetics Raw materials for production.It is detected Chinese torreya essential oil and contains limonene, australene, nopinene, ocimenum, 3- amphene, β-phellandrene, laurene It is edible or as the fragrant main source in daily chemical product Deng tens kinds of volatile aromatic ingredients, there is very high economy Value.It is reported that also containing a variety of flavones such as Kaempferol, acacetin, chrysoeriol, wogonin, chlorogenic acids in Chinese torreya And polyphenol compound, the presence of these pharmacological components make Chinese torreya aril have antibacterial analgesia, adjust blood lipid, is anti-oxidant With the functions such as antitumor, there is positive health benefit to related disease is prevented and treated.
One importance of hair cleaning and nursing is control dandruff.The appearance of dandruff is often accompanied by irritation itch, People would generally be caused to scratch with oneself not feeling, so as to cause scalp breakage and infected, and the mistake in self-healing of damaged scalp It can cause itch in journey again.In addition, modern by reason of heavy pressure, diet is irregular and the reasons such as environmental pollution cause on scalp President's small pox will lead to small pox breakage infection if scalp is excessively cleaned during hair washing, if scalp cleaning is not thorough It will lead to grease blocking scalp pore, a series of problems, such as this two o'clock can cause dandruff, itch and alopecia.It is returned certainly current Under right trend, shampoo product is naturally changed, nutrient laden and nontoxicity are increasingly favored by masses.It is therefore, a to be directed to Chinese torreya, Can sufficiently excite its antibacterial, antipruritic and control sebum secretion characteristic and the shampoo for having effects that recuperate of special allotment with good Good market prospects.
[summary of the invention]
The object of the invention is to solve the problems of the prior art, a kind of Chinese torreya shampoo and preparation method thereof is proposed, It can be by adding chelating agent, moisturizer, bleeding agent, surfactant, film forming agent, aromatic, anti-corrosion in Chinese torreyanut extract Agent, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, emollients, hair restorer, acid-base modifier, head Conditioner and cosolvent are sent out, making the shampoo prepared is in the colourless transparent liquid shape with unique fragrance, is given full play of Chinese torreyanut inhibits the effect of growth of acne pathogenic bacteria, antipruritic and adjusting grease glandular secretion, and various plant hydrosols act synergistically, Moisturizing is releived under the conditions of sufficiently clean to scalp, is balanced scalp fat secretion, is effectively slowed down scalp dandruff and long acne problem.
To achieve the above object, the present invention is achieved through the following technical solutions:
A kind of Chinese torreya shampoo, including Chinese torreyanut extract, chelating agent, moisturizer, bleeding agent, surfactant, film forming agent, Aromatic, preservative, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, emollients, hair restorer, acid Alkali regulator, hair conditioner, cosolvent and water, the weight ratio of the Chinese torreyanut extract are 0.25-0.45 parts, the chelating The weight ratio of agent is EDETATE SODIUM 0.04-0.06 parts, and the weight ratio of the moisturizer is panthenol 0.2-0.4 parts, lysine 0.1-0.3 parts, 0.1-0.3 parts of phenylalanine and 0.1-0.3 parts of arginine, the weight ratio of the bleeding agent are 1,2- hexylene glycol 0.4-0.6 parts, the weight ratio of the surfactant is 12-14 parts of laureth sulfuric ester ammonium and cocamidopropyl propyl amide sweet tea 6-8 parts of dish alkali, the weight ratio of the film forming agent is guar hydroxypropyltrimonium chloride 0.2-0.4 parts, the aromatic Weight ratio be daily essence 0.5-0.7 part, the weight ratio of the preservative is sodium benzoate 0.4-0.6 parts, described to resist The weight ratio of electrostatic agent is the Polyquaternium-10 and 0.2-0.4 of stearamidopropyl dimethylamine 0.4-0.6 parts, 0.2-0.4 parts The laureth -4 of part, the weight ratio of the skin conditioning agent is 0.04-0.06 parts of monkey-bread tree seed extract, tremella mentions Take 0.04-0.06 parts of object, 0.04-0.06 parts of Radix Salviae Miltiorrhizae root extract, 0.04-0.06 parts of Black Ganoderma extract, black tea extract 0.04-0.06 parts, 0.04-0.06 parts of kuh-seng root extract, 0.04-0.06 parts of lotus flower water, Chinese herbaceous peony root extract 0.04-0.06 Part, 0.04-0.06 parts of white pond lily flower extract, 0.04-0.06 parts of tuckahoe extracts and 0.04-0.06 parts of coptis extract, institute The weight ratio for stating foaming agent is 1-3 parts of laurel alcohol sulfuric ester ammonium, and the weight ratio of the hydrophily thickening agent is coconut oleoyl amine 0.5-1.5 parts of DEA, the weight ratio of the salubrious agent is 0.04-0.06 parts of leaf of Mentha piperita extract, the weight of the emollients Amount ratio is 0.5-1.5 parts of PEG-7 glyceryl cocoate, 0.2-0.4 parts of cetanol and 0.2-0.4 parts of stearyl alcohol, the hair tonic The weight ratio of agent is Candida/glucose/0.2-0.4 parts of rapeseed methyl oleate tunning, the acid-base modifier Weight ratio be citric acid 0.2-0.4 part, the weight ratio of the hair conditioner is coconut water 0.04-0.06 parts, described The weight ratio of cosolvent is rilanit special 0.5-0.7 parts, and the weight ratio of the water is 63.11-74.99 parts.
Preferably, the extraction step of the Chinese torreyanut extract includes the following:
1. Chinese torreya pericarp is added in agitator tank, it is stirred for that mixed material, the Chinese torreya pericarp is made after soaking in water Weight ratio with water is 3:10, soaking time 60-90min, mixing time 25-35min;
2. being sucked mixed material in distillation still using vacuum pump, while the mixed material in distillation still is added while stirring Heat;
3. remaining temperature-resistant, and pass through the steam distilled out successively when the temperature of mixed material reaches 120-130 DEG C Cross condenser and chiller treatment, distillation time 300min;
4. the cooling oil water mixture out of condensation is successively imported quiet in the first oil water separator and the second oil water separator It sets until oil water mixture is layered;
5. by being saved in the second oil water separator at the middle and upper levels essential oil importing essential oil storage tank.
A kind of preparation method of Chinese torreya shampoo, includes the following steps:
1. a part of water and other load weighted A phase raw materials are added in main agitated kettle, stirring and dissolving, temperature is 70~75 DEG C, revolving speed 100-300rpm, when a length of 60min;
2. remaining water and other load weighted B phase raw materials are individually dissolved by heating in advance, temperature is 70-75 DEG C, Revolving speed is 100-300rpm, and the B phase raw material dissolved is added in A phase raw material and is stirred, and temperature is 70-75 DEG C, and revolving speed is 200rpm, when a length of 180min;
3. load weighted C phase raw material is individually dissolved in advance, revolving speed 100-300rpm, C phase raw material is added and is led Agitated kettle stirring, temperature are 70-75 DEG C, revolving speed 200rpm, when a length of 30min;
4. load weighted D phase raw material is individually dissolved in advance, revolving speed 100-300rpm, D phase raw material is added and is led Stirred in agitated kettle, temperature is 70-75 DEG C, revolving speed 100rpm, when a length of 15min;
5. load weighted E phase raw material is individually dissolved in advance, main agitated kettle is cooled to 40 by revolving speed 100-300rpm ~50 DEG C, E phase raw material is added in main agitated kettle and is stirred, revolving speed 100rpm, duration 15min;
6. degassing, sample detection carry out filling, packaging after all qualifieds.
Preferably, the A phase raw material is laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium, stearamide propyl Dimethylamine, EDETATE SODIUM and water, the B phase raw material are guar hydroxypropyltrimonium chloride and water, and the C phase raw material is coconut palm Oleamide propyl betaine, PEG-7 glyceryl cocoate, coconut oleoyl amine DEA, rilanit special, panthenol, Polyquaternium-10, whale Ceryl alcohol, stearyl alcohol, laureth -4, lysine, phenylalanine and arginine, the D phase raw material are Candida/grape Sugar/rapeseed methyl oleate tunning, monkey-bread tree seed extract, dried tremella extract, Radix Salviae Miltiorrhizae root extract, Black Ganoderma extract Object, black tea extract, leaf of Mentha piperita extract, kuh-seng root extract, lotus flower water, Chinese herbaceous peony root extract, coconut water, white pond lily flower Extract, tuckahoe extracts, coptis extract, Chinese torreyanut extract and daily essence, the E phase raw material are 1,2- hexylene glycol, benzene Sodium formate and citric acid.
Beneficial effects of the present invention: the present invention in Chinese torreyanut extract by adding chelating agent, moisturizer, bleeding agent, table Face activating agent, film forming agent, aromatic, preservative, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, Emollients, hair restorer, acid-base modifier, hair conditioner and cosolvent, making the shampoo prepared is in unique fragrance Colourless transparent liquid shape, give full play of Chinese torreyanut inhibit acne pathogenic bacteria growth, it is antipruritic and adjust grease glandular secretion The effect of, various plant hydrosol synergistic effects, moisturizing is releived under the conditions of sufficiently clean to scalp, balance scalp grease point It secretes, effectively slows down scalp dandruff and long acne problem.
Feature and advantage of the invention will be described in detail by embodiment.
[specific embodiment]
A kind of Chinese torreya shampoo of the present invention, including weight ratio are Chinese torreyanut extract, chelating agent, moisturizer, bleeding agent, table Face activating agent, film forming agent, aromatic, preservative, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, The weight ratio of emollients, hair restorer, acid-base modifier, hair conditioner, cosolvent and water, the Chinese torreyanut extract is 0.25-0.45 parts, the weight ratio of the chelating agent is EDETATE SODIUM 0.04-0.06 parts, and the weight ratio of the moisturizer is 0.2-0.4 parts of panthenol, 0.1-0.3 parts of lysine, 0.1-0.3 parts of phenylalanine and 0.1-0.3 parts of arginine, the bleeding agent Weight ratio is 0.4-0.6 parts of 1,2- hexylene glycol, and the weight ratio of the surfactant is laureth sulfuric ester ammonium 12- 14 parts and Cocoamidopropyl betaine 6-8 parts, the weight ratio of the film forming agent is guar hydroxypropyltrimonium chloride 0.2-0.4 parts, the weight ratio of the aromatic is daily essence 0.5-0.7 parts, and the weight ratio of the preservative is benzene first Sour sodium 0.4-0.6 parts, the weight ratio of the antistatic agent is stearamidopropyl dimethylamine 0.4-0.6 parts, 0.2-0.4 parts Polyquaternium-10 and 0.2-0.4 parts of laureth -4, the weight ratio of the skin conditioning agent are the extraction of the baobab seeds of trees 0.04-0.06 parts of object, 0.04-0.06 parts of dried tremella extract, 0.04-0.06 parts of Radix Salviae Miltiorrhizae root extract, Black Ganoderma extract 0.04- 0.06 part, 0.04-0.06 parts of black tea extract, 0.04-0.06 parts of kuh-seng root extract, 0.04-0.06 parts of lotus flower water, Chinese herbaceous peony 0.04-0.06 parts of root extract, 0.04-0.06 parts of white pond lily flower extract, 0.04-0.06 parts of tuckahoe extracts and the coptis mention 0.04-0.06 parts of object are taken, the weight ratio of the foaming agent is 1-3 parts of laurel alcohol sulfuric ester ammonium, the hydrophily thickening agent Weight ratio is 0.5-1.5 parts of coconut oleoyl amine DEA, and the weight ratio of the salubrious agent is leaf of Mentha piperita extract 0.04-0.06 Part, the weight ratio of the emollients is 0.5-1.5 parts of PEG-7 glyceryl cocoate, 0.2-0.4 parts of cetanol and stearyl alcohol 0.2-0.4 parts, the weight ratio of the hair restorer is Candida/glucose/rapeseed methyl oleate tunning 0.2-0.4 Part, the weight ratio of the acid-base modifier is citric acid 0.2-0.4 parts, and the weight ratio of the hair conditioner is coconut water 0.04-0.06 parts, the weight ratio of the cosolvent is rilanit special 0.5-0.7 parts, and the weight ratio of the water is 63.11-74.99 parts.
The extraction step of the Chinese torreyanut extract includes the following:
1. Chinese torreya pericarp is added in agitator tank, it is stirred for that mixed material, the Chinese torreya pericarp is made after soaking in water Weight ratio with water is 3:10, soaking time 60-90min, mixing time 25-35min;
2. being sucked mixed material in distillation still using vacuum pump, while the mixed material in distillation still is added while stirring Heat;
3. remaining temperature-resistant, and pass through the steam distilled out successively when the temperature of mixed material reaches 120-130 DEG C Cross condenser and chiller treatment, distillation time 300min;
4. the cooling oil water mixture out of condensation is successively imported quiet in the first oil water separator and the second oil water separator It sets until oil water mixture is layered;
5. by being saved in the second oil water separator at the middle and upper levels essential oil importing essential oil storage tank.
A kind of preparation method of Chinese torreya shampoo includes the following steps:
1. a part of water and other load weighted A phase raw materials are added in main agitated kettle, stirring and dissolving, temperature is 70~75 DEG C, revolving speed 100-300rpm, when a length of 60min;
2. remaining water and other load weighted B phase raw materials are individually dissolved by heating in advance, temperature is 70-75 DEG C, Revolving speed is 100-300rpm, and the B phase raw material dissolved is added in A phase raw material and is stirred, and temperature is 70-75 DEG C, and revolving speed is 200rpm, when a length of 180min;
3. load weighted C phase raw material is individually dissolved in advance, revolving speed 100-300rpm, C phase raw material is added and is led Agitated kettle stirring, temperature are 70-75 DEG C, revolving speed 200rpm, when a length of 30min;
4. load weighted D phase raw material is individually dissolved in advance, revolving speed 100-300rpm, D phase raw material is added and is led Stirred in agitated kettle, temperature is 70-75 DEG C, revolving speed 100rpm, when a length of 15min;
5. load weighted E phase raw material is individually dissolved in advance, main agitated kettle is cooled to 40 by revolving speed 100-300rpm ~50 DEG C, E phase raw material is added in main agitated kettle and is stirred, revolving speed 100rpm, duration 15min;
6. degassing, sample detection carry out filling, packaging after all qualifieds.
The A phase raw material be laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium, stearamidopropyl dimethylamine, EDETATE SODIUM and water, the B phase raw material are guar hydroxypropyltrimonium chloride and water, and the C phase raw material is coconut oleoyl amine Propyl betaine, PEG-7 glyceryl cocoate, coconut oleoyl amine DEA, rilanit special, panthenol, Polyquaternium-10, cetanol, Stearyl alcohol, laureth -4, lysine, phenylalanine and arginine, the D phase raw material are Candida/glucose/rape Seed methyl oleate tunning, monkey-bread tree seed extract, dried tremella extract, Radix Salviae Miltiorrhizae root extract, Black Ganoderma extract, black tea Extract, leaf of Mentha piperita extract, kuh-seng root extract, lotus flower water, Chinese herbaceous peony root extract, coconut water, white pond lily flower extract, Tuckahoe extracts, coptis extract, Chinese torreyanut extract and daily essence, the E phase raw material be 1,2- hexylene glycol, sodium benzoate and Citric acid.
Embodiment one:
A certain amount of A phase raw material, B phase raw material, C phase raw material, D phase raw material and E phase raw material are weighed, A phase feed components Weight ratio be 12 parts of laureth sulfuric ester ammonium, 1 part of laurel alcohol sulfuric ester ammonium, 0.4 part of stearamidopropyl dimethylamine, 0.04 part and 60 parts of water of EDETATE SODIUM, the weight ratio of B phase feed components is 0.2 part of guar hydroxypropyltrimonium chloride With 14.99 parts of water, the weight ratio of C phase feed components is 6 parts of Cocoamidopropyl betaine, PEG-7 glyceryl cocoate 0.5 part, DEA0.5 parts of coconut oleoyl amine, 0.5 part of rilanit special, 0.2 part of panthenol, 0.2 part of Polyquaternium-10, cetanol 0.2 part, 0.3 part of stearyl alcohol, 0.2 part of laureth -4,0.1 part of lysine, 0.1 part of phenylalanine and arginine 0.1 Part, the weight ratio of D phase feed components is Candida/glucose/0.2 part of rapeseed methyl oleate tunning, monkey face It is 0.04 part of packet seeds of trees extract, 0.04 part of dried tremella extract, 0.04 part of Radix Salviae Miltiorrhizae root extract, 0.04 part of Black Ganoderma extract, red 0.04 part of tea extraction, 0.04 part of leaf of Mentha piperita extract, 0.04 part of kuh-seng root extract, 0.04 part of lotus flower water, Peony Root mention Take 0.04 part of object, 0.04 part of coconut water, 0.04 part of white pond lily flower extract, 0.04 part of tuckahoe extracts, coptis extract 0.04 Part, 0.25 part of Chinese torreyanut extract and 0.5 part of daily essence, the weight ratio of E phase feed components be 0.4 part of 1,2- hexylene glycol, 0.4 part and 0.2 part of citric acid of sodium benzoate, a part of water and other load weighted A phase raw materials are added in main agitated kettle, stirring Dissolution, temperature are 70~75 DEG C, revolving speed 100-300rpm, when a length of 60min, by remaining water and other load weighted B phases Raw material is individually dissolved by heating in advance, and temperature is 70-75 DEG C, revolving speed 100-300rpm, and the B phase raw material dissolved is added Stirred in A phase raw material, temperature is 70-75 DEG C, revolving speed 200rpm, when a length of 180min, load weighted C phase raw material is independent It is dissolved in advance, revolving speed 100-300rpm, main agitated kettle is added in C phase raw material and is stirred, temperature is 70-75 DEG C, and revolving speed is 200rpm, when a length of 30min, load weighted D phase raw material is individually dissolved in advance, revolving speed 100-300rpm, by D phase Raw material is added in main agitated kettle and stirs, and temperature is 70-75 DEG C, revolving speed 100rpm, when a length of 15min, by load weighted E phase Raw material is individually dissolved in advance, revolving speed 100-300rpm, and main agitated kettle is cooled to 40~50 DEG C, and E phase raw material is added and is led It is stirred in agitated kettle, revolving speed 100rpm, duration 15min, degassing, sample detection, filling, packet is carried out after all qualifieds Dress, used equipment is agitator tank (sus304,2000L, explosion-proof, logical association is mechanical), (sus304,3000L prevent emulsion tank Quick-fried, it is mechanical to lead to association), single filter (No. 10, it is mechanical to lead to association by sus304), with liquid transfer tank, (sus304,1000L lead to association's machine Tool) and pure steam generator (LDR0.068-0.7,68kg/h, 0.7mpa, still hundred million thermal energy).
Embodiment two:
A certain amount of A phase raw material, B phase raw material, C phase raw material, D phase raw material and E phase raw material are weighed, A phase feed components Weight ratio be 13 parts of laureth sulfuric ester ammonium, 2 parts of laurel alcohol sulfuric ester ammonium, 0.5 part of stearamidopropyl dimethylamine, 0.05 part and 60 parts of water of EDETATE SODIUM, the weight ratio of B phase feed components is 0.3 part of guar hydroxypropyltrimonium chloride With 9.25 parts of water, the weight ratio of C phase feed components is 7 parts of Cocoamidopropyl betaine, PEG-7 glyceryl cocoate 1 Part, DEA1 parts of coconut oleoyl amine, 0.6 part of rilanit special, 0.3 part of panthenol, 0.3 part of Polyquaternium-10,0.3 part of cetanol, 0.3 part of stearyl alcohol, 0.3 part of laureth -4,0.2 part of lysine, 0.2 part of phenylalanine and 0.2 part of arginine, D phase are former The weight ratio of material each component is Candida/glucose/0.3 part of rapeseed methyl oleate tunning, the baobab seeds of trees mention Take 0.05 part of object, 0.05 part of dried tremella extract, 0.05 part of Radix Salviae Miltiorrhizae root extract, 0.05 part of Black Ganoderma extract, black tea extract 0.05 part, 0.05 part of leaf of Mentha piperita extract, 0.05 part of kuh-seng root extract, 0.05 part of lotus flower water, Chinese herbaceous peony root extract 0.05 Part, 0.05 part of coconut water, 0.05 part of white pond lily flower extract, 0.05 part of tuckahoe extracts, 0.05 part of coptis extract, Chinese torreyanut 0.35 part and 0.6 part of daily essence of extract, the weight ratio of E phase feed components is 0.5 part of 1,2- hexylene glycol, benzoic acid 0.5 part and 0.3 part of citric acid of sodium, a part of water and other load weighted A phase raw materials are added in main agitated kettle, stirring and dissolving, Temperature is 70~75 DEG C, revolving speed 100-300rpm, when a length of 60min, by remaining water and other load weighted B phase raw material lists It is solely dissolved by heating in advance, temperature is 70-75 DEG C, revolving speed 100-300rpm, and it is former that A phase is added in the B phase raw material dissolved Stirred in material, temperature is 70-75 DEG C, revolving speed 200rpm, when a length of 180min, load weighted C phase raw material is individually carried out in advance It first dissolves, revolving speed 100-300rpm, main agitated kettle is added in C phase raw material and is stirred, temperature is 70-75 DEG C, and revolving speed is 200rpm, when a length of 30min, load weighted D phase raw material is individually dissolved in advance, revolving speed 100-300rpm, D phase is former Material is added in main agitated kettle and stirs, and temperature is 70-75 DEG C, revolving speed 100rpm, when a length of 15min, by load weighted E phase original Material list is solely dissolved in advance, revolving speed 100-300rpm, and main agitated kettle is cooled to 40~50 DEG C, and master is added in E phase raw material and is stirred It mixing in pot and stirs, revolving speed 100rpm, duration 15min, degassing, sample detection carry out filling, packaging after all qualifieds, Used equipment be agitator tank (sus304,2000L, explosion-proof, it is mechanical to lead to association), emulsion tank (sus304,3000L, it is explosion-proof, lead to Association is mechanical), single filter (No. 10, it is mechanical to lead to association by sus304), with liquid transfer tank (it is mechanical to lead to association by sus304,1000L) and Pure steam generator (LDR0.068-0.7,68kg/h, 0.7mpa, still hundred million thermal energy)
Embodiment three:
A certain amount of A phase raw material, B phase raw material, C phase raw material, D phase raw material and E phase raw material are weighed, A phase feed components Weight ratio be 14 parts of laureth sulfuric ester ammonium, 3 parts of laurel alcohol sulfuric ester ammonium, 0.6 part of stearamidopropyl dimethylamine, 0.06 part and 50 parts of water of EDETATE SODIUM, the weight ratio of B phase feed components is 0.4 part of guar hydroxypropyltrimonium chloride With 13.11 parts of water, the weight ratio of C phase feed components is 8 parts of Cocoamidopropyl betaine, PEG-7 glyceryl cocoate 1.5 parts, DEA1.5 parts of coconut oleoyl amine, 0.7 part of rilanit special, 0.4 part of panthenol, 0.4 part of Polyquaternium-10, cetanol 0.4 part, 0.4 part of stearyl alcohol, 0.4 part of laureth -4,0.3 part of lysine, 0.3 part of phenylalanine and arginine 0.3 Part, the weight ratio of D phase feed components is Candida/glucose/0.4 part of rapeseed methyl oleate tunning, monkey face It is 0.06 part of packet seeds of trees extract, 0.06 part of dried tremella extract, 0.06 part of Radix Salviae Miltiorrhizae root extract, 0.06 part of Black Ganoderma extract, red 0.06 part of tea extraction, 0.06 part of leaf of Mentha piperita extract, 0.06 part of kuh-seng root extract, 0.06 part of lotus flower water, Peony Root mention Take 0.06 part of object, 0.06 part of coconut water, 0.06 part of white pond lily flower extract, 0.06 part of tuckahoe extracts, coptis extract 0.06 Part, 0.45 part of Chinese torreyanut extract and 0.7 part of daily essence, the weight ratio of E phase feed components be 0.6 part of 1,2- hexylene glycol, 0.6 part and 0.4 part of citric acid of sodium benzoate, a part of water and other load weighted A phase raw materials are added in main agitated kettle, stirring Dissolution, temperature are 70~75 DEG C, revolving speed 100-300rpm, when a length of 60min, by remaining water and other load weighted B phases Raw material is individually dissolved by heating in advance, and temperature is 70-75 DEG C, revolving speed 100-300rpm, and the B phase raw material dissolved is added Stirred in A phase raw material, temperature is 70-75 DEG C, revolving speed 200rpm, when a length of 180min, load weighted C phase raw material is independent It is dissolved in advance, revolving speed 100-300rpm, main agitated kettle is added in C phase raw material and is stirred, temperature is 70-75 DEG C, and revolving speed is 200rpm, when a length of 30min, load weighted D phase raw material is individually dissolved in advance, revolving speed 100-300rpm, by D phase Raw material is added in main agitated kettle and stirs, and temperature is 70-75 DEG C, revolving speed 100rpm, when a length of 15min, by load weighted E phase Raw material is individually dissolved in advance, revolving speed 100-300rpm, and main agitated kettle is cooled to 40~50 DEG C, and E phase raw material is added and is led It is stirred in agitated kettle, revolving speed 100rpm, duration 15min, degassing, sample detection, filling, packet is carried out after all qualifieds Dress, used equipment is agitator tank (sus304,2000L, explosion-proof, logical association is mechanical), (sus304,3000L prevent emulsion tank Quick-fried, it is mechanical to lead to association), single filter (No. 10, it is mechanical to lead to association by sus304), with liquid transfer tank, (sus304,1000L lead to association's machine Tool) and pure steam generator (LDR0.068-0.7,68kg/h, 0.7mpa, still hundred million thermal energy)
The present invention in Chinese torreyanut extract by adding chelating agent, moisturizer, bleeding agent, surfactant, film forming agent, virtue Pastil, preservative, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, emollients, hair restorer, soda acid Regulator, hair conditioner and cosolvent, making the shampoo prepared is in the colourless transparent liquid shape with unique fragrance, is filled Distribution shoots the effect of Chinese torreyanut inhibits the growth of acne pathogenic bacteria, antipruritic and adjusting grease glandular secretion, various plant hydrosols Synergistic effect, to scalp sufficiently it is clean under the conditions of moisturizing releive, balance scalp fat secretion, effectively slow down scalp dandruff and Long acne problem.Chinese torreyanut extract plays the role of preferably adjusting and improving to the grease glandular secretion of scalp.Moisturizer lysine There is good repair to impaired hair with phenylalanine.Monkey-bread tree seed extract can be a kind of rich in natural polysaccharide Gelinite, can help to maintain hyaluronic acid synthetase HAS2 balance expression, effectively facilitate hyaluronic acid synthesis, have long-acting Humectant properties, while its a carboxylic acid included can reduce the imperfection of cuticula and improve surface view of epidermis, help to subtract The thickness of few cuticula.Dried tremella extract is rich in hyaluronic acid and tremella polysaccharides, can promote the generation of collagen, increases skin Elasticity, also have effects that moisturizing and oxidation resistant.Radix Salviae Miltiorrhizae root extract has fine facilitation to collagen proliferation, therefore The metabolism of dermal layer of the skin can be enhanced, furthermore there is inoxidizability, can be used in skin-active anti-wrinkle cosmetic, to hyalomitome The generation of acid has facilitation, has good moistening effect.Ganoderma lucidum polysaccharide contained by Black Ganoderma extract has significantly quasi- SOD Activity, can significantly remove the free radical of body generation, so that free radical is prevented to prevent the peroxidating of rouge body to the damage of body, Protect cell, delaying cell aging.Black tea extract can help to be metabolized aging cutin, reduce the generation of dandruff, and it is extra to eliminate Grease." the southern regions of the Yunnan Province book on Chinese herbal medicine " once pointed out kuh-seng cool blood, relieving heat toxin, scabies leprosy, impetigo poison;Pruitus is treated, blood wind tinea sore is naughty white Bits, detumescence poison, acute purulent lymphadenitis.Therefore kuh-seng root extract, which is used in shampoo, can balance hair follicle fat secretion, dredge and restrain hair Capsule removes the toxin impurity in hair follicle, promotes the growth and reparation of impaired hair follicle cell, restores hair follicle cell vigor.Lotus flower tool Have and releive and refrigerant property, lotus flower water energy increases the melanin production in normal human subject melanocyte, in shampoo It also can reduce itch and improve moisturizing and repair feature.Its Chinese herbaceous peony active constituent of Chinese herbaceous peony root extract to interleukin-1 α (it is a kind of by Keratinocyte release Pro-inflammatory mediator) generations have certain inhibitory effect, have anti-inflammatory, anti-irritant, inhibition junket ammonia Phytase activity, it is anti-oxidant, effectively remove free radical, antipollution and other effects.White pond lily flower extract has calm anti-inflammatory, flesh of releiving The effects of pore is dredged in skin, help.Tuckahoe extracts have antibacterial, anti-inflammatory, height moisturizing, adjust fat secretion, adjust immunity, Oxidation resistant effect.Coptis extract has the effect of heat-clearing and damp-drying drug, purging fire for removing toxin, and the alkaloid contained can kill scalp On fungi bacterium, to inhibit bacteroidal dandruff.Leaf of Mentha piperita extract can bring refrigerant skin sense, energy as salubrious agent Enough mitigate pruitus, reduces inflammatory phenomena, releive tired out, prevent the generation of fat granule.Candida/glucose/rapeseed Methyl oleate tunning is anti-grease excessive as hair restorer energy oil-control, promotes hair growth.Acid-base modifier citric acid is to adjust Hair conditioner PH is in OK range.Hair conditioner coconut water is to be present in a kind of intracavitary composite natral liquid of coconut fruit, Rich in various nutrients, there is unique flavor and aromatic substance, main component includes acids, alcohols, esters, alkane alkenes, aldehyde Class, ketone and phenols etc. can inhibit tyrosinase activity, and eliminate free radical, have good antioxidation.
Above-described embodiment is the description of the invention, is not limitation of the invention, after any pair of simple transformation of the present invention Scheme all belong to the scope of protection of the present invention.

Claims (4)

1. a kind of Chinese torreya shampoo, it is characterised in that: including Chinese torreyanut extract, chelating agent, moisturizer, bleeding agent, surface-active It is agent, film forming agent, aromatic, preservative, antistatic agent, skin conditioning agent, foaming agent, hydrophily thickening agent, salubrious agent, soft and moist Agent, hair restorer, acid-base modifier, hair conditioner, cosolvent and water, the weight ratio of the Chinese torreyanut extract are 0.25- 0.45 part, the weight ratio of the chelating agent is EDETATE SODIUM 0.04-0.06 parts, and the weight ratio of the moisturizer is panthenol 0.2-0.4 parts, 0.1-0.3 parts of lysine, 0.1-0.3 parts of phenylalanine and 0.1-0.3 parts of arginine, the weight of the bleeding agent Ratio is 0.4-0.6 parts of 1,2- hexylene glycol, and the weight ratio of the surfactant is 12-14 parts of laureth sulfuric ester ammonium With 6-8 parts of Cocoamidopropyl betaine, the weight ratio of the film forming agent is guar hydroxypropyltrimonium chloride 0.2- 0.4 part, the weight ratio of the aromatic is daily essence 0.5-0.7 parts, and the weight ratio of the preservative is sodium benzoate 0.4-0.6 parts, the weight ratio of the antistatic agent is the poly- season of stearamidopropyl dimethylamine 0.4-0.6 parts, 0.2-0.4 parts Ammonium salt -10 and 0.2-0.4 parts of laureth -4, the weight ratio of the skin conditioning agent are monkey-bread tree seed extract 0.04-0.06 parts, 0.04-0.06 parts of dried tremella extract, 0.04-0.06 parts of Radix Salviae Miltiorrhizae root extract, Black Ganoderma extract 0.04- 0.06 part, 0.04-0.06 parts of black tea extract, 0.04-0.06 parts of kuh-seng root extract, 0.04-0.06 parts of lotus flower water, Peony Root 0.04-0.06 parts of extract, 0.04-0.06 parts of white pond lily flower extract, 0.04-0.06 parts of tuckahoe extracts and coptis extract 0.04-0.06 parts, the weight ratio of the foaming agent is 1-3 parts of laurel alcohol sulfuric ester ammonium, the weight of the hydrophily thickening agent Ratio is 0.5-1.5 parts of coconut oleoyl amine DEA, and the weight ratio of the salubrious agent is 0.04-0.06 parts of leaf of Mentha piperita extract, The weight ratio of the emollients is 0.5-1.5 parts of PEG-7 glyceryl cocoate, 0.2-0.4 parts of cetanol and stearyl alcohol 0.2- 0.4 part, the weight ratio of the hair restorer is Candida/glucose/0.2-0.4 parts of rapeseed methyl oleate tunning, The weight ratio of the acid-base modifier is citric acid 0.2-0.4 parts, and the weight ratio of the hair conditioner is coconut water 0.04-0.06 parts, the weight ratio of the cosolvent is rilanit special 0.5-0.7 parts, and the weight ratio of the water is 63.11-74.99 parts.
2. a kind of Chinese torreya shampoo as described in claim 1, it is characterised in that the extraction step of the Chinese torreyanut extract includes It is as follows:
1. Chinese torreya pericarp is added in agitator tank, it is stirred for that mixed material, the Chinese torreya pericarp and water is made after soaking in water Weight ratio be 3:10, soaking time 60-90min, mixing time 25-35min;
2. being sucked mixed material in distillation still using vacuum pump, while the mixed material in distillation still is heated while stirring;
3. remaining temperature-resistant, and make the steam distilled out successively through being subcooled when the temperature of mixed material reaches 120-130 DEG C Condenser and chiller treatment, distillation time 300min;
It is stood directly 4. the cooling oil water mixture out of condensation is successively imported in the first oil water separator and the second oil water separator It is layered to oil water mixture;
5. by being saved in the second oil water separator at the middle and upper levels essential oil importing essential oil storage tank.
3. a kind of preparation method of Chinese torreya shampoo, it is characterised in that include the following steps:
1. a part of water and other load weighted A phase raw materials are added in main agitated kettle, stirring and dissolving, temperature is 70~75 DEG C, Revolving speed is 100-300rpm, when a length of 60min;
2. remaining water and other load weighted B phase raw materials are individually dissolved by heating in advance, temperature is 70-75 DEG C, revolving speed For 100-300rpm, the B phase raw material dissolved being added in A phase raw material and is stirred, temperature is 70-75 DEG C, revolving speed 200rpm, when A length of 180min;
3. load weighted C phase raw material is individually dissolved in advance, revolving speed 100-300rpm, main stirring is added in C phase raw material Pot stirring, temperature are 70-75 DEG C, revolving speed 200rpm, when a length of 30min;
4. load weighted D phase raw material is individually dissolved in advance, revolving speed 100-300rpm, main stirring is added in D phase raw material Stirred in pot, temperature is 70-75 DEG C, revolving speed 100rpm, when a length of 15min;
5. load weighted E phase raw material is individually dissolved in advance, main agitated kettle is cooled to 40~50 by revolving speed 100-300rpm DEG C, E phase raw material is added in main agitated kettle and is stirred, revolving speed 100rpm, duration 15min;
6. degassing, sample detection carry out filling, packaging after all qualifieds.
4. a kind of preparation method of Chinese torreya shampoo as claimed in claim 3, it is characterised in that: the A phase raw material is laurel Alcohol polyethers sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium, stearamidopropyl dimethylamine, EDETATE SODIUM and water, the B phase raw material are melon Youngster's glue hydroxypropyl-trimethyl ammonium chloride and water, the C phase raw material be Cocoamidopropyl betaine, PEG-7 glyceryl cocoate, Coconut oleoyl amine DEA, rilanit special, panthenol, Polyquaternium-10, cetanol, stearyl alcohol, laureth -4, lysine, benzene Alanine and arginine, the D phase raw material are Candida/glucose/rapeseed methyl oleate tunning, the baobab seeds of trees Extract, dried tremella extract, Radix Salviae Miltiorrhizae root extract, Black Ganoderma extract, black tea extract, leaf of Mentha piperita extract, radix sophorae Extract, lotus flower water, Chinese herbaceous peony root extract, coconut water, white pond lily flower extract, tuckahoe extracts, coptis extract, Chinese torreyanut mention Object and daily essence are taken, the E phase raw material is 1,2- hexylene glycol, sodium benzoate and citric acid.
CN201811106921.0A 2018-09-21 2018-09-21 A kind of Chinese torreya shampoo and preparation method thereof Pending CN109288768A (en)

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CN110101643A (en) * 2019-06-21 2019-08-09 广州睿森生物科技有限公司 A kind of moisturizing remediation composition and the cosmetics containing the composition
CN111700841A (en) * 2020-06-11 2020-09-25 梧州市华夏医药科技有限公司 Hair loss preventing and hair growing shampoo containing ganoderma atrum plant extract essence and preparation method thereof
CN111920726A (en) * 2020-09-27 2020-11-13 广州德谷个人护理用品有限公司 Multi-effect quick scalp itching relieving composition, preparation method thereof and shampoo composition
CN112603874A (en) * 2020-12-24 2021-04-06 上海懿林生物科技股份有限公司 Formula for improving skin nutrition absorption and preparation method thereof
CN113197798A (en) * 2021-05-10 2021-08-03 上海应用技术大学 Plant hydrolat with antioxidant and anti-aging effects and preparation method and application thereof
CN113908087A (en) * 2021-06-22 2022-01-11 广州臻颜化妆品有限公司 Natural moisturizing combined extract, preparation method and application thereof
CN116712374A (en) * 2023-08-08 2023-09-08 广州善元堂健康科技股份有限公司 High-stability alopecia-preventing composition and preparation method thereof
CN117338687A (en) * 2023-11-17 2024-01-05 开远市洁白洗涤用品有限公司 Hair-protecting and developing composition and preparation method and application thereof

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Publication number Priority date Publication date Assignee Title
CN110101643A (en) * 2019-06-21 2019-08-09 广州睿森生物科技有限公司 A kind of moisturizing remediation composition and the cosmetics containing the composition
CN111700841A (en) * 2020-06-11 2020-09-25 梧州市华夏医药科技有限公司 Hair loss preventing and hair growing shampoo containing ganoderma atrum plant extract essence and preparation method thereof
CN111920726A (en) * 2020-09-27 2020-11-13 广州德谷个人护理用品有限公司 Multi-effect quick scalp itching relieving composition, preparation method thereof and shampoo composition
CN111920726B (en) * 2020-09-27 2023-01-10 广州德谷个人护理用品有限公司 Multi-effect quick scalp itching relieving composition, preparation method thereof and shampoo composition
CN112603874A (en) * 2020-12-24 2021-04-06 上海懿林生物科技股份有限公司 Formula for improving skin nutrition absorption and preparation method thereof
CN113197798A (en) * 2021-05-10 2021-08-03 上海应用技术大学 Plant hydrolat with antioxidant and anti-aging effects and preparation method and application thereof
CN113908087A (en) * 2021-06-22 2022-01-11 广州臻颜化妆品有限公司 Natural moisturizing combined extract, preparation method and application thereof
CN116712374A (en) * 2023-08-08 2023-09-08 广州善元堂健康科技股份有限公司 High-stability alopecia-preventing composition and preparation method thereof
CN116712374B (en) * 2023-08-08 2023-10-31 广州善元堂健康科技股份有限公司 High-stability alopecia-preventing composition and preparation method thereof
CN117338687A (en) * 2023-11-17 2024-01-05 开远市洁白洗涤用品有限公司 Hair-protecting and developing composition and preparation method and application thereof

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